CN117187014A - Tricholoma matsutake wine rich in organic germanium and preparation method thereof - Google Patents
Tricholoma matsutake wine rich in organic germanium and preparation method thereof Download PDFInfo
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses an organic germanium-rich tricholoma matsutake wine and a preparation method thereof, and particularly relates to the field of preparation of medicinal liquor. The method comprises the steps of raw material treatment, soaking, mixing and blending. The product of the invention mainly utilizes precious traditional Chinese medicinal materials in northeast, is helpful for the national health industry, and improves social and economic benefits. The tricholoma matsutake wine disclosed by the invention is rich in organic germanium, so that the tricholoma matsutake wine not only has the functions of medicinal and edible raw materials, but also has the effects of enhancing the immunity of a human body, delaying senescence and the like.
Description
Technical Field
The invention relates to the field of preparation of medicinal liquor, in particular to an organic germanium-rich tricholoma matsutake wine and a preparation method thereof.
Background
With the development of the age, the life and work rhythm of people are gradually accelerated; the environmental pollution is increased, and the food sanitation is bad; leading to poorer physical condition and immunity of people and more cancer patients. Therefore, how to improve the immunity of human bodies has become a general concern. The method for resisting cancer and improving the immunity of human bodies through a diet therapy method is effective, and meanwhile, the method does not cause burden to the human bodies. Proper amount of medicated wine is widely accepted by people in dietary therapy. The medicinal liquor is clear liquid prepared by soaking and extracting the medicaments with white spirit. Because wine has the characteristics of promoting blood circulation, being easy to absorb and increasing the efficacy, the medicinal wine is more and more valued by people; the health care medicinal liquor in the current market has various types, and the medicinal liquor capable of achieving the functions of resisting cancer and improving the immunity of human bodies only comprises tricholoma matsutake and pine needle wine, and the tricholoma matsutake wine has better anticancer effect. However, the prior tricholoma matsutake wine in the market can not exert the best drug effect due to the problem of the formula, thereby greatly reducing the effects of resisting cancer and improving the immunity of human bodies. How to make the tricholoma matsutake exert the best efficacy, and make the prepared tricholoma matsutake wine achieve better anticancer and immunity improving effects, is a technical problem which needs to be solved by the technicians in the field.
The wine soaking is prepared from different raw materials and has different health care functions. The wine has the health care effects, firstly, the wine has a certain function, more importantly, the wine is a good organic solvent and has better penetrability, the effect can enable the wine to easily enter into food tissue cells, so that a plurality of insoluble active ingredients in food can be dissolved out, and the wine is drunk and simultaneously the body is built.
However, the mixed raw materials are soaked in disorder, so that the respective effects of the raw materials are affected, and the effect of soaking out the soaked matter is reduced.
Disclosure of Invention
Therefore, the invention provides the pine mushroom wine rich in organic germanium and the preparation method thereof, so as to solve the problem of low effect of the existing soaked wine.
In order to achieve the above object, the present invention provides the following technical solutions:
according to one aspect of the invention, a preparation method of the pine mushroom wine rich in organic germanium comprises the following steps:
step one, processing and soaking raw materials
Respectively pretreating Ginseng radix, ganoderma, fructus Lycii and Tricholoma matsutake to obtain pretreated Ginseng radix, pretreated Ganoderma, pretreated fructus Lycii and pretreated Tricholoma matsutake; soaking pretreated Ginseng radix, pretreated Ganoderma, pretreated fructus Lycii and pretreated Tricholoma matsutake with Kaoliang spirit respectively; obtaining ginseng extract, ganoderma extract, medlar extract and tricholoma matsutake extract, concentrating the extracts respectively to obtain ginseng liquid, ganoderma liquid, medlar liquid and tricholoma matsutake liquid;
step two, mixing
Mixing Ginseng radix solution, ganoderma solution, fructus Lycii solution and Tricholoma matsutake solution, adding high-alcohol Chinese liquor, soaking for the second time, and filtering to obtain initial liquor;
step three, blending
Adding Mel and organic germanium water solution into the initial liquor, mixing, and filtering for the second time to obtain Tricholoma matsutake liquor rich in organic germanium.
