CN1995250A - Thermostable heat-isolating coating and its preparation method - Google Patents
Thermostable heat-isolating coating and its preparation method Download PDFInfo
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- CN1995250A CN1995250A CN 200610000111 CN200610000111A CN1995250A CN 1995250 A CN1995250 A CN 1995250A CN 200610000111 CN200610000111 CN 200610000111 CN 200610000111 A CN200610000111 A CN 200610000111A CN 1995250 A CN1995250 A CN 1995250A
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Abstract
The invention discloses a high-temperature proof insulating paint and making method, which comprises the following parts: 400-500g organic silica resin, 50-100g thermostable dye, 100-200g fill, 80-150 hollow ceramic microball, 30-60g bergmeal, 20-50g potassium titanate whisker, 100-150g solvent and 5-15g adjuvant.
Description
Technical field
The present invention relates to a kind of heat insulating coatings and preparation method thereof, relate in particular to a kind of can be at medium-term and long-term thermostable heat-isolating coating that uses of hot environment and preparation method thereof.Coating of the present invention is mainly used in the surface that needs heat-insulation and heat-preservation to handle of industry high temperature services (place) such as oil, chemical industry, metallurgy, electric power, as is coated on appearances such as iron and steel chimney, high-temperature pipe, High-temp. kiln, petroleum cracking device and war industry equipment.
Technical background
The existing heat-insulation and heat-preservation material that is applied to high temperature service (place) is generally the conventional lagging material of fiber-like and hard class.These conventional lagging materials are because thermal insulation layer is thicker, many genotypes material again, and seam is many, and therefore construction is inconvenient, and is poor with substrate bonding, anti-vibration not, work-ing life is short.
Summary of the invention
The present invention will solve the above-mentioned technical problem that existing heat-insulation and heat-preservation material exists, and provides that a kind of coating is thin, sticking power is good, long service life, the significant thermostable heat-isolating coating of heat insulation and preservation effect.
For this reason, thermostable heat-isolating coating of the present invention adopts following component and proportioning thereof, and wherein the consumption of each component is represented with weight part:
Silicone resin 400～500 weight parts, high-temperature resisting pigment 50～100 weight parts, filler 100～200 weight parts, hollow ceramic microballon 80～150 weight parts, diatomite 30～60 weight parts, potassium titanate crystal whisker 20～50 weight parts, solvent 100～150 weight parts, auxiliary agent 5～15 weight parts.
Described high-temperature resisting pigment adopts the high temperature resistant type carbon black.
Described filler is made up of glass powder with low melting point, the mica powder of 30～60 weight parts, 20～40 weight part kaolin of 60～100 weight parts.
Described solvent is made up of the propyl carbinol of 20～30 weight parts, the dimethylbenzene of 30～50 weight parts and the N-BUTYL ACETATE of 50～70 weight parts.
Described auxiliary agent comprises the thickening material of defoamer, 1～3 weight part flow agent and 1～3 weight part of dispersion agent, 1～3 weight part of 3～5 weight parts.
The environment that is to reach a high temperature is medium-term and long-term to be used and best heat insulation and preservation effect, and thermostable heat-isolating coating of the present invention is according to silicone resin: high-temperature resisting pigment: filler: hollow ceramic microballon: diatomite: potassium titanate crystal whisker: solvent: auxiliary agent is 450: 70: 150: 120: 40: 30: 130: 10 weight proportion is prepared.Further preferably according to silicone resin: high-temperature resisting pigment: glass powder with low melting point: mica powder: kaolin: hollow ceramic microballon: diatomite: potassium titanate crystal whisker: propyl carbinol: dimethylbenzene: N-BUTYL ACETATE: dispersion agent: defoamer: flow agent: thickening material is 450: 70: 80: 40: 30: 120: 40: 30: 25: 40: 65: 4: 2: 2: 2 weight proportion is prepared.
The preparation method of thermostable heat-isolating coating of the present invention is as follows:
A, the propyl carbinol with above-mentioned weight proportion, dimethylbenzene and acetic acid butanols mix, and stir, and make solvent;
B, solvent is dropped in the Scattered Kettle, in stirring, add high-temperature resisting pigment successively and the filler formed by glass powder, mica powder, kaolin and diatomite, potassium titanate crystal whisker, stir and make slurry;
C, above-mentioned slurry, silicone resin, dispersion agent, flow agent are mixed together grinding, make its fineness≤20 micron;
D, adding hollow ceramic microballon and defoamer stir;
E, dropping thickening material stir, and are adjusted to suitable viscosity, filter and package then and promptly make the thermostable heat-isolating coating finished product.
