CN1613312A - Agricultural bactericide containing cyclosulfamuron and aureofuscin, its preparation and uses - Google Patents
Agricultural bactericide containing cyclosulfamuron and aureofuscin, its preparation and uses Download PDFInfo
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- CN1613312A CN1613312A CN 200310108359 CN200310108359A CN1613312A CN 1613312 A CN1613312 A CN 1613312A CN 200310108359 CN200310108359 CN 200310108359 CN 200310108359 A CN200310108359 A CN 200310108359A CN 1613312 A CN1613312 A CN 1613312A
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- jinggangmeisu
- golden caryomycin
- caryomycin
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Abstract
An agricultural bactericide for preventing and treating the hoja blanca, bacterial streak disease, etc of rice, ulcer of orange, etc is prepared from aureonuclemycin, jianganmycin, wetting agent, and filler. Its advantages are broad spectrum and high effect.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of binary built composition and method of making the same and application that contains golden caryomycin and jinggangmeisu.
Background technology
Gold caryomycin (aureonuclemycin) is the disinfectant use in agriculture of a kind of new structure of being provided by the inventor, in application on March 18th, 1987 Chinese invention patent, and in (the patent No.: ZL87100250.7) of obtaining the authorization on July 15 nineteen ninety-five.Its molecular structure is:
Gold caryomycin former medicine outward appearance be that white golden caryomycin content is insoluble in various organic solvents and water more than 90% to the crystallization of gray powder powder, and fusing point is (decomposition) more than 146 ℃.
According to Chinese invention patent ZL87100250.7, golden caryomycin can be by cultivating streptomyces aureus Suzhou mutation SP-371, by fermentation, and separation and purification from zymotic fluid and making.
This bactericide can be used for preventing and treating the disinfectant use in agriculture of the bacterial disease that bacterial blight of rice, bacterial leaf streak of rice etc. cause by the wax yellow Bacillus bacteria of system (Xanthomonas), the crop fungal disease is not had effect, and improper use may cause the local poisoning of paddy rice.
Jinggangmeisu (jinggangmycin) is the disinfectant use in agriculture that is used to prevent and treat rice sheath blight disease, and its molecular structure is:
The former medicine outward appearance of jinggangmeisu is coffee-like powder, contains jinggangmeisu more than 50%, and is water-soluble fully, 102 ℃ of fusing points, the easily moisture absorption.
The former medicine of jinggangmeisu can be by cultivating the ridge mutation of streptomyces hygroscopicus well, and by fermentation, separation and purification from zymotic fluid and making perhaps obtains by commercially available.
Jinggangmycin does not have control efficiency to bacterial disease.Therefore said two devices all has certain limitation as disinfectant use in agriculture when using separately.
Summary of the invention
Purpose of the present invention just is to provide a kind of wetting powder that utilizes golden caryomycin and jinggangmeisu binary built to be prepared into.
Another object of the present invention is to provide a kind of golden caryomycin and jinggangmeisu and additive compound to make the production technology of wetting powder.
The application that provides a kind of golden caryomycin and jinggangmeisu and additive compound to make wetting powder is provided another purpose of the present invention.
In order to achieve the above object, the present invention is achieved in that
A kind of binary built composition that contains golden caryomycin and jinggangmeisu involved in the present invention composed as follows:
(1). weight concentration is the golden caryomycin of 5%-30%;
(2). weight concentration is the jinggangmeisu of 5%-60%;
(3). weight concentration is the wetting agent of 1%-5%;
(4). weight concentration is the filling additive of 20%-60%.
The binary built wetting powder that contains golden caryomycin and jinggangmeisu of the present invention can prepare by the following method:
The former medicine of golden caryomycin by mechanical crushing, is added jinggangmeisu again, mix with wetting agent, filling additive, mechanical crushing is mixed again again, at last with mixing packing behind the comminution by gas stream.
The used wetting agent of the present invention is dodecyl sodium sulfate, draws back monomers or composite such as powder that filling additive is monomers or composite such as diatomite, talcum powder, potter's clay, lignosulfonates.
The composition that contains golden caryomycin and jinggangmeisu of the present invention can be used for preventing and treating following crop pest: bacterial blight of rice, bacterial stripe, banded sclerotial blight, citrus bacterial canker disease.
