CN1730583A - Lavender flavor type environment protective latex paint and its preparation method - Google Patents
Lavender flavor type environment protective latex paint and its preparation method Download PDFInfo
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- CN1730583A CN1730583A CN 200510085791 CN200510085791A CN1730583A CN 1730583 A CN1730583 A CN 1730583A CN 200510085791 CN200510085791 CN 200510085791 CN 200510085791 A CN200510085791 A CN 200510085791A CN 1730583 A CN1730583 A CN 1730583A
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- emulsion
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Abstract
The invention discloses a Lavender flavor type environment protective latex paint and its preparation method, wherein the emulsion paint is prepared mainly from essential oil of larender, floral water, emulsion, titanium dioxide, porcelain clay, talcum powder, dispersing agent, levelling agent and water through mixing, grinding, charging ammonia and agitating homogeneously.
Description
Technical field
The present invention relates to inner wall of building coating, particularly a kind of lavender flavor type environment protective latex paint and preparation method thereof.
Background technology
Along with the continuous development of building coating technology, emulsion paint is of a great variety on market at present, and the quality of product constantly improves.For example: owing to do not contain organic compound such as formaldehyde, Pentachlorophenol, this kind emulsion paint is nontoxic, and is harmless free from environmental pollution to the person, and has good water tolerance and abrasion resistance in the prescription of environment-friendly type emulsion paint.But along with the raising of people's level of consumption, need the environment friendly emulsion paint of some specific functions, to satisfy the ever-increasing demand of people.Existing environment friendly emulsion paint then seems function singleness can't satisfy the higher consumer demand of some consumption levels.
Summary of the invention
The object of the present invention is to provide a kind of lavender flavor type environment protective latex paint, not only have an environment friendly emulsion paint anti-ly scrub, strong adhesion, free of contamination advantage, and can give out the fragrance of lavandula angustifolia, produce refreshing effect to the mind, tranquilizing and allaying excitement helps healthy.
Another object of the present invention provides the preparation method of lavandula angustifolia type environment friendly emulsion paint.
For realizing that the technical scheme that purpose of the present invention adopts is: a kind of lavender flavor type environment protective latex paint, it is made up of Herba Lysimachiae foenumgraeci quintessence oil, toilet water, emulsion, titanium dioxide, kaolin, talcum powder, dispersion agent, flow agent and water, its moiety and part by weight following (weight percent): Herba Lysimachiae foenumgraeci quintessence oil 0.1-0.4, toilet water 12-17, emulsion 13-19, titanium dioxide 14-20, kaolin 4-7, talcum powder 8-12, dispersion agent 0.5-1, flow agent 0.25-0.4, water 30-40.
The ratio range of the formula optimization weight ratio of preparation emulsion paint of the present invention is: Herba Lysimachiae foenumgraeci quintessence oil 0.2-0.3, toilet water 14-16, emulsion 15-18, titanium dioxide 16-18, kaolin 5-6, talcum powder 9-11, dispersion agent 0.6-0.8, flow agent 0.25-0.35, water 32-38.
Emulsion is vinylbenzene polyacrylic acid emulsion or polyacrylic acid emulsion or polymerizable organosilicon ACRYLIC EMULSION.Dispersion agent is Sodium hexametaphosphate 99 or ten stilbene-4,4'-bis-(1-azo-3, 4-dihydroxy-benzene)-2,2'-disulfonates.Flow agent is liquid wax class or polymerization acid amides salt.
The production method of above-mentioned each component being made emulsion paint of the present invention is:
1, Jiang Shui, toilet water and Herba Lysimachiae foenumgraeci quintessence oil add in the dispersion machine, and dispersion machine stirred 30-50 minute with 1100-1300 rev/min rotating speed, added 1/3 dispersion agent in whipping process;
2, stir after, shut down 25-35 minute, add titanium dioxide, kaolin, talcum powder and remaining dispersion agent again, start was stirred 40-60 minute with 700-900 rev/min rotating speed;
3, the material of mixing thoroughly with step 2 adds in the sand mill, grinds 100-130 minute, obtains levigate slurry;
4, levigate slurry is added in the dispersion machine, with rotating speed 320-380 rev/min stirring, add ammoniacal liquor, the ammoniacal liquor add-on is the 0.01-0.03% of levigate slurry weight ratio, regulates to add emulsion, flow agent again after pH value reaches 7-8, and stirring gets final product.
