CN1305461C - Inorganic nanometer sunshade emulsion of maniod eibish and its preparation process - Google Patents
Inorganic nanometer sunshade emulsion of maniod eibish and its preparation process Download PDFInfo
- Publication number
- CN1305461C CN1305461C CNB2005100414718A CN200510041471A CN1305461C CN 1305461 C CN1305461 C CN 1305461C CN B2005100414718 A CNB2005100414718 A CN B2005100414718A CN 200510041471 A CN200510041471 A CN 200510041471A CN 1305461 C CN1305461 C CN 1305461C
- Authority
- CN
- China
- Prior art keywords
- parts
- phase
- emulsion
- sunshade
- inorganic nanometer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Cosmetics (AREA)
Abstract
The present invention discloses a sunset abelmoschus inorganic nanometer sunscreen lotion and a preparation method. The sunscreen lotion is an oil-in-water type emulsifying system with cool skin feeling, which is prepared from sunset abelmoschus flower extract, konjak finemeal, nanometer titanium dioxide, nanometer zinc dioxide and relevant auxiliary material. The ultraviolet absorption spectrum of 250 and 400 nm of the alcohol-water extract of sunset abelmoschus root has two absorption bands, the titanium dioxide and the zinc dioxide as inorganic nanometer sunscreen agents are added in a prescription for enhancing sunscreen action on ultraviolet rays, and simultaneously, the product is endowed with certain effects of whitening and shielding. The sunset abelmoschus flower extract has the effects of clearing heat, cooling the blood, removing toxicity, etc. besides the sunscreen action, and has positive action for eliminating scytitis and repairing injury after skin is solarized, when the sunset abelmoschus flower extract is used in the product.
Description
Technical field
The present invention relates to cosmetics, is ultra light sun block lotion that contains Abelmoschus manihot and preparation method thereof specifically.
Background technology
Ultraviolet in the sunlight can be divided into by its wavelength: wavelength is the long wave ultraviolet of 320～400nm, is called A type ultraviolet (UVA); Wavelength is the ultraviolet B radiation of 290～320nm, and being called Type B ultraviolet (UVB) and wavelength is the short wave ultraviolet of 200～290nm, is called C type ultraviolet (UVC).Because ultraviolet wavelength is very short, energy is quite high.Its destructive power is very big, shines the skin that can damage the people on the health for a long time, causes inflammation or sunburn, and serious meeting produces skin carcinoma.Ultraviolet B radiation UVB is the principal element that causes scytitis and sunburn.Result of study in recent years proves, and is long-term not by the long wave ultraviolet UVA that people paid attention to, and the infringement of skin depths is had serious summation, can cause the photoaging of skin and tanned, also is one of inducement that causes skin carcinoma.Along with the destruction of atmospheric ozone layer is on the rise, cause more ultraviolet radiation to earth surface.It is reported that ozone layer reduces 10%, will make the ultraviolet that arrives earth surface increase by 20%, the sickness rate of skin carcinoma increases by 30%.Therefore, society increases rapidly the demand of various sunscreen and sun-proof skin care agent.
The sunscreen that adds in the sun care preparations is broadly divided into two classes: a class is inorganic sunscreen such as nano titanium oxide, zinc oxide, has scattering and absorbs ultraviolet ability, is difficult to reach very high sun-proof result and good result of use but use separately.Another kind of then is the organic sunscreen agent, esters and derivant, cinnamate derivative, salicylic acid esters, benzophenone and derivant thereof etc. as para-amino benzoic acid, this class sunscreen often is a transmission substance, can absorb ultraviolet, but majority exists side effect such as skin allergy, cutaneous metabolism.
Summary of the invention
The ultra light sun block lotion and the preparation method that the purpose of this invention is to provide a kind of composite Abelmoschus manihot and Rhizoma amorphophalli, nano titanium oxide and zinc oxide, on the one hand, performance Abelmoschus manihot extracting solution all has the characteristic of better absorption to entire ultraviolet light zone, and a kind of good natural plant sun agent that has no side effect is provided; On the other hand, add a spot of nano titanium oxide, zinc oxide, strengthened sun-proof result, but be unlikely to cause infringement skin; On the one hand, the Rhizoma amorphophalli main component is Rhizoma amorphophalli glucomannan and starch again, and Rhizoma amorphophalli glucomannan has excellent film forming characteristics, adds the effect that has thickening and stable emulsion system in the ultra light sun block lotion, simultaneously skin is had protective effect.
