CN1974711A - 稀土荧光体材料的微波烧成方法 - Google Patents
稀土荧光体材料的微波烧成方法 Download PDFInfo
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- CN1974711A CN1974711A CN 200610130334 CN200610130334A CN1974711A CN 1974711 A CN1974711 A CN 1974711A CN 200610130334 CN200610130334 CN 200610130334 CN 200610130334 A CN200610130334 A CN 200610130334A CN 1974711 A CN1974711 A CN 1974711A
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- Prior art keywords
- rare
- earth
- microwave
- phosphor material
- firing method
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- 239000000463 material Substances 0.000 title claims abstract description 28
- 238000009768 microwave sintering Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 claims abstract description 26
- 239000000843 powder Substances 0.000 claims abstract description 18
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 37
- 150000002910 rare earth metals Chemical class 0.000 claims description 31
- 238000010304 firing Methods 0.000 claims description 21
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 17
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- -1 rare earth aluminate Chemical class 0.000 claims description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 claims description 4
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 3
- 229910000480 nickel oxide Inorganic materials 0.000 claims description 3
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 claims description 3
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 2
- 239000005083 Zinc sulfide Substances 0.000 claims description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 2
- DVRDHUBQLOKMHZ-UHFFFAOYSA-N chalcopyrite Chemical compound [S-2].[S-2].[Fe+2].[Cu+2] DVRDHUBQLOKMHZ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052951 chalcopyrite Inorganic materials 0.000 claims description 2
- 229910000428 cobalt oxide Inorganic materials 0.000 claims description 2
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims description 2
- 229960004643 cupric oxide Drugs 0.000 claims description 2
- 229940056932 lead sulfide Drugs 0.000 claims description 2
- 229910052981 lead sulfide Inorganic materials 0.000 claims description 2
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 claims description 2
- 229910052683 pyrite Inorganic materials 0.000 claims description 2
- 239000011028 pyrite Substances 0.000 claims description 2
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 abstract description 9
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000013078 crystal Substances 0.000 abstract description 2
- 150000004645 aluminates Chemical class 0.000 abstract 1
- 229910000323 aluminium silicate Inorganic materials 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 230000005855 radiation Effects 0.000 abstract 1
- 239000010431 corundum Substances 0.000 description 7
- 229910052593 corundum Inorganic materials 0.000 description 7
- 229910017639 MgSi Inorganic materials 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 238000001354 calcination Methods 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000002829 reductive effect Effects 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 239000011358 absorbing material Substances 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000000498 ball milling Methods 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000005672 electromagnetic field Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen(.) Chemical compound [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 238000010532 solid phase synthesis reaction Methods 0.000 description 1
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Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2006101303346A CN100497519C (zh) | 2006-12-18 | 2006-12-18 | 稀土荧光体材料的微波烧成方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2006101303346A CN100497519C (zh) | 2006-12-18 | 2006-12-18 | 稀土荧光体材料的微波烧成方法 |
Publications (2)
Publication Number | Publication Date |
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CN1974711A true CN1974711A (zh) | 2007-06-06 |
CN100497519C CN100497519C (zh) | 2009-06-10 |
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CNB2006101303346A Active CN100497519C (zh) | 2006-12-18 | 2006-12-18 | 稀土荧光体材料的微波烧成方法 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102516999A (zh) * | 2011-12-08 | 2012-06-27 | 天津理工大学 | 一种显色性大于90的暖白光混合荧光材料及其制备方法 |
CN103194218A (zh) * | 2013-04-12 | 2013-07-10 | 天津理工大学 | 一种红色稀土荧光材料的高温微波制备方法 |
-
2006
- 2006-12-18 CN CNB2006101303346A patent/CN100497519C/zh active Active
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102516999A (zh) * | 2011-12-08 | 2012-06-27 | 天津理工大学 | 一种显色性大于90的暖白光混合荧光材料及其制备方法 |
CN103194218A (zh) * | 2013-04-12 | 2013-07-10 | 天津理工大学 | 一种红色稀土荧光材料的高温微波制备方法 |
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Publication number | Publication date |
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CN100497519C (zh) | 2009-06-10 |
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Owner name: HANDAN SHENGDE TECHNOLOGY GLASS CO., LTD. Free format text: FORMER OWNER: TIANJIN UNIVERSITY OF TECHNOLOGY Effective date: 20130802 |
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Free format text: CORRECT: ADDRESS; FROM: 300191 NANKAI, TIANJIN TO: 056001 HANDAN, HEBEI PROVINCE |
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Effective date of registration: 20130802 Address after: 056001, Hebei, Handan province Handan County on behalf of the township on behalf of the Village West 309 State Road South Patentee after: HANDAN SHENGDE TECHNOLOGY GLASS Co.,Ltd. Address before: 300191 No. 263 Hongqi South Road, Tianjin, Nankai District Patentee before: Tianjin University of Technology |
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Effective date of registration: 20210715 Address after: 056000 Dai Zhao Xiang Dai Zhao Cun Xi 309 National Road South, Hanshan District, Handan City, Hebei Province Patentee after: Handan time Zhonghe Glass Technology Co.,Ltd. Address before: 056001 Dai Zhao Xiang Dai Zhao Cun Xi 309 National Road South, Handan County, Handan City, Hebei Province Patentee before: HANDAN SHENGDE TECHNOLOGY GLASS Co.,Ltd. |
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Effective date of registration: 20220705 Address after: 056001 west of Daizhao village, Daizhao Township, Hanshan District, Handan City, Hebei Province (southwest corner of the intersection of 309 National Highway and linxiangru Street) Patentee after: Aikegu ecological agriculture development (Hebei) Co.,Ltd. Address before: 056000 Dai Zhao Xiang Dai Zhao Cun Xi 309 National Road South, Hanshan District, Handan City, Hebei Province Patentee before: Handan time Zhonghe Glass Technology Co.,Ltd. |
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