CN1212075C - Micro particle feed for rockfish fry and its production procss - Google Patents
Micro particle feed for rockfish fry and its production procss Download PDFInfo
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- CN1212075C CN1212075C CNB031141765A CN03114176A CN1212075C CN 1212075 C CN1212075 C CN 1212075C CN B031141765 A CNB031141765 A CN B031141765A CN 03114176 A CN03114176 A CN 03114176A CN 1212075 C CN1212075 C CN 1212075C
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- 239000011859 microparticle Substances 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 7
- 241001529596 Pontinus kuhlii Species 0.000 title 1
- 241000251468 Actinopterygii Species 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 235000016709 nutrition Nutrition 0.000 claims abstract description 7
- 238000001694 spray drying Methods 0.000 claims abstract description 6
- 108091005804 Peptidases Proteins 0.000 claims abstract description 5
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 5
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 5
- 235000019197 fats Nutrition 0.000 claims abstract description 5
- 230000000091 immunopotentiator Effects 0.000 claims abstract description 5
- 239000002245 particle Substances 0.000 claims abstract description 5
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 5
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 5
- 235000019750 Crude protein Nutrition 0.000 claims abstract description 4
- 235000019784 crude fat Nutrition 0.000 claims abstract description 4
- 241001417495 Serranidae Species 0.000 claims description 17
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 8
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 8
- 230000000366 juvenile effect Effects 0.000 claims description 8
- 239000004365 Protease Substances 0.000 claims description 7
- 235000013372 meat Nutrition 0.000 claims description 6
- 230000000050 nutritive effect Effects 0.000 claims description 6
- 241000238371 Sepiidae Species 0.000 claims description 5
- 239000008344 egg yolk phospholipid Substances 0.000 claims description 5
- AZJQQNWSSLCLJN-UHFFFAOYSA-N 2-ethoxyquinoline Chemical compound C1=CC=CC2=NC(OCC)=CC=C21 AZJQQNWSSLCLJN-UHFFFAOYSA-N 0.000 claims description 4
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 4
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 4
- 229930003268 Vitamin C Natural products 0.000 claims description 4
- 229930003427 Vitamin E Natural products 0.000 claims description 4
- 235000006708 antioxidants Nutrition 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000002372 labelling Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 239000003921 oil Substances 0.000 claims description 4
- 235000019198 oils Nutrition 0.000 claims description 4
- 235000019419 proteases Nutrition 0.000 claims description 4
- 235000019154 vitamin C Nutrition 0.000 claims description 4
- 239000011718 vitamin C Substances 0.000 claims description 4
- 235000019165 vitamin E Nutrition 0.000 claims description 4
- 229940046009 vitamin E Drugs 0.000 claims description 4
- 239000011709 vitamin E Substances 0.000 claims description 4
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 3
- 235000016425 Arthrospira platensis Nutrition 0.000 claims description 3
- 240000002900 Arthrospira platensis Species 0.000 claims description 3
- 241000237536 Mytilus edulis Species 0.000 claims description 3
- 108090000526 Papain Proteins 0.000 claims description 3
- 235000020638 mussel Nutrition 0.000 claims description 3
- 235000019834 papain Nutrition 0.000 claims description 3
- 229940055729 papain Drugs 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 229940083466 soybean lecithin Drugs 0.000 claims description 3
- 229940082787 spirulina Drugs 0.000 claims description 3
- 241000243686 Eisenia fetida Species 0.000 claims description 2
- 239000003026 cod liver oil Substances 0.000 claims description 2
- 235000012716 cod liver oil Nutrition 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 150000004676 glycans Chemical class 0.000 claims description 2
- 210000004185 liver Anatomy 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 229920001282 polysaccharide Polymers 0.000 claims description 2
- 239000005017 polysaccharide Substances 0.000 claims description 2
- 235000015097 nutrients Nutrition 0.000 abstract description 4
- 238000002474 experimental method Methods 0.000 abstract description 3
- 102000035195 Peptidases Human genes 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 235000019833 protease Nutrition 0.000 abstract 1
- 235000019688 fish Nutrition 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000013535 sea water Substances 0.000 description 3
- 241000700141 Rotifera Species 0.000 description 2
- 241001494106 Stenotomus chrysops Species 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 229910052736 halogen Inorganic materials 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 235000018102 proteins Nutrition 0.000 description 2
- 230000004083 survival effect Effects 0.000 description 2
- 241000143060 Americamysis bahia Species 0.000 description 1
- 241000972773 Aulopiformes Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000694873 Paralichthyidae Species 0.000 description 1
- 101710173866 Seminase Proteins 0.000 description 1
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000003872 anastomosis Effects 0.000 description 1
- 235000021120 animal protein Nutrition 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
