CN1943549A - Hair shampoo article and its preparing method - Google Patents
Hair shampoo article and its preparing method Download PDFInfo
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- CN1943549A CN1943549A CN 200610127314 CN200610127314A CN1943549A CN 1943549 A CN1943549 A CN 1943549A CN 200610127314 CN200610127314 CN 200610127314 CN 200610127314 A CN200610127314 A CN 200610127314A CN 1943549 A CN1943549 A CN 1943549A
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Abstract
The invention relates to the field of article for hair washing and specifically a kind of hair washing article is disclosed. Said article is made of materials from litchi extracts.
Description
[technical field]
The invention belongs to the hair shampoo article technical field, be specifically related to a kind of hair shampoo article that contains Semen Litchi extract and preparation method thereof.
[background technology]
Semen Litchi is the mature seed of Sapindaceae aiphyllium plant Fructus Litchi (Litchi chinsis Sonn.).Main product in Fujian, ground such as Guangdong, Guangxi.Pluck mature fruit summer, remove peel and meat aril, clean, dry.Give birth to or saline process usefulness.Time spent smashes.Semen Litchi acrid in the mouth, little hardship, temperature.Return liver, stomach through being mainly used in colicky, painful and swollen testis.This product catharsis of working hard has the merit of depressed liver-energy dispersing and QI regulating, promoting QI to circulate and dispersing the agglomeration of the pathogens, dispersing cold for relieving pain.Semen Litchi is controlled colic of cold type pain, can be equal to usefulness with Fructus Foeniculi, Fructus Evodiae, Semen Citri Reticulatae, as the hernia internal diabetes ball of " Beijing's Chinese traditional patent formulation selected works ".Control painful and swollen testis, many and Semen Citri Reticulatae, Fructus Toosendan are equal to usefulness.Semen Litchi also can be used for gastral cavilty pain of a specified duration, dysmenorrhea, puerperal abdonimal pain.It is logical that the hot row of this product hardship is let out temperature, and dispersing the stagnated liver-QI for regulating the stomach, regulating QI to relieve pain effect are arranged.The gastral cavilty pain of a specified duration of Semen Litchi treating the liver stagnation of QI knot, incoordination between the liver and stomach can be ground clothes into powder with the Radix Aucklandiae, looses as the Jing-Yue Complete Works litchi is fragrant, the dysmenorrhea and the puerperal abdonimal pain of the strongly fragrant qi depression to blood stasis for the treatment of the liver, can grind clothes into powder with perfume (or spice) limit, diffusing bitterly as " married woman's good recipe " stannum, or be equal to usefulness with Rhizoma Chuanxiong, Radix Angelicae Sinensis, Radix Bupleuri.
Semen Litchi is Long Circle or oval, and is slightly flat, long 1.5～2.2cm, diameter 0.6～1.5cm.Surface brownish red or purple brown, glossy, slightly cave in and insertion waves.One end has the hilum of similar round or oval yellowish-brown, diameter 5～7mm.Matter is hard, cuts 2 of the visible plump cotyledons in back open with water infiltration, and orange-yellow or pale brown color is combined closely with kind of a skin.Feeble QI, it is little sweet, bitter, puckery to distinguish the flavor of.Big, full, bright person is good with grain.Its microscopical identification is: Semen Litchi (middle part) cross section: all plant the chrotoplast wall and be pale brown color.Plant the exocuticle cell extend radially of skin.About 10～15 row of parenchyma cell are arranged in it, and cell tangentially prolongs, the visible sparse Kong Wen that has.Brown oil cell similar round or Long Circle.The interrupted annular arrangement of vascular bundle.Decadent near the several layers of parenchyma cell of planting the skin epidermis, cell shrinkage, the gap is big.The endepidermis of planting skin is 1 row parenchyma cell, and is flat different in size.Be full of starch grain in the parenchyma cell of cotyledon, and as seen have brown oil cell to be dispersed in.
