CN1402993A - Water dispersed nimbin granule and its prepn - Google Patents
Water dispersed nimbin granule and its prepn Download PDFInfo
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- CN1402993A CN1402993A CN02133828.0A CN02133828A CN1402993A CN 1402993 A CN1402993 A CN 1402993A CN 02133828 A CN02133828 A CN 02133828A CN 1402993 A CN1402993 A CN 1402993A
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- nimbin
- water dispersed
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Abstract
The present invention is water dispersed nimbin granule and its preparation. One formula consists of nimbin 0.05-60 wt% and the assistant the rest. One other formula consists of nimbin 0.05-50 wt.%, humectant 5-15 wt%, adhesive 10-20 wt%, disintegrating agent 10-30 wt% and carrier 20-60 wt%. The preparation process includes superfine grinding, pelletizing, drying, sieving, inspection and other steps.
Description
Technical field
The invention belongs to vegetable insecticide and preparation method thereof, be specifically related to water dispersed nimbin granule and preparation method.
Technical background
Now, a large amount of chemical insecticides that use on agricultural, because its toxic and side effect, the protection for the mankind, livestock and natural environment has all brought great harm and many negative effects.Thereby such as using the person poultry poisoning of institute's initiations generation to put aside poisoning for a long time, manslaughtering a large amount of useful natural enemies and be harmful to the ecotope disequilibrium that natural enemy easily develops immunity to drugs and causes ... or the like.Therefore, many developed countries and area have been ordered and have been forbidden promoting the use of chemical insecticide, make great efforts development and apply biopesticide.So, no matter be domestic or external, all in the usage ratio that reduces chemical pesticide by every means as early as possible.
Summary of the invention
The objective of the invention is to disclose and a kind of nimbin is processed into water dispersible granules, avoid with an organic solvent, improve the content and the stability of nimbin in the preparation, improve drug effect, be convenient to the water dispersed nimbin granule and the preparation method that store and transport and use.
Prescription of the present invention is
Prescription one (weight %):
All the other are auxiliary agent for nimbin 0.05%-60%.
Prescription two (weight %):
Nimbin 0.05%-50% wetting agent 5%-15% binding agent 10%-20%
Disintegrant 10%-30% carrier 20%-60%.
The nimbin of above-mentioned prescription is one or more among seal chinaberry A, B, D, E, F, G, H, I, K, the L.Can be the pure product of nimbin, also can be neem oil, also can be vegetable oil extraction thing or the nimbin preparation that contains nimbin.When use was multiple, total amount can not be greater than the deal of prescription proportion.Nimbin can be pure product, also can be neem oil, also can be vegetable oil extraction thing or the nimbin preparation that contains nimbin.
The auxiliary agent of above-mentioned prescription is made up of wetting agent, binding agent, disintegrant and carrier.
Wetting agent is: saponin, lignosulfite; the hydrolysate of animal waste, alkyl sulfate, alkene sulfonate; benzene sulfonamide acid alkali metal salt and amine salt, dialkyl group succinic acid sulfonate sodium, fatty alcohol, fatty acid amide N methyl taurine sodium salt, aliphatic alcohol polyethenoxy sulphate, alkyl tea sodium sulfonate, fatty acid or fatty acid ester sulphate, sodium lignin sulfonate, petroleum sodium sulfonate, alkyl biphenyl ether sulfonic acid sodium, tea phenol sulfonic formaldehyde condensation compound sodium salt, polyoxyethylene carboxylate sodium sulfonate and amine salt, alkylphenol polyoxyethylene, fatty alcohol-polyoxyethylene ether.
Binding agent is: starch, dextrin, gum Arabic, soybean protein, casein, gelatine and gelatin, sodium silicate, gypsum, poly-cruel vinyl acetate, polyvinyl alcohol, rosin, shellac, paraffin, pitch, ethene-vinyl acetate copolymer resins.
Disintegrant is: sulphur ammonium, calcium chloride, salt, aluminium chloride, urea, bentonite.
Carrier can be: soybean, tobacco, acorn, corncob cellulose, rice husk, sulphur, diatomite, quicklime, magnesium lime, apatite, calcite, dolomite, gypsum, mica, talcum, pyrophyllite, clay, kaolinite, nacrite, dickite, anauxite, montmorillonite, activity go up in vain, float stone etc.
Manufacture craft of the present invention is;
The formulation material mixture is carried out granulation after the ultra-fine grinding, drying, screening, sample analysis, qualified can the packing.
The present invention has following advantage:
1, present seal chinaberry preparation mostly is missible oil greatly, it is a kind of compound from plant seal chinaberry, has good insecticidal activity, very fast degraded in environment, do not injure natural enemy and other non-target organism, its shortcoming is unstable, and the processing formulation is less, consume a large amount of organic solvents, and cause pollution environment.After nimbin is made water dispersible granules, can widen the scope of application of medicament, prolong the lasting period, improve drug effect.Save organic solvent, do not cause pollution environment.
2, after nimbin is made water dispersible granules,, not only alleviated destruction, and reduced production cost ecotope owing to do not contain organic solution.
3, after nimbin is made water dispersible granules, can greatly alleviate toxic action to various natural enemies.
4, after nimbin is made water dispersible granules, be convenient to the packing storing.
Embodiment
In order to understand the present invention better, describe the technology contents of invention below in detail with example.
