CN1253415C - Leaf surface fertilizer of reducing pesticide residue and promoting cropper growth - Google Patents
Leaf surface fertilizer of reducing pesticide residue and promoting cropper growth Download PDFInfo
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- CN1253415C CN1253415C CN 200410023955 CN200410023955A CN1253415C CN 1253415 C CN1253415 C CN 1253415C CN 200410023955 CN200410023955 CN 200410023955 CN 200410023955 A CN200410023955 A CN 200410023955A CN 1253415 C CN1253415 C CN 1253415C
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- rare earth
- saccharide
- foliage fertilizer
- liquid
- leaf fertilizer
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Abstract
The present invention relates to a method for preparing leaf fertilizer for reducing residual pesticide and promoting plant growth. The method comprises the following steps that firstly, after monosaccharide, sugar alcohol and sugar derivatives or oligosaccharide and other saccharide are dissolved in water, and rare earth nitrate for agriculture use or rare earth previously dissolved by dilute acid is added to the solution, wherein the adding amount of the rare earth accounts for 0.4% to 30.8% of the saccharide; then, a reaction is carried out to a mixed solution of the saccharide and the rare earth for twenty-four hours at a temperature of 10 DEG C to 40 DEG C, a pH value of the reaction liquid is regulated to 4 to 7 so as to obtain liquid leaf fertilizer, and the liquid leaf fertilizer is further dried so as to obtain the solid leaf fertilizer, wherein the saccharide can be one kind of or a mixture of several kinds of monosaccharide, sugar alcohol and sugar derivatives or oligosaccharide, the content of the saccharide is controlled between 250g and 650g per mu, and the total rare earth content is controlled between 1g and 25g per mu. The degradation rate of organic phosphorus pesticide is more than 80% after the leaf fertilizer of the present invention is sprayed for several days, and a crop yield increase rate ranges from 3 to 20%. The present invention has the advantages of simple production process, easy acquirement of raw material, less investment, no pollution and requirement satisfaction for producing green food.
Description
Technical field
The present invention relates to the foliage fertilizer preparation method of the short plant growth of a kind of decreasing organic phosphorous pesticide residue.
Background technology
China has a large population in a small area, and how to guarantee that food quantity safety and quality safety are long-term and difficult task.With regard to plant-sourced food, no matter be large grain-production, or the production of vegetable and fruit, their growth busy season is also mostly to be that the busy season takes place in insect pest.Present stage, the peasant also needed to use the chemical pesticide control insect pest in order to improve their output and quality.Along with the complete prohibition use and the pyrethroid pesticide of organochlorine pesticide easily makes insect develop immunity to drugs, organophosphorus pesticide has accounted for 70% of sterilant total amount at present.Long-term scale operation and use organophosphorus pesticide not only causes severe contamination to environment, residual in food and feed people and cultivated animals is also seriously influenced.And carry out research, the pollution-free food production base of transgenic pest-resistant, disease-resistant crop construction, biological pesticide and organophosphorus pesticide development of substitutes, set up the superseded use of Food Quality and Safety security system, food quality and safety (QS) market access mechanism and some organophosphorus pesticide or in food hygienic standard, reach not have to detect and all to need to require etc. very strong science and technology and funds support, apply from developing to as a kind of agricultural chemicals, need multi-disciplinary cooperations such as chemistry, agronomy, medical science and environment, go through more than ten years.According to the national conditions of China, present stage is the use of impossible total ban organophosphorus pesticide also.Therefore, can degrade and make organophosphorus pesticide in the object, the foliage fertilizer that can promote plant growth again is current and presses for from now on.
The foliage fertilizer of China's development at present is more, and its main purpose is to promote plant growth and improve quality.As a kind of solubility compound powder (ZL98103155.2) and a kind of efficient many bacterium energy foliage fertilizers and preparation method thereof patented products such as (ZL92109659.3) as fertile medicine, and existing promotion plant growth has the product for agriculture of decreasing organic phosphorous agricultural chemicals to have not yet to see patent report.