American documentation literature US2004/0101508A1 discloses the purposes of extract aspect cosmetics and medicine of Fructus Litchi.Chinese patent literature (200410022559) provides Fructus Litchi extract and preparation method thereof, and this invention also provides the application of this Fructus Litchi extract in medicine, health food and cosmetics.But to the deep development of Semen Litchi extract, especially Semen Litchi extract does not have document to mention in the application of hair shampoo article, does not have product open yet.Zheng Linying etc. reported Semen Litchi have suppress hbs antigen, effect (Chinese medicine journal, 1998 (5): 51-53) such as blood sugar lowering, enhancing mouse liver albumen and RNA be synthetic; (Chinese Journal of New Drugs, 2000 (1): 14-16) reported that also Semen Litchi has blood lipid regulation and antioxidation such as Pan Jing clanging or clanking sound except above effect.
[summary of the invention]
The Semen Litchi that the objective of the invention is to annual about 500,000 tons is turned waste into wealth, and development and use are used to prepare hair shampoo article, and this hair shampoo article has the effect of killing acarid and removal dandruff and a kind of hair shampoo article of inventing.
Another object of the present invention is to provide the hair shampoo article preparation method.
Hair shampoo article of the present invention contains Semen Litchi extract.
Hair shampoo article of the present invention contains Semen Litchi extract and hair shampoo article adjuvant.
Above-mentioned hair shampoo article, the Semen Litchi extract weight ratio in hair shampoo article is 0.1-25%, preferred 0.1-15%, more preferably 0.5-10%, most preferably 1-5%.
Above-mentioned hair shampoo article comprises shampoo, shampoo, hair washing breast, shampoo, hair cream, hair conditioner, sends out the rock mud of film and maintenance hair.
Above-mentioned hair shampoo article can also add Herba Leonuri extract, Radix Salviae Miltiorrhizae extract, Radix Angelicae Sinensis extract, Rhizoma Chuanxiong extract, Semen Tritici aestivi extract, Radix Polygoni Multiflori extract, Radix Ginseng extract, Margarita, Margarita micropowder, Rhizoma Atractylodis Macrocephalae extract, Fructus Lycii extract, Radix Saposhnikoviae extract, Radix Angelicae Dahuricae extract, Radix Astragali extract, Rhizoma Dioscoreae extract, Semen Cuscutae extract, Radix Rehmanniae extract, alfalfa extract, Sargassum extract liquid, Aloe extract, Radix Arnebiae extract, the XINGTAO extract, the arnica montana extract, Laurel extract extract, the Fructus Citri Sarcodactylis extract, the sprout of birch extract, the Fructus Arctii extract, Flos Inulae extract, Camellia extract, camomile extract, green algal extract, Radix Glycyrrhizae extract, Caulis Hederae Sinensis extract, Herba Euphrasiae Regelii extract, Radix Oenotherae erythrosepalae oil, Fructus Foeniculi extract, Rhizoma Zingiberis Recens extract, in Semen Ginkgo extrac and the root of Gentiana lutea root extract one or more.
The preparation method of above-mentioned Semen Litchi extract is: water and alcoholic acid mixed solvent extraction were 2-3 time after Semen Litchi was pulverized, and each 1-2 hour, concentrated after drying promptly got Semen Litchi extract, with the Semen Litchi extract irradiation sterilization after, the dressing that adds bath oil, stirring and evenly mixing, packing is promptly.Wherein the water content of Semen Litchi extract is controlled at 2.5-3.5%.
Can adopt vacuum packaging during above-mentioned hair shampoo article packing, also can be above-mentioned charge in nitrogen, helium, the carbon dioxide one or more during the hair shampoo article packing.
Semen Litchi extract among the present invention also can adopt commercially available product (existing at present Semen Litchi extract is sold), can also obtain by other organic solvents or water extraction.
