CN1324181C - Poly fleece textile using polypropylene glycol terephthalate as material and its production method - Google Patents
Poly fleece textile using polypropylene glycol terephthalate as material and its production method Download PDFInfo
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- CN1324181C CN1324181C CNB2005101033592A CN200510103359A CN1324181C CN 1324181 C CN1324181 C CN 1324181C CN B2005101033592 A CNB2005101033592 A CN B2005101033592A CN 200510103359 A CN200510103359 A CN 200510103359A CN 1324181 C CN1324181 C CN 1324181C
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Abstract
The present invention discloses a poly fleece textile using polypropylene glycol terephthalate as raw materials and a production method thereof. A veil is made of polypropylene glycol terephthalate yarn or filament yarn, and bottom yarn is made of other types of natural fiber or synthetic fiber yarn or filament yarn, and the veil and the bottom yarn are weaved by adopting a knitting weaving method. Because of the application of PTT to poly fleece products, the poly fleece products produced according to the method of the present invention can solve the defects of conventional poly fleece at present and also has the advantages of soft hand feeling, fluffiness, elasticity, pollution resistance, resistance to fuzzing and pilling and superior resistance to static electricity.
Description
One, technical field
The present invention relates to a kind of fleece textile and production method thereof, more particularly relating to a kind of is the production method of fleece textile of raw material and the product of preparation thereof with polytrimethylene terephthalate (PTT).
Two, background technology
Polar fleece is with its unique hand feeling and thermal property, and the style with hair is admitted by consumers in general deeply.But along with the passing of service time, conventional polar fleece displays gradually as the shortcoming of wearing fabric, is raw material owing to adopt conventional polyester, its anti-fuzz balls poor performance, feel is hard partially, sends out puckery, easily get dirty, nursing cost is high, has seriously restricted the development of polar fleece product.
Because the special molecular structure of polytrimethylene terephthalate (PTT) has brought up its low modulus and excellent elasticity response rate, make the PTT lining have unique soft feel, fluffy and whippy performance.The PTT macromolecular chain has helicoidal structure, thereby makes PTT have good resilience.Because strand gets the special construction form, it passes through to get acting in conjunction between strand self and the strand, thereby has given the rebound performance of PTT excellence.
The volume resistivity of PTT, induced voltage and discharge all are lower than PET and PA6 the half-life, in antistatic requirement is not very high purposes, can substitute terylene and polyamide fibre fully.And, show that PTT has antistatic preferably new capability in induced voltage and discharge half-life and cotton approaching.
The PTT antifouling property is with the oil repellent of fiber and easily soil release characteristics is relevant.The chemical constitution of macromolecular chain is very big to its effect of surface tension, and methylene is that the polymer of odd number is lower than the critical surface tension of even number, so ptt fiber has pollution resistance preferably.
The PTT fabric has good anti-fluffing and anti-pilling performance, this is because the ptt fiber excellent elasticity has been slowed down the active force that fiber is hit, the breaks of fiber have under external force been reduced, add excellent tensile elasticity and recovery characteristic, make ptt fiber that good antifatigue damage be arranged, the PTT antistatic property is good in addition, and everything makes that PTT anti-fluffing and anti-pilling performance is very good.
For this reason, adopt new raw material, new technology improving the traditional drawback of polar fleece, and keeps its advantage, becomes the important behave that the polar fleece product continues to advance.
Three, summary of the invention
One of purpose of the present invention provides a kind of soft feel that has, fluffy and high resilience, and have antifouling property, anti-fluffing and anti-pilling performance, what antistatic property was good is the fleece textile of raw material with the polytrimethylene terephthalate.
It is the production method of the fleece textile of raw material with the polytrimethylene terephthalate that two of purpose of the present invention provides a kind of.
These and other objects of the present invention will further embody and illustrate by following detailed.