Summary of the invention
The a large amount of uses that The present invention be directed to present organophosphorus pesticide are developed a kind of organophosphorus pesticide degraded in the object that can promote to do to the present situation that food pollutes, and can improve the foliage fertilizer of crop yield again.
Preparation method of the present invention or technology: carbohydrate or sugar derivatives earlier with after the water dissolution, are added rare earth element, and re-adjustment reacting liquid pH value to 4～7 are filtered the back and are concentrated and just obtains liquid foliage fertilizer, further are drying to obtain solid-state foliage fertilizer.Carbohydrate wherein is monose, sugar alcohol and sugar derivatives or oligose, or appoint wherein a kind of, the also mixture that they can be formed in any ratio; Wherein rare earth element is agricultural rare earth nitrate, or uses diluted acid dissolved rare earth in advance.No matter be liquid foliage fertilizer or solid-state foliage fertilizer, every mu of contents of saccharide is controlled at 250g～650g in use; The rare earth element overall control is at 1g～25g.
Therefore, essence of the present invention is to utilize carbohydrate to be part and rare earth element ligand complex, the malt sugar of preparing soil mixture.Use this mixture on the crop that has sprayed organophosphorus pesticide organophosphorus pesticide degradation rate in a couple of days is reached more than 80%, the crop yield rate is 3～20%, and the crop yield probability is about 85%.And production technique of the present invention is simple, and raw material is easy to get, and less investment is pollution-free, meets the needs and the requirement of current and pollution-free food production from now on.
Embodiment
Preparation method of the present invention: the carbohydrate that will comprise monose, sugar alcohol and sugar derivatives or oligose is earlier with after the water dissolution, add agricultural rare earth nitrate or use diluted acid dissolved rare earth in advance, rare earth adding quantity is 0.4%～30.8% (accounting for the per-cent of carbohydrate weight), conditioned reaction liquid pH value to 4～7 behind reaction 24h under 10 ℃～40 ℃, obtain liquid foliage fertilizer, further be drying to obtain solid-state foliage fertilizer.Carbohydrate wherein can be with appointing mixture a kind of or that they are formed in any ratio in monose, sugar alcohol and sugar derivatives or the oligose, but wherein contents of saccharide is controlled at every mu of 250g～650g.Total amount of rare earth is controlled at 1g～20g for every mu.
Above-mentioned described monose is semi-lactosi, fructose, and described sugar alcohol is arabitol, melampyrum, glucitol, Xylitol, and described sugar derivatives is a glucosamine, and described oligose is trehalose, lactose, raffinose, maltose.Used agricultural rare-earth can be that " Chang Le " board benefit is planted element (the little fertile factory in Shangqiu produces) or other agricultural rare-earth; Also can add single rare earth element or the mishmetal of using dilute nitric acid dissolution in advance, conditioned reaction liquid pH value is meant that being fine-tuning to pH with alkali is 4～7.If reaction solution has before reached required pH value, can add the adjusting PH with base value again.
Embodiment 1
Semi-lactosi or fructose 50g are dissolved in the 100ml water, slowly add 0.3g " Chang Le " board benefit and plant element, remain on 25 ℃ of reaction 24h after, liquid foliage fertilizer, or dry solid-state foliage fertilizer.Solid-state in every mu of usage quantity is 400g, and liquid should contain solid substance 400g, and they are foliage fertilizer using method use routinely all.
Embodiment 2
Be dissolved in the 100ml water at the mid-semi-lactosi of acid-resistant container and each 25g of fructose, slowly add the 0.2g rare earth nitrate, remain on 25 ℃ of reaction 24h after, be must liquid foliage fertilizer after 6.0 with bicarbonate of ammonia conditioned reaction liquid pH value, or dry must solid-state foliage fertilizer.Solid-state in every mu of usage quantity is 350g, and liquid should contain solid substance 350g, they all routinely the foliage fertilizer using method use.
Embodiment 3
Glucosamine 50g is dissolved in the 100ml water, slowly adds 0.3g " Chang Le " board benefit and plants element, remain on 25 ℃ of reaction 24h after, liquid foliage fertilizer, or dry solid-state foliage fertilizer.Solid-state in every mu of usage quantity is 500g, and liquid should contain solid substance 500g.They are foliage fertilizer using method use routinely all.