Because Guangdong and Guangxi Provinces, Fujian and Taiwan Fructus Litchi output are huge, many mountain areas, the Fructus Litchi place of production and hills, have inconvenient traffic, and Fructus Litchi requires very harsh to storage and traffic condition, often occur going mouldy owing to Fructus Litchi can not be caused by place of production outward transport in time, at this moment pulp and Fructus Litchi kind skin have not all had value, Semen Litchi can also add in the hair shampoo article by drying, sterilization and pulverizing back or processing extraction only, turn waste into wealth, produce bigger economic worth, also can increase farmers' income for the Fructus Litchi grower retrieves a loss.
China's Fructus Litchi output is huge, and Fructus Litchi output was about 1,500,000 tons in 2005, and resource is very abundant, because the difference of Fructus Litchi kind accounts for Fructus Litchi gross weight 1/3 with Semen Litchi and calculates, annual China just has 500,000 tons of Semen Litchi resources to develop.From the raw material as hair shampoo article, Semen Litchi has than the better advantage of Fructus Litchi, says that from content of effective difference of them is little, but because Fructus Litchi is in the fruit outside, contacts with air, and active component is oxidized easily; And Fructus Litchi is as a kind of fruit, by people edible after, peel is difficult to collect, the gross weight ratio that Fructus Litchi accounts for litchi fruits is little; And Semen Litchi weight is big, is easy to collect after eating; Directly Semen Litchi is taken out when also having businessman to produce canned litchi, be more convenient for the collection of Semen Litchi like this.
Fructus Litchi is since ancient times owing to the well-known phrase of " rides the human society imperial concubine laughs at; nobody knows Fructus Litchi " fires one's imagination, become a kind of and beautiful fruit of becoming attached to, Semen Litchi really is used to beautify people's life, also be not used in the preparation hair shampoo article but also have no talent at present.
The present invention verifies by experiment, hair shampoo article performance among the present invention is removed the dandruff and removed the acarid effect is that various compositions comprehensively play a role in the Semen Litchi extract, rather than a certain or a certain compounds plays a role, therefore Semen Litchi extract is as a kind of raw material of cosmetics, has the incomparable effect of other hair shampoo article, especially has significant improvement effect aspect the removal dandruff and the acarid, in addition, Semen Litchi extract also has favorable compatibility, also can make hair shampoo article by compatibility with other plant or plant extract, also have the effect of removing the dandruff and removing the acarid effect, wherein the effect of Semen Litchi extract is indispensable.
The inventor attempts to adopt the active component of the extract of litchi rind as hair shampoo article, but experimental results show that hair shampoo article that litchi rind is made does not possess in the obvious effect of removing aspect the dandruff and the acarid.
[specific embodiment]
Following embodiment further describes the present invention, but described embodiment only is used to illustrate the present invention rather than restriction the present invention.
The preparation of embodiment 1-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 2.5 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 2 are got 1-2 hour at every turn 2-3 time, the temperature of extracting is 55-65 ℃, concentrates the back under 70 ℃ of conditions, vacuum drying oven 6 hours, promptly get Semen Litchi extract, water content is 2.8%.
The preparation of embodiment 2-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and ethanol and being 1: 3 are got 1-2 hour at every turn 2-3 time, the temperature of extracting is 55-70 ℃, concentrates the back under 80 ℃ of conditions, vacuum drying oven 5 hours, promptly get Semen Litchi extract, water content is 2.9%.
The preparation of embodiment 3-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 2.5 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 2 are got 2-3 time, and each 1-2 hour, the temperature of extraction was 55-70 ℃, and concentrated, spray drying promptly get Semen Litchi extract, and water content is 3.1%.
The preparation of embodiment 4-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 3 are got 2-3 time, each 1-2 hour, the temperature of extracting is 55-70 ℃, concentrate, after the spray drying under 75 ℃ of conditions, vacuum drying oven 5 hours promptly gets Semen Litchi extract, and water content is 3.0%.
The preparation of embodiment 5-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and ethyl acetate and being 1: 3 are got 2-3 time, each 1-2 hour, the temperature of extracting is 55-70 ℃, concentrate, after the spray drying under 50 ℃ of conditions, vacuum drying oven 8 hours promptly gets Semen Litchi extract, and water content is 2.5%.