The wetting powder that golden caryomycin of utilization of the present invention and jinggangmeisu binary built are prepared into, fungicidal spectrum and drug effect can improve greatly, residual significantly reducing, applicable crops increases, and to the rice drug misadventuring sx, has reduced use cost simultaneously.
Embodiment
The present invention give further instruction in order to illustrate better below by embodiment:
Embodiment 1:
In 1000 ml beakers, add golden caryomycin (folding hundred) 100 grams, jinggangmeisu (folding hundred) 33 grams, draw back powder 6 grams, dodecyl sodium sulfate 3 grams, lignosulfonates 6 grams, diatomite 185 grams, mix, earlier through mechanical crushing, as use the SF-100 type cracker of Shanghai Chinese traditional medicine machine factory, pass through comminution by gas stream again, as using the AO type airslide disintegrating mill of Sino-Japan joint Yixing clear powder machinery company, mix, promptly obtain the binary built composition that contains golden caryomycin and jinggangmeisu of the present invention.
Embodiment 2:
In 1000 ml beakers, add golden caryomycin (folding hundred) 50 grams, jinggangmeisu (folding hundred) 100 grams, draw back powder 6 grams, dodecyl sodium sulfate 3 grams, lignosulfonates 6 grams, diatomite 168 grams, mix, earlier through mechanical crushing, as use the SF-100 type cracker of Shanghai Chinese traditional medicine machine factory, pass through comminution by gas stream again, as using the AO type airslide disintegrating mill of Sino-Japan joint Yixing clear powder machinery company, mix, promptly obtain the binary built composition that contains golden caryomycin and jinggangmeisu of the present invention.
Embodiment 3:
In 1000 ml beakers, add golden caryomycin (folding hundred) 30 grams, jinggangmeisu (folding hundred) 180 grams, draw back powder 6 grams, dodecyl sodium sulfate 3 grams, lignosulfonates 6 grams, diatomite 108 grams, mix, earlier through mechanical crushing, as use the SF-100 type cracker of Shanghai Chinese traditional medicine machine factory, pass through comminution by gas stream again, as using the AO type airslide disintegrating mill of Sino-Japan joint Yixing clear powder machinery company, mix, promptly obtain the binary built composition that contains golden caryomycin and jinggangmeisu of the present invention.
Embodiment 4:
With the bactericidal agent for preventing and treating bacterial blight of rice that the embodiment of the invention 1,2,3 obtains, get it filled agent 500 grams, 250 grams, 125 grams add in 750 kg of water, after stirring, dissolving, in the spraying control of rice pathogenesis initial stage, spray medicine more once after 6 days, according to incidence investigation prevention effect.Result of the test sees Table 1.
Embodiment 5:
With the bactericidal agent for preventing and treating bacterial leaf streak of rice that the embodiment of the invention 1,2,3 obtains, get it filled agent 500 grams, 250 grams, 125 grams add in 750 kg of water, after stirring, dissolving, in the spraying control of rice pathogenesis initial stage, spray medicine more once after 6 days, according to incidence investigation prevention effect.Result of the test sees Table 1.
Embodiment 6:
With the bactericidal agent for preventing and treating rice sheath blight disease that the embodiment of the invention 1,2,3 obtains, get it filled agent 500 grams, 250 grams, 125 grams add in 750 kg of water, after stirring, dissolving, in the spraying control of rice pathogenesis initial stage, spray medicine more once after 6 days, according to incidence investigation prevention effect.Result of the test sees Table 1.
Embodiment 7:
With the bactericidal agent for preventing and treating citrus bacterial canker disease that the embodiment of the invention 1,2,3 obtains, get it filled agent 700 grams, 350 grams, 175 grams add in 1050 kg of water, after stirring, dissolving, the spraying control is sprayed medicine once after 6 days, again according to incidence investigation prevention effect when the oranges and tangerines spring tip, summer shoot or autumn growth.Result of the test sees Table 2.
The effect such as the following table of the various diseases of bactericidal agent for preventing and treating of the present invention.