Of the present invention is the fleece textile of raw material with the polytrimethylene terephthalate, veil is the polytrimethylene terephthalate yarn, filling is natural fabric or the synthetic fibre yarn or the long filament (comprising cotton, fiber crops, silk, hair and terylene, acrylic fibers and polyamide fibre etc.) of other types, adopts knitting braid method to weave and forms.
Further, of the present invention is the fleece textile of raw material with the polytrimethylene terephthalate, veil is the polytrimethylene terephthalate long filament, and filling is natural fabric or the synthetic fibre yarn or the long filament of other types, adopts knitting braid method to weave and forms.
Of the present invention is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, comprises that grey cloth check, the dyeing of deoiling, cylinder add hydrophily raising agent, dehydration, oven dry, bristle, carding, cropping, shake grain and finished product fixating shape step.
Wherein: the described staining procedure that deoils is for adding dyestuff and auxiliary agent in the time of 25 ℃ in dyeing caldron, turned round 5-15 minute, be warmed up to 80-90 ℃ with per minute 0.5-1.2 ℃ speed then, be incubated 3-7 minute, be warmed up to 100-120 ℃ with per minute 0.8-1.2 ℃ speed again, be incubated 3-7 minute, be warmed up to 120-140 ℃ with per minute 0.8-1.2 ℃ speed again, insulation dyeing 40-50 minute, speed with 1 ℃ of per minute cools to 80 ℃ then, sample cutting, qualified back overflow washing 5 minutes, Warm Wash is 10 minutes again.
Be preferably, of the present invention be in the production method of fleece textile of raw material with the polytrimethylene terephthalate, the described staining procedure that deoils is for adding dyestuff and auxiliary agent in the time of 25 ℃ in dyeing caldron, turned round 10 minutes, speed with 0.8 ℃ of per minute is warmed up to 85 ℃ then, be incubated 5 minutes, speed with 1 ℃ of per minute is warmed up to 110 ℃ again, be incubated 5 minutes, the speed with 1 ℃ of per minute is warmed up to 130 ℃ again, insulation dyeing 45 minutes, speed with 1 ℃ of per minute cools to 80 ℃ then, sample cutting, qualified back overflow washing 5 minutes, Warm Wash is 10 minutes again.
Of the present invention be in the production method of fleece textile of raw material with the polytrimethylene terephthalate, in the dyeing post processing, in dye vat, add hydrophily raising agent and softener, process conditions are:
Raising agent 1-3% (owf) softener 0.5-1.5% (owf)
Treatment temperature 35-55 ℃ of bath raio 1: 15
Processing time 15-25 minute.
Of the present invention be in the production method of fleece textile of raw material with the polytrimethylene terephthalate, in bristle, tension force is than the minimizing 10-20% of routine, the carding rate is greater than 130%, the shearing machine speed of a motor vehicle be 30-35 rice/minute, 1000-1300 rev/min of dise knife rotating speed, the style steam time is 8-20 minute in shaking a step.In the finished product fixating shape step, setting temperature is 120-170 ℃, and typing faces up, the speed of a motor vehicle be 30-45 rice/minute, wind speed is 1100-1500 rev/min, overfeeding 110-125%, add hydrophilizing agent when finished product is finalized the design, the addition of hydrophilizing agent is 1-3%, and hydrophilizing agent is Z 80 preferably.
Further, PTT polar fleece dyeing and finishing processing method flow process of the present invention is:
Grey cloth check-removing the work-margin to seam-dyeing-the cylinder that deoils adds hydrophily raising agent-dewater-dry-the cut open width of cloth-bristle-carding-cropping-shake grain-finished product typing (adding hydrophilic additive)-check-clot-packing.
Cylinder adds the hydrophily raising agent and softener is in order to reduce the electric charge position of ptt fiber in PTT polar fleece dyeing and finishing processing method of the present invention, overcome the shortcoming that the easy balling of fiber is stain owing to static, in the dyeing post processing, added hydrophilic raising agent and the softener that is applicable to polyester fiber.