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- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 230000001846 repelling effect Effects 0.000 description 1
- 235000019515 salmon Nutrition 0.000 description 1
- 238000012549 training Methods 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
- Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
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- Fodder In General (AREA)
- Feed For Specific Animals (AREA)
Abstract
The present invention relates to strengthened nutrient microparticle feed for striped fish whelp, larvae and young fish and a production process of the strengthened nutrient microparticle feed. The feed uses microparticles with the grain diameter of 100 to 1000 um predominantly, the content of crude protein is from 55 to 68%, the crude fat is from 14 to 22%, the phosphatide is from 3 to 5%, ash content is from 5 to 15%, n-3HUFA is from 2 to 4%, DHA/EPA is from 1 to 3%, DHA is from 1 to 2% and EPA is from 0.6 to 1 %. The feed is obtained by that after a protein source raw material, a fat source raw material, a raw material and an immunopotentiator are zymolytic by proteinases, the antioxidant is added, hydrolyzate is obtained by filtration, and then, the strengthened nutrient microparticle feed is obtained by spray drying. The microparticle feed of the present invention can satisfy the nutritional requirement of striped fish fries, the settling speed is low, the microparticle feed has good stay time, and the particle size is suitable for the aperture of the striped fish fries at each stage. Cultivation experiments indicate that the present invention can effectively and partially substitute biologic bait, and the present invention solves the bottleneck that the current biologic bait supply is not enough and has a significant meaning to the cultivation of striped fish cultivation and has high economic value.
Description
Technical field
The present invention relates to a kind of be grouper son, young, enriched nutritive micro-granulated feed and production technology thereof that juvenile fish provides.
Technical background
What the famousst and precious economic fish grouper of sea-farming was cultured popularizes, and the demand of seedling is increasing, but the wild seedling limited amount, major part depends on import, and uses up a large amount of foreign exchanges every year, and market demand breach is huge.Artificial breeding of grouper and adult fish culture are the fairly obvious high-valued technical industries of economic benefit, have vast market prospect.
The technology of relevant grouper micro-granulated feed does not see that as yet relevant data is arranged both at home and abroad at present, does not have the launch face of this respect yet.And the raising of grouper prelarva is all replaced with the mixed feed of biological feed or other seawater fishes.And the particle mixed bait water repelling property that current technology is produced is poor, generally promptly takes place defeated and dispersedly in water in 20～40 minutes, and the molten mistake of nutrition is big, causes bait utilization low, and polluted water easily causes fish body resistance to descend and falls ill.
Summary of the invention
The purpose of this invention is to provide a kind of grouper son who can be effectively partly substitutes biological feed, young, juvenile fish enriched nutritive micro-granulated feed and production technology thereof, to solve the problem of current biological feed supply wretched insufficiency.
Grouper son of the present invention, young, juvenile fish enriched nutritive micro-granulated feed, microparticle based on particle diameter 100～1000um, the nutritional labeling of feed is formed: crude protein 55-68%, crude fat 14-22%, phosphatidase 13-5%, ash 5-15%, n-3HUFA2-4%, DHA 1-2%, EPA 0.6-1%, moisture 3-9%.Common DHA/EPA=1～3.
Grouper son of the present invention, production method young, juvenile fish enriched nutritive micro-granulated feed are: count ratio earlier by weight with 60～80 parts of protein sources raw materials. 0.5～5 part of 14～24 parts of fat source raw materials and immunopotentiator, one reinstates protease (vigor is 50-100 ten thousand units) 50～70 ℃ of constant temperature enzymolysis after 1-5 hour in Cooling or heating jar that account for gross weight 0.1～1%, add the antioxidant that accounts for gross weight 0.5-3% again, filter hydrolyzate, in Highspeedcentrifugingandsprayingdrier, carry out spray-drying then and promptly obtain required micro-granulated feed; Spray-dired shower nozzle rotating speed is 8000-22000r/min (being generally 12000-20000r/min), and inlet temperature is 150～221 ℃ (being generally 200～211 ℃), and outlet temperature is 90～107 ℃ (being generally 100～103 ℃).
Described protein sources raw material can be selected from mussel meat, spirulina powder, egg, cuttlefish meat, in the animal protein raw materials such as red worm one or more: the fat source raw material can be selected from cod-liver oil, the crude mixture of DHA and EPA, cuttlefish liver oil, soybean lecithin, egg lecithin, in the fish-egg lecithin one or more: antioxidant can be selected from vitamin E, vitamin C phosphoric ester, in the ethoxyquinoline one or more: immunopotentiator can be that poly-polysaccharide is or/and Vit C.
Described protease can be trypsase or/and papain.
The nutritional labeling index of micro-granulated feed of the present invention and feed proterties are respectively as shown in Table 1 and Table 2.