An important feature of the present invention is to contain Herba Lysimachiae foenumgraeci quintessence oil and toilet water in the prescription in the emulsion paint of the present invention.Put down in writing according to Uygur's medicinal material standard that Xinjiang science and technology health press in October, 1999 first version is published: lavandula angustifolia belongs to the dry aerial parts of the narrow leaf lavandula angustifolia of Labiatae (LaVandula angustifolia Mill), and pluck, dry in the shade summer.Its composition herb contains and contains Geraniol, safrole, isothymol, phantol, geraniol, citral, vernol, tonka bean camphor etc. in volatile oil 1%-3%, the oil.For heart, a kind of calm and tonic effect is arranged, conduce to sleep and diminish inflammation.Herba Lysimachiae foenumgraeci quintessence oil is wide, the most effective volatile oil of purposes, and its attribute display goes out the balance between a kind of Yin and Yang, belongs to neutral, and is obvious for Ginseng Extract, calm neural effect.
Toilet water is to add the makeup that volatile oil that fragrant organic substance such as rose, rose extracts is made in the Diluted Alcohol.
Volatile oil in Herba Lysimachiae foenumgraeci quintessence oil and the toilet water is complicated small organic molecule, as the important component part in the emulsion paint of the present invention.Emulsion paint of the present invention is coated on the inner wall surface in room, and the volatile oil small molecules has suitable biological activity within a certain period of time in the emulsion paint, can give out the fragrance of lavandula angustifolia in the long time.Many compositions in Herba Lysimachiae foenumgraeci quintessence oil and the toilet water such as Geraniol, phantol, acetate phantol, terpene compound etc. all can directly enter tissue and blood circulation participates in metabolism from skin organ and respiratory organs by the human body respiration effect, have produce refreshing effect to the mind, the effect of tranquilizing and allaying excitement.The fragrance of lavandula angustifolia has mosquito repellent and keeps away worm, the germ-resistant effect of detoxicating.
Subordinate list 1 is the survey report table 1 of Herba Lysimachiae foenumgraeci quintessence oil
Assay gathers | ||||
Sequence number | Interventions Requested title and unit | Technical requirements | Assay | Individual event is judged |
1 | Outward appearance | Clarification, fluxion | Meet the requirements | Meet |
2 | Color and luster | Little Huang is to light yellow | Little yellow | Meet |
3 | Fragrance | Pure, the characteristic perfume of homemade lavender flower piece in having | Fragrance still can | Meet |
4 | Relative density (20/20 ℃) | 0.876-0.895 | 0.883 | Meet |
5 | Refractive index (20 ℃) | 1.4570-1.4640 | 1.46 | Meet |
6 | Specific rotation (20 ℃) | -11.0°~-7.5° | -9.9° | Meet |
7 | Miscible degree (20 ℃) | 1 volume sample is settled solution in the ethanol that is no more than 3 volumes 70% (V/V) | Meet the requirements | Meet |
8 | Acid number | ≤1.0 | 0.5 | Meet |
9 | Ester value (in phanteine) | ≥108 | 132 | Meet |
10 | Camphor content % | ≤0.5 | 0.2 | Meet |
Table 2 is for to test by the standard of GB/T9756-2001 " synthetic resin emulsion interior wall coating " to the capability and performance of lavender flavor type environment protective latex paint of the present invention.
Table 2
Sequence number | Interventions Requested | Unit | Technical requirements | Assay | Individual event is judged |
1 | Application property | The road | It is accessible to brush two roads | Meet | Qualified |
2 | Appearance of film | / | Normally | Meet | Qualified |
3 | Abrasion resistance | Inferior | ≥200 | >200 | Qualified |
Application property, appearance of film and the abrasion resistance of table 2 pair lavender flavor type environment protective latex paint of the present invention are checked.Assay shows that lavender flavor type environment protective latex paint of the present invention meets the standard of GB/T9756-2001 " synthetic resin emulsion interior wall coating " fully.
Table 3 is for to test according to the GB18582-2001 standard to the environmental-protecting performance of lavender flavor type environment protective latex paint of the present invention.
Table 3
Sequence number | Interventions Requested | Unit | Technical requirements | Assay | Individual event is judged |
1 | Free formaldehyde | g/kg | ≤0.1 | 0.1 | Qualified |
Assay according to table 3 shows that the free formaldehyde content in the lavender flavor type environment protective coating of the present invention meets the standard of GB18582-2001 " harmful substance contents in indoor decorating material, the interior wall coating ".
By above-mentioned survey report show that anti-that lavender flavor type environment protective latex paint of the present invention not only has an environment friendly emulsion paint scrubbed, strong adhesion, free of contamination function and advantage, but also can give out lavandula angustifolia fragrance, produce refreshing effect to the mind, tranquilizing and allaying excitement, help healthy.