The long fine flannelette of PTT because the single fiber fineness is thin, if bristle is very easily broken fiber even tissue with destroying by force, makes that cloth cover is easier to be fallen mao and balling; Behind the hydrophily raising agent that has used hydroxyl and sulfonation base, it can make ptt fiber expand and make looped pile become fluffy, reaches the effect that is easy to bristle, avoids by force bristle to cause fiber broken and causes too much undercoat bits.Add because it has amido link, can produce hydrogen bond with hydrone, so give the fabric good antistatic effect.Introduce hydrophilic radical in amino polysilane, what overcome general organic silicone finishing agent refuses the water defective, when keeping flexibility also with anti-soil and antistatic behaviour.In the softener of amidatioon modification,, can form hydrogen bond with water because amido link is strong polar bond, connect water with hydrogen bond, amido link is a polar centers, combines with other water again, make it to keep continuity, thereby make it have good feel and hydrophily, easily decontamination and antistatic behaviour.
In technology of the present invention, for in the bristle process, the fine TOWEL of the ultra-fine length of PTT can obtain broken fully circle, is unlikely to excessive brute force again and makes the fracture of PTT superfine fibre cause too much tags, we have changed conventional technology mode, adopt the pattern of the light brush of many brushing machine low-tensions.By many machine bristles, PTT flannelette looped pile is brushed out fully, and the low-tension bristle should break the looped pile brush phenomenon that brush can not produce vertical bar, broken hole thoroughly and seriously fall hair, with the undercoat bits that fabric behind the reduction finished product is hidden, help the ANTIPILLING of fabric.The carding rate remains on more than 130%, helps numerous settings of covering hair and stands, and can cut only covering hair in the cropping process, shakes a back cloth cover knot grain size unanimity thereby improve flannelette, and cloth cover is smooth, the style unanimity.For the lower PTT of brute force, necessarily to guarantee the sharp of dise knife and bed plate earlier, cropping machine knife bed is lowerd, speed of a motor vehicle 30-35 rice/minute, 1000-1300 rev/min of dise knife rotating speed, it is clean to help cutting of floating hair.Shook a steam 8-20 minute according to style, carry out the unimpeded of exhaust duct, fully cooling, the floating hair that will fall as far as possible sops up.The finished product typing time adds hydrophilizing agent, and hydrophilizing agent has good hydrophilic effect, and to the polyester fiber particularly suitable, but consumption is too much, can reduce fibre strength, thereby causes the pernicious mao phenomenon of falling, and can fastness that dye product be affected.
In technology of the present invention, ptt fiber since fiber to dye temperature on initial low, specific area is bigger, the speed of dying on initial is very high, if heating rate is controlled badly when dyeing the starting stage like this, is easy to cause the phenomenon of dyeing look flower.During dyeing, must guarantee the speed of temperature-gradient method and the time of segmentation insulation by technological operation, in case produce the look flower, look stain etc. is dyed defect.Rate of temperature fall must be about 0.5-1.5 ℃/minute, in case cloth cover produces wrinkle.Make fabric have the characteristics of ANTIPILLING for eliminating static, make fabric in the whole processing in back, be easy to fluffing simultaneously, in the dyeing post processing, in dye vat, add hydrophilic raising agent and softener.The pickling of dyeing back guarantees that the cloth cover pH value is even, will guarantee the soak time of fabric in auxiliary agent simultaneously, allows the full and uniform nexine that penetrates into fiber of auxiliary agent, and with intermolecular formation Van der Waals force and conjugated double bond, improve the puffed degree of fiber.