Table 1. nutritional labeling index (w/w) table 2. micro-granulated feed proterties
| Moisture | ?3-9％ |
| Crude protein | ?55-68％ |
| Crude fat | ?14-22％ |
| Phosphatide | ?3-5％ |
| Ash | ?5-15％ |
| n-3HUFA | ?2-4％ |
| DHA/EPA | ?1-3 |
| DHA | ?1-2％ |
| EPA | ?0.6-1％ |
| Deliberated index | Evaluation result |
| Particle diameter | Diameter 0.1～0.5um's is main |
| Volume weight (g/ml) | On average be about 0.64g/ml (the heavy 12.81g of feed in the 20ml volume) |
| Palatability (taste) | Cake fragrance is arranged when dry, |
| Sinking speed | 10mm/s (decline 12cm needs 2 minutes highly approximately) |
| Water-resistance | Feed in 12 hours more than 90% is insoluble to loose |
| Dilatancy | (1.1/1 becoming 0.44um behind the 0.40um feed suction 12h during drying) |
| Dispersed | Can scatter well in that the water surface is very fast when the few and material of the amount of throwing is dry |
| Cause the rotten time | The shortest time of ammonia nitrogen＞0.25mg/l is about 48 hours |
The present invention is according to the formulated of uniqueness and grouper son, young, the juvenile fish microparticle mixed feed that adopts spray drying process to obtain, show through raising experiment and can be successfully partly to substitute biological feed, solved the bottleneck of current biological feed supply wretched insufficiency, the grouper breed has been had great importance and higher economic value.
The present invention has as advantage grouper son, enriched nutritive micro-granulated feed young, that juvenile fish provides:
1. show that from the feed nutrient analysis result protein content is higher, ash is low, and more seminase hydrolysis products such as small peptide etc. are arranged, and meets the demand of grouper son, young, juvenile fish nutrition substantially.
2. the physical behavior measurement result shows that it has the time of staying preferably at the water surface, and granular size has a wider gradient, with the bore in each stage of grouper anastomose property is preferably arranged, and can solve the size issue that begins to ingest; The color aspect also biology commonly used with marine is close, and orange and salmon pink has food calling effect preferably; It is longer to cause the rotten time, and the water pollution that is caused in having the cultivating system of flowing water will be littler; Sinking speed is also slower.
3. the raising experiment result through prelarva shows, partly substitutes biological feed with micro-granulated feed of the present invention and has good effect, and be fully feasible.
Feed of the present invention also is suitable for porgy section seawater fishes such as porgy, lefteye flounder, and the training seedling of aquatic/marine animals such as seawater shrimps uses.
The specific embodiment
Embodiment one: proportionally mussel meat (100kg), egg lecithin (8kg), cod oil (10kg), 50% vitamin E (1kg), vitamin C (0.5kg) earlier with papain (vigor is 1,000,000 units) 70～72 ℃ of constant temperature enzymolysis after 3 hours in Cooling or heating jar, add ethoxyquinoline 100 grams, filter hydrolyzate, be evacuated to and carry out spray-drying in the QZR-150 type Highspeedcentrifugingandsprayingdrier and obtain a kind of micro-granulated feed (proterties as table), shower nozzle rotating speed: 15000r/min inlet temperature: 200～211 ℃ of outlet temperatures: 100～103 ℃.Through raising the grouper fry, growth and survival rate and the wheel animalcule of throwing something and feeding, halogen worm do not have significant difference, have reached the better effects that partly substitutes biological feed.
Embodiment two: proportionally cuttlefish meat (100kg), soybean lecithin (8kg), cod oil (10kg), 50% vitamin E (1kg), vitamin C (0.5kg), spirulina powder (1kg) is earlier with trypsase (vigor is 500,000 units) 60～62 ℃ of constant temperature enzymolysis after 3 hours in Cooling or heating jar, add ethoxyquinoline 100 grams, filter hydrolyzate, be evacuated to and carry out spray-drying in the QZR-150 type Highspeedcentrifugingandsprayingdrier and obtain a kind of micro-granulated feed (proterties as table), shower nozzle rotating speed: 18000r/min inlet temperature: 200～211 ℃ of outlet temperatures: 100～103 ℃.Through raising the grouper fry, growth and survival rate and the wheel animalcule of throwing something and feeding, halogen worm do not have significant difference, have reached the better effects that partly substitutes biological feed equally.
Claims (5)
1. a grouper son, young, juvenile fish enriched nutritive micro-granulated feed, it is characterized in that the microparticle of this micro-granulated feed based on particle diameter 100～1000um, the nutritional labeling of feed is formed: crude protein 55-68%, crude fat 14-22%, phosphatidase 13-5%, ash 5-15%, n-3HUFA 2-4%, DHA 1-2%, EPA 0.6-1%, moisture 3-9%.
