CN105542541A - Anti-radiation, heat-insulation and heat-preservation coating material and preparation method thereof - Google Patents
Anti-radiation, heat-insulation and heat-preservation coating material and preparation method thereof Download PDFInfo
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- CN105542541A CN105542541A CN201610062882.3A CN201610062882A CN105542541A CN 105542541 A CN105542541 A CN 105542541A CN 201610062882 A CN201610062882 A CN 201610062882A CN 105542541 A CN105542541 A CN 105542541A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1656—Antifouling paints; Underwater paints characterised by the film-forming substance
- C09D5/1662—Synthetic film-forming substance
- C09D5/1675—Polyorganosiloxane-containing compositions
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/02—Organic and inorganic ingredients
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/346—Clay
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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Abstract
The invention discloses an anti-radiation, heat-insulation and heat-preservation coating material and a preparation method of the anti-radiation, heat-insulation and heat-preservation coating material. The anti-radiation, heat-insulation and heat-preservation coating material is prepared from the following raw materials in parts by mass: 15 to 25 parts of diatomite, 10 to 18 parts of kaolin, 30 to 45 parts of silicone foam resin, 10 to 20 parts of butyl acetate, 0.2 to 2 parts of defoaming agent, 12 to 20 parts of heat insulation powder, 0.5 to 5 parts of nano SiO2, 0.2 to 2 parts of dispersing agent, 13 to 19 parts of anti-radiation agent, 1 to 10 parts of reflective pigment, 1 to 5 parts of preservative, 1 to 4 parts of coalescing agent, 18 to 38 parts of anti-freezing agent, 20 to 35 parts of water and 12 to 22 parts of conductive mica. The preparation method comprises the following steps: mixing and dispersing the water, the silicone foam resin, the butyl acetate, the defoaming agent, the heat insulation powder and the dispersing agent; adding the diatomite, the kaolin, the conductive mica and the nano SiO2 in sequence during dispersing, adding the anti-radiation agent, the reflective pigment, the preservative, the coalescing agent and the anti-freezing agent in sequence during dispersing, and dispersing until a mixed solution is uniform. The anti-radiation, heat-insulation and heat-preservation coating material disclosed by the invention not only can be used for insulating heat, but also can be used for storing energy, the heat preservation effect is good, the heat insulation and heat preservation effect is high, and the storage performance is good; meanwhile, a preparation technology of the anti-radiation, heat-insulation and heat-preservation coating material is simple, the cost is low, no toxicity and no pollution are generated, and the stability is high.
Description
Technical field
The present invention relates to building material technical field, specifically a kind of anti-radiation insulation thermal insulation coatings and preparation method thereof.
Background technology
In today that global heat effect is aggravated, the energy and environmental problem have become the obstacle of restriction human economy fast development, and therefore, the green energy resource of exploitation low-carbon (LC), environmental protection and reduction energy consumption, improve energy utilization rate, become a global problem.Current coating technology develops to environment-friendly and energy-efficient coating direction.Thermal isolation technique be utilize reduce sunlight absorption, reduce heat trnasfer, reduce the intrusion etc. of energy and reach heat insulation object.Existing have radiation-resistant thermal insulating coating mainly there to be three types: isolated conduction type thermal insulating coating, reflection type thermal insulation coating and Radiation Heat-insulated Paint.In addition, heat insulating coatings made by the type material of the hollow microvesicle of existing application at present, but start late at home, current affect this type of paint development have following problem: 1, mainly with hollow be main be main lagging material, this type of material often has effect of heat insulation at short notice, but when being through prolonged exposure or the thermal conduction of 1 ~ 2 hour, lose effect of heat insulation along with reaching boundary's balance inside and outside the slow thermal conduction finally of vacuum layer.2, the quality of cenosphere is uneven, and the parameters such as size all cannot effectively detect, can only by Performance Detection after formation product; Another part take ceramic fine bead as carrier, but cannot effectively ensure the quality of products with cenosphere is the same.3, cenosphere has low-density singularity, and cause the storage short period of time after adding this kind of material in thermal insulating coating that surperficial conjunctiva just occurs, the time, longer rete was thicker, serious even whole barrel knot block.Cannot ensure the stable of construction, the invalid coating of final formation, causes most enterprises to be hung back to real thermal insulating coating.