The preparation of embodiment 6-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 2.5 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 20 are got 2-3 time, and each 1-2 hour, the temperature of extraction was 55-70 ℃, and concentrated, spray drying promptly get Semen Litchi extract, and water content is 3.5%.
The preparation of embodiment 7-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and acetone and being 20: 1 are got 2-3 time, each 1-2 hour, the temperature of extracting is 55-70 ℃, concentrate, after the spray drying under 50 ℃ of conditions, vacuum drying oven 5 hours promptly gets Semen Litchi extract, and water content is 3.0%.
The preparation of embodiment 9-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and ethanol and being 20: 1 are got 2-3 time, each 1-2 hour, the temperature of extracting is 40-70 ℃, concentrate, after the spray drying 200 Pascals, under 50 ℃ of conditions, vacuum drying oven 5 hours, promptly get Semen Litchi extract, water content is 5.2%.
The preparation of embodiment 10-Semen Litchi extract
500 gram Semen Litchis, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and ethyl acetate and being 1: 5 are got 2-3 time, each 1-2 hour, the temperature of extracting is 40-70 ℃, concentrate, after the spray drying 200 Pascals, under 50 ℃ of conditions, vacuum drying oven 8 hours, promptly get Semen Litchi extract, water content is 6.3%.
The preparation of embodiment 11-Semen Litchi extract
500 gram Semen Litchis are pulverized the back and are got 2-3 time with acetone 2.5 ascending, and each 1-2 hour, the temperature of extraction was 40-70 ℃, and concentrated, spray drying promptly get Semen Litchi extract, and water content is 3.8%.
The preparation of embodiment 12-Semen Litchi extract
500 gram Semen Litchis are pulverized the back and are got 2-3 time with ethyl acetate 3 ascending, each 1-2 hour, the temperature of extracting is 40-70 ℃, concentrate, after the spray drying 200 Pascals, under 50 ℃ of conditions, vacuum drying oven 5 hours promptly gets Semen Litchi extract, and water content is 5.2%.
The preparation of embodiment 13-Semen Litchi extract
500 gram Semen Litchis are pulverized the back and are got 2-3 time with ethanol 3 ascending, and 1-2 hour at every turn, the temperature of extraction was 40-70 ℃, and 200 Pascals, under 50 ℃ of conditions, vacuum drying oven 3 hours promptly gets Semen Litchi extract after concentrated, the spray drying, and water content is 7.1%.
Embodiment 14-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (embodiment 1) of 1g, behind the irradiation sterilization, after adding 550g dimethyl siloxane, 200g glycerol, 100g distearyl acid ethylene glycol vinegar, 130g propylene glycol, 5g retinoic acid, 10g sodium lauryl sulphate and 3.5g dodecyltriethanolamine sulfate, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 10 shampoo packings under the aseptic condition.
Embodiment 15-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (embodiment 2) of 5g, behind the irradiation sterilization, behind adding 4.5g Flos Pelargonii quintessence oil, 500g dimethyl siloxane, 250g propylene glycol and the stearic alcohol ester of 240g Palmic acid, high-speed stirred, add the 0.5g sodium benzoate, stirring and evenly mixing, fill is 10 shampoo packings under the aseptic condition.
Embodiment 16-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (embodiment 3) of 10g, behind the irradiation sterilization, after adding 580g dimethyl siloxane, 10g Semen Tritici aestivi extract, 5g Semen Tritici aestivi extract, 45g hydroxy-methylbenzene dibutyl ester, 4.5g dichloroacetic acid, 350g glycerol, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 10 shampoo packings under the aseptic condition.
Embodiment 17-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (embodiment 4) of 50g, behind the irradiation sterilization, after adding 160g hexadecanol, 150g spermaceti siloxanes, 360g Palmic acid spermaceti ester, 229.5g glycerol and 100g methylcellulose, high-speed stirred, add the 0.5g sodium benzoate, stirring and evenly mixing, fill is 10 hair conditioner packings under the aseptic condition.
