CN105475303B - A kind of composition pesticide containing kasugarnycin and gold alloy hydride - Google Patents
A kind of composition pesticide containing kasugarnycin and gold alloy hydride Download PDFInfo
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- CN105475303B CN105475303B CN201510899381.6A CN201510899381A CN105475303B CN 105475303 B CN105475303 B CN 105475303B CN 201510899381 A CN201510899381 A CN 201510899381A CN 105475303 B CN105475303 B CN 105475303B
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
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- General Health & Medical Sciences (AREA)
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of composition pesticide containing kasugarnycin and gold alloy hydride, the composition pesticide includes active component kasugarnycin and gold alloy hydride, and the weight of active component kasugarnycin and gold alloy hydride ratio is 1 in the composition pesticide:50~50:1.There is obvious synergistic function after kasugarnycin and gold alloy hydride compounding used in the present invention, improve prevention effect;Reduce dosage, so as to reduce cost and alleviate the pollution to environment.
Description
Technical field
The present invention relates to technical field of pesticide combination, and in particular to a kind of composition pesticide containing kasugarnycin and gold alloy hydride.
Background technology
Kiwi berry contains the nutrients such as substantial amounts of vitamin group, several amino acids and natural inositol, be known as " fruit it
The good reputation of king ", there is huge economic value.In recent years, the cultivated area of Kiwi berry constantly increases, at low bottom in 2012, China
Kiwi berry cultivated area is more than 1,500,000 mu, and total output breaks through 1,100,000 tons, and area and yield rank first in the world.Kiwi berry industry is
As Chaoyang rich people's pillar industry with competitive advantage.But Prospect on Kiwifruit Bacterial Canker large area breaks out in recent years, it was reported that
2009-2011 Kiwis canker has reached more than 80% in part orchard diseased plant rate(Its yellow tinkling of pieces of jade 2013).Kiwi berry
Canker has turned into our province and China's Kiwi berry plants most important disease, has a strong impact on the development for constraining Kiwi berry industry.
Prospect on Kiwifruit Bacterial Canker is that one kind has destructive bacteriosis, and at present, Prospect on Kiwifruit Bacterial Canker is prevented both at home and abroad
The technology of controlling is mainly:(1)Control orchard environmental sanitation, protection wound site;(2)Cultivate disease-resistant variety;(3)Spray chemical sterilization
Agent.Streptomysin and copper agent are the preventing and treating most important bactericide of the disease.Research shows that copper agent and streptomysin, which is excessively used, to be produced
The raw resistance to the action of a drug;Simultaneously, it was also found that copper agent and streptomysin have poisoning, leaf chlorosis, stalk cracking can be made.At present, in the market
There is no the product of effective preventive effect Prospect on Kiwifruit Bacterial Canker, especially biological pesticide.In recent years, Practice for Pesticide Residue in Agricultural Products problem compares again
It is prominent.And biological pesticide has the characteristics that efficient, low toxicity, low-residual, therefore, the biological pesticide of exploitation preventing and treating Prospect on Kiwifruit Bacterial Canker is compeled
In the eyebrows and eyelashes.
The content of the invention
In view of this, for overcome the deficiencies in the prior art, the present invention provides a kind of new mould containing kasugarnycin and golden core
The composition pesticide of element, said composition is efficient, safe and environment-friendly and be advantageous to germ resistance management.
The invention provides a kind of composition pesticide containing kasugarnycin and gold alloy hydride, the composition pesticide includes living
Property component kasugarnycin and gold alloy hydride, the weight percent of active component kasugarnycin and gold alloy hydride in the composition pesticide
Than for 1:50~50:1.
Further, the active component kasugarnycin and gold alloy hydride percentage by weight are 1:20~20:1.
Further, the weight sum of active component kasugarnycin and gold alloy hydride accounts for pesticide combination in the composition pesticide
The percentage of thing gross weight is 2% one 60%, and remaining component is acceptable auxiliary element in agricultural chemicals.