Technical scheme of the present invention is as follows:
Inorganic nanometer sunshade emulsion of maniod eibish is characterized in that being made up of the component preparation of following weight proportion:
A phase: 2～4 parts of dimethyl siloxanes
1～2 part of caprylic/capric triglyceride
C
12-151～2 part of benzoate
2～2.5 parts of glyceryl monostearates
0.5～1 part of stearic acid
0.5～1 part of 16/18 mixed alcohol
4～5 parts of nano zine oxides
Ceteareth-2 2～3 part
Ceteareth-21 1～2 part
0.05～0.1 part of propyl p-hydroxybenzoate;
B phase: 25～30 parts of 1% konjaku powder solution
4～5 parts of glycerol
2～3 parts of nano titanium oxides
0.1～0.2 part of methyl parahydroxybenzoate
The extracting solution of 60% (V/V) ethanol water of 4 weight portion Flos abelmoschi manihots, being concentrated into weight portion is 8～10 parts
Adding the Purified Water ad pond om after Purified Water A phase+B phase+C is mixed mutually is 100 parts;
C phase: 0.1～0.2 part of two imidazolidinyl urea
4～5 parts of Purified Waters.
Described inorganic nanometer sunshade emulsion of maniod eibish is characterized in that being made up of the component preparation of following weight proportion:
A phase: 3 parts of dimethyl siloxanes
2 parts of caprylic/capric triglyceride
C
12-152 parts of benzoate
2.5 parts of glyceryl monostearates
1 part of stearic acid
1 part of 16/18 mixed alcohol
5 parts of nano zine oxides
Ceteareth-2 3 part
Ceteareth-21 2 part
0.1 part of propyl p-hydroxybenzoate;
B phase: 30 parts of 1% konjaku powder solution
5 parts of glycerol
3 parts of nano titanium oxides
0.2 part of methyl parahydroxybenzoate
The extracting solution of 60% (V/V) ethanol water of 4 weight portion Flos abelmoschi manihots, being concentrated into weight portion is 8～10 parts
Adding the Purified Water ad pond om after Purified Water A phase+B phase+C is mixed mutually is 100 parts;
C phase: 0.2 part of two imidazolidinyl urea
5 parts of Purified Waters.
Described inorganic nanometer sunshade emulsion of maniod eibish is characterized in that being made up of the component preparation of following weight proportion:
A phase: 2 parts of dimethyl siloxanes
1 part of caprylic/capric triglyceride
C
12-151 part of benzoate
2 parts of glyceryl monostearates
0.5 part of stearic acid
0.5 part of 16/18 mixed alcohol
4 parts of nano zine oxides
Ceteareth-2 2 part
Ceteareth-21 1 part
0.05 part of propyl p-hydroxybenzoate;
B phase: 25 parts of 1% konjaku powder solution
4 parts of glycerol
2 parts of nano titanium oxides
0.1 part of methyl parahydroxybenzoate
The extracting solution of 60% (V/V) ethanol water of 4 weight portion Flos abelmoschi manihots, being concentrated into weight portion is 8～10 parts
Adding the Purified Water ad pond om after Purified Water A phase+B phase+C is mixed mutually is 100 parts;
C phase: 0.1 part of two imidazolidinyl urea
4 parts of Purified Waters.
Described Purified Water is pure water, distilled water or deionized water.
Described methyl parahydroxybenzoate, propyl p-hydroxybenzoate, two imidazolidinyl urea can be replaced by other antiseptic, and the ethanol extract of described Abelmoschus manihot is the extracting solution of 60% (V/V) ethanol water of Flos abelmoschi manihot.
The preparation method of above-mentioned inorganic nanometer sunshade emulsion of maniod eibish, it is biphase to 75～80 ℃ to it is characterized in that heating respectively A, B, makes decorating film dissolving wherein; While stirring B is mutually slowly added the A phase then, treat that B is added to after, be stirred to fast that emulsifying is complete, mastic is even; Slowly cooling reduces mixing speed simultaneously, adds the C phase in the time of 50 ℃, stops when being cooled to room temperature stirring.
Amorphophallus herbaceos perennial, its main component are Rhizoma amorphophalli glucomannan and starch, contain a spot of protein, fat and tryptophan etc. in addition; Rhizoma amorphophalli glucomannan has excellent film forming characteristics, adds in the ultra light sun block lotion to have thickening and Stabilization, simultaneously skin is had protective effect.
