CN116650347B

CN116650347B - Anti-wrinkle essential oil facial mask containing pink microalgae and spilanthol and preparation method thereof

Info

Publication number: CN116650347B
Application number: CN202310735156.3A
Authority: CN
Inventors: 周威; 毛建林
Original assignee: Campari Science & Technology Suzhou Co ltd
Current assignee: Campari Science & Technology Suzhou Co ltd
Priority date: 2023-06-20
Filing date: 2023-06-20
Publication date: 2023-12-01
Anticipated expiration: 2043-06-20
Also published as: CN116650347A

Abstract

The application relates to the field of skin care products, and particularly discloses an anti-wrinkle essential oil facial mask containing pink microalgae and spilanthol and a preparation method thereof. The anti-wrinkle essential oil mask comprises the following raw materials in percentage by weight: 25-30% of caprylic/capric triglyceride, 10-15% of jojoba seed oil, 5-10% of glycerol, 1-5% of sucrose laurate, 1-5% of sucrose stearate, 2-6% of cytoprotective agent, 2-4% of skin relaxing agent, 1-3% of anti-inflammatory agent, 1-2% of bergamot fruit oil, 1-2% of lime peel oil, 1-2% of grapefruit peel oil, 5-8% of squalane, 0-2% of antioxidant, 0-1% of tocopherol, 0-1% of phenoxyethanol, 0-1% of caprylyl glycol, 0-5% of hyaluronic acid, 0-3% of betaine and the balance of water. The facial mask disclosed by the application has excellent effects of moisturizing, moistening, tightening skin and resisting wrinkle.

Description

Anti-wrinkle essential oil facial mask containing pink microalgae and spilanthol and preparation method thereof

Technical Field

The application relates to the field of skin care products, in particular to an anti-wrinkle essential oil facial mask containing pink microalgae and spilanthol and a preparation method thereof.

Background

Aging is an inevitable natural process of all organisms over time, including the degradation of various visceral functions of the organism, the most intuitive manifestation of which is skin aging. Skin aging refers to disorder of skin structural components, leading to skin protection against external stimulus and hyposecretion regulation of homeostasis in organism, and further leading to appearance phenomena such as wrinkle, sagging, color deposit, freckle, roughness, telangiectasia, etc.

At present, anti-aging products on the market mainly form a film on the surface of skin through contained film-forming substances, and reduce the pulling of muscle activities, thereby realizing the anti-wrinkle effect. However, the anti-aging product has short action time, does not solve the problem of the microstructure in the skin from the deep layer of the skin, has obvious defects and needs to be further improved.

Therefore, the anti-wrinkle essential oil mask provided by the application has long acting time, and can lighten fine lines, smooth skin and nourish skin.

Disclosure of Invention

In order to improve the wrinkle and roughness of skin, the application provides an anti-wrinkle essential oil facial mask containing pink microalgae and spilanthol and a preparation method thereof.

In a first aspect, the application provides an anti-wrinkle essential oil facial mask containing pink microalgae and spilanthol, which adopts the following technical scheme:

an anti-wrinkle essential oil mask containing pink microalgae and spilanthol is prepared from the following raw materials in percentage by weight: 25-30% of caprylic/capric triglyceride, 10-15% of jojoba seed oil, 5-10% of glycerol, 1-5% of sucrose laurate, 1-5% of sucrose stearate, 2-6% of cytoprotective agent, 2-4% of skin relaxing agent, 1-3% of anti-inflammatory agent, 1-2% of bergamot fruit oil, 1-2% of lime peel oil, 1-2% of grapefruit peel oil, 5-8% of squalane, 0-2% of antioxidant, 0-1% of tocopherol, 0-1% of phenoxyethanol, 0-1% of caprylyl glycol, 0-5% of hyaluronic acid, 0-3% of betaine and the balance of water.