Embodiment
Take by weighing raw material (kg) by following proportioning:
Herba Lysimachiae foenumgraeci quintessence oil 0.2, toilet water 14.4, vinylbenzene polyacrylic acid emulsion 16, titanium dioxide 17, kaolin 5.4, talcum powder 10, Sodium hexametaphosphate 99 0.7, polymerization amide salt 0.3, water 36.
Production method is as follows:
1, Jiang Shui, toilet water and Herba Lysimachiae foenumgraeci quintessence oil add in the dispersion machine, and dispersion machine stirred 45 minutes with 1200 rev/mins rotating speed, added 1/3 Sodium hexametaphosphate 99 in whipping process;
2, stir after, shut down 30 minutes, add titanium dioxide, kaolin, talcum powder and remaining Sodium hexametaphosphate 99 again, start was stirred 50 minutes with 800 rev/mins rotating speed;
3, the material of mixing thoroughly with step 2 adds in the sand mill, grinds 120 minutes, obtains levigate slurry;
4, levigate slurry is added in the dispersion machine, with 360 rev/mins of stirrings of rotating speed, add ammoniacal liquor, the ammoniacal liquor add-on is the 0.01-0.03% of levigate slurry weight ratio, add vinylbenzene polyacrylic acid emulsion, polymerization amide salt again after the adjusting pH value reaches 7-8, stir to pack and dispatch from the factory.
Claims (6)
1, a kind of lavender flavor type environment protective latex paint is characterized in that the weight percent of this latex paint formulation is:
Herba Lysimachiae foenumgraeci quintessence oil 0.1-0.4, toilet water 12-17, emulsion 13-19, titanium dioxide 14-20, kaolin 4-7, talcum powder 8-12, dispersion agent 0.5-1, flow agent 0.25-0.4, water 30-40.
2, lavender flavor type environment protective latex paint according to claim 1, the weight percent that it is characterized in that the prescription of this emulsion paint are Herba Lysimachiae foenumgraeci quintessence oil 0.2-0.3, toilet water 14-16, emulsion 15-18, titanium dioxide 16-18, kaolin 5-6, talcum powder 9-11, dispersion agent 0.6-0.8, flow agent 0.25-0.35, water 32-38.
3, lavender flavor type environment protective latex paint according to claim 1 and 2 is characterized in that emulsion is vinylbenzene polyacrylic acid emulsion or polyacrylic acid emulsion or polymerizable organosilicon ACRYLIC EMULSION.
4, lavender flavor type environment protective latex paint according to claim 1 and 2 is characterized in that dispersion agent is Sodium hexametaphosphate 99 or ten stilbene-4,4'-bis-(1-azo-3, 4-dihydroxy-benzene)-2,2'-disulfonates.
5, lavender flavor type environment protective latex paint according to claim 1 and 2 is characterized in that flow agent is liquid wax class or polymerization acid amides salt.
6, the preparation method of lavender flavor type environment protective latex paint according to claim 1, it is characterized in that having the following steps: (1), water, toilet water and Herba Lysimachiae foenumgraeci quintessence oil are added in the dispersion machine, dispersion machine stirred 30-50 minute with 1100-1300 rev/min rotating speed, added 1/3 dispersion agent in whipping process; (2), stir after, shut down 25-35 minute, add titanium dioxide, kaolin, talcum powder and remaining dispersion agent again, start was stirred 40-60 minute with 700-900 rev/min rotating speed; (3), the material of mixing thoroughly of step (2) is added in the sand mill, ground 100-130 minute, obtain levigate slurry; (4), levigate slurry is added in the dispersion machine, with rotating speed 320-380 rev/min stirring, add ammoniacal liquor, the ammoniacal liquor add-on is the 0.01-0.03% of levigate slurry weight ratio, regulates to add emulsion, flow agent again after pH value reaches 7-8, and stirring gets final product.