Abelmoschus manihot is a Malvaceae Abelmoschus plant, but all herbal medicine, and it spends cunning sweet in flavor and cold in property, nontoxic, have the effect of eliminating damp-heat, eliminating inflammation and expelling toxin, five types of stranguria, the edema of curing mainly for oral administration, external curing swollen ulcer drug, scald, its main component are flavone compounds such as hyperin.Find that after deliberation the extracting solution of the ethanol water of Flos abelmoschi manihot all has better absorption in the entire ultraviolet zone, is good natural plant sun agent.
Ultra light sun block lotion of the present invention is the oil-in-water type emulsion system, and the skin sense is salubrious; Selected nonionic emulsifier ceteareth-2 and ceteareth-21 are used directly that emulsifying contains ethanol system, have characteristics such as emulsified particles is thin, mastic light; The main component of konjaku powder is Rhizoma amorphophalli glucomannan (being called for short KGM), is used as thickening agent and emulsion stabilizer; Can be by the thick product extraction ratio of extraction sunscreen in the Flos abelmoschi manihot up to 36.2%, the ultra-violet absorption spectrum in 250～400nm interval has two absorption bands, specific absorptivity E
1% Lcm(λ
Man) be respectively 1.0 * 10
2(259nm), 73 (370nm) are used for cosmetics and will have certain sun-proof effect; For satisfying needs to the high protection of ultraviolet, added inorganic nano sunlight screening agent titanium dioxide and zinc oxide in the prescription, given product certain brightening and covering effect simultaneously; The Flos abelmoschi manihot extracting solution also has effects such as heat clearing away, removing heat from blood, detoxifcation concurrently except that having anti-sunlight function, being used for product can be to the elimination of scytitis after shining and the positive effect of reparation performance of damage.
The specific embodiment
One, the prescription of inorganic nanometer sunshade emulsion of maniod eibish
The composition weight portion
A phase dimethyl siloxane 3
Caprylic/capric triglyceride 2
C
12-15Benzoate 2
Glyceryl monostearate 2.5
Stearic acid 1
16/18 mixed alcohols 1
Nano zine oxide 5
Ceteareth-2 3
Ceteareth-21 2
Propyl p-hydroxybenzoate 0.1
B is 1% konjaku powder solution 30 mutually
Glycerol 5
Nano titanium oxide 3
Methyl parahydroxybenzoate 0.2
4 weight portion Flos abelmoschi manihot ethanol extracts and to be concentrated into weight portion be 10
Adding the Purified Water ad pond om after Purified Water A phase+B phase+C is mixed mutually is 100
The two mutually imidazolidinyl urea 0.2 of C
Deionized water 5
Two, the preparation method of ultra light sun block lotion
It is biphase to 75～80 ℃ of decorating film dissolvings that make wherein to heat A, B respectively; While stirring B is mutually slowly added the A phase then, treat that B is added to after, be stirred to fast that emulsifying is complete, mastic is even; Slowly cooling reduces mixing speed simultaneously, adds the C phase in the time of 50 ℃, stops when being cooled to room temperature stirring.
Three, the preparation of Flos abelmoschi manihot extracting solution
Accurately take by weighing 20.0g Abelmoschus manihot dry flower powder, with the ethanol water 500mL of 60% (V/V) 50 ℃ of supersound extraction 20 minutes.After the filtration, filtrate decompression is distilled to 50g, promptly makes the Flos abelmoschi manihot extracting solution, standby.
Present embodiment also can adopt technical scheme cited in the description and parameter, does not influence effect of the present invention.
Claims (6)
1, inorganic nanometer sunshade emulsion of maniod eibish is characterized in that being made up of the component preparation of following weight proportion:
A phase: 2～4 parts of dimethyl siloxanes
1～2 part of caprylic/capric triglyceride
C
12-151～2 part of benzoate
2～2.5 parts of glyceryl monostearates
0.5～1 part of stearic acid
0.5～1 part of 16/18 mixed alcohol
4～5 parts of nano zine oxides
Ceteareth-2 2～3 part
Ceteareth-21 1～2 part
0.05～0.1 part of propyl p-hydroxybenzoate;
B phase: 25～30 parts of 1% konjaku powder solution
4～5 parts of glycerol
2～3 parts of nano titanium oxides
0.1～0.2 part of methyl parahydroxybenzoate
The extracting solution of 60% (V/V) ethanol water of 4 weight portion Flos abelmoschi manihots, being concentrated into weight portion is 8～10 parts
Adding the Purified Water ad pond om after Purified Water A phase+B phase+C is mixed mutually is 100 parts;
C phase: 0.1～0.2 part of two imidazolidinyl urea
4～5 parts of Purified Waters.