Further, the weight sum of active component kasugarnycin and gold alloy hydride accounts for pesticide combination in the composition pesticide
The percentage of thing gross weight is 5% one 40%, and remaining component is acceptable auxiliary element in agricultural chemicals.
According to the above-mentioned wettable powder composition containing kasugarnycin and gold alloy hydride agricultural chemicals, wrap by weight percentage
Include:Active component kasugarnycin 1~50%, active component gold alloy hydride 1~50%, dispersant 4~10%, wetting agent 2~10%,
Filler supplies 100%.Its compound method:By active component kasugarnycin active compound, active component gold alloy hydride active compound, dispersant, profit
Humectant, filler are knocked down in blender and mixed, then after airslide disintegrating mill crushes be well mixed, that is, be made the present composition can
WP product.
According to the above-mentioned water dispersible granules composition containing kasugarnycin and gold alloy hydride agricultural chemicals, wrap by weight percentage
Include:Active component kasugarnycin 1~50%, active component gold alloy hydride 1~50%, dispersant 2~12%, wetting agent 1~8%, collapse
Agent 1~10% is solved, binding agent 1~8%, filler supplies 100%.Its compound method:By active component kasugarnycin active compound, activearm
Parting caryomycin active compound, dispersant, wetting agent, disintegrant, binding agent, filler etc. are well mixed in the ratio of formula, through air-flow
Wettable powder is ground into, other auxiliary agents such as binding agent is added and material is made in a certain amount of water mixing extruding, be then dried,
The water dispersible granules product of the present composition is made in screening.
According to the above-mentioned suspension agent composition containing kasugarnycin and gold alloy hydride agricultural chemicals, include by weight percentage:
Active component kasugarnycin 1~50%, active component gold alloy hydride 1~50%, wetting agent 2~10%, dispersant 2~10%, disappear
Infusion 0.1~2%, thickener 0.1~2%, antifreezing agent 0.1~10%, add water to 100%.Its compound method:In being formulated by more than
By cutting at a high speed in active component kasugarnycin active compound, active component gold alloy hydride active compound, wetting agent, dispersant input mixing kettle
Mixing is cut, then adds defoamer, thickener, antifreezing agent, ball milling 2~3 hours in ball milling kettle so that diameter of particle is in 5mm
Hereinafter, the suspending agent product of the present composition is made.
According to the above-mentioned aqua composition containing kasugarnycin and gold alloy hydride agricultural chemicals, include by weight percentage:It is living
Property component kasugarnycin 1~50%, active component gold alloy hydride 1~50%, wetting agent 1-8%, adds water to 100%.Its compound method:
Active component kasugarnycin active compound, active component gold alloy hydride active compound, wetting agent, water are mixed in proportion, stirred, is filtered, system
Obtain the aqua product of the present composition.
Dispersant, wetting agent belong to auxiliary agent, auxiliary agent and filler in composition pesticide of the present invention(Carrier)It is this area skill
Well known to art personnel.Can also contain according to different dosage forms, in composition thickener known to one of skill in the art, defoamer,
Disintegrant, binding agent or antifreezing agent etc..
The auxiliary agent is selected from:600# phosphates, sodium lignin sulfonate, alkyl benzene sulfonate calcium salt, AEO,
Dispersing agent MF, APES phosphate, alkyl phenol formaldehyde resin polyoxyethylene ether, the condensation of phosphate naphthalenesulfonateformaldehyde formaldehyde
It is thing, condensation compound of methyl naphthalene sulfonic acid and formaldehyde, spaonin powder, sodium metnylene bis-naphthalene sulfonate, sodium lignin sulfonate, sldium lauryl sulfate, poly-
Oxygen ethene sorbitan fatty acid ester, Nekal BX, sodium methylene bis-naphthalene sulfonate, sodium butylnaphthalenesulfonate, polymer wood quality
Modifier, agriculture breast 600#, agriculture breast 1601#, dispersant NNO, lauryl sodium sulfate, polycarboxylate, phenethyl phenol polyoxypropylene
APEO, APES, three phenethyl phenol polyethenoxy ethers, dinaphthylmethanedisulfonic acid sodium, Lauxite
Performed polymer, sodium alginate etc..