Embodiment 18-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (Tai Ping Bioisystech Co., Ltd in Ningbo provides) of 100g, behind the irradiation sterilization, after adding 450g dimethyl siloxane, 280g glycerol, 10g distearyl acid ethylene glycol vinegar, 150g propylene glycol, 5g retinoic acid, 0.5g sodium lauryl sulphate and 4.5g dodecyltriethanolamine sulfate, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 100 shampoo packings under the aseptic condition.
Embodiment 19-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (embodiment 1) of 150g, behind the irradiation sterilization, after adding 400g dimethyl siloxane, 280g glycerol, 10g distearyl acid ethylene glycol vinegar, 150g propylene glycol, 5g retinoic acid, 0.5g sodium lauryl sulphate and 4.5g dodecyltriethanolamine sulfate, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 200 shampoo packings under the aseptic condition.
Embodiment 20-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (embodiment 1) of 50g, behind the irradiation sterilization, after adding 160g hexadecanol, 150g spermaceti siloxanes, 360g Palmic acid spermaceti ester, 225g glycerol, 4.59 Radix Ginseng extracts and 100g methylcellulose, high-speed stirred, add the 0.5g sodium benzoate, stirring and evenly mixing, fill is 10 hair conditioner packings under the aseptic condition.
Embodiment 21-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (Tai Ping Bioisystech Co., Ltd in Ningbo provides) of 200g, behind the irradiation sterilization, after adding 450g dimethyl siloxane, 280g glycerol, 10g Oleum Ricini, 150g propylene glycol, 5g Radix Polygoni Multiflori extract, 0.5g sodium lauryl sulphate and 4.5g dodecyltriethanolamine sulfate, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 100 shampoo packings under the aseptic condition.
Embodiment 22-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (the great Tang in Shaanxi science and technology limited Company provides) of 10g, behind the irradiation sterilization, after adding 590g dimethyl siloxane, 5g Radix Astragali extract, 45g hydroxy-methylbenzene dibutyl ester, 4.5g cinnamon essential oil, 350g glycerol, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 10 shampoo packings under the aseptic condition.
Embodiment 23-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (Tai Ping Bioisystech Co., Ltd in Ningbo provides) of 200g, behind the irradiation sterilization, after adding 390g dimethyl siloxane, 5g Radix Angelicae Dahuricae extract, 45g hydroxy-methylbenzene dibutyl ester, 4.5g dichloroacetic acid, 350g glycerol, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 10 hair cream packings under the aseptic condition.
Embodiment 24-contains the preparation of Semen Litchi extract hair shampoo article
Get the Semen Litchi extract (embodiment 2) of 10g, behind the irradiation sterilization, after adding 590g dimethyl siloxane, 5g Radix Angelicae Sinensis extract, 45g hydroxy-methylbenzene dibutyl ester, 4.5g dichloroacetic acid, 350g glycerol, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 100 hair conditioner packings under the aseptic condition.
The preparation of Comparative Examples 1-litchi rind extract
500 gram litchi rinds, mixed solvent 2.5 ascending of pulverizing the two weight ratio of back water and acetone and being 1: 2 are got 2-3 time, each 1-2 hour, the temperature of extracting is 40-85 ℃, concentrate the back 200 Pascals, under 50 ℃ of conditions, vacuum drying oven 6 hours, promptly get Semen Litchi extract, extraction ratio is 5.9%.
The preparation of Comparative Examples 2-litchi rind extract
500 gram litchi rinds, mixed solvent 3 ascending of pulverizing the two weight ratio of back water and ethanol and being 1: 3 are got 1-2 hour at every turn 2-3 time, the temperature of extracting is 40-70 ℃, concentrates the back 200 Pascals, under 50 ℃ of conditions, vacuum drying oven 10 hours promptly gets Semen Litchi extract, and extraction ratio is 6.7%.