Summary of the invention
The object of the present invention is to provide that a kind of cost is low, nontoxic pollution-free, strong adhesion, water-alkali resistance is good, paint film is fine and smooth, cover trickle slight crack, scrubbing resistance, easy clean anti-soil, quality is homogeneous, stability is high anti-radiation insulation thermal insulation coatings and preparation method thereof, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the invention provides following technical scheme:
A kind of anti-radiation insulation thermal insulation coatings, comprises according to the raw material of mass parts: diatomite 15-25 part, kaolin 10-18 part, silicon bubble resin 30-45 part, N-BUTYL ACETATE 10-20 part, defoamer 0.2-2 part, heat-insulating powder 12-20 part, Nano-meter SiO_2
20.5-5 part, dispersion agent 0.2-2 part, antiradiation agent 13-19 part, reflective paint 1-10 part, sanitas 1-5 part, film coalescence aid 1-4 part, frostproofer 18-38 part, water 20-35 part, Conductive mica 12-22 part.
As the further scheme of the present invention: described anti-radiation insulation thermal insulation coatings, comprises according to the raw material of mass parts: diatomite 15-22 part, kaolin 10-15 part, silicon bubble resin 33-42 part, N-BUTYL ACETATE 10-15 part, defoamer 0.2-1 part, heat-insulating powder 15-20 part, Nano-meter SiO_2
20.5-3 part, dispersion agent 0.2-1 part, antiradiation agent 13-15 part, reflective paint 2-8 part, sanitas 2-4 part, film coalescence aid 2-3 part, frostproofer 20-35 part, water 20-30 part, Conductive mica 15-20 part.
The preparation method of described anti-radiation insulation thermal insulation coatings, according to the following step preparation sequentially carried out:
1), add water, silicon bubble resin, N-BUTYL ACETATE, defoamer, heat-insulating powder and dispersion agent successively in dispersion cup after, under the rotating speed of 600-800r/min, 2-4 minute is disperseed;
2) adjust dispersing speed to 1200-1800r/min, dispersion limit, limit adds diatomite, kaolin, Conductive mica and Nano-meter SiO_2 successively
2, dispersion 18-22 minute;
3) adjust dispersing speed to 1000-1200r/min, dispersion limit, limit adds antiradiation agent, reflective paint, sanitas, film coalescence aid and frostproofer successively, disperse 18-22 minute even to mixing solutions.
As the further scheme of the present invention: disperse 3 minutes under the rotating speed of 700r/min in step 1).
As the further scheme of the present invention: step 2) in adjustment dispersing speed to 1500r/min.
As the further scheme of the present invention: adjust dispersing speed in step 3) to 1100r/min.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention can be heat insulation, again can accumulation of energy, high insulating effect, heat insulation and preservation effect is high, stability in storage good, simultaneously its preparation technology is simple, cost is low, nontoxic pollution-free, and strong adhesion, water-alkali resistance is good, paint film is fine and smooth, cover trickle slight crack, scrubbing resistance, easy clean anti-soil, quality is homogeneous, and stability is high.Construction technology is simple, and difficulty of construction is low, is convenient to large-scale promotion application, has more wide market and application prospect.
Embodiment
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of anti-radiation insulation thermal insulation coatings, comprises according to the raw material of mass parts: 15 parts, diatomite, kaolin 10 parts, silicon bubble resin 30 parts, N-BUTYL ACETATE 10 parts, defoamer 0.2 part, heat-insulating powder 12-20, Nano-meter SiO_2
20.5 part, dispersion agent 0.2 part, antiradiation agent 13 parts, reflective paint 1 part, sanitas 1 part, film coalescence aid 1 part, frostproofer 18 parts, 20 parts, water, Conductive mica 12 parts.
The preparation method of described anti-radiation insulation thermal insulation coatings, according to the following step preparation sequentially carried out:
1), add water, silicon bubble resin, N-BUTYL ACETATE, defoamer, heat-insulating powder and dispersion agent successively in dispersion cup after, disperse 2 minutes under the rotating speed of 600r/min.
2) adjust dispersing speed to 1200r/min, dispersion limit, limit adds diatomite, kaolin, Conductive mica and Nano-meter SiO_2 successively
2, disperse 18 minutes.
3) adjust dispersing speed to 1000r/min, dispersion limit, limit adds antiradiation agent, reflective paint, sanitas, film coalescence aid and frostproofer successively, disperse 18 minutes even to mixing solutions.
Embodiment 2
In the embodiment of the present invention, a kind of anti-radiation insulation thermal insulation coatings, comprises according to the raw material of mass parts: 25 parts, diatomite, kaolin 18 parts, silicon bubble resin 45 parts, N-BUTYL ACETATE 20 parts, defoamer 2 parts, heat-insulating powder 20 parts, Nano-meter SiO_2
25 parts, dispersion agent 2 parts, antiradiation agent 19 parts, reflective paint 10 parts, sanitas 5 parts, film coalescence aid 4 parts, frostproofer 38 parts, 35 parts, water, Conductive mica 22 parts.