By adopting the technical scheme, the texture of the caprylic/capric triglyceride is not greasy, the extensibility of the emulsion can be improved, and the effects of lubricating and softening skin are achieved; jojoba seed oil can improve the spreadability and ductility of emulsion, can penetrate into the deep layer of epidermis, and has excellent skin moisturizing effect; the glycerol can form a protective film on the surface of the skin to isolate the external air from the skin, so that the skin moisturizing effect is achieved; the anti-inflammatory agent can reduce the irritation of the emulsion to the skin, reduce the adverse effect of skin inflammation on the skin repair of the emulsion, and enable the emulsion to better exert the skin repair effect;

sucrose laurate has effects of softening skin and keeping moisture, and can help components in the emulsion to permeate into skin after skin is softened, so as to promote the emulsion to exert better effect; sucrose stearate has effects of repairing skin barrier, preventing skin dehydration, reducing skin surface dehydration, thereby enriching skin moisture, improving skin elasticity and plumpness, improving skin relaxation, and reducing skin wrinkles; the cell protectant can penetrate deep into the skin, repair damaged cells, protect intact cells, deeply condition the skin, and enable the skin to be full and elastic; the skin relaxing agent can promote the aged and contracted muscles and cells to relax, and promote the active ingredients in the emulsion to penetrate into the skin and be absorbed by the cells, so that the skin can be promoted to recover the original elasticity and collagen, and the effect of improving skin wrinkles is achieved;

the bergamot fruit oil has anti-inflammatory effect, can balance the acid and alkali values of skin, helps the formation of skin collagen, and has the effects of whitening and moisturizing; the lime peel oil has a moisturizing effect on skin, can balance the pH value of the skin, promote collagen formation, and can promote cells to produce hyaluronic acid, wherein the hyaluronic acid has a strong moisturizing effect, and can enable the skin to have elasticity, so that skin wrinkles can be relieved; the grapefruit peel oil can remove free radicals, has the effects of resisting aging, resisting oxidation and resisting inflammation, can promote cholesterol secretion, promote skin to keep soft, and can promote cells to produce hyaluronic acid so that skin is moist and elastic; the squalane has strong penetrating power, can be compatible with moisture and grease in skin, plays a role in protecting the skin, and can promote skin pores to open after the squalane is quickly penetrated into the skin, so that other components in the emulsion can be easily penetrated into deep layers of the skin, and the skin repairing effect is effectively exerted.

The skin is softened by utilizing sucrose laurate and sucrose stearate, aged and contracted skin cells are relaxed by utilizing a skin relaxing agent, cells are repaired and protected by utilizing a cell protecting agent, the skin acid and base numbers are balanced and hyaluronic acid production is promoted by utilizing bergamot fruit oil, lime fruit oil and grapefruit peel oil, meanwhile, the components are promoted to effectively permeate into the deep layer of the skin by utilizing squalane, and the components are cooperated with each other, so that the emulsion has the effects of permanently improving wrinkles and nourishing the skin.

Preferably, the cytoprotective agent is a mixture of Dunaliella salina extract and jojoba seed oil, and the weight ratio of the Dunaliella salina extract in the cytoprotective agent is 8-10%.

By adopting the technical scheme, the dunaliella salina extract is commonly called pink microalgae, after penetrating into the skin, the dunaliella salina extract can wrap cells, repair aged and damaged cells, protect intact cells, play roles in conditioning the skin and delaying aging, and the dunaliella salina seed oil can dissolve the dunaliella salina extract, so that the dunaliella salina extract can be uniformly mixed with other raw materials, and meanwhile, the dunaliella salina extract can be promoted to penetrate into the skin.

Preferably, the skin relaxing agent is a mixture of spilanthus altissima extract and caprylic/capric triglyceride, and the spilanthus altissima extract accounts for 3-5% of the skin relaxing agent.

By adopting the technical scheme, the spilanthus altissima extract is called spilanthus altissima essence in the field, can relax aged and contracted muscles and cells, and enables emulsion components to better permeate into skin and be absorbed by the cells, so that the skin can be promoted to recover elasticity, the effect of improving wrinkles is achieved, the spilanthus altissima extract can be dissolved by caprylic/capric triglyceride, and the spilanthus altissima extract is better mixed with other components.

Preferably, the anti-inflammatory agent is a mixture of caper fruit extract and octyl dodecanol myristate, and the weight ratio of the caper fruit extract in the anti-inflammatory agent is 30-50%.