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Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101781489B (en) * | 2009-12-31 | 2012-03-14 | 潍坊三强集团有限公司 | Method for producing interior wall healthcare latex paint by using lavender natural extract |
CN102796428A (en) * | 2012-08-31 | 2012-11-28 | 植彩美瑞涂料(北京)有限公司 | Plant paint and preparation method thereof |
CN103242729A (en) * | 2013-05-31 | 2013-08-14 | 滁州市宏源喷涂有限公司 | Anti-mosquito water-soluble environmental-friendly nanometer activated carbon wall paint and preparation method thereof |
CN103709336A (en) * | 2012-09-29 | 2014-04-09 | 上海绿色建材研究中心有限公司 | Herbal essential oil emulsion covered by utilization of core-shell technology, and preparation method thereof |
CN103709842A (en) * | 2012-09-29 | 2014-04-09 | 上海绿色建材研究中心有限公司 | Herbal essence health paint and preparation method thereof |
CN103897507A (en) * | 2013-11-11 | 2014-07-02 | 东南大学 | Preparation raw material and method of environment-friendly emulsion paint |
CN104945987A (en) * | 2015-07-16 | 2015-09-30 | 松阳县凯华化工有限公司 | Emulsion paint with function of slowly releasing fragrance and preparation method thereof |
CN105949891A (en) * | 2016-05-14 | 2016-09-21 | 河北晨阳工贸集团有限公司 | Antibacterial interior wall water paint and preparation method thereof |
CN106118167A (en) * | 2016-07-14 | 2016-11-16 | 太仓卡斯特姆新材料有限公司 | A kind of high-quality anti-rusting antibiotic coating and preparation thereof and application process |
CN106189734A (en) * | 2016-07-18 | 2016-12-07 | 贵州合润铝业新材料科技股份有限公司 | A kind of can the building wall water paint of expelling mosquito |
CN107384068A (en) * | 2017-06-26 | 2017-11-24 | 界首市通泽建材销售有限公司 | A kind of preparation method of high-quality mosquito repellent interior wall coating |
CN108659640A (en) * | 2018-03-21 | 2018-10-16 | 河北晨阳工贸集团有限公司 | Except the Chinese herbal medicine interior wall coating and preparation method thereof of formaldehyde |
-
2005
- 2005-08-17 CN CN 200510085791 patent/CN1730583A/en active Pending
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101781489B (en) * | 2009-12-31 | 2012-03-14 | 潍坊三强集团有限公司 | Method for producing interior wall healthcare latex paint by using lavender natural extract |
CN102796428A (en) * | 2012-08-31 | 2012-11-28 | 植彩美瑞涂料(北京)有限公司 | Plant paint and preparation method thereof |
CN103709336B (en) * | 2012-09-29 | 2016-02-17 | 上海绿色建材研究中心有限公司 | Coated essential oils of herbs emulsion of a kind of Core-shell technology and preparation method thereof |
CN103709336A (en) * | 2012-09-29 | 2014-04-09 | 上海绿色建材研究中心有限公司 | Herbal essential oil emulsion covered by utilization of core-shell technology, and preparation method thereof |
CN103709842A (en) * | 2012-09-29 | 2014-04-09 | 上海绿色建材研究中心有限公司 | Herbal essence health paint and preparation method thereof |
CN103709842B (en) * | 2012-09-29 | 2016-01-20 | 上海绿色建材研究中心有限公司 | A kind of Herbal essence health paint and preparation method thereof |
CN103242729A (en) * | 2013-05-31 | 2013-08-14 | 滁州市宏源喷涂有限公司 | Anti-mosquito water-soluble environmental-friendly nanometer activated carbon wall paint and preparation method thereof |
CN103897507A (en) * | 2013-11-11 | 2014-07-02 | 东南大学 | Preparation raw material and method of environment-friendly emulsion paint |
CN104945987A (en) * | 2015-07-16 | 2015-09-30 | 松阳县凯华化工有限公司 | Emulsion paint with function of slowly releasing fragrance and preparation method thereof |
CN105949891A (en) * | 2016-05-14 | 2016-09-21 | 河北晨阳工贸集团有限公司 | Antibacterial interior wall water paint and preparation method thereof |
CN106118167A (en) * | 2016-07-14 | 2016-11-16 | 太仓卡斯特姆新材料有限公司 | A kind of high-quality anti-rusting antibiotic coating and preparation thereof and application process |
CN106189734A (en) * | 2016-07-18 | 2016-12-07 | 贵州合润铝业新材料科技股份有限公司 | A kind of can the building wall water paint of expelling mosquito |
CN107384068A (en) * | 2017-06-26 | 2017-11-24 | 界首市通泽建材销售有限公司 | A kind of preparation method of high-quality mosquito repellent interior wall coating |
CN107384068B (en) * | 2017-06-26 | 2018-10-02 | 界首市通泽建材销售有限公司 | A kind of preparation method of high-quality mosquito repellent interior wall coating |
CN108659640A (en) * | 2018-03-21 | 2018-10-16 | 河北晨阳工贸集团有限公司 | Except the Chinese herbal medicine interior wall coating and preparation method thereof of formaldehyde |
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