The preparation method of described anti-radiation insulation thermal insulation coatings, according to the following step preparation sequentially carried out:
1), add water, silicon bubble resin, N-BUTYL ACETATE, defoamer, heat-insulating powder and dispersion agent successively in dispersion cup after, disperse 4 minutes under the rotating speed of 800r/min.
2) adjust dispersing speed to 1800r/min, dispersion limit, limit adds diatomite, kaolin, Conductive mica and Nano-meter SiO_2 successively
2, disperse 22 minutes.
3) adjust dispersing speed to 1200r/min, dispersion limit, limit adds antiradiation agent, reflective paint, sanitas, film coalescence aid and frostproofer successively, disperse 22 minutes even to mixing solutions.
Embodiment 3
In the embodiment of the present invention, a kind of anti-radiation insulation thermal insulation coatings, comprises according to the raw material of mass parts: 15 parts, diatomite, kaolin 10 parts, silicon bubble resin 33 parts, N-BUTYL ACETATE 10 parts, defoamer 0.2 part, heat-insulating powder 15 parts, Nano-meter SiO_2
20.5 part, dispersion agent 0.2 part, antiradiation agent 13 parts, reflective paint 2 parts, sanitas 2 parts, film coalescence aid 2 parts, frostproofer 20 parts, 20 parts, water, Conductive mica 15 parts.
The preparation method of described anti-radiation insulation thermal insulation coatings, according to the following step preparation sequentially carried out:
1), add water, silicon bubble resin, N-BUTYL ACETATE, defoamer, heat-insulating powder and dispersion agent successively in dispersion cup after, disperse 2.5 minutes under the rotating speed of 650r/min.
2) adjust dispersing speed to 1300r/min, dispersion limit, limit adds diatomite, kaolin, Conductive mica and Nano-meter SiO_2 successively
2, disperse 19 minutes.
3) adjust dispersing speed to 1050r/min, dispersion limit, limit adds antiradiation agent, reflective paint, sanitas, film coalescence aid and frostproofer successively, disperse 19 minutes even to mixing solutions.
Embodiment 4
In the embodiment of the present invention, a kind of anti-radiation insulation thermal insulation coatings, comprises according to the raw material of mass parts: 22 parts, diatomite, kaolin 15 parts, silicon bubble resin 42 parts, N-BUTYL ACETATE 15 parts, defoamer 1 part, heat-insulating powder 20 parts, Nano-meter SiO_2
23 parts, dispersion agent 1 part, antiradiation agent 15 parts, reflective paint 8 parts, sanitas 4 parts, film coalescence aid 3 parts, frostproofer 35 parts, 30 parts, water, Conductive mica 20 parts.
The preparation method of described anti-radiation insulation thermal insulation coatings, according to the following step preparation sequentially carried out:
1), add water, silicon bubble resin, N-BUTYL ACETATE, defoamer, heat-insulating powder and dispersion agent successively in dispersion cup after, disperse 3.5 minutes under the rotating speed of 750r/min.
2) adjust dispersing speed to 1700r/min, dispersion limit, limit adds diatomite, kaolin, Conductive mica and Nano-meter SiO_2 successively
2, disperse 21 minutes.
3) adjust dispersing speed to 1150r/min, dispersion limit, limit adds antiradiation agent, reflective paint, sanitas, film coalescence aid and frostproofer successively, disperse 21 minutes even to mixing solutions.
Embodiment 5
In the embodiment of the present invention, a kind of anti-radiation insulation thermal insulation coatings, comprises according to the raw material of mass parts: 18 parts, diatomite, kaolin 12 parts, silicon bubble resin 37 parts, N-BUTYL ACETATE 12 parts, defoamer 0.7 part, heat-insulating powder 17 parts, Nano-meter SiO_2
21.5 parts, dispersion agent 0.8 part, antiradiation agent 14 parts, reflective paint 5 parts, sanitas 3 parts, film coalescence aid 2.5 parts, frostproofer 28 parts, 25 parts, water, Conductive mica 17 parts.
The preparation method of described anti-radiation insulation thermal insulation coatings, according to the following step preparation sequentially carried out:
1), add water, silicon bubble resin, N-BUTYL ACETATE, defoamer, heat-insulating powder and dispersion agent successively in dispersion cup after, disperse 3 minutes under the rotating speed of 700r/min.
2) adjust dispersing speed to 1500r/min, dispersion limit, limit adds diatomite, kaolin, Conductive mica and Nano-meter SiO_2 successively
2, disperse 20 minutes.