Further, in the first step, the ginseng pretreatment includes drying the ginseng until the water content is not more than 5%, and pulverizing the ginseng until the mesh number is not more than 300 mesh.
In the first step, the ganoderma lucidum pretreatment comprises the steps of drying ganoderma lucidum, and then breaking the wall to ensure that the wall breaking rate of ganoderma lucidum spore powder is more than 99%.
In the first step, the pretreatment of the medlar and the pretreatment of the tricholoma matsutake comprise respectively freeze-drying the medlar and the tricholoma matsutake, and then crushing the medlar and the tricholoma matsutake, wherein the mesh number is not more than 300 meshes.
Further, in the first step, the pretreated ginseng, the pretreated ganoderma lucidum, the pretreated matrimony vine and the pretreated matsutake are respectively soaked and soaked to obtain the sorghum liquor with the concentration of 32% vol white liquor, and the usage amount of 5 per mill, 7.5 per mill, 15 per mill and 7.5 per mill of the 32% vol white liquor respectively.
Further, in the second step, the time for soaking for the second time is not less than 15 days.
Further, in the second step, the number of the filtered meshes is 120 meshes.
Further, in the third step, the adding amount of the honey is 5-15 per mill based on 32% vol white spirit; the addition amount of the organic germanium is 5 per mill based on 32 percent volume of white spirit.
Further, in the third step, the pore size of the secondary filtration membrane is 0.65. Mu.m.
According to another aspect of the present invention, there is provided an organic germanium-rich matsutake wine comprising ginseng, ganoderma lucidum, wolfberry, matsutake, honey and organic germanium.
Ginseng: the name of the traditional Chinese medicine. Is root of Panax ginseng C.A.Mey. Has effects of invigorating primordial qi, invigorating spleen, benefiting lung, promoting salivation, tranquilizing mind, and improving intelligence. Is mainly used for treating qi deficiency, hypofunction of pulse, spleen qi deficiency, sinking of middle-jiao qi, lung deficiency, asthma and cough, short breath and hypodynamia, body fluid deficiency and thirst, deficiency heat and thirst, insomnia and amnesia, palpitation, blood deficiency and sallow complexion, impotence and cold womb, etc.
Ganoderma lucidum: ganoderma lucidum and Chinese medicine. Is a dried fruiting body of Ganoderma lucidum Ganoderma lucidum (Leys. Ex Fr.) Karst or Ganoderma sinense Ganoderma sinense Zhao, xu et Zhang belonging to Polyporaceae genus Ganoderma. Has effects of invigorating qi, tranquilizing mind, relieving cough and asthma. It is mainly used for treating restlessness, insomnia, palpitation, cough, asthma, excessive phlegm, and consumptive disease.
Medlar: wolfberry fruit and Chinese medicine. Is mature fruit of Lycium barbarum L. Has effects of nourishing liver and kidney, and replenishing vital essence. It is indicated for deficiency of liver-yin and kidney-yin and premature senility.
Pine mushroom: the tricholoma matsutake has high nutritive value and medicinal value. Modern medicine shows that tricholoma matsutake has various effects of improving immunity, resisting cancer and tumor, treating diabetes and cardiovascular diseases, resisting aging and beautifying, promoting intestines and stomach and protecting liver, etc., so the tricholoma matsutake is widely used for developing medicines, health care products and cosmetics in the global scope.
Honey: the honey has effects of invigorating spleen and stomach, moistening dryness, relieving pain, removing toxic substances, relieving cough, promoting granulation and healing sore. Sweet honey and flat; enter spleen, stomach, lung and large intestine meridians. The honey contains various inorganic salts and vitamins, iron, calcium, copper, manganese, potassium, phosphorus and other organic acids with the concentration similar to that of human serum, and microelements beneficial to human health, and fructose, glucose, amylase, oxidase, reductase and the like, and has the effects of nourishing, moistening dryness, detoxifying, whitening, beautifying, relaxing bowel.
Organic germanium: organic germanium is an element required by the human body and has multiple functions. Because it has the function of dehydrogenation and oxygen enrichment, can keep sufficient oxygen, thereby maintaining human health. In the human body, the decomposition of food is performed by means of oxygen, and a large amount of oxygen is consumed during the decomposition of food, while water and carbon dioxide are produced. If there is insufficient oxygen, it is possible to cause various diseases to the body. The organic germanium can bring hydrogen ions in a human body out of the body, so that the oxygen demand of the body is reduced, and the health is facilitated.