The filler(Carrier)It is selected from:White carbon, kaolin, precipitated calcium carbonate, talcum powder, clay, diatomite, swelling
Soil, attapulgite, pyrophyllite, montmorillonite, clay, illite, mica powder, perlite, calcite, deionized water, water or castor-oil plant
One or more in oil etc..
The thickener is selected from:Arabic gum, xanthans, white carbon etc..
The defoamer is selected from:Organosilicon etc..
The disintegrant is selected from:Sodium acid carbonate, urea, ammonium sulfate etc..
The binding agent is selected from:Starch, gelatin, corn flour, polyvinyl alcohol, carboxymethyl cellulose etc..
The antifreezing agent is selected from:Polyvinyl alcohol, ethylene glycol, propane diols, glycerine etc..
Kasugarnycin molecular structure:
Kasugarnycin is a kind of biological bactericide a kind of as caused by little Jin actinomyces, has very strong interior sorptivety permeability,
There is preventive and therapeutic action simultaneously, its therapeutic action is more notable, is currently used primarily in preventing and treating rice blast, cucumber bacterium
The diseases such as property angular leaf spot, soft rot of Chinese cabbage.
Gold alloy hydride molecular structure:
Gold alloy hydride is that Shanghai pesticide research is developed, and is obtained by the mutation of streptomyces aureus Suzhou through cultivation and fermentation, to mandarin orange
The bacterial diseases such as tangerine canker, bacterial leaf streak of rice have preferable preventing and treating.
The bactericidal composition of the present invention can apply to prevent and treat in plant disease agriculturally, especially prevents and treats Kiwi berry and bursts
Ulcer disease.
The composition generally use spraying of the present invention or the method smeared use, and can also be adopted according to agriculture needs of production
Other are taken to use technology.
Compared with prior art, the beneficial effects of the present invention are:
1. there is obvious synergistic function after the kasugarnycin and gold alloy hydride compounding used in the present invention, improve
Prevention effect;
2. reduce dosage after the kasugarnycin and gold alloy hydride compounding used in the present invention, so as to reduce cost.
Embodiment
The present invention is further illustrated in the following embodiments, and this does not limit the scope of the invention.
Toxicity determines embodiment
Kasugarnycin compounds the Toxicity Determination to Prospect on Kiwifruit Bacterial Canker with gold alloy hydride
Subjects:Prospect on Kiwifruit Bacterial Canker pathogen pseudomonas syringae Kiwi berry pvs oryzae and oryzicola, from Zhouzhi County macaque
Peach orchard morbidity branch sampling, is isolated and purified using dilution method of scoring, the isolate of purifying is carried out obtained by Molecular Identification.
Test method:Cell containing pathogen 10 is prepared with sterilized water6-107Individual/mL bacteria suspension, often add bacteria suspension in ware
1.5mL, about 12mL NA culture mediums are poured into, flat board is made after shaking up.Each medicament sets 5 concentration gradients, by a diameter of 6mm
Sterilized filter paper piece be put into decoction immersion 1 hour after, taking-up is put into plate, using sterilized water immersion filter paper to compare, is placed in
28 DEG C of cultures, often handle and repeat three times.Observed after 48 hours, measure antibacterial circle diameter, calculate bacteriostasis rate.Bacteriostasis rate is converted into
Antibacterial probability, using the mass concentration for setting medicament as abscissa, regression straight line is made as ordinate using antibacterial probability, obtains each medicament
It is dense in virulence regression equation and suppression to Prospect on Kiwifruit Bacterial Canker(EC50).
The toxicity index and co-toxicity coefficient (CTC) of medicament are calculated according to the abundant methods of Sun Yun.