In the method for the invention, bristle need be taked the mode of operation of many light brushes.Because in order to give fabric antistatic behaviour and hydrophily, what we used is the hydrophily raising agent, and after fabric added this type of raising agent, feel after feel can be handled than conventional raising agent is stick-slip slightly, effect during bristle naturally can be poor slightly like this, if at this moment simply the bristle dynamics and the tension force that just increase the weight of the separate unit machine, can't make the fluffing rate that much improvement are arranged, also cause the bristle broken hole on the contrary easily, vertical bar, it is unusual to fall hair etc., gropes through test of many times and scene, and we have finally determined the processing modes of the ultra-fine PTT suede series products of many light brushes.Be that single machine bristle dynamics is transferred gently, guaranteeing not produce vertical bar, under the situation of broken hole, improve the bristle effect by platform, may the bristle flow process can some extend slightly like this, but very little to the damage of fiber, processing effect is also better, can guarantee the external and interior quality of expensive goods.
In finished product fixating shape step of the present invention, setting temperature is: light 150-165 ℃, middle look 145-155 ℃, dark 120-130 ℃, typing faces up.
According to the polar fleece product of method production of the present invention, because PTT is applied in the polar fleece product, can the existing defective of the present conventional polar fleece of fine solution.And have soft feel, fluffy and high resilience, antifouling property, anti-fluffing and anti-pilling performance and excellent antistatic energy.
Below further specify the present invention by specific embodiment, but embodiment only be used for the explanation, can not limit the scope of the invention.
In the present invention, if not refer in particular to, all parts, amount are the unit of weight based on gross weight, all raw materials all can be buied from market, need to prove, all technology and raw material do not described all can use conventional use the in the prior art, and those skilled in the art is need not spend creative work for the selection of these auxiliary agents, can buy from sea, Quanzhou City, a Fujian Province day grouping of the world economy factory.。
Four, the specific embodiment
Embodiment 1
The lining title: single-loop towel-two brushes singly shake (veil is: PTT is ultra-fine long fine, and filling is a cotton yarn)
Color name: purple
The dyeing and finishing processing method flow process of the knitting flannelette of the fine hydrophily of the ultra-fine length of PTT is:
Grey cloth check-removing the work-margin to seam-dyeing-the cylinder that deoils adds hydrophily raising agent-dewater-dry-the cut open width of cloth-bristle-carding-cropping-shake grain-finished product typing (adding hydrophilic additive)-check-clot-packing
Wherein: the staining procedure that deoils is for adding dyestuff and auxiliary agent (routine) in the time of 25 ℃ in dyeing caldron, turned round 10 minutes, the speed with 0.8 ℃ of per minute is warmed up to 85 ℃ then, is incubated 5 minutes, speed with 1 ℃ of per minute is warmed up to 110 ℃ again, be incubated 5 minutes, the speed with 1 ℃ of per minute is warmed up to 130 ℃ again, insulation dyeing 45 minutes, speed with 1 ℃ of per minute cools to 80 ℃ then, sample cutting, qualified back overflow washing 5 minutes, Warm Wash is 10 minutes again.
Add hydrophily raising agent and softener (routine) in the dyeing post processing in dye vat, process conditions are:
Raising agent 2% (owf) softener 1% (owf)
45 ℃ of 1: 15 treatment temperatures of bath raio
20 minutes processing times.
In bristle, adopt the pattern of the light brush of many brushing machine low-tensions, tension force is than the minimizing 10-20% of routine; The carding rate is greater than 130%, and the setting that guarantee to cover hair stands, and will cover hair and cut only, and cloth cover is smooth, and the style unanimity is convenient to shake the big or small unanimity of the back cloth cover knot of grain grain like this; The shearing machine speed of a motor vehicle is 30 meters/minute, and 1200 rev/mins of dise knife rotating speeds must will float hair and cut clean.The style steam time is 8-20 minute in shaking a step, in the unimpeded while of carrying out exhaust duct, in time fully cooling, and the floating hair that will fall as far as possible sops up.In the finished product fixating shape step, setting temperature is 150 ℃, the typing that faces up, and the speed of a motor vehicle is 40 meters/minute, wind speed is 1400 rev/mins, overfeeding 115%.Spray into hydrophilizing agent when finished product is finalized the design, the addition of hydrophilizing agent is 2%, and hydrophilizing agent is Z80 preferably.