Thermostable heat-isolating coating of the present invention can be under 600 ℃ of working temperatures life-time service, strong adhesion, snappiness is good, heat insulation and preservation effect is remarkable, thereby has realized energy-saving and cost-reducing.For example, at the thermostable heat-isolating coating of the present invention of industrial furnace surface-coated 0.9 mm thick, the stove surface temperature is reduced to 215 ℃ by original 600 ℃; Apply the coating of 0.9 mm thick on heat distribution pipeline, the pipe surface temperature is reduced to 115 ℃ by original 350 ℃.Thermostable heat-isolating coating of the present invention also has performances such as acid and alkali-resistance, corrosion-resistant, good waterproof performance, electrical isolation.
Embodiment
The present invention is further illustrated below in conjunction with embodiment:
Embodiment 1
Main purpose of the present invention is high temperature resistant and heat-insulation and heat-preservation, and component of Cai Yonging and proportioning thereof (weight part) are in the present embodiment: silicone resin 450, high temperature resistant type carbon black 70, glass powder with low melting point 80, mica powder 40, kaolin 30, hollow ceramic microballon 120, diatomite 40, potassium titanate crystal whisker 30, propyl carbinol 25, dimethylbenzene 40, N-BUTYL ACETATE 65, dispersion agent 4, defoamer 2, flow agent 2, thickening material 2.Wherein, the high temperature tolerance of high temperature resistant sooty reaches 800 ℃, and it is 560 ℃ that glass powder adopts unleaded type fusing point, and mica powder, kaolin, diatomaceous specification are 800 orders, and the particle diameter of hollow ceramic microballon is 20 microns, and potassium titanate crystal whisker adopts powder-type six potassium titanates.The dispersion agent that the present invention selects for use, defoamer, flow agent and thickening material all adopt the former liquid product of German BYK company.
Embodiment 2
In the present embodiment, the component and the proportioning (weight part) thereof of the present invention's employing are: silicone resin 400, high temperature resistant type carbon black 100, glass powder with low melting point 100, mica powder 30, kaolin 20, hollow ceramic microballon 150, diatomite 30, potassium titanate crystal whisker 20, propyl carbinol 20, dimethylbenzene 30, N-BUTYL ACETATE 50, dispersion agent 5, defoamer 3, flow agent 3, thickening material 3.Wherein, the high temperature tolerance of high temperature resistant sooty reaches 850 ℃, and it is 500 ℃ that glass powder adopts unleaded type fusing point, and mica powder, kaolin, diatomaceous specification are 750 orders, and the particle diameter of hollow ceramic microballon is 18 microns, and potassium titanate crystal whisker adopts powder-type six potassium titanates.
Embodiment 3
Main purpose of the present invention is high temperature resistant and heat-insulation and heat-preservation, and component that it adopts and proportioning thereof (weight part) are: silicone resin 500, high temperature resistant type carbon black 50, glass powder with low melting point 60, mica powder 60, kaolin 40, hollow ceramic microballon 80, diatomite 60, potassium titanate crystal whisker 50, propyl carbinol 30, dimethylbenzene 50, N-BUTYL ACETATE 70, dispersion agent 3, defoamer 1, flow agent 1, thickening material 1.Wherein, the high temperature tolerance of high temperature resistant sooty reaches 900 ℃, and it is 600 ℃ that glass powder adopts unleaded type fusing point, and mica powder, kaolin, diatomaceous specification are 850 orders, and the particle diameter of hollow ceramic microballon is 15 microns, and potassium titanate crystal whisker adopts powder-type six potassium titanates.
In the component of above-mentioned thermostable heat-isolating coating, described high temperature resistant type carbon black can replace with high temperature oxidation resisting iron pigment (black, red, blue, green, Huang); N-BUTYL ACETATE in the solvent can replace with ethylene glycol monobutyl ether.
The preparation method of above-mentioned thermostable heat-isolating coating is as follows:
A, the propyl carbinol with above-mentioned weight proportion, dimethylbenzene and N-BUTYL ACETATE mix, and stir 15 minutes to evenly, make standby mixed solvent;
B, standby mixed solvent is dropped in the Scattered Kettle, under agitation add carbon black, glass powder, mica powder, kaolin, diatomite and potassium titanate crystal whisker successively, high-speed stirring was disperseed 40 minutes, made slurry;
C, with mixed grinding in slurry, silicone resin, dispersion agent, flow agent, the input shredder 40 minutes, make its fineness≤20 micron, make the mixed with resin slurry;
D, in the mixed with resin slurry, drop into hollow ceramic microballon and defoamer, middling speed dispersed with stirring 20 minutes;
E, under stirring at low speed, slowly add thickening material, stir, be adjusted to appropriate viscosity, promptly make the thermostable heat-isolating coating finished product after the filtration.