Survey toxicity index (ATI)=(standard agent EC50/ reagent agent EC50) ×100
A percentage composition+B medicament toxicity index x mixtures in theoretical toxicity index (TTI)=A medicament toxicity index × mixture
Middle B percentage composition
Co-toxicity coefficient (CTC)=[mixture actual measurement toxicity index (ATI)/mixture theoretical toxicity index (TTI) × 100
When CTC≤80, then composition shows as Hangzhoupro effect short of money, when 80<CTC<120, then composition show as summation action,
When CTC >=120, then composition shows as synergistic effect.
Toxicity Determination result see the table below 1:
The kasugarnycin of table 1 compounds the Toxicity Determination result to Prospect on Kiwifruit Bacterial Canker with gold alloy hydride
Toxicity Determination result shows that kasugarnycin is matched 1 with gold alloy hydride:50~50:Between 1, to Kiwi berry
Canker has synergistic effect, especially 1:20~20:Between 1, for co-toxicity coefficient more than 150, synergy is more obvious.
The composition pesticide of the present invention can be prepared into any one formulation of suitable agricultural use with known method, than
Preferable formulation is wettable powder, suspending agent, water dispersible granules, aqua.
In order to make the purpose , technical scheme and advantage of the present invention be clearer, present invention specific examples below
Illustrate, but the present invention is limited to absolutely not these examples.
Embodiment 1:21% kasugarnycin gold alloy hydride suspending agent
Ingredient names percentage by weight
Kasugarnycin 1.0%
Gold alloy hydride 20.0%
Dispersant NNO(Dispersant) 2.0%
Alkyl phenol formaldehyde resin polyoxyethylene ether(Wetting agent) 2.0%
Polyoxyethylene sorbitan fatty acid ester(Wetting agent) 1.0%
Xanthans (thickener) 0.2%
White carbon(Thickener) 0.5%
Organosilicon (defoamer) 0.2%
Ethylene glycol (antifreezing agent) 3.0%
Water complements to 100.0%
The each components such as active component, dispersant, thickener, wetting agent and water are well mixed in the ratio of formula, through grinding
21% kasugarnycin gold alloy hydride suspending agent is obtained after mill and/or high speed shear.
Embodiment 2:51% kasugarnycin gold alloy hydride wettable powder
Ingredient names percentage by weight
Kasugarnycin 50.0%
Gold alloy hydride 1.0%
Lauryl sodium sulfate (wetting agent) 2.0%
Sodium lignin sulfonate (dispersant) 5.0%
White Carbon black (filler) 10.0%
Kaolin (filler) complements to 100.0%
Active component, various auxiliary agents and filler etc. are sufficiently mixed in the ratio of formula, after ultra-fine pulverizer disintegrating, i.e.,
Obtain 51% kasugarnycin gold alloy hydride wettable powder.
Embodiment 3:42% kasugarnycin gold alloy hydride water dispersible granules
Ingredient names percentage by weight
Kasugarnycin 40.0%
Gold alloy hydride 2.0%
Lauryl sodium sulfate (wetting agent) 5.0%
Sodium lignin sulfonate (dispersant) 6.0%
Ammonium sulfate (disintegrant) 5.0%
Starch(Binding agent) 2.0%
Precipitated calcium carbonate (filler) complements to 100.0%
Active component, dispersant, wetting agent, disintegrant and filler are well mixed in the ratio of formula, through air-flow crushing
Into wettable powder, add a certain amount of water mixing extruding and make material, it is mould to obtain 42% kasugarnycin gold core after drying and sieving
Plain water dispersible granules.
Embodiment 4:2% kasugarnycin gold alloy hydride aqua
Ingredient names percentage by weight
Kasugarnycin 1.0%
Gold alloy hydride 1.0%
Alkyl phenol formaldehyde resin polyoxyethylene ether(Wetting agent) 2.0%
Water complements to 100.0%
Active component kasugarnycin active compound, active component gold alloy hydride active compound, wetting agent, water are mixed in proportion, stirred,
Filtering, 2% kasugarnycin gold alloy hydride aqua is made.