Comparative Examples 3-contains the preparation of litchi rind extract hair shampoo article
Get the litchi rind extract (Comparative Examples 1) of 50g, behind the irradiation sterilization, behind adding 4.5g Flos Pelargonii quintessence oil, 500g dimethyl siloxane, 250g propylene glycol and the stearic alcohol ester of 240g Palmic acid, high-speed stirred, add the 0.5g sodium benzoate, stirring and evenly mixing, fill is 10 shampoo packings under the aseptic condition.
Comparative Examples 4-contains the preparation of litchi rind extract hair shampoo article
Get the litchi rind extract (Comparative Examples 2) of 200g, behind the irradiation sterilization, after adding 590g dimethyl siloxane, 5g Semen Tritici aestivi extract, 45g hydroxy-methylbenzene dibutyl ester, 4.5g dichloroacetic acid, 350g glycerol, high-speed stirred, add the 0.5g methyl parahydroxybenzoate, stirring and evenly mixing, fill is 10 shampoo packings under the aseptic condition.
Experimental example 1-hair shampoo article is to the removal effect of the dandruff
Prepared hair shampoo article has dandruff women (age 20-38 year) on probation at 72, the length of its selected hair is 60-80 centimetre, be divided into is 6 groups, every group 12 people, promptly A group (blank group), B group (embodiment 15), C group (embodiment 16), D group (embodiment 17), E group (embodiment 18), F organize (Comparative Examples 4).Ginseng survey personnel and experimenter do not know the kind (double-blind method) of employed hair shampoo article.
Experimental technique: before 6 groups of women use, its hair is all pruned 10 centimetres, respectively take by weighing 10 gram hairs, detection head scurf quantity under magnifier, the record area is greater than the above dandruff quantity of 0.2 * 0.2 millimeter size.After 5 groups of women wash one's face with the warm water that cleans evening, the hair shampoo article of the about 10g correspondence of coating (A group is coated with the glycerol of equivalent) every day 1 time on hair, continue 5 days, the improvement situation of viewing head scurf, again its hair is all pruned 10 centimetres, respectively take by weighing 10 gram hairs, detection head scurf quantity under 15 times of magnifieres, the record area is greater than 0.05 * 0.05 centimetre dandruff quantity.Effect is divided into 5 grades: 1 grade: the dandruff reduces more than 80%, 2 grades: the dandruff reduces 60-80%, 3 grades: the dandruff reduces 40-59%, 4 grades: the dandruff reduces 20-39%, and 5 grades: the dandruff reduces below 20%.Concrete data see Table 1
Table 1 is respectively organized experimenter's the dandruff and is improved situation
| Group | 1 grade of number | 2 grades of numbers | 3 grades of numbers | 4 grades of numbers | 5 grades of numbers |
| A group (blank group) B group (embodiment 15) C group (embodiment 16) D group (embodiment 17) E group (embodiment 18) | 0 1 3 4 3 | 0 4 5 4 5 | 1 5 3 3 4 | 8 2 1 1 0 | 3 0 0 0 0 |
| F organizes (Comparative Examples 4) | 0 | 0 | 1 | 9 | 2 |
Above data declaration hair shampoo article of the present invention obviously reduces the dandruff, has the significant dandruff and improves effect.And the hair shampoo article of litchi rind extract preparation does not possess the effect that reduces the dandruff.
Experimental example 2-hair shampoo article is to the removal effect of acarid
Prepared hair shampoo article is on probation 72 male university students, the length of its selected original hair is 35-50 centimetre, be divided into is 6 groups, every group 12 people, promptly A group (blank group), B group (embodiment 15), C group (embodiment 16), D group (embodiment 17), E group (embodiment 18), F organize (Comparative Examples 4).Ginseng survey personnel and experimenter do not know the kind (double-blind method) of employed hair shampoo article.