Claims (9)
1, a kind of is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, comprise the grey cloth check, the dyeing of deoiling, cylinder adds the hydrophily raising agent, dehydration, oven dry, bristle, carding, cropping, shake grain and finished product fixating shape step, it is characterized in that in the staining procedure that deoils, in dyeing caldron, in the time of 25 ℃, add dyestuff and auxiliary agent, turned round 5-15 minute, be warmed up to 80-90 ℃ with per minute 0.5-1.2 ℃ speed then, be incubated 3-7 minute, be warmed up to 100-120 ℃ with per minute 0.8-1.2 ℃ speed again, be incubated 3-7 minute, be warmed up to 120-140 ℃ with per minute 0.8-1.2 ℃ speed again, insulation dyeing 40-50 minute, the speed with 1 ℃ of per minute cools to 80 ℃, sample cutting then, qualified back overflow washing 5 minutes, Warm Wash is 10 minutes again.
2, according to claim 1 is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that in the staining procedure that deoils, in dyeing caldron, in the time of 25 ℃, add dyestuff and auxiliary agent, turned round 10 minutes, speed with 0.8 ℃ of per minute is warmed up to 85 ℃ then, be incubated 5 minutes, speed with 1 ℃ of per minute is warmed up to 110 ℃ again, be incubated 5 minutes, the speed with 1 ℃ of per minute is warmed up to 130 ℃ again, insulation dyeing 45 minutes, speed with 1 ℃ of per minute cools to 80 ℃ then, sample cutting, qualified back overflow washing 5 minutes, Warm Wash is 10 minutes again.
3, according to claim 1 is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that adding hydrophily raising agent and softener in the dyeing post processing in dye vat, and process conditions are:
Raising agent 1-3% (owf) softener 0.5-1.5% (owf)
Treatment temperature 35-55 ℃ of bath raio 1: 15
Processing time 15-25 minute.
4, according to claim 1 is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that when bristle, tension force is than the minimizing 10-20% of routine, the carding rate is greater than 130%, the shearing machine speed of a motor vehicle be 30-35 rice/minute, 1000-1300 rev/min of dise knife rotating speed.
5, according to claim 1 is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that the style steam time is 8-20 minute in shaking a step.
6, according to claim 1 is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that in the finished product fixating shape step, setting temperature is 120-170 ℃, typing faces up, the speed of a motor vehicle be 30-45 rice/minute, wind speed is 1100-1500 rev/min, overfeeding 110-125%.
7, according to claim 1 is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that adding hydrophilizing agent when finished product is finalized the design, and the addition of hydrophilizing agent is 1-3%.
8, according to claim 1 is the production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that described hydrophilizing agent is Z80.
9, described with one of claim 1-8 is the prepared fleece textile of production method of the fleece textile of raw material with the polytrimethylene terephthalate, it is characterized in that veil is polytrimethylene terephthalate yarn or long filament, filling is natural fabric or the synthetic fibre yarn or the long filament of other types, adopts knitting braid method to weave and forms.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005101033592A CN1324181C (en) | 2005-09-20 | 2005-09-20 | Poly fleece textile using polypropylene glycol terephthalate as material and its production method |
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2005101033592A CN1324181C (en) | 2005-09-20 | 2005-09-20 | Poly fleece textile using polypropylene glycol terephthalate as material and its production method |
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| CN1730758A CN1730758A (en) | 2006-02-08 |
| CN1324181C true CN1324181C (en) | 2007-07-04 |
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| EP2781647A4 (en) * | 2011-11-14 | 2015-08-26 | Junglimtextile | Method for dyeing textiles using metallic yarn and polyester yarn and textile manufactured thereby |
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| CN1730758A (en) | 2006-02-08 |
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