Table 1 is prevented and treated the control efficiency of bacterial blight of rice, bacterial stripe, banded sclerotial blight
| Handle medicament | Dosage, commodity amount gram/hectare | Control efficiency (%) | The poisoning situation | ||
| Bacterial leaf spot | The slice disease | Banded sclerotial blight | |||
| Embodiment 1 | 500 | ?87.8 | ?89.2 | ?85.4 | Do not have |
| 250 | ?82.9 | ?78.6 | ?80.2 | Do not have | |
| 125 | ?66.3 | ?73.2 | ?76.2 | Do not have | |
| Embodiment 2 | 500 | ?82.3 | ?90.1 | ?88.2 | Do not have |
| 250 | ?73.5 | ?83.1 | ?86.4 | Do not have | |
| 125 | ?80.7 | ?66.4 | ?81.3 | Do not have | |
| Embodiment 3 | 500 | ?83.3 | ?89.9 | ?94.3 | Do not have |
| 250 | ?79.9 | ?79.3 | ?91.2 | Do not have | |
| 125 | ?79.6 | ?76.2 | ?90.2 | Do not have | |
| 30% gold medal caryomycin WP | 500 | ?81.7 | ?85.3 | ?0 | The little Huang of blade tip |
| 250 | ?80.6 | ?77.8 | ?0 | The little Huang of blade tip | |
| 125 | ?74.6 | ?72.4 | ?0 | Do not have | |
| 5% jinggangmeisu | 1500 | ?5.1 | ?7.9 | ?88.6 | Do not have |
| Blank | / | Do not have | |||
Table 2, the control efficiency (%) of control citrus bacterial canker disease
| Handle medicament | Dosage (commodity amount, gram/hectare) | Control efficiency | The poisoning situation |
| Embodiment 1 | 700 | ?82.3 | Do not have |
| 350 | ?79.2 | Do not have | |
| 175 | ?66.7 | Do not have | |
| Embodiment 2 | 700 | ?84.3 | Do not have |
| 350 | ?79.8 | Do not have | |
| 175 | ?70.4 | Do not have | |
| Embodiment 3 | 700 | ?86.8 | Do not have |
| 350 | ?70.2 | Do not have | |
| 175 | ?73.4 | Do not have | |
| 30% gold medal caryomycin WP | 700 | ?79.8 | Do not have |
| 350 | ?76.2 | Do not have | |
| 175 | ?69.6 | Do not have | |
| 5% jinggangmeisu | 2100 | ?5.1 | Do not have |
| Blank | / | ?/ | Do not have |
Composite disinfectant use in agriculture of the present invention is compared with original medicament, and following advantage is arranged:
The drug injury problem that has produced when 1, having overcome golden caryomycin and use on paddy rice, it is safer that product is used.
2, overcome the limitation that golden caryomycin can only be prevented and treated bacterial disease, enlarged antimicrobial spectrum, the user only needs a drug can prevent and treat the banded sclerotial blight of bacteroidal bacterial leaf-blight or cecospora spot and fungoid simultaneously, has reduced cost of labor.
3, reduce the usage amount of golden caryomycin, reduced drug cost.
Claims (9)
1, a kind of composition that contains golden caryomycin and jinggangmeisu is characterized in that being made up of active ingredient, wetting agent, filling additive.
2, a kind of composition that contains golden caryomycin and jinggangmeisu according to claim 1 is characterized in that described active ingredient is golden caryomycin and jinggangmeisu.
3, a kind of composition that contains golden caryomycin and jinggangmeisu according to claim 1, the weight concentration that it is characterized in that described active ingredient is the golden caryomycin of 5%-30% and the jinggangmeisu of 5%-60%.
4, a kind of composition that contains golden caryomycin and jinggangmeisu according to claim 1 is characterized in that described wetting agent is dodecyl sodium sulfate, draws back powder or composite.
5, a kind of composition that contains golden caryomycin and jinggangmeisu according to claim 1, the weight concentration that it is characterized in that described wetting agent is 1%-5%.
6, a kind of composition that contains golden caryomycin and jinggangmeisu according to claim 1 is characterized in that described filling additive is diatomite, talcum powder, potter's clay, sodium lignin sulfonate or composite.
7, a kind of composition that contains golden caryomycin and jinggangmeisu according to claim 1, the weight concentration that it is characterized in that described filling additive is 20%-60%.
8, according to the described a kind of preparation of compositions method that contains golden caryomycin and jinggangmeisu of claim 1, it is characterized in that golden caryomycin, jinggangmeisu, wetting agent, filling additive are mixed, pulverize, mix and get final product.
