CN105342973A - Tea polyphenol sun cream and preparation method thereof - Google Patents
Tea polyphenol sun cream and preparation method thereof Download PDFInfo
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- CN105342973A CN105342973A CN201510922161.0A CN201510922161A CN105342973A CN 105342973 A CN105342973 A CN 105342973A CN 201510922161 A CN201510922161 A CN 201510922161A CN 105342973 A CN105342973 A CN 105342973A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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Abstract
Tea polyphenol sun cream is prepared from the following components in parts by weight: 5-10 parts of cetostearyl alcohol, 10-15 parts of glycerinum, 1-5 parts of cetanol, 5-10 parts of red spinach extract, 0.5-3 parts of tea polyphenol, 5-10 parts of scutellaria baicalensis extract, 0.1-0.5 part of pearl powder, 0.1-0.5 part of titanium dioxide, 0.1-0.5 part of 3,4minute-methyl benzylidene camphor, 0.5-3 parts of dicapryl carbonate, 0.5-3 parts of bisabolol, 0.5-3 parts of hyaluronic acid, 0.5-3 parts of surfactant and 50-80 parts of deionized water. A preparation method comprises preparation of the red spinach extract, preparation of the scutellaria baicalensis extract, preparation of an aqueous phase, preparation of an oil phase and preparation of the tea polyphenol sun cream. The tea polyphenol sun cream is gentle in color, fresh in smell, refreshing in texture, capable of enabling a user to be relaxed and happy, and suitable for being used by mass.
Description
Technical field
The present invention relates to a kind of cosmetics.
Background technology
Solar radiation comprises to the ultraviolet on ground the UV-A that wavelength is UV-B and 320nm-400nm of 290nm-320nm.Excessively accepting these two kinds of ultraviolet irradiations all can sun-damaged skin, the inflammatory mediators such as the release of intradermal various kinds of cell histamine, 5-hydroxy tryptamine, kassinin kinin, makes intradermal vasodilation, permeability increases.Generally show as erythema, edema, vesicle and pigmentation, desquamation etc.Therefore, tea polyphenols sunscreen cream smear very necessary.
The generally commercially available tea polyphenols sunscreen cream quality rate of exchange are thick and heavy, and with the addition of some chemical sun.Smear the thick and heavy tea polyphenols sunscreen cream of quality during the broiling summer and can cause uncomfortable sensation to skin, and the use of some chemical sun also increases the probability of skin allergy, even makes skin occur disease.
Summary of the invention
For above-mentioned technical problem, the invention provides a kind of tea polyphenols sunscreen cream and preparation method thereof.Tea polyphenols sunscreen cream of the present invention is made up of the component of following weight portion: cetearyl alcohol 5 ~ 10 parts, glycerol 10 ~ 15 parts, hexadecanol 1 ~ 5 part, Herba Gynurae bicoloris extract 5 ~ 10 parts, tea polyphenols 0.5 ~ 3 part, Radix Scutellariae extract 5 ~ 10 parts, Margarita powder 0.1 ~ 0.5 part, titanium dioxide 0.1 ~ 0.5 part, 3,4 '-methyl benzylidene camphor 0.1 ~ 0.5 part, dicaprylyl carbonate 0.5 ~ 3 part, bisabolol 0.5 ~ 3 part, hyaluronic acid 0.5 ~ 3 part, 0.5 ~ 3 part, surfactant, deionized water 50 ~ 80 parts.
Further, be made up of the component of following weight portion: cetearyl alcohol 6 ~ 9 parts, glycerol 12 ~ 14 parts, hexadecanol 2 ~ 4 parts, Herba Gynurae bicoloris extract 6 ~ 9 parts, tea polyphenols 0.8 ~ 2 part, Radix Scutellariae extract 6 ~ 9 parts, Margarita powder 0.2 ~ 0.4 part, titanium dioxide 0.2 ~ 0.4 part, 3,4 '-methyl benzylidene camphor 0.2 ~ 0.4 part, dicaprylyl carbonate 0.8 ~ 2 part, bisabolol 0.8 ~ 2 part, hyaluronic acid 0.8 ~ 2 part, 0.8 ~ 2 part, surfactant, deionized water 60 ~ 75 parts.
Particularly, be made up of the component of following weight portion: cetearyl alcohol 8 parts, glycerol 13 parts, hexadecanol 3 parts, Herba Gynurae bicoloris extract 8 parts, tea polyphenols 1 part, Radix Scutellariae extract 8 parts, Margarita powder 0.3 part, titanium dioxide 0.3 part, 3,4 '-methyl benzylidene camphor 0.3 part, dicaprylyl carbonate 1 part, bisabolol 1 part, hyaluronic acid 1 part, 1 part, surfactant, deionized water 70 parts.
Particularly, one or more mixture in the preferred cocoamido propyl hydroxy sulfobetaine of described surfactant, Coconut Fatty Acid Monoethanolamide sulfosuccinic acid monoesters disodium, cocamido propyl betaine; More preferably cocamido propyl betaine.
The preparation method of tea polyphenols sunscreen cream of the present invention comprises the following steps:
(1). the preparation of aqueous phase: under stirring, is dissolved in deionized water by the hyaluronic acid of described formula ratio, surfactant, is heated to 60 ~ 80 DEG C;
(2). the preparation of oil phase: under stirring, by the cetearyl alcohol of described formula ratio, glycerol, hexadecanol, Margarita powder, titanium dioxide, 3,4 '-methyl benzylidene camphor, dicaprylyl carbonate, bisabolol mix homogeneously, be heated to 60 ~ 80 DEG C;
(3). the preparation of tea polyphenols sunscreen cream: the oil phase that step (2) is obtained is slowly added in the obtained aqueous phase of step (2) under insulation, 2000 ~ 3000r/min homogenizing, 2 ~ 5min, 600 ~ 800r/min stirs lower slow cooling to 40 ~ 50 DEG C, adds the Herba Gynurae bicoloris extract of formula ratio, tea polyphenols and Radix Scutellariae extract, continues to be stirred to homogenizing discharging.
Particularly, the preparation method of described Herba Gynurae bicoloris extract is as follows: be broken into slurry after Herba Gynurae bicoloris being cleaned, the ratio being 1: 2 ~ 3 according to extractant and the weight ratio of Herba Gynurae bicoloris extractant is mixed homogeneously with Herba Gynurae bicoloris slurry after ultrasonic 20min ~ 1h at 40 DEG C, elimination insoluble matter, obtains Herba Gynurae bicoloris extract.Wherein said extractant to be percent by volume be 10% alcoholic solution.
Particularly, the preparation method of described Radix Scutellariae extract is as follows: Radix Scutellariae is the ratio of 1: 2 ~ 3 according to the weight ratio of deionized water and Baical Skullcap Root, is added to the water by Baical Skullcap Root after cleaning and pulverizing, reflux, extract, 2 ~ 3h, after cooling, namely elimination insoluble matter obtains Radix Scutellariae extract.
Anthocyanidin (Anthocyanidin), also known as anthocyanidin, is the water-soluble natural pigment that nature one class is extensively present in plant, and belonging to flavonoids, is also the main color-generation material in plant petals.Can produce free radical in skin under solar exposure, these free radicals can accelerate skin aging, and anthocyanidin can protect human body from the damage of free radical, contribute to reducing the damage of being exposed to the sun to skin.Herba Gynurae bicoloris contains lot of anthocyanin and physical stability is better.Compared with other natural pigment, the anthocyanidin in Herba Gynurae bicoloris (Latin literary fame: Amaranthustricolor) has raw material sources convenience, cheapness, low cost, the feature such as pollution-free, and good stability, non-oxidizability is stronger.Extract from Herba Gynurae bicoloris is obtain the both economical and approach easily of of anthocyanidin.
Radix Scutellariae sweet in the mouth, light, be slightly cold; Return spleen, lung, kidney channel.Dampness removing spleen invigorating; Arthralgia relieving by relaxing muscles and tendons; Clearing away heat and discharging pus.Main edema; Foot gas; Dribbling urination; Damp-warm diseases; To have loose bowels leukorrhagia; Rheumatic arthralgia; The contracture of muscle arteries and veins; Lung abscess; Intestinal carbuncle; Verruca plana etc.Radix Scutellariae also has good beautification function to skin.
Tea polyphenols is the general name of Polyphenols of Tea, comprises flavanol compound, anthocyanin class, flavonoid, flavonols and phenolic acids etc.Be mainly flavonol (catechin) class, catechin accounts for 60 ~ 80%.The removing toxic substances of tea polyphenols isoreactivity material tool, radioprotective and antioxidation.
Tea polyphenols sunscreen cream of the present invention, in the physical sunscreen mode of Margarita powder and titanium dioxide, decreases the consumption of chemical sun, and with the addition of multiple natural substance having sun-screening function, and quality is salubrious, better can avoid the generation of allergic phenomena.Bisabolol and Radix Scutellariae extract have the effect of antiinflammatory antiallergic for shining injury, and hyaluronic acid has good moistening effect, can be skin moisturizing in time.Tea polyphenols sunscreen cream color of the present invention is soft, and abnormal smells from the patient is pure and fresh, invigorating, is applicable to public use.
In order to understand better and implement, the following detailed description of the present invention.
Detailed description of the invention
preparation embodiment
The preparation of tea polyphenols sunscreen cream of the present invention comprises the following steps:
(1). the preparation of Herba Gynurae bicoloris extract: be broken into slurry after Herba Gynurae bicoloris being cleaned, the ratio be the alcoholic solution of 10% according to percent by volume being 1: 2 ~ 3 with the weight ratio of Herba Gynurae bicoloris extractant is mixed homogeneously with Herba Gynurae bicoloris slurry after ultrasonic 20min ~ 1h at 40 DEG C, elimination insoluble matter, obtains Herba Gynurae bicoloris extract.
(2). the preparation of Radix Scutellariae extract: Radix Scutellariae is the ratio of 1: 2 ~ 3 according to the weight ratio of deionized water and Baical Skullcap Root, is added to the water by Baical Skullcap Root, reflux, extract, 2 ~ 3h after cleaning and pulverizing, and after cooling, namely elimination insoluble matter obtains Radix Scutellariae extract.
(3). the preparation of aqueous phase: under stirring, is dissolved in deionized water by the hyaluronic acid of table 1 formula ratio, surfactant, is heated to 60 ~ 80 DEG C;
(4). the preparation of oil phase: under stirring, by the cetearyl alcohol of table 1 formula ratio, glycerol, hexadecanol, Margarita powder, titanium dioxide, 3,4 '-methyl benzylidene camphor, dicaprylyl carbonate, bisabolol mix homogeneously, be heated to 60 ~ 80 DEG C;
(5). the preparation of tea polyphenols sunscreen cream: the oil phase that step (2) is obtained is slowly added in the obtained aqueous phase of step (2) under insulation, 2000 ~ 3000r/min homogenizing, 2 ~ 5min, 600 ~ 800r/min stirs lower slow cooling to 40 ~ 50 DEG C, adds the Herba Gynurae bicoloris extract of table 1 formula ratio, tea polyphenols and Radix Scutellariae extract, continues to be stirred to homogenizing discharging.
The each component formula amount of < table 1, with parts by weight >
effect example
Natural plants tea polyphenols sunscreen cream of the present invention is to the Protection of mouse skin
Method is as follows: 12 mices are divided into 3 groups at random, often organize 4, label is 1,2,3,4 respectively, thorax abdomen loses hair or feathers about 4cm, uniform application 1 gram of 3 kinds of cream (product that comparative example is obtained, commercially available tea polyphenols sunscreen cream, the product that embodiment 3 is obtained) respectively, hide all the other positions, coating place is given to the ultraviolet radiation (irradiating 20min apart from uviol lamp 50cm) of 40 biological doses.Then wash away cream, Continuous Observation one week, the results are shown in Table 2.Other commercially available tea polyphenols sunscreen cream are better than by visible sun-proof result of the present invention in table.
< table 2 natural plants tea polyphenols of the present invention sunscreen cream is to the protective effect > of mouse skin
The present invention is not limited to above-mentioned embodiment, if do not depart from the spirit and scope of the present invention to various change of the present invention or distortion, if these are changed and distortion belongs within claim of the present invention and equivalent technologies scope, then the present invention is also intended to comprise these changes and distortion.
Claims (9)
1. a tea polyphenols sunscreen cream, it is characterized in that being made up of the component of following weight portion: cetearyl alcohol 5 ~ 10 parts, glycerol 10 ~ 15 parts, hexadecanol 1 ~ 5 part, Herba Gynurae bicoloris extract 5 ~ 10 parts, tea polyphenols 0.5 ~ 3 part, Radix Scutellariae extract 5 ~ 10 parts, Margarita powder 0.1 ~ 0.5 part, titanium dioxide 0.1 ~ 0.5 part, 3,4 '-methyl benzylidene camphor 0.1 ~ 0.5 part, dicaprylyl carbonate 0.5 ~ 3 part, bisabolol 0.5 ~ 3 part, hyaluronic acid 0.5 ~ 3 part, 0.5 ~ 3 part, surfactant, deionized water 50 ~ 80 parts.
2. tea polyphenols sunscreen cream according to claim 1, it is characterized in that being made up of the component of following weight portion: cetearyl alcohol 6 ~ 9 parts, glycerol 12 ~ 14 parts, hexadecanol 2 ~ 4 parts, Herba Gynurae bicoloris extract 6 ~ 9 parts, tea polyphenols 0.8 ~ 2 part, Radix Scutellariae extract 6 ~ 9 parts, Margarita powder 0.2 ~ 0.4 part, titanium dioxide 0.2 ~ 0.4 part, 3,4 '-methyl benzylidene camphor 0.2 ~ 0.4 part, dicaprylyl carbonate 0.8 ~ 2 part, bisabolol 0.8 ~ 2 part, hyaluronic acid 0.8 ~ 2 part, 0.8 ~ 2 part, surfactant, deionized water 60 ~ 75 parts.
3. tea polyphenols sunscreen cream according to claim 2, it is characterized in that being made up of the component of following weight portion: cetearyl alcohol 8 parts, glycerol 13 parts, hexadecanol 3 parts, Herba Gynurae bicoloris extract 8 parts, tea polyphenols 1 part, Radix Scutellariae extract 8 parts, Margarita powder 0.3 part, titanium dioxide 0.3 part, 3,4 '-methyl benzylidene camphor 0.3 part, dicaprylyl carbonate 1 part, bisabolol 1 part, hyaluronic acid 1 part, 1 part, surfactant, deionized water 70 parts.
4. the tea polyphenols sunscreen cream according to claims 1 to 3 any one, is characterized in that: described surfactant is one or more mixture in cocoamido propyl hydroxy sulfobetaine, Coconut Fatty Acid Monoethanolamide sulfosuccinic acid monoesters disodium, cocamido propyl betaine.
5. tea polyphenols sunscreen cream according to claim 4, is characterized in that: described surfactant is cocamido propyl betaine.
6. prepare the tea polyphenols sunscreen cream described in claims 1 to 3 any one, it is characterized in that comprising the following steps:
(1) preparation of aqueous phase: under stirring, is dissolved in deionized water by the hyaluronic acid of described formula ratio, surfactant, is heated to 60 ~ 80 DEG C;
(2) preparation of oil phase: under stirring, by the cetearyl alcohol of described formula ratio, glycerol, hexadecanol, Margarita powder, titanium dioxide, 3,4 '-methyl benzylidene camphor, dicaprylyl carbonate, bisabolol mix homogeneously, be heated to 60 ~ 80 DEG C;
(3) preparation of tea polyphenols sunscreen cream: the oil phase that step (2) is obtained is slowly added in the obtained aqueous phase of step (2) under insulation, 2000 ~ 3000r/min homogenizing, 2 ~ 5min, 600 ~ 800r/min stirs lower slow cooling to 40 ~ 50 DEG C, adds the Herba Gynurae bicoloris extract of formula ratio, tea polyphenols and Radix Scutellariae extract, continues to be stirred to homogenizing discharging.
7. tea polyphenols sunscreen cream according to claim 6, it is characterized in that: the preparation method of described Radix Scutellariae extract is as follows: after Radix Scutellariae is cleaned and pulverized, be the ratio of 1: 2 ~ 3 according to the weight ratio of deionized water and Baical Skullcap Root, Baical Skullcap Root is added to the water, reflux, extract, 2 ~ 3h, after cooling, namely elimination insoluble matter obtains Radix Scutellariae extract.
8. the preparation method of tea polyphenols sunscreen cream according to claim 6, it is characterized in that: the preparation method of described Herba Gynurae bicoloris extract is as follows: after Herba Gynurae bicoloris being cleaned, be broken into slurry, the ratio being 1: 2 ~ 3 according to extractant and the weight ratio of Herba Gynurae bicoloris extractant is mixed homogeneously with Herba Gynurae bicoloris slurry after ultrasonic 20min ~ 1h at 40 DEG C, elimination insoluble matter, obtains Herba Gynurae bicoloris extract.
9. the preparation method of tea polyphenols sunscreen cream according to claim 8, is characterized in that: described extractant to be percent by volume be 10% alcoholic solution.
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| CN201510922161.0A CN105342973A (en) | 2015-12-11 | 2015-12-11 | Tea polyphenol sun cream and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106038360A (en) * | 2016-04-26 | 2016-10-26 | 曾新民 | A preparing method of a compound sunscreen cream containing nanometer graphene |
| WO2017172523A1 (en) * | 2016-03-31 | 2017-10-05 | L'oreal | Cosmetic compositions and methods for providing broad and full spectrum photo protection |
| CN107648141A (en) * | 2017-10-27 | 2018-02-02 | 李创华 | A kind of sunscreen composition for absorbing ultraviolet |
| CN107982181A (en) * | 2018-01-29 | 2018-05-04 | 成都懿和唯美科技有限公司 | Tea polyphenols whitening spot-relieving cream |
| US10137072B2 (en) | 2016-03-31 | 2018-11-27 | L'oreal | Methods and compositions for providing broad spectrum photo protection using antioxidants |
| US10149808B2 (en) | 2016-03-31 | 2018-12-11 | L'oreal | Cosmetic compositions and methods for providing full spectrum photo protection |
| CN109288758A (en) * | 2018-11-22 | 2019-02-01 | 林锡慧 | A kind of mosquito-expelling and antipruritic formula of sun screen |
| CN110179683A (en) * | 2019-05-30 | 2019-08-30 | 汕头大学 | A kind of cosmetics containing natural substance having sun-screening function |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017172523A1 (en) * | 2016-03-31 | 2017-10-05 | L'oreal | Cosmetic compositions and methods for providing broad and full spectrum photo protection |
| US10137072B2 (en) | 2016-03-31 | 2018-11-27 | L'oreal | Methods and compositions for providing broad spectrum photo protection using antioxidants |
| US10149808B2 (en) | 2016-03-31 | 2018-12-11 | L'oreal | Cosmetic compositions and methods for providing full spectrum photo protection |
| CN106038360A (en) * | 2016-04-26 | 2016-10-26 | 曾新民 | A preparing method of a compound sunscreen cream containing nanometer graphene |
| CN107648141A (en) * | 2017-10-27 | 2018-02-02 | 李创华 | A kind of sunscreen composition for absorbing ultraviolet |
| CN107982181A (en) * | 2018-01-29 | 2018-05-04 | 成都懿和唯美科技有限公司 | Tea polyphenols whitening spot-relieving cream |
| CN109288758A (en) * | 2018-11-22 | 2019-02-01 | 林锡慧 | A kind of mosquito-expelling and antipruritic formula of sun screen |
| CN110179683A (en) * | 2019-05-30 | 2019-08-30 | 汕头大学 | A kind of cosmetics containing natural substance having sun-screening function |
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