Above-mentioned make thermostable heat-isolating coating, can spray during construction, rinse and be coated with and roller coat, when finished product concentration is thick partially, can use solvent cut.
Thermostable heat-isolating coating of the present invention can be widely used in the surperficial heat-insulation and heat-preservation of industry high temperature services (place) such as oil, chemical industry, metallurgy, electric power, mine, boats and ships, food-processing, military affairs, and is energy-saving and cost-reducing.
Claims (5)
1, a kind of thermostable heat-isolating coating is characterized in that adopting following component and proportioning thereof:
Silicone resin 400～500 weight parts, high-temperature resisting pigment 50～100 weight parts, filler 100～200 weight parts, hollow ceramic microballon 80～150 weight parts, diatomite 30～60 weight parts, potassium titanate crystal whisker 20～50 weight parts, solvent 100～150 weight parts, auxiliary agent 5～15 weight parts, wherein, described high-temperature resisting pigment adopts high temperature resistant type carbon black or high temperature resistant type iron oxide pigment, described filler is by the glass powder with low melting point of 60～100 weight parts, the mica powder of 30～60 weight parts, 20～40 weight part kaolin are formed, described solvent is by the propyl carbinol of 20～30 weight parts, the N-BUTYL ACETATE of the dimethylbenzene of 30～50 weight parts and 50～70 weight parts or ethylene glycol methyl-n-butyl ether are formed, and described auxiliary agent comprises the dispersion agent of 3～5 weight parts, the defoamer of 1～3 weight part, the thickening material of 1～3 weight part flow agent and 1～3 weight part.
2,, it is characterized in that adopting following ingredients weight parts proportioning according to the thermostable heat-isolating coating of claim 1:
Silicone resin: high-temperature resisting pigment: filler: hollow ceramic microballon: diatomite: potassium titanate crystal whisker: solvent: auxiliary agent is 450: 70: 150: 120: 40: 30: 130: 10.
3,, it is characterized in that adopting following ingredients weight parts proportioning according to the thermostable heat-isolating coating of claim 1:
Silicone resin: high-temperature resisting pigment: glass powder with low melting point: mica powder: kaolin: hollow ceramic microballon: diatomite: potassium titanate crystal whisker: propyl carbinol: dimethylbenzene: N-BUTYL ACETATE or ethylene glycol methyl-n-butyl ether: dispersion agent: defoamer: flow agent: thickening material is 450: 70: 80: 40: 30: 120: 40: 30: 25: 40: 65: 4: 2: 2: 2.
4, a kind of method that is used to prepare the thermostable heat-isolating coating of claim 1 is characterized in that may further comprise the steps:
A, propyl carbinol, dimethylbenzene and acetic acid butanols or ethylene glycol methyl-n-butyl ether are mixed, stir, make solvent;
B, described solvent is dropped in the Scattered Kettle, in stirring, add high-temperature resisting pigment successively and the filler formed by glass powder, mica powder, kaolin and diatomite, potassium titanate crystal whisker, make slurry;
C, described slurry, silicone resin, dispersion agent, flow agent are mixed together grinding, make its fineness≤20 micron;
D, adding hollow ceramic microballon and defoamer stir;
E, dropping thickening material stir, and are adjusted to suitable viscosity, filter then.
5, a kind of method that is used to prepare the thermostable heat-isolating coating of claim 1 is characterized in that may further comprise the steps:
A, propyl carbinol, dimethylbenzene and N-BUTYL ACETATE or ethylene glycol methyl-n-butyl ether are mixed, stirs 15 minutes, make standby mixed solvent to even;
B, mixed solvent is dropped in the Scattered Kettle, under agitation add carbon black, glass powder, mica powder, kaolin, diatomite and potassium titanate crystal whisker successively, high-speed stirring was disperseed 40 minutes, made slurry;
C, with slurry, silicone resin, dispersion agent, flow agent mixed grinding 40 minutes, make its fineness≤20 micron, make the mixed with resin slurry;
D, in the mixed with resin slurry, drop into hollow ceramic microballon and defoamer, middling speed dispersed with stirring 20 minutes;
E, under stirring at low speed, slowly add thickening material, stir, be adjusted to appropriate viscosity, filter then.
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| CN200610000111A CN100584910C (en) | 2006-01-04 | 2006-01-04 | Thermostable heat-isolating coating and its preparation method |
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| CN200610000111A CN100584910C (en) | 2006-01-04 | 2006-01-04 | Thermostable heat-isolating coating and its preparation method |
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| CN100584910C CN100584910C (en) | 2010-01-27 |
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