9, a kind of application that contains the composition of golden caryomycin and jinggangmeisu according to claim 1 is characterized in that described bactericide can prevent and treat following crop pest: bacterial blight of rice, bacterial stripe, banded sclerotial blight, citrus bacterial canker disease.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310108359 CN1613312A (en) | 2003-11-04 | 2003-11-04 | Agricultural bactericide containing cyclosulfamuron and aureofuscin, its preparation and uses |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200310108359 CN1613312A (en) | 2003-11-04 | 2003-11-04 | Agricultural bactericide containing cyclosulfamuron and aureofuscin, its preparation and uses |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1613312A true CN1613312A (en) | 2005-05-11 |
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| CN 200310108359 Pending CN1613312A (en) | 2003-11-04 | 2003-11-04 | Agricultural bactericide containing cyclosulfamuron and aureofuscin, its preparation and uses |
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| CN (1) | CN1613312A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105475303A (en) * | 2015-12-09 | 2016-04-13 | 陕西麦可罗生物科技有限公司 | Pesticide composition containing kasugamycin and aureonucleomycin |
| CN105494370A (en) * | 2015-12-09 | 2016-04-20 | 陕西麦可罗生物科技有限公司 | Pesticide composition prepared from aureonucleomycin and tetramycin |
| CN107668049A (en) * | 2017-10-24 | 2018-02-09 | 张颂忠 | A kind of complex composition containing gold alloy hydride and Osthole |
| CN107711860A (en) * | 2017-10-24 | 2018-02-23 | 张锡林 | A kind of complex composition containing gold alloy hydride and doxycycline monohydrate |
| CN107743970A (en) * | 2017-12-06 | 2018-03-02 | 惠州市支持网知识产权运营有限公司 | Bactericidal composition containing psoralen and gold alloy hydride |
| CN108531488A (en) * | 2018-03-30 | 2018-09-14 | 辽宁大学 | New controlling gene AurT and its application in improving aureofuscin yield |
| CN109662097A (en) * | 2018-12-18 | 2019-04-23 | 广西壮族自治区农业科学院园艺研究所 | A kind of composition pesticide for preventing and treating citrus bacterial canker disease |
| CN114521566A (en) * | 2022-02-21 | 2022-05-24 | 广西壮族自治区农业科学院 | Synergistic composition for preventing and treating soft rot of taro |
-
2003
- 2003-11-04 CN CN 200310108359 patent/CN1613312A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105475303A (en) * | 2015-12-09 | 2016-04-13 | 陕西麦可罗生物科技有限公司 | Pesticide composition containing kasugamycin and aureonucleomycin |
| CN105494370A (en) * | 2015-12-09 | 2016-04-20 | 陕西麦可罗生物科技有限公司 | Pesticide composition prepared from aureonucleomycin and tetramycin |
| CN105475303B (en) * | 2015-12-09 | 2018-02-27 | 陕西麦可罗生物科技有限公司 | A kind of composition pesticide containing kasugarnycin and gold alloy hydride |
| CN107668049A (en) * | 2017-10-24 | 2018-02-09 | 张颂忠 | A kind of complex composition containing gold alloy hydride and Osthole |
| CN107711860A (en) * | 2017-10-24 | 2018-02-23 | 张锡林 | A kind of complex composition containing gold alloy hydride and doxycycline monohydrate |
| CN107743970A (en) * | 2017-12-06 | 2018-03-02 | 惠州市支持网知识产权运营有限公司 | Bactericidal composition containing psoralen and gold alloy hydride |
| CN108531488A (en) * | 2018-03-30 | 2018-09-14 | 辽宁大学 | New controlling gene AurT and its application in improving aureofuscin yield |
| CN109662097A (en) * | 2018-12-18 | 2019-04-23 | 广西壮族自治区农业科学院园艺研究所 | A kind of composition pesticide for preventing and treating citrus bacterial canker disease |
| CN109662097B (en) * | 2018-12-18 | 2021-05-07 | 广西壮族自治区农业科学院园艺研究所 | Pesticide composition for preventing and treating citrus canker |
| CN114521566A (en) * | 2022-02-21 | 2022-05-24 | 广西壮族自治区农业科学院 | Synergistic composition for preventing and treating soft rot of taro |
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