3) adjust dispersing speed to 1100r/min, dispersion limit, limit adds antiradiation agent, reflective paint, sanitas, film coalescence aid and frostproofer successively, disperse 20 minutes even to mixing solutions.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (6)
1. an anti-radiation insulation thermal insulation coatings, is characterized in that, comprises according to the raw material of mass parts: diatomite 15-25 part, kaolin 10-18 part, silicon bubble resin 30-45 part, N-BUTYL ACETATE 10-20 part, defoamer 0.2-2 part, heat-insulating powder 12-20 part, Nano-meter SiO_2
20.5-5 part, dispersion agent 0.2-2 part, antiradiation agent 13-19 part, reflective paint 1-10 part, sanitas 1-5 part, film coalescence aid 1-4 part, frostproofer 18-38 part, water 20-35 part, Conductive mica 12-22 part.
2. anti-radiation insulation thermal insulation coatings according to claim 1, it is characterized in that, comprise according to the raw material of mass parts: diatomite 15-22 part, kaolin 10-15 part, silicon bubble resin 33-42 part, N-BUTYL ACETATE 10-15 part, defoamer 0.2-1 part, heat-insulating powder 15-20 part, Nano-meter SiO_2
20.5-3 part, dispersion agent 0.2-1 part, antiradiation agent 13-15 part, reflective paint 2-8 part, sanitas 2-4 part, film coalescence aid 2-3 part, frostproofer 20-35 part, water 20-30 part, Conductive mica 15-20 part.
3. a preparation method for the anti-radiation insulation thermal insulation coatings as described in as arbitrary in claim 1-2, is characterized in that, according to the following step preparation sequentially carried out:
1), add water, silicon bubble resin, N-BUTYL ACETATE, defoamer, heat-insulating powder and dispersion agent successively in dispersion cup after, under the rotating speed of 600-800r/min, 2-4 minute is disperseed;
2) adjust dispersing speed to 1200-1800r/min, dispersion limit, limit adds diatomite, kaolin, Conductive mica and Nano-meter SiO_2 successively
2, dispersion 18-22 minute;
3) adjust dispersing speed to 1000-1200r/min, dispersion limit, limit adds antiradiation agent, reflective paint, sanitas, film coalescence aid and frostproofer successively, disperse 18-22 minute even to mixing solutions.
4. the preparation method of anti-radiation insulation thermal insulation coatings according to claim 3, is characterized in that, disperses 3 minutes in step 1) under the rotating speed of 700r/min.
5. the preparation method of anti-radiation insulation thermal insulation coatings according to claim 3, is characterized in that, step 2) in adjustment dispersing speed to 1500r/min.
6. the preparation method of anti-radiation insulation thermal insulation coatings according to claim 3, is characterized in that, adjusts dispersing speed to 1100r/min in step 3).
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| CN201610062882.3A CN105542541A (en) | 2016-01-30 | 2016-01-30 | Anti-radiation, heat-insulation and heat-preservation coating material and preparation method thereof |
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| CN201610062882.3A CN105542541A (en) | 2016-01-30 | 2016-01-30 | Anti-radiation, heat-insulation and heat-preservation coating material and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1995250A (en) * | 2006-01-04 | 2007-07-11 | 北京国邦技术发展中心 | Thermostable heat-isolating coating and its preparation method |
| CN101531864A (en) * | 2009-04-16 | 2009-09-16 | 山东大学 | High temperature resistant heat insulation coating and preparation method thereof |
| US20120190777A1 (en) * | 2011-01-26 | 2012-07-26 | Elastikote, Llc | Coating composition containing biobased materials |
| CN102676014A (en) * | 2012-05-30 | 2012-09-19 | 浙江好途程新型建材有限公司 | Staining-resistant heat-insulationcoating and preparation method thereof |
| CN103396734A (en) * | 2013-08-07 | 2013-11-20 | 常州市特种涂料有限公司 | Anti-radiation heat-insulation coating and preparation method thereof |
-
2016
- 2016-01-30 CN CN201610062882.3A patent/CN105542541A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1995250A (en) * | 2006-01-04 | 2007-07-11 | 北京国邦技术发展中心 | Thermostable heat-isolating coating and its preparation method |
| CN101531864A (en) * | 2009-04-16 | 2009-09-16 | 山东大学 | High temperature resistant heat insulation coating and preparation method thereof |
| US20120190777A1 (en) * | 2011-01-26 | 2012-07-26 | Elastikote, Llc | Coating composition containing biobased materials |
| CN102676014A (en) * | 2012-05-30 | 2012-09-19 | 浙江好途程新型建材有限公司 | Staining-resistant heat-insulationcoating and preparation method thereof |
| CN103396734A (en) * | 2013-08-07 | 2013-11-20 | 常州市特种涂料有限公司 | Anti-radiation heat-insulation coating and preparation method thereof |
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