2. the production method of the described micro-granulated feed of claim 1, it is characterized in that comparing protein sources raw material 60～80 by dry matter weight earlier, fat source raw material 14～24 and immunopotentiator 0.5～5, one reinstates the protease that accounts for gross weight 0.1～1%, vigor is 50～1,000,000 units, at 50～70 ℃ of constant temperature enzymolysis of Cooling or heating jar after 1-5 hour, add the antioxidant that accounts for gross weight 0.5-3% again, filter hydrolyzate, in Highspeedcentrifugingandsprayingdrier, carry out spray-drying then and promptly obtain required micro-granulated feed; Spray-dired shower nozzle rotating speed is 8000-22000r/min, and inlet temperature is 150～221 ℃, and outlet temperature is 90～107 ℃.
3. in accordance with the method for claim 2, it is characterized in that described protein sources raw material is selected from one or more in mussel meat, spirulina powder, egg, cuttlefish meat, the red worm; The fat source raw material is selected from one or more in the crude mixture, cuttlefish liver oil, soybean lecithin, egg lecithin, fish-egg lecithin of cod-liver oil, DHA and EPA; Antioxidant is selected from one or more in vitamin E, vitamin C phosphoric ester, the ethoxyquinoline; Immunopotentiator is for gathering polysaccharide or/and Vit C.
4. in accordance with the method for claim 2, it is characterized in that used protease is that trypsase is or/and papain.
5. in accordance with the method for claim 2, it is characterized in that described spray-dired shower nozzle rotating speed is 12000-20000r/min, inlet temperature is 200～211 ℃, and outlet temperature is 100～103 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB031141765A CN1212075C (en) | 2003-04-10 | 2003-04-10 | Micro particle feed for rockfish fry and its production procss |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB031141765A CN1212075C (en) | 2003-04-10 | 2003-04-10 | Micro particle feed for rockfish fry and its production procss |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1442078A CN1442078A (en) | 2003-09-17 |
| CN1212075C true CN1212075C (en) | 2005-07-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB031141765A Expired - Fee Related CN1212075C (en) | 2003-04-10 | 2003-04-10 | Micro particle feed for rockfish fry and its production procss |
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Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101803673B (en) * | 2010-04-22 | 2012-09-26 | 广东恒兴饲料实业股份有限公司 | Grouper compound feed and preparation method thereof |
| CN101953437B (en) * | 2010-09-15 | 2012-06-13 | 福建省水产研究所 | Compound feed for grouper larvae and juveniles and preparation method thereof |
| CN103005183B (en) * | 2012-11-30 | 2014-04-16 | 中山大学 | Perfect compound feed for groupers |
| CN103478497B (en) * | 2013-10-10 | 2015-02-11 | 山东升索渔用饲料研究中心 | Sea fish mixed feed for deepwater net cage culture and manufacturing method thereof |
| CN104322914B (en) * | 2014-09-26 | 2016-09-21 | 浙江海洋学院 | A kind of star column nutritional solution |
| CN104543455A (en) * | 2014-12-12 | 2015-04-29 | 青岛无为保温材料有限公司 | Compound feed for grouper and preparation method |
| CN104509753A (en) * | 2015-01-16 | 2015-04-15 | 上海农好饲料有限公司 | Microparticle feed for grouper fries and preparation method for microparticle feed |
| CN104757326A (en) * | 2015-04-17 | 2015-07-08 | 天津市英创技术有限公司 | Aquatic larva microcapsule bait and production method thereof |
| CN106071400A (en) * | 2016-06-22 | 2016-11-09 | 卢映辰 | Crucian carp feed |
| CN105994958A (en) * | 2016-06-22 | 2016-10-12 | 卢映辰 | Parabramis pekinensis feed |
| CN108094693A (en) * | 2017-12-29 | 2018-06-01 | 福建省淡水水产研究所 | A kind of grouper larvae micro-encapsulated diet and preparation method thereof |
| CN114271406B (en) * | 2021-12-08 | 2023-11-14 | 华中农业大学 | Micro-pellet feed formula for domestication of micropterus salmoides offspring seeds and application thereof |
-
2003
- 2003-04-10 CN CNB031141765A patent/CN1212075C/en not_active Expired - Fee Related
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| CN1442078A (en) | 2003-09-17 |
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Assignee: Qingyuan Haibei Biological Technology Co., Ltd. Assignor: Sun Yat-sen University Contract record no.: 2010440001529 Denomination of invention: Micro particle feed for rockfish fry and its production procss Granted publication date: 20050727 License type: Exclusive License Open date: 20030917 Record date: 20101221 |
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