Experimental technique: before 6 groups of male university students use, its hair is all pruned 10 centimetres, respectively take by weighing the 50g hair, under 100 power microscopes, detect acarid quantity, record respectively.6 groups of male university students are coated with the hair shampoo article (glycerol of A group coating equivalent) of about 10g correspondence evening on hair, after the hair washing, and the flushing hair shampoo article.Continue 5 days every day 1 time, again its hair all pruned 10 centimetres, respectively takes by weighing the 50g hair, detects acarid quantity at microscopically, record, the situation that detects of observing acarid.Effect is divided into 4 grades: 1 grade: no acarid detects in the 50g hair, 2 grades: the 50g hair has 1 acarid to detect 3 grades: the 50g hair has 2-4 acarid to detect 4 grades: the 50g hair has 5 or 5 above acarids to detect.Concrete data see Table 2
Table 2 is respectively organized experimenter's acarid situation
| Before the use | ||||
| Group | 1 grade of number | 2 grades of numbers | 3 grades of numbers | 4 grades of numbers |
| A group (blank group) B group (embodiment 15) C group (embodiment 16) D group (embodiment 17) E group (embodiment 18) F group (Comparative Examples 4) | 0 0 0 0 0 0 | 1 2 1 1 2 1 | 2 1 2 3 1 3 | 9 9 9 8 9 8 |
| After the use | ||||
| Group | 1 grade of number | 2 grades of numbers | 3 grades of numbers | 4 grades of numbers |
| A group (blank group) B group (embodiment 15) C group (embodiment 16) D group (embodiment 17) E group (embodiment 18) F group (Comparative Examples 4) | 1 4 8 7 6 1 | 1 4 2 3 2 2 | 8 3 2 3 4 7 | 3 1 0 0 0 2 |
Above data declaration hair shampoo article of the present invention has remarkable result to removing acarid; And the hair shampoo article of litchi rind extract preparation does not possess the effect of removing acarid.
Claims (10)
1. a hair shampoo article is characterized in that described hair shampoo article contains Semen Litchi extract.
2. a hair shampoo article is characterized in that described hair shampoo article contains Semen Litchi extract and hair shampoo article adjuvant.
3. according to the arbitrary described hair shampoo article of claim 1-2, it is characterized in that the weight ratio of described Semen Litchi extract in hair shampoo article is 0.1-25%.
4. according to the described hair shampoo article of claim 3, it is characterized in that the weight ratio of described Semen Litchi extract in hair shampoo article is 0.1-15%.
5. according to the described hair shampoo article of claim 4, it is characterized in that the weight ratio of described Semen Litchi extract in hair shampoo article is 1-10%.
6. according to the described hair shampoo article of claim 5, it is characterized in that the weight ratio of described Semen Litchi extract in hair shampoo article is 1-5%.
7. according to the arbitrary described hair shampoo article of claim 1-6, it is characterized in that described hair shampoo article comprises the rock mud of shampoo, shampoo, hair washing breast, shampoo, hair cream, hair conditioner, a film and maintenance hair.
8. according to the arbitrary described hair shampoo article of claim 3-7, it is characterized in that described hair shampoo article can also add Herba Leonuri extract, Radix Salviae Miltiorrhizae extract, Radix Angelicae Sinensis extract, Rhizoma Chuanxiong extract, Semen Tritici aestivi extract, Radix Polygoni Multiflori extract, Radix Ginseng extract, Margarita, Margarita micropowder, Rhizoma Atractylodis Macrocephalae extract, Fructus Lycii extract, Radix Saposhnikoviae extract, Radix Angelicae Dahuricae extract, Radix Astragali extract, Rhizoma Dioscoreae extract, Semen Cuscutae extract, Radix Rehmanniae extract, alfalfa extract, Sargassum extract liquid, Aloe extract, Radix Arnebiae extract, the XINGTAO extract, the arnica montana extract, Laurel extract extract, the Fructus Citri Sarcodactylis extract, the sprout of birch extract, the Fructus Arctii extract, Flos Inulae extract, Camellia extract, camomile extract, green algal extract, Radix Glycyrrhizae extract, Caulis Hederae Sinensis extract, Herba Euphrasiae Regelii extract, Radix Oenotherae erythrosepalae oil, Fructus Foeniculi extract, Rhizoma Zingiberis Recens extract, in Semen Ginkgo extrac and the root of Gentiana lutea root extract one or more.