Embodiment 5:51% kasugarnycin gold alloy hydride water dispersible granules
Ingredient names percentage by weight
Kasugarnycin 1%
Gold alloy hydride 50%
Lauryl sodium sulfate (wetting agent) 5.0%
Sodium lignin sulfonate (dispersant) 6.0%
Ammonium sulfate (disintegrant) 5.0%
Starch(Binding agent) 2.0%
Precipitated calcium carbonate (filler) complements to 100.0%
Active component, dispersant, wetting agent, disintegrant and filler are well mixed in the ratio of formula, through air-flow crushing
Into wettable powder, add a certain amount of water mixing extruding and make material, it is mould to obtain 51% kasugarnycin gold core after drying and sieving
Plain water dispersible granules.
The kasugarnycin gold alloy hydride wettable powder of embodiment 6 60%
Ingredient names percentage by weight
Kasugarnycin 17.0%
Gold alloy hydride 43.0%
Lauryl sodium sulfate (wetting agent) 2.0%
Sodium lignin sulfonate (dispersant) 5.0%
White Carbon black (filler) 10.0%
Kaolin (filler) complements to 100.0%
Active component, various auxiliary agents and filler etc. are sufficiently mixed in the ratio of formula, after ultra-fine pulverizer disintegrating, i.e.,
Obtain 60% kasugarnycin gold alloy hydride wettable powder.
Embodiment 7:5% kasugarnycin gold alloy hydride aqua
Ingredient names percentage by weight
Kasugarnycin 2.0%
Gold alloy hydride 3.0%
Alkyl phenol formaldehyde resin polyoxyethylene ether(Wetting agent) 2.0%
Water complements to 100.0%
Active component kasugarnycin active compound, active component gold alloy hydride active compound, wetting agent, water are mixed in proportion, stirred,
Filtering, 5% kasugarnycin gold alloy hydride aqua is made.
Embodiment 8:40% kasugarnycin gold alloy hydride suspending agent
Ingredient names percentage by weight
Kasugarnycin 10.0%
Gold alloy hydride 30.0%
Dispersant NNO(Dispersant) 2.0%
Alkyl phenol formaldehyde resin polyoxyethylene ether(Wetting agent) 2.0%
Polyoxyethylene sorbitan fatty acid ester(Wetting agent) 1.0%
Xanthans (thickener) 0.2%
White carbon(Thickener) 0.5%
Organosilicon (defoamer) 0.2%
Ethylene glycol (antifreezing agent) 5.0%
Water complements to 100.0%
The each components such as active component, dispersant, thickener, wetting agent and water are well mixed in the ratio of formula, through grinding
40% kasugarnycin gold alloy hydride suspending agent is obtained after mill and/or high speed shear.
Above-described embodiment is applied to preventing and treating Prospect on Kiwifruit Bacterial Canker, is added using spraying and smears the method being combined after striking off scab
Dispenser, different preparation compositions are shown in Table 2 to the prevention effect of Prospect on Kiwifruit Bacterial Canker.
Prevention effect of the 2 different preparation compositions of table to Prospect on Kiwifruit Bacterial Canker
Kasugarnycin is prevented Prospect on Kiwifruit Bacterial Canker with gold alloy hydride complex composition it can be seen from the result of the test of table 2
Effect is significantly higher than single dose comparison medicament and Routine control medicament more than 86%.Testing each processing, not occur poisoning etc. bad
Reaction problem.Thus illustrate that kasugarnycin is significantly better than single dose with gold alloy hydride compounded combination using actual prevention effect, the knot
Fruit is consistent with indoor biometricses embodiment experimental result, illustrates that the two compounding has significant synergies.
Kasugarnycin can reduce dosage with gold alloy hydride compounding use, reduce use cost, while can delay medicine
The generation of agent resistance problem, agricultural synthesis is administered have it is important significant.
Although by referring to some preferred embodiments of the present invention, invention has been described, this area
It is to be appreciated by one skilled in the art that various changes can be made to it in the form and details, without departing from appended
The spirit and scope of the present invention that claims are limited.
Claims (9)
1. a kind of composition pesticide containing kasugarnycin and gold alloy hydride, the composition pesticide includes active component kasugarnycin
And gold alloy hydride, the weight of active component kasugarnycin and gold alloy hydride ratio is 1 in the composition pesticide:50~50:1;Institute
The composition pesticide stated includes or not comprising other activity.
2. composition pesticide according to claim 1, the active component kasugarnycin is with gold alloy hydride weight than preferred
For 1:5~5:1.
3. composition pesticide according to claim 1 or 2, active component kasugarnycin and golden core in the composition pesticide
The percentage that the weight sum of mycin accounts for composition pesticide gross weight is 2%-60%, and remaining component is that acceptable is auxiliary in agricultural chemicals
Co-ingredients.
4. composition pesticide according to claim 3, active component kasugarnycin and golden core are mould in the composition pesticide
The weight sum of element accounts for the percentage of composition pesticide gross weight as 5% one 40%.
5. composition pesticide according to claim 1 or 2, described composition pesticide is wettable powder composition, water
Dispersible granule composition, suspension agent composition or aqua composition.
6. composition pesticide according to claim 5, described composition pesticide is wettable powder composition, by weight
Percentages include:Active component kasugarnycin 1~50%, active component gold alloy hydride 1~50%, dispersant 4~10%, profit
Humectant 2~10%, filler supplies 100%;Its compound method:Active component kasugarnycin active compound, active component gold alloy hydride is former
Medicine, dispersant, wetting agent, filler are knocked down in blender and mixed, then are well mixed after airslide disintegrating mill crushes, that is, are made wettable
Property powder product.
7. composition pesticide according to claim 5, described composition pesticide is suspension agent composition, by weight percentage
Include than meter:Active component kasugarnycin 1~50%, active component gold alloy hydride 1~50%, wetting agent 2~10%, dispersant 2
~10%, defoamer 0.1~2%, thickener 0.1~2%, antifreezing agent 0.1~10%, add water to 100%;Its compound method:By more than
Passed through in active component kasugarnycin active compound, active component gold alloy hydride active compound, wetting agent, dispersant input mixing kettle in formula
High speed shear-mixed is crossed, then adds defoamer, thickener, antifreezing agent, ball milling 2~3 hours in ball milling kettle so that particulate grain
Footpath is in below 5mm, obtained suspending agent product.
8. composition pesticide according to claim 5, described composition pesticide is aqua composition, by weight percentage
Meter includes:Active component kasugarnycin 1~50%, active component gold alloy hydride 1~50%, wetting agent 1-8%, add water to 100%;Its
Compound method:Active component kasugarnycin active compound, active component gold alloy hydride active compound, wetting agent, water are mixed in proportion, stirred
Mix, filter, the aqua product of composition is made.
9. application of the composition pesticide described in claim 1-7 any one in controlling plant diseases.
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CN107711858A (en) * | 2017-10-24 | 2018-02-23 | 邓杵娇 | A kind of complex composition containing gold alloy hydride and bromothalonil |
CN107668049A (en) * | 2017-10-24 | 2018-02-09 | 张颂忠 | A kind of complex composition containing gold alloy hydride and Osthole |
CN107821399A (en) * | 2017-12-15 | 2018-03-23 | 陕西麦可罗生物科技有限公司 | A kind of composition pesticide containing kasugarnycin and D methyl-P-tyrosines and preparation method thereof |
CN108041066A (en) * | 2017-12-28 | 2018-05-18 | 陕西麦可罗生物科技有限公司 | A kind of kasugarnycin and streptomycin sulphate composition pesticide and detection method |
CN109662097B (en) * | 2018-12-18 | 2021-05-07 | 广西壮族自治区农业科学院园艺研究所 | Pesticide composition for preventing and treating citrus canker |
WO2020261126A1 (en) * | 2019-06-28 | 2020-12-30 | Insecticides (India) Ltd. | Fungicidal compositions and methods related thereto |
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