2, inorganic nanometer sunshade emulsion of maniod eibish according to claim 1 is characterized in that being made up of the component preparation of following weight proportion:
A phase: 3 parts of dimethyl siloxanes
2 parts of caprylic/capric triglyceride
C
12-152 parts of benzoate
2.5 parts of glyceryl monostearates
1 part of stearic acid
1 part of 16/18 mixed alcohol
5 parts of nano zine oxides
Ceteareth-2 3 part
Ceteareth-21 2 part
0.1 part of propyl p-hydroxybenzoate;
B phase: 30 parts of 1% konjaku powder solution
5 parts of glycerol
3 parts of nano titanium oxides
0.2 part of methyl parahydroxybenzoate
The extracting solution of 60% (V/V) ethanol water of 4 weight portion Flos abelmoschi manihots, being concentrated into weight portion is 8～10 parts
Adding the Purified Water ad pond om after Purified Water A phase+B phase+C is mixed mutually is 100 parts;
C phase: 0.2 part of two imidazolidinyl urea
5 parts of Purified Waters.
3, inorganic nanometer sunshade emulsion of maniod eibish according to claim 1 and 2 is characterized in that being made up of the component preparation of following weight proportion:
A phase: 2 parts of dimethyl siloxanes
1 part of caprylic/capric triglyceride
C
12-151 part of benzoate
2 parts of glyceryl monostearates
0.5 part of stearic acid
0.5 part of 16/18 mixed alcohol
4 parts of nano zine oxides
Ceteareth-2 2 part
Ceteareth-21 1 part
0.05 part of propyl p-hydroxybenzoate;
B phase: 25 parts of 1% konjaku powder solution
4 parts of glycerol
2 parts of nano titanium oxides
0.1 part of methyl parahydroxybenzoate
The extracting solution of 60% (V/V) ethanol water of 4 weight portion Flos abelmoschi manihots, being concentrated into weight portion is 8～10 parts
Adding the Purified Water ad pond om after Purified Water A phase+B phase+C is mixed mutually is 100 parts;
C phase: 0.1 part of two imidazolidinyl urea
4 parts of Purified Waters.
4,, it is characterized in that described Purified Water is pure water, distilled water or deionized water according to claim 1,2 or 3 described inorganic nanometer sunshade emulsion of maniod eibish.
5,, it is characterized in that described methyl parahydroxybenzoate, propyl p-hydroxybenzoate, two imidazolidinyl urea can be replaced by other antiseptic according to claim 1,2 or 3 described inorganic nanometer sunshade emulsion of maniod eibish.
6, the preparation method of inorganic nanometer sunshade emulsion of maniod eibish according to claim 1 and 2, it is biphase to 75～80 ℃ to it is characterized in that heating respectively A, B, makes decorating film dissolving wherein; While stirring B is mutually slowly added the A phase then, treat that B is added to after, be stirred to fast that emulsifying is complete, mastic is even; Slowly cooling reduces mixing speed simultaneously, adds the C phase in the time of 50 ℃, stops when being cooled to room temperature stirring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100414718A CN1305461C (en) | 2005-08-09 | 2005-08-09 | Inorganic nanometer sunshade emulsion of maniod eibish and its preparation process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100414718A CN1305461C (en) | 2005-08-09 | 2005-08-09 | Inorganic nanometer sunshade emulsion of maniod eibish and its preparation process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1732886A CN1732886A (en) | 2006-02-15 |
| CN1305461C true CN1305461C (en) | 2007-03-21 |
Family
ID=36075642
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100414718A Expired - Fee Related CN1305461C (en) | 2005-08-09 | 2005-08-09 | Inorganic nanometer sunshade emulsion of maniod eibish and its preparation process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1305461C (en) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE531318C2 (en) * | 2007-02-22 | 2009-02-24 | Tigran Technologies Ab Publ | Injectable suspension comprising microstructure titanium titanium, titanium alloy or titanium oxide particles |
| SE531319C2 (en) * | 2007-02-22 | 2009-02-24 | Tigran Technologies Ab Publ | Porous implant granule |
| CN101317912B (en) * | 2008-06-10 | 2011-10-12 | 骆金根 | Orally taken traditional Chinese medicine for treating chronic gonorrhea |
| CN101406442B (en) * | 2008-11-25 | 2012-06-06 | 上海应用技术学院 | Nanometer lipid sun-prevention microparticle suspending liquid and preparation method thereof |