Embodiment 4
At the mid-raffinose of acid-resistant container or fructose 50g, tap water 90ml, slowly add in advance with dilute nitric acid dissolution, concentration is the earth solution 10ml of 30mg/ml, after remaining on 25 ℃ of reaction 24h, with bicarbonate of ammonia conditioned reaction liquid pH value be after 6.0 liquid foliage fertilizer, or dry solid-state foliage fertilizer.Solid-state in every mu of usage quantity is 400g, and liquid should contain solid substance 400g.They are foliage fertilizer using method use routinely all.
Embodiment 5
Be dissolved in the 90ml water at mid-glucosamine of acid-resistant container or melampyrum 50g, slowly adding is the earth solution 10ml of 30mg/ml in advance with diluted acid dissolved, concentration, after remaining on 25 ℃ of reaction 24h, with bicarbonate of ammonia conditioned reaction liquid pH value be after 6.5 liquid foliage fertilizer, or dry solid-state foliage fertilizer.Solid-state in every mu of usage quantity is 350g, and liquid should contain solid substance 350g.They are foliage fertilizer using method use routinely all.
Claims (1)
1, the foliage fertilizer preparation method of the short plant growth of a kind of decreasing organic phosphorous pesticide residue, it is characterized in that any or mixture that they are formed in any ratio in monose, sugar alcohol, sugar derivatives or the oligose earlier with after the water dissolution, add agricultural rare earth nitrate or use diluted acid dissolved rare earth in advance, the per-cent that rare earth adding quantity accounts for carbohydrate weight is 0.4%～30.8%, conditioned reaction liquid pH value to 4～7 behind reaction 24h under 10 ℃～40 ℃, obtain liquid foliage fertilizer, further be drying to obtain solid-state foliage fertilizer;
Wherein said monose is semi-lactosi, fructose, and sugar alcohol is arabitol, melampyrum, glucitol, Xylitol, and sugar derivatives is a glucosamine, and oligose is trehalose, lactose, raffinose, maltose.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410023955 CN1253415C (en) | 2004-04-22 | 2004-04-22 | Leaf surface fertilizer of reducing pesticide residue and promoting cropper growth |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410023955 CN1253415C (en) | 2004-04-22 | 2004-04-22 | Leaf surface fertilizer of reducing pesticide residue and promoting cropper growth |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1562898A CN1562898A (en) | 2005-01-12 |
| CN1253415C true CN1253415C (en) | 2006-04-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410023955 Expired - Fee Related CN1253415C (en) | 2004-04-22 | 2004-04-22 | Leaf surface fertilizer of reducing pesticide residue and promoting cropper growth |
Country Status (1)
| Country | Link |
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| CN (1) | CN1253415C (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103797955B (en) * | 2014-01-28 | 2015-09-09 | 广西喷施宝股份有限公司 | A kind of method reducing Organo-phosphorus Pesticide Residues in Vegetables |
| CN105036923A (en) * | 2015-07-22 | 2015-11-11 | 烟台嘉禾生物科技有限公司 | Multifunctional water soluble fertilizer |
| CN105152745A (en) * | 2015-07-30 | 2015-12-16 | 合肥元政农林生态科技有限公司 | Petasites tatewakianus foliar fertilizer |
| CN107266166A (en) * | 2017-06-15 | 2017-10-20 | 宿松县宝利鑫家庭农场 | A kind of water retention organic fertilizer of degrading pesticide residues |
| CN108835511A (en) * | 2018-06-04 | 2018-11-20 | 陕西日日新生物科技有限公司 | A kind of fruits and vegetables coloring modifying agent |
| CN108484299A (en) * | 2018-06-24 | 2018-09-04 | 覃海平 | A kind of general foliar fertilizer and preparation method thereof |
| CN108503453A (en) * | 2018-06-24 | 2018-09-07 | 覃海平 | A kind of general foliar fertilizer and preparation method thereof promoting flowering of plant result |
-
2004
- 2004-04-22 CN CN 200410023955 patent/CN1253415C/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN1562898A (en) | 2005-01-12 |
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| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060426 |