Embodiment one: produce 3% nimbin water-dispersible granules:
(1) adds 8% (weight) calcium lignosulfonate as wetting agent;
(2) add 9% (weight) ethene-vinyl acetate copolymer resins as stick;
(3) add 60% (weight) atlapulgite as carrier;
(4) add 20% (weight) urea as disintegrant;
(5) add 3% (weight) nimbin;
Mixture is carried out granulation after the ultra-fine grinding, drying, screening, sample analysis, qualified can the packing.
Embodiment two: produce 40% nimbin water-dispersible granules;
(1) adds 8% (weight) sodium lignin sulfonate as wetting agent;
(2) add 19% (weight) polyvinyl acetate as stick;
(3) add 20% (weight) anauxite as carrier;
(4) add 13% (weight) bentonite as disintegrant;
(5) add 40% (weight) nimbin;
Mixture is carried out granulation after the ultra-fine grinding, drying, screening, sample analysis, eligible can be packed.
With 3% nimbin water-dispersible granules of the present invention the field efficacy of diamondback moth larvae is illustrated the advantage of preparation of the present invention below:
After 3% nimbin water-dispersible granules of the present invention, 0.3% nimbin emulsion diluted 20000 times, 1500 times respectively to diamondback moth larvae spraying handle, the 3rd, 7, the 14 day investigation insect population rate of going down is respectively 50.25%, 40.45% after medication; The 7th day the insect population rate of going down is respectively 84.50%, 80.63%; The 14th day the insect population rate of going down is respectively 92.91%, 60.21%.The preventive effect that 3% nimbin water-dispersible granules of the present invention is described is higher than 0.3% nimbin emulsion, both can reduce dosage, can prolong the lasting period of medicament again.
Claims (3)
1, a kind of water dispersed nimbin granule and preparation method is characterized in that:
Prescription one (weight %):
All the other are auxiliary agent for nimbin 0.05%-60%.
2, a kind of water dispersed nimbin granule according to claim 1 and preparation method is characterized in that:
Prescription two (weight %):
Nimbin 0.05%-50% wetting agent 5%-15% binding agent 10%-20%
Disintegrant 10%-30% carrier 20%-60%.
3 a kind of water dispersed nimbin granule according to claim 1 and preparation methods is characterized in that:,
Manufacture craft is;
With granulation after the formulation material ultra-fine grinding, drying, screening, analytical control, eligible warehouse-in.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021338280A CN1178579C (en) | 2002-09-28 | 2002-09-28 | Water dispersed nimbin granule and its prepn |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021338280A CN1178579C (en) | 2002-09-28 | 2002-09-28 | Water dispersed nimbin granule and its prepn |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1402993A true CN1402993A (en) | 2003-03-19 |
| CN1178579C CN1178579C (en) | 2004-12-08 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB021338280A Expired - Fee Related CN1178579C (en) | 2002-09-28 | 2002-09-28 | Water dispersed nimbin granule and its prepn |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1178579C (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101961017A (en) * | 2010-10-20 | 2011-02-02 | 华南理工大学 | Flubendiamide and azadirachtin compounded water dispersible granules and preparation method thereof |
| CN103627194A (en) * | 2013-11-05 | 2014-03-12 | 林世旺 | Degradable foamed buffer material |
| CN109315429A (en) * | 2018-11-30 | 2019-02-12 | 成都绿金生物科技有限责任公司 | A kind of water dispersed nimbin granule and preparation method thereof of prevention and control anthracnose of tobacco |
| CN111820230A (en) * | 2020-08-11 | 2020-10-27 | 成都绿金生物科技有限责任公司 | Azadirachtin for preventing and treating ginger nematode and preparation method thereof |
-
2002
- 2002-09-28 CN CNB021338280A patent/CN1178579C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101961017A (en) * | 2010-10-20 | 2011-02-02 | 华南理工大学 | Flubendiamide and azadirachtin compounded water dispersible granules and preparation method thereof |
| CN101961017B (en) * | 2010-10-20 | 2013-11-13 | 华南理工大学 | Flubendiamide and azadirachtin compounded water dispersible granules and preparation method thereof |
| CN103627194A (en) * | 2013-11-05 | 2014-03-12 | 林世旺 | Degradable foamed buffer material |
| CN103627194B (en) * | 2013-11-05 | 2015-11-18 | 林世旺 | A kind of degradable foaming type cushioning material |
| CN109315429A (en) * | 2018-11-30 | 2019-02-12 | 成都绿金生物科技有限责任公司 | A kind of water dispersed nimbin granule and preparation method thereof of prevention and control anthracnose of tobacco |
| CN111820230A (en) * | 2020-08-11 | 2020-10-27 | 成都绿金生物科技有限责任公司 | Azadirachtin for preventing and treating ginger nematode and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1178579C (en) | 2004-12-08 |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: CHENGDU LVJIN HI-TECH CO.LTD. Free format text: FORMER OWNER: CHENGDU LVJIN BIOTECHNOLOGY CO.,LTD. Effective date: 20071026 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20071026 Address after: High tech Zone Gaopeng road in Chengdu city of Sichuan province 610041 No. 5 A innovation center, 3 floor Patentee after: CHENGDU GREENGOLD HIGH-TECH Co.,Ltd. Address before: High tech Zone Gaopeng road in Chengdu city of Sichuan province 610041 No. 5 Chengdu gold green biotechnology limited liability company Patentee before: CHENGDU LYUJIN BIOLOGICAL SCIENCE & TECHNOLOGY CO.,LTD. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20041208 Termination date: 20210928 |