After the organic germanium enters the human body, the organic germanium can be uniformly distributed in each organ tissue and completely discharged out of the body after 24 hours, belongs to trace elements which cannot be accumulated in the body, and has extremely low toxicity and no side effect. The cells of each organ of the human body generate waste in the life process, one part of the waste is discharged out of the body through a secretion system, and the other part of the waste exists in each organ in the form of free radicals to form lesions, so that the organ functions are reduced to affect the health, and the organic germanium can be discharged out of the body after being combined with the free radicals, thereby enhancing the life of the organ.
Clinical studies have found that the HAPPY organic germanium which is widely accepted at present has good therapeutic effect on various diseases. The main appearance is that: anti-tumor, immunity enhancing, antiaging, arteriosclerosis preventing, blood viscosity reducing, rheumatoid arthritis resisting, endocrine regulating, analgesic, antiinflammatory, blood pressure lowering, osteoporosis treating, endocrine regulating, and chronic hepatitis treating effects.
The organic germanium is used for functional health care foods, medicines, beauty cosmetics and the like, and the functions of the organic germanium are stated to have physiological functions of enhancing human immunity, regulating blood pressure, blood fat, blood sugar and the like, widely treating cancers, preventing and treating various diseases and body building, obvious anti-aging effects, whitening and beautifying effects, treating rheumatoid arthritis, treating chronic hepatitis, treating osteoporosis and the like, and in 1922, doctors in the United states begin to treat anemia by using the inorganic germanium. Inorganic germanium has also been used for other treatments, but the efficacy is questionable. Its efficacy against cancer has been discussed. The U.S. food and drug administration has concluded that germanium is "potentially harmful" to human health when used as a dietary supplement.
The invention has the following advantages:
the product of the invention mainly utilizes precious traditional Chinese medicinal materials in northeast, is helpful for the national health industry, and improves social and economic benefits.
The tricholoma matsutake wine disclosed by the invention is rich in organic germanium, so that the tricholoma matsutake wine not only has the functions of medicinal and edible raw materials, but also has the effects of enhancing the immunity of a human body, delaying senescence and the like.
Detailed Description
Other advantages and advantages of the present invention will become apparent to those skilled in the art from the following detailed description, which, by way of illustration, is to be read in connection with certain specific embodiments, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Drying is one of the methods of keeping the material from spoilage. Many drying methods, such as sun drying, boiling drying, spray drying, vacuum drying and the like, are carried out at higher temperatures, and the dried product usually has reduced volume, hardened texture, oxidation of some substances, loss of some volatile components, denaturation of some heat-sensitive substances such as proteins, vitamins and the like, loss of biological activity of microorganisms, difficult dissolution of the dried substances in water and the like, so that the dried product has a great difference in properties from the product before drying. Freeze-drying is a technique of drying by using the principle of sublimation, in which a substance containing a large amount of water is quickly frozen at a low temperature, and then the frozen water molecules are sublimated directly into water vapor under a proper vacuum environment to escape. The material to be dried is always in a low temperature (frozen state) after pretreatment before freeze-drying, ice crystals are uniformly distributed in the material, namely, the material is left in an ice frame during freezing, the concentration phenomenon caused by dehydration in the sublimation process can not occur, the volume of the material after freeze-drying is unchanged, and the side effects of foam, oxidation and the like generated by water vapor are avoided.