| CN102228412A (en) * | 2011-05-10 | 2011-11-02 | 蒲科 | Oil phase dispersion sunblocking concentrate of nanometer titania and preparation method thereof |
| CN103550096B (en) * | 2013-10-31 | 2015-03-04 | 金陵科技学院 | Tender okra pod facial mask essence and preparation method thereof |
| CN103911040B (en) * | 2014-03-31 | 2016-01-20 | 苏州科斯伍德油墨股份有限公司 | Nondiscoloration water color ink containing Flos abelmoschi manihot extract and preparation method thereof |
| CN103911041B (en) * | 2014-03-31 | 2016-02-10 | 苏州科斯伍德油墨股份有限公司 | Nondiscoloration oil-based ink containing Flos abelmoschi manihot extract and preparation method thereof |
| CN106074238B (en) * | 2016-06-14 | 2019-01-18 | 广州暨南生物医药研究开发基地有限公司 | A kind of Golden flower whitening and spot eliminating cream and preparation method thereof |
| CN106214539A (en) * | 2016-08-17 | 2016-12-14 | 柳州市亿廷贸易有限责任公司 | Shampoo used also as bath lotion |
| CN113749958B (en) * | 2021-08-21 | 2023-08-08 | 百特威(上海)化妆品有限公司 | Sun-proof emulsion composition |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1068732A (en) * | 1992-08-29 | 1993-02-10 | 西南农业大学 | Its production method of health care face scrape along |
| CN1335123A (en) * | 2001-07-26 | 2002-02-13 | 王雪梅 | Acne-eliminating beautifying sunset abelmoschus liquid and its prepn |
| CN1493578A (en) * | 2002-10-29 | 2004-05-05 | 中国人民解放军北京军医学院 | Preparation method of golden peach glycoside and its new use in medicine |
-
2005
- 2005-08-09 CN CNB2005100414718A patent/CN1305461C/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1068732A (en) * | 1992-08-29 | 1993-02-10 | 西南农业大学 | Its production method of health care face scrape along |
| CN1335123A (en) * | 2001-07-26 | 2002-02-13 | 王雪梅 | Acne-eliminating beautifying sunset abelmoschus liquid and its prepn |
| CN1493578A (en) * | 2002-10-29 | 2004-05-05 | 中国人民解放军北京军医学院 | Preparation method of golden peach glycoside and its new use in medicine |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1732886A (en) | 2006-02-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1305461C (en) | Inorganic nanometer sunshade emulsion of maniod eibish and its preparation process | |
| CN102973471B (en) | Antiaging sunscreen cream containing natural plant active ingredients and preparation method thereof | |
| CN109939058B (en) | Blue-light-proof cosmetic composition and preparation method thereof | |
| CN104586727B (en) | A kind of plant and tea oil radiation proof moisturizing liquid | |
| CN107412043A (en) | A kind of cosmetic composition and its application | |
| CN102018637A (en) | Preparation of novel sunscreen and moisturizing cream | |
| CN101933892B (en) | New application of kaempferol extractive and sunscreen cosmetic containing kaempferol extractive | |
| CN101623240B (en) | Preparation method of sunscreen cream | |
| CN105342973A (en) | Tea polyphenol sun cream and preparation method thereof | |
| CN105726365A (en) | Cosmetic containing calophyllum inophyllum kernel oil and preparation method thereof | |
| CN102552093B (en) | Sunscreen skin care product and preparation method thereof | |
| CN101342131B (en) | Sun cream containing natural plant sun-proof composition and preparation method thereof | |
| CN103784348A (en) | Plant sunscreen cream and preparation method thereof | |
| CN107260634A (en) | A kind of green Chinese nti-freckle suncream and preparation method thereof | |
| CN104027282A (en) | Sunscreen composition and preparation method thereof | |
| KR101370990B1 (en) | Anti-heat aging effect of fermented Limonia acidissima extract and its cosmetic usage to improve skin problems | |
| CN106691977A (en) | Preparation method for natural compound plant extract sunscreen cream | |
| CN104248572A (en) | Lotus root-containing after-sun repair mask powder | |
| CN106580747A (en) | Sunscreen cream and preparation method thereof | |
| CN101161231A (en) | Ocean medicine hairdressing sun cream containing shuck powder | |
| CN104414867A (en) | Sunscreen skin care cream containing xanthophyll | |
| CN108524392A (en) | A kind of sunscreen composition and suncream containing barley young leaf powder and calophyllum inophyllum kernel oil | |
| CN114129461A (en) | Sunscreen skin care product containing composite titanium dioxide and preparation method thereof | |
| CN102274129A (en) | Nano-sized core-shell composite material used for cosmetics and preparation method thereof | |
| CN113576935A (en) | Sunscreen repair composition and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |