CN1279937C - Antiseptic and insect killing washing liquid and preparing method - Google Patents

Antiseptic and insect killing washing liquid and preparing method Download PDF

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Publication number
CN1279937C
CN1279937C CN 200410060829 CN200410060829A CN1279937C CN 1279937 C CN1279937 C CN 1279937C CN 200410060829 CN200410060829 CN 200410060829 CN 200410060829 A CN200410060829 A CN 200410060829A CN 1279937 C CN1279937 C CN 1279937C
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China
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washing liquid
rutin
rhizoma chuanxiong
oil
pure water
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Expired - Fee Related
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CN 200410060829
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CN1615988A (en
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袁晓
袁萍
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Wuhan Botanical Garden of CAS
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Wuhan Botanical Garden of CAS
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Abstract

The present invention discloses a sterilizing and insect killing washing liquid and a preparing method. The washing liquid is prepared from acrylic acid styrene cross-linked polymers, potassium alkyl phosphate, cationic guar gum, emulsified silica oil, potassium hydroxide, glycol dipropionate distearate, sodium ethylenediamine tetracetate, diphenyl ketone-4, litsea cubeba extraction oil, extracting liquids, hydrogenated castor oil and purified water through the following steps: dissolving the acrylic acid styrene cross-linked polymers, the potassium alkyl phosphate, the sodium ethylenediamine tetracetate and the diphenyl ketone-4 by the purified water; dissolving the guar gum by the purified water, the glycol dipropionate distearate and the emulsified silica oil; crushing doubleteeth pubesscent angelica root, szechwan lovage rhizome, baical skullcap root and rutin, and then extracting and concentrating; mixing the solutions and the extracting liquids; emulsifying the litsea cubeba extraction oil and the hydrogenated castor oil; mixing the mixed liquids and the emulsified liquids, and then adding the purified water so as to obtain the washing liquid. The present invention has the advantages of good sterilizing and insect killing effect and simple technology, and can be used for human body skin to effectively treat acne, vaginitis and dermatophytosis caused by acarid, fungi and mycete.

Description

A kind of antibiotic parasite killing washing liquid and preparation method
Technical field
The present invention relates to a kind of washing liquid of Pesticidal and sterilizing, the washing liquid that more specifically relates to a kind of parasite killing, sterilizes, goes demodicid mite, removes cicatrix also relates to the preparation method of this washing liquid simultaneously.
Background technology
Acarid is the common a kind of parasite of people.The average infection rate of domestic crowd's vermiform mite is 31.54%.Hair follicle and sebaceous gland that face amount portion, external auditory meatus, scalp, nipple, breast, arm that can extensively parasitize healthy population etc. locates, also can cause seborrheic dermatitis, acne, rosacea, blepharitis, alopecia under certain condition as under the factor effects such as resistance decline or bacterial infection.The skin of human body also is vulnerable to the infection of fungus, mycete except the infection that is subject to acarid, in case when the skin of human body is subjected to fungus, fungal infection, just common beriberi, gynecological inflammation etc., it is incomparable very to itch, and misery is unbearably.
Acne is commonly called as acne, is a kind of pilosebaceous unit chronic skin inflammation, good sending out in the adolescence men and women, and sickness rate is higher, facial red varioliform exanthema sample and the fester of taking place of the lighter, the hair follicle abscess takes place in weight person, knot is silly.Even normal healing, damaging part leave the loose Cuo cicatrix of the calm speckle of color rope or pockmark shape atrophy cicatrix and pimple shape mostly, have a strong impact on the outward appearance beauty treatment, and cause psychological wound to the patient.
At present, both at home and abroad parasites of adopting chemicals to kill people's body surface more.Yet after chemicals used, the toxicity of chemical drugs, zest and anaphylaxis also came one after another.In addition, for the control of acne, the external frost that contains benzoyl peroxide or metronidazole commonly used is both at home and abroad controlled it, though certain curative effect is arranged, drug side effect is very big, easily stays mottle and cicatrix after healing.Chemical drugs life-time service effect and safety issue have caused people's worry.Simultaneously, the environmental protection problem that causes of product industry is also following.
Summary of the invention
The object of the present invention is to provide a kind of antibiotic parasite killing washing liquid, prescription is rationally treated acne, vaginitis, beriberi that human body skin causes owing to acarid, fungus, mycete effectively.Also have blood circulation promoting and blood stasis dispelling simultaneously, go effect such as cicatrix.The pesticide-germicide effect is obvious, alternative existing like product.
Another object of the present invention is to prepare the method for antibiotic parasite killing washing liquid, and this method technology is simple, cost is low, easy operation, and it is nontoxic, pollution-free also to have nature simultaneously, nontoxic to human body, and many-sided physiological function is arranged.
China's plant resources is abundant, and is floristic various, and plant and physiological function composition thereof varied utilizes plant resources to excavate and the development of new service of goods becomes effective in society's day.Removing speckle, go the medicinal plants of cicatrix to have in the natural medicinal plant: Rhizoma Chuanxiong, Radix Saposhnikoviae, Radix Glehniae, Rhizoma Ligustici, Radix Angelicae Pubescentis etc., dredge the meridian passage, expelling wind and activating blood circulation, antiheumatic medicinal plants have: Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Cyathulae, Radix Gentianae Macrophyllae, Rhizoma Et Radix Notopterygii etc.In addition, the volatile oil that from the Fructus Litseae fruit, extracts.Tens of kinds of chemical constituents are wherein arranged, have certain relieving asthma, effect such as antiallergic, antithrombotic, arrhythmia, antimicrobial and trichomonas vaginitis, anti-plant insect, aflatoxin degradation.Use aspects such as litsea cubeba oil treatment chronic bronchitis, cerebral thrombosis, burn infection clinically, obtained curative effect preferably.
In order to realize above-mentioned task, the present invention adopts following technical measures: it is all formulated by a certain percentage by acrylic acid styrene cross linked polymer, monoalkyl phosphoric acid esters potassium, guar gum, emulsified silicone oil, potassium hydroxide, glycol distearate, disodiumedetate, benzophenone-4, Fructus Litseae essential oil, Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae, rutin extracting solution, castor oil hydrogenated and pure water, and the percentage by weight of each raw material (%) is:
Acrylic acid styrene cross linked polymer 10.0-20.0% monoalkyl phosphoric acid esters potassium 20-25.0%
Guar gum 0.4-0.6% emulsified silicone oil 2.0-5.0%
Glycol distearate 2.0-5.0% disodiumedetate 0.3-0.5%
Benzophenone-4 0.3-0.5% Fructus Litseae essential oil 1.0-2.0%
Castor oil hydrogenated 2.0-4.0% pure water 32.4-58.0%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin (1: 1: 1: 1) 4.0-5.0%
Fragrant plant Pesticidal and sterilizing, the washing liquid of removing cicatrix the steps include:
(1) add the doubly heavy pure water of acrylic acid styrene cross linked polymer 0.8-1.2 in acrylic acid styrene cross linked polymer, abundant dispersed with stirring adds monoalkyl phosphoric acid esters potassium, disodiumedetate, benzophenone-4 again and stirs, mixed liquor.
(2) in guar gum, add the doubly heavy pure water of guar gum 8-12, stir, add glycol distearate and emulsified silicone oil again, be stirred to the even mixed liquor that gets until evenly.
(3) will wait the Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae of weight and rutin to pulverize after, cross the 10-20 mesh sieve, 95% ethanol ultrasonic extraction with the gross weight of 8-12 times of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin, leach solution, get extracting solution, repeat supersound extraction 2-3 time, merge extractive liquid,, and be concentrated into 1 times of gross weight concentrated solution to Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin, get Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin extracting solution.
(4) mixed liquor of (1) step and two kinds of solution of mixed liquor of (2) step are mixed with the extracting solution of (3) step, be stirred to the even mixed liquor that gets.
(5) fully mix Fructus Litseae essential oil and add the hydrogenation Oleum Ricini, obtain a kind of mixed liquor.
(6) mixed liquor of above-mentioned (4) step and the mixed liquor of (5) step are mixed, and add pure water, obtain a kind of washing liquid.
The present invention is main Pesticidal and sterilizing, goes speckle to remove the scar composition with medicinal plants active component and aromatic essential oil, is equipped with the fine emulsifying agent that mixes of its energy, reaches bath gel substrate etc., is mixed with the Pesticidal and sterilizing with natural aromatic flavor and goes the scar washing liquid.Acrylic acid styrene cross linked polymer monoalkyl phosphoric acid esters potassium is bath gel substrate, and cation guar gum, emulsified silicone oil, glycol distearate are conditioner, and disodiumedetate is used to the metal ion that boils together.Benzophenone-4 is used to absorb ultraviolet, and Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin extracting solution can bactericidal antiphlogistics.Remove cicatrix, Fructus Litseae essential oil plays the killing acarus and bacteria effect, and castor oil hydrogenated is used for the emulsifying plants essential oil.
Litsea cubeba oil in this washing liquid has killing effect through evidence to acarid; To the valid density of killing fungus is 2%; To the valid density of killing mycete is 1 ‰.And the toxicological test proof is nontoxic to human body, and concrete outcome is as follows:
The present invention utilizes the active component with pesticide-germicide in the litsea cubeba oil; The effect that Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin extracting solution have cicatrix is mixed with the washing liquid with natural faint scent, and washing liquid can not only cleaning skin, and can kill the acarid sterilization, to acne rosacea, the red pimple that is caused by acarid on the skin.Freckle on the skin and cicatrix.Beriberi, skin pruritus, the vaginitis that is caused by the fungus mycete has the effect of good anti-inflammatory anti-itch, and technology of the present invention is simple, processing ease.
The specific embodiment
Embodiment 1: the percentage by weight of each raw material (%) is:
Acrylic acid styrene cross linked polymer 10.0% monoalkyl phosphoric acid esters potassium 20.0%
Guar gum 0.4% emulsified silicone oil 2.0%
Glycol distearate 2.0% disodiumedetate 0.3%
Benzophenone-4 0.3% Fructus Litseae essential oil 1.0%
Castor oil hydrogenated 2.0% pure water 58.0%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin (1: 1: 1: 1) 4.0%
A kind of step for preparing antibiotic parasite killing washing liquid is as follows:
(1) add the doubly heavy pure water of acrylic acid styrene cross linked polymer 0.8-1.2 in acrylic acid styrene cross linked polymer, abundant dispersed with stirring adds monoalkyl phosphoric acid esters potassium, disodiumedetate, benzophenone-4 again and stirs, mixed liquor.
(2) in guar gum, add the doubly heavy pure water of guar gum 8-12, stir, add glycol distearate and emulsified silicone oil again, be stirred to the even mixed liquor that gets until evenly.
(3) will wait the Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae of weight and rutin to pulverize after, cross the 10-20 mesh sieve, 95% ethanol ultrasonic extraction with the gross weight of 8-12 times of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin, leach solution, get extracting solution, repeat supersound extraction 2-3 time, merge extractive liquid,, and be concentrated into 1 times of gross weight concentrated solution to Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin, get Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin extracting solution.
(4) will mix with the extracting solution of (3) step with mixed liquor of above-mentioned (1) step and the mixed liquor of (2) step, be stirred to the even mixed liquor that gets.
(5) Fructus Litseae essential oil and castor oil hydrogenated is fully emulsified, obtain emulsion.
(6) mixed liquor of above-mentioned (4) step and the emulsion of (5) step are mixed, and add pure water, obtain a kind of antibiotic parasite killing washing liquid.
Embodiment 2: the percentage by weight of each raw material (%) is:
Acrylic acid styrene cross linked polymer 15% monoalkyl phosphoric acid esters potassium 22.5%
Guar gum 0.5% emulsified silicone oil 3.5%
Glycol distearate 3.5% disodiumedetate 0.4%
Benzophenone-4 0.4% Fructus Litseae essential oil 1.5%
Castor oil hydrogenated 3.0% pure water 45.2%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin (1: 1: 1: 1) 4.5%
Preparation process is identical with embodiment 1.
Embodiment 3: the percentage by weight of each raw material (%) is:
Acrylic acid styrene cross linked polymer 20.0% monoalkyl phosphoric acid esters potassium 25.0%
Guar gum 0.6% emulsified silicone oil 5.0%
Glycol distearate 5.0% disodiumedetate 0.5%
Benzophenone-4 0.5% Fructus Litseae essential oil 2.0%
Castor oil hydrogenated 4.0% pure water 32.4%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin (1: 1: 1: 1) 5.0%
Preparation process is identical with embodiment 1.

Claims (5)

1, a kind of antibiotic parasite killing washing liquid, it is made by following raw materials by weight percent:
Acrylic acid styrene cross linked polymer 10.0-20.0% monoalkyl phosphoric acid esters potassium 20-25.0%
Guar gum 0.4-0.6% emulsified silicone oil 2.0-5.0%
Glycol distearate 2.0-5.0% disodiumedetate 0.3-0.5%
Benzophenone-4 0.3-0.5% Fructus Litseae essential oil 1.0-2.0%
Castor oil hydrogenated 2.0-4.0% pure water 32.4-58.0%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin 1: 1: 1: 1 4.0-5.0%.
2, a kind of antibiotic parasite killing washing liquid according to claim 1 is characterized in that:
Acrylic acid styrene cross linked polymer 10.0% monoalkyl phosphoric acid esters potassium 20.0%
Guar gum 0.4% emulsified silicone oil 2.0%
Glycol distearate 2.0% disodiumedetate 0.3%
Benzophenone-4 0.3% Fructus Litseae essential oil 1.0%
Castor oil hydrogenated 2.0% pure water 58.0%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin 1: 1: 1: 1 4.0%.
3, a kind of antibiotic parasite killing washing liquid according to claim 1 is characterized in that:
Acrylic acid styrene cross linked polymer 15% monoalkyl phosphoric acid esters potassium 22.5%
Guar gum 0.5% emulsified silicone oil 3.5%
Glycol distearate 3.5% disodiumedetate 0.4%
Benzophenone-4 0.4% Fructus Litseae essential oil 1.5%
Castor oil hydrogenated 3.0% pure water 45.2%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin 1: 1: 1: 1 4.5%.
4, a kind of antibiotic parasite killing washing liquid according to claim 1 is characterized in that:
Acrylic acid styrene cross linked polymer 20.0% monoalkyl phosphoric acid esters potassium 25.0%
Guar gum 0.6% emulsified silicone oil 5.0%
Glycol distearate 5.0% disodiumedetate 0.5%
Benzophenone-4 0.5% Fructus Litseae essential oil 2.0%
Castor oil hydrogenated 4.0% pure water 32.4%
The extracting solution of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin 1: 1: 1: 1 5.0%.
5, the preparation method of the described a kind of antibiotic parasite killing washing liquid of a kind of claim 1 the steps include:
A, add pure water in acrylic acid styrene cross linked polymer, dispersed with stirring adds monoalkyl phosphoric acid esters potassium, disodiumedetate, benzophenone-4 again and stirs, mixed liquor;
B, in guar gum, add pure water, stir, add glycol distearate and emulsified silicone oil again, be stirred to even mixed liquor until evenly;
After C, the Radix Angelicae Pubescentis that will wait weight, Rhizoma Chuanxiong, Radix Scutellariae and rutin are pulverized, cross the 10-20 mesh sieve, 95% ethanol ultrasonic extraction with the gross weight of 8-12 times of Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin, leach solution, get extracting solution, supersound extraction 2-3 time, merge extractive liquid,, and be concentrated into 1 times of gross weight concentrated solution to Radix Angelicae Pubescentis, Rhizoma Chuanxiong, Radix Scutellariae and rutin;
D, the mixed liquor of A step and two kinds of solution of mixed liquor of B step are mixed with the extracting solution of C step, be stirred to even mixed liquor;
E, Fructus Litseae essential oil and castor oil hydrogenated is fully emulsified obtains emulsion;
F, the emulsion of the mixed liquor of D step and E step is mixed, and add pure water, obtain a kind of antibiotic parasite killing washing liquid.
CN 200410060829 2004-09-10 2004-09-10 Antiseptic and insect killing washing liquid and preparing method Expired - Fee Related CN1279937C (en)

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CN1279937C true CN1279937C (en) 2006-10-18

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CN102352554A (en) * 2011-07-29 2012-02-15 苏州卡奇特纺织有限公司 Mildew preventive for pure silk fabrics

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