The protein, the microorganism and the like of the freeze-dried substance cannot be denatured or lose biological activity, and in the freeze-drying process, the growth of the microorganism and the action of enzyme cannot be performed, so that the original property of the freeze-dried substance can be kept, the volume of the freeze-dried substance is almost unchanged, the original structure is kept, and the concentration phenomenon cannot occur; the freeze-dried material is loose and porous, is spongy, and can be dissolved quickly and completely after being added with water, and can be restored to original property almost immediately, and because the drying is carried out under vacuum, the oxygen is very little, and some easily-oxidized substances are protected, and the drying can remove more than 95-99% of water, so that the dried product can be stored for a long time without deterioration. The invention carries out freeze drying treatment on the raw materials of tricholoma matsutake, medlar and jujube, the freeze-dried tricholoma matsutake, the freeze-dried medlar and the freeze-dried jujube are in a dry sponge porous shape, the shape is basically unchanged, the shelf life is long, the rehydration is good, and the characteristics of good color, aroma and taste nutrition components are provided, so that the change of physicochemical and biological characteristics of freeze-dried substances is prevented to the greatest extent. The freeze-dried substance and high-alcohol sorghum liquor are prepared into the sparkling wine, and the sparkling wine has the health-care effects of strengthening body, activating blood, benefiting intestines and stomach, relieving pain, regulating qi, resolving phlegm, expelling parasites, resisting cancer, enhancing immunity and the like, and the medlar, the Chinese date and the rock sugar can also play a role in regulating the mouthfeel of the freeze-dried tricholoma matsutake sparkling wine.
Example 1
The embodiment provides a preparation method of an organic germanium-rich tricholoma matsutake wine, which comprises the following steps:
step one: preprocessing the ginseng: drying Ginseng radix until the water content is not more than 5%, pulverizing, and sieving with 300 mesh sieve;
pretreatment of ganoderma lucidum: drying Ganoderma, and breaking cell wall to obtain Ganoderma spore powder with cell wall breaking rate greater than 99%;
pretreatment of medlar and pretreatment of matsutake: freeze-drying fructus Lycii and Tricholoma matsutake respectively, and pulverizing to obtain powder with mesh number not greater than 300;
soaking pretreated Ginseng radix, pretreated Ganoderma, pretreated fructus Lycii and pretreated Tricholoma matsutake with 32% vol Kaoliang spirit respectively; obtaining ginseng extract, ganoderma extract, medlar extract and tricholoma matsutake extract, concentrating the extracts respectively to obtain ginseng liquid, ganoderma liquid, medlar liquid and tricholoma matsutake liquid;
wherein, the concentration of the sorghum liquor obtained by respectively soaking and soaking the pretreated ginseng, the pretreated ganoderma lucidum, the pretreated medlar and the pretreated matsutake is 32 percent vol white liquor, and the use amount is 5 per mill, 7.5 per mill, 15 per mill and 7.5 per mill of the 32 percent vol white liquor;
step two, mixing
Mixing Ginseng radix solution, ganoderma solution, fructus Lycii solution and Tricholoma matsutake solution, adding high-alcohol Chinese liquor, soaking for 15 days, and filtering with 120 mesh sieve to obtain initial liquor;
step three, blending
Adding Mel and organic germanium water solution into the initial liquor, mixing, and filtering with 0.65 μm filter membrane for the second time to obtain Tricholoma matsutake liquor rich in organic germanium;
wherein the adding amount of the honey is 5 per mill according to the volume of 32 percent of white spirit; the addition amount of the organic germanium is 5 per mill based on 32 percent volume of white spirit.
Example 2
The embodiment provides a preparation method of an organic germanium-rich tricholoma matsutake wine, which comprises the following steps:
step one: preprocessing the ginseng: drying Ginseng radix until the water content is not more than 5%, pulverizing, and sieving with 300 mesh sieve;
pretreatment of ganoderma lucidum: drying Ganoderma, and breaking cell wall to obtain Ganoderma spore powder with cell wall breaking rate greater than 99%;
pretreatment of medlar and pretreatment of matsutake: freeze-drying fructus Lycii and Tricholoma matsutake respectively, and pulverizing to obtain powder with mesh number not greater than 300;
soaking pretreated Ginseng radix, pretreated Ganoderma, pretreated fructus Lycii and pretreated Tricholoma matsutake with 32% vol Kaoliang spirit respectively; obtaining ginseng extract, ganoderma extract, medlar extract and tricholoma matsutake extract, concentrating the extracts respectively to obtain ginseng liquid, ganoderma liquid, medlar liquid and tricholoma matsutake liquid;
wherein, the concentration of the sorghum liquor obtained by respectively soaking and soaking the pretreated ginseng, the pretreated ganoderma lucidum, the pretreated medlar and the pretreated matsutake is 32 percent vol white liquor, and the use amount is 5 per mill, 7.5 per mill, 15 per mill and 7.5 per mill of the 32 percent vol white liquor;
step two, mixing
Mixing Ginseng radix solution, ganoderma solution, fructus Lycii solution and Tricholoma matsutake solution, adding high-alcohol Chinese liquor, soaking for 15 days, and filtering with 120 mesh sieve to obtain initial liquor;
step three, blending
Adding Mel and organic germanium water solution into the initial liquor, mixing, and filtering with 0.65 μm filter membrane for the second time to obtain Tricholoma matsutake liquor rich in organic germanium;
wherein the adding amount of the honey is 10 per mill according to the volume of 32 percent of white spirit; the addition amount of the organic germanium is 5 per mill based on 32 percent volume of white spirit.