9. the preparation method of the arbitrary described hair shampoo article of claim 1-8, it is characterized in that described preparation method is: water and alcoholic acid mixed solvent extraction were 2-3 time after Semen Litchi was pulverized, each 1-2 hour, concentrated after drying promptly gets Semen Litchi extract, with the Semen Litchi extract irradiation sterilization after, the dressing that adds bath oil, stirring and evenly mixing, packing is promptly.
10. according to the preparation method of the described hair shampoo article of claim 9, it is characterized in that the water content of wherein said Semen Litchi extract is controlled at 2.5-3.5%.
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| CN200610127314A CN1943549B (en) | 2006-09-13 | 2006-09-13 | Application of litchi seed extract in hair shampoo article |
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| CN200610127314A CN1943549B (en) | 2006-09-13 | 2006-09-13 | Application of litchi seed extract in hair shampoo article |
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| CN1943549A true CN1943549A (en) | 2007-04-11 |
| CN1943549B CN1943549B (en) | 2010-05-12 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009062804A1 (en) * | 2007-11-14 | 2009-05-22 | Henkel Ag & Co. Kgaa | Hair treatment agent having lychee extract and taurine |
| CN101889967A (en) * | 2010-08-06 | 2010-11-24 | 徐利明 | Shampoo or hair conditioner additive and method for preparing same |
| CN102579308A (en) * | 2012-03-31 | 2012-07-18 | 两面针(扬州)酒店用品有限公司 | Scalp care and itching relieving shampoo made from Chinese medicinal herb shinyleaf prickly ash root |
| CN103169630A (en) * | 2011-12-22 | 2013-06-26 | 大连创达技术交易市场有限公司 | Mosquito repellent shampoo |
| CN106491431A (en) * | 2016-11-21 | 2017-03-15 | 福建泉州飞扬生物科技有限公司 | A kind of natural botanical hair dye |
| CN108635267A (en) * | 2018-06-21 | 2018-10-12 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of deep layer moistens ferment hair film and preparation method thereof |
| CN109172480A (en) * | 2018-10-23 | 2019-01-11 | 南通季德胜科技有限公司 | A kind of antipruritic leaves shampoo of anti-mite and preparation process |
| CN109939061A (en) * | 2019-05-14 | 2019-06-28 | 连云港诗碧曼生物科技有限公司 | A kind of safe and non-stimulating white hair blackening Essence and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009062804A1 (en) * | 2007-11-14 | 2009-05-22 | Henkel Ag & Co. Kgaa | Hair treatment agent having lychee extract and taurine |
| CN101889967A (en) * | 2010-08-06 | 2010-11-24 | 徐利明 | Shampoo or hair conditioner additive and method for preparing same |
| CN103169630A (en) * | 2011-12-22 | 2013-06-26 | 大连创达技术交易市场有限公司 | Mosquito repellent shampoo |
| CN102579308A (en) * | 2012-03-31 | 2012-07-18 | 两面针(扬州)酒店用品有限公司 | Scalp care and itching relieving shampoo made from Chinese medicinal herb shinyleaf prickly ash root |
| CN106491431A (en) * | 2016-11-21 | 2017-03-15 | 福建泉州飞扬生物科技有限公司 | A kind of natural botanical hair dye |
| CN106491431B (en) * | 2016-11-21 | 2019-07-02 | 福建泉州飞扬生物科技有限公司 | A kind of natural botanical hair dye |
| CN108635267A (en) * | 2018-06-21 | 2018-10-12 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of deep layer moistens ferment hair film and preparation method thereof |
| CN109172480A (en) * | 2018-10-23 | 2019-01-11 | 南通季德胜科技有限公司 | A kind of antipruritic leaves shampoo of anti-mite and preparation process |
| CN109939061A (en) * | 2019-05-14 | 2019-06-28 | 连云港诗碧曼生物科技有限公司 | A kind of safe and non-stimulating white hair blackening Essence and preparation method thereof |
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| CN1943549B (en) | 2010-05-12 |
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