Example 3
The embodiment provides a preparation method of an organic germanium-rich tricholoma matsutake wine, which comprises the following steps:
step one: preprocessing the ginseng: drying Ginseng radix until the water content is not more than 5%, pulverizing, and sieving with 300 mesh sieve;
pretreatment of ganoderma lucidum: drying Ganoderma, and breaking cell wall to obtain Ganoderma spore powder with cell wall breaking rate greater than 99%;
pretreatment of medlar and pretreatment of matsutake: freeze-drying fructus Lycii and Tricholoma matsutake respectively, and pulverizing to obtain powder with mesh number not greater than 300;
soaking pretreated Ginseng radix, pretreated Ganoderma, pretreated fructus Lycii and pretreated Tricholoma matsutake with 32% vol Kaoliang spirit respectively; obtaining ginseng extract, ganoderma extract, medlar extract and tricholoma matsutake extract, concentrating the extracts respectively to obtain ginseng liquid, ganoderma liquid, medlar liquid and tricholoma matsutake liquid;
wherein, the concentration of the sorghum liquor obtained by respectively soaking and soaking the pretreated ginseng, the pretreated ganoderma lucidum, the pretreated medlar and the pretreated matsutake is 32 percent vol white liquor, and the use amount is 5 per mill, 7.5 per mill, 15 per mill and 7.5 per mill of the 32 percent vol white liquor;
step two, mixing
Mixing Ginseng radix solution, ganoderma solution, fructus Lycii solution and Tricholoma matsutake solution, adding high-alcohol Chinese liquor, soaking for 15 days, and filtering with 120 mesh sieve to obtain initial liquor;
step three, blending
Adding Mel and organic germanium water solution into the initial liquor, mixing, and filtering with 0.65 μm filter membrane for the second time to obtain Tricholoma matsutake liquor rich in organic germanium;
wherein the adding amount of the honey is 15 per mill based on 32 percent of volume white spirit; the addition amount of the organic germanium is 5 per mill based on 32 percent volume of white spirit.
Step four, packaging
And (3) packaging the obtained pine mushroom wine rich in organic germanium after the pine mushroom wine is qualified by inspection, and warehousing and storing after 500 ml/bottle of pine mushroom wine is qualified by spot inspection.
100 cases of clinical experiments prove that the tricholoma matsutake wine prepared in the embodiment 1 of the invention has the obvious effect of assisting in treating cancers up to 95%, and has the advantages of obvious effect, safe and reliable use and no toxic or side effect.
Case 1: gastric cancer patient: king x, male, 30 years old, hospital diagnosis: the pine mushroom wine prepared by the method of the example 1 is drunk for early gastric cancer every day, 50ml of auxiliary anticancer drugs are drunk for each time in the morning and evening, and cancer cells are not further spread after 1 year.
Case 2: breast cancer patients, wang×,52 years old, women. The hospital diagnosis is as follows: the pine mushroom wine prepared by the method of example 1 is drunk once a day, 50ml of the pine mushroom wine is drunk once a day, and after 3 years, the auxiliary anticancer medicine is used, so that cancer cells are not further spread.
Case 3: gastric cancer patients, liu, female, 55 years old, were diagnosed by the hospital: the pine mushroom wine prepared by the method of the example 1 is drunk every day for gastric cancer in the middle period, 50ml of the pine mushroom wine is drunk every morning and evening, 1 year of auxiliary anticancer drugs are drunk until now, and the diffusion speed of cancer cells is slowed down.
Case 4: liver cancer patients, zhao, male, 62 years old, hospital diagnosed: lung cancer in the middle stage. The pine mushroom wine prepared by the method of the example 1 is drunk every day, 50ml of the pine mushroom wine is drunk every morning and evening, the auxiliary anticancer medicine is drunk for half a year so far, the diffusion speed of cancer cells is slowed down, and the pain of patients is obviously slowed down.
The tricholoma matsutake wine aims at enhancing immunity: the medicinal liquor of the invention has 100 experiments, wherein 90 effective cases account for 90%, 11 effective cases account for 10%, and the total effective rate is 100%. No adverse reaction was found.
While the invention has been described in detail in the foregoing general description and specific examples, it will be apparent to those skilled in the art that modifications and improvements can be made thereto. Accordingly, such modifications or improvements may be made without departing from the spirit of the invention and are intended to be within the scope of the invention as claimed.
Claims (10)
1. A preparation method of an organic germanium-rich tricholoma matsutake wine is characterized by comprising the following steps:
step one, processing and soaking raw materials
Respectively pretreating Ginseng radix, ganoderma, fructus Lycii and Tricholoma matsutake to obtain pretreated Ginseng radix, pretreated Ganoderma, pretreated fructus Lycii and pretreated Tricholoma matsutake; soaking pretreated Ginseng radix, pretreated Ganoderma, pretreated fructus Lycii and pretreated Tricholoma matsutake with Kaoliang spirit respectively;
obtaining ginseng extract, ganoderma extract, medlar extract and tricholoma matsutake extract, concentrating the extracts respectively to obtain ginseng liquid, ganoderma liquid, medlar liquid and tricholoma matsutake liquid;
step two, mixing
Mixing Ginseng radix solution, ganoderma solution, fructus Lycii solution and Tricholoma matsutake solution, adding high-alcohol Chinese liquor, soaking for the second time, and filtering to obtain initial liquor;
step three, blending
Adding Mel and organic germanium water solution into the initial liquor, mixing, and filtering for the second time to obtain Tricholoma matsutake liquor rich in organic germanium.
2. The method of claim 1, wherein the ginseng pretreatment comprises drying the ginseng until the moisture content is not more than 5%, and pulverizing the ginseng until the mesh size is not more than 300 mesh.
3. The method for preparing the pine mushroom wine rich in organic germanium according to claim 1, wherein in the first step, the ganoderma lucidum pretreatment comprises the steps of drying ganoderma lucidum, and then breaking the wall to ensure that the wall breaking rate of ganoderma lucidum spore powder is more than 99%.
4. The method for preparing an organic germanium-rich tricholoma matsutake wine according to claim 1, wherein in the first step, the pretreatment of the wolfberry fruit and the pretreatment of the tricholoma matsutake comprise freeze-drying the wolfberry fruit and the tricholoma matsutake respectively, and pulverizing the wolfberry fruit and the tricholoma matsutake respectively, wherein the mesh size is not more than 300 meshes.
5. The method of claim 1, wherein the concentration of the sorghum liquor obtained by soaking the pretreated ginseng, the pretreated ganoderma lucidum, the pretreated wolfberry fruit and the pretreated pine mushroom in the first step is 32% vol white spirit, and the usage amounts are 5 per mill, 7.5 per mill, 15 per mill and 7.5 per mill of the 32% vol white spirit respectively.
6. The method for preparing an organogermanium enriched matsutake wine according to claim 1, wherein in said step two, the time of the second soaking is not less than 15 days.
7. The method for preparing an organogermanium enriched matsutake wine according to claim 1, wherein in said step two, the mesh size of the filtration is 120 mesh.
8. The method for preparing the pine mushroom wine rich in organic germanium according to claim 1, wherein in the third step, the adding amount of the honey is 5-15 per mill based on 32% vol white spirit; the addition amount of the organic germanium is 5 per mill based on 32 percent volume of white spirit.
9. The method for preparing an organogermanium enriched matsutake wine according to claim 1, wherein in said step three, the pore size of the secondary filtration membrane is 0.65. Mu.m.
10. An organic germanium-rich tricholoma matsutake wine is characterized by comprising ginseng, ganoderma lucidum, medlar, tricholoma matsutake, honey and organic germanium.
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