By adopting the technical scheme, the caper fruit extract has excellent anti-inflammatory and analgesic effects, can effectively relieve the irritation of emulsion to skin inflammation, reduces the possibility that the skin is stimulated to block the emulsion component from penetrating into the skin, and ensures that the emulsion component can effectively penetrate into the deep layer of the skin and play a role.

Preferably, the antioxidant is a mixture of wild soybean oil, carrot root extract and beta-carotene, and the weight ratio of the carrot root extract to the beta-carotene in the antioxidant is 15-20%.

By adopting the technical scheme, the wild soybean oil has the effects of softening skin and moisturizing, and the carrot root extract has the effects of resisting oxidation, scavenging free radicals and resisting aging and wrinkling; beta-carotene can react irreversibly with oxygen-containing free radical, so as to reach the effect of scavenging free radical.

Preferably, the weight ratio of the cytoprotective agent, squalane and skin relaxant is 1:2:1.

by adopting the technical scheme, skin pores are opened by virtue of squalane, emulsion components are promoted to permeate into deep layers of skin, skin relaxing agents relax aged and contracted cells, the cells can be promoted to absorb the emulsion components, after the cytoprotective agents permeate into the skin, the aged cells can be repaired, and meanwhile, intact undamaged cells are protected and absorbed, and the effects of repairing the skin can be effectively exerted by compounding the three components according to a specific proportion, so that the skin wrinkles are effectively improved, and the skin is nourished.

Preferably, the composition further comprises 3-5% of hyaluronic acid, wherein the hyaluronic acid comprises the following components in percentage by weight of 1: small molecule hyaluronic acid and medium molecule hyaluronic acid of (2-3).

By adopting the technical scheme, the small molecular hyaluronic acid can permeate into dermal tissues of skin and slightly dilate capillaries, so that the absorption of emulsion components by the skin can be promoted, meanwhile, the small molecular hyaluronic acid has high hydrophilicity, and can keep moisture in the skin after penetrating into the skin, so that the skin can recover elasticity; the particles of the medium molecular hyaluronic acid are larger, the moisturizing effect is more durable, and after capillary expansion is promoted by the small molecular hyaluronic acid, the water molecules carried by the medium molecular hyaluronic acid contain emulsion active ingredients, so that the emulsion active ingredients carried by the medium molecular hyaluronic acid can be absorbed by skin more easily, further the emulsion active ingredients can exert better effects, the skin is promoted to recover elasticity, and wrinkles are improved.

Preferably, the weight ratio of the sum of the weights of the lime peel oil and the grapefruit peel oil to the hyaluronic acid is 1:2.

by adopting the technical scheme, the lime peel oil, the grapefruit peel oil and the hyaluronic acid are added according to a specific proportion, so that after the emulsion is absorbed by skin, the hyaluronic acid firstly plays a role in moisturizing and nourishing the skin, and along with the prolongation of time, the hyaluronic acid of which the lime peel oil and the grapefruit peel oil promote the secretion of cells also plays a role in moisturizing and tightening the skin, and the applicant finds that when the component proportion is adjusted to be the above, the emulsion can play the effects of improving skin wrinkles and nourishing the skin more permanently.

Preferably, the preparation method further comprises betaine, wherein the mass ratio of betaine to hyaluronic acid is 1: (1.5-2).

Through adopting above-mentioned technical scheme, betaine is as the zwitterion, and biocompatibility is high, and very easily dissolve in water, betaine easily carries water and easily releases water, use betaine and hyaluronic acid complex, betaine and hyaluronic acid all can carry the infiltration of hydrone inside the skin, other active ingredient of dissolving in the hydrone also permeate inside the skin along with betaine and hyaluronic acid simultaneously, when skin cell absorbs the hydrone, the hydrone releases the hydrone for cell absorption first, then hyaluronic acid releases the hydrone for cell absorption, thereby make skin cell can be continuous contain sufficient moisture, through the adjustment of proportion, and then make skin keep lasting wettability, and then can make skin resume elasticity and compactness.

In a second aspect, the application provides a preparation method of an anti-wrinkle essential oil mask containing pink microalgae and spilanthol, which adopts the following technical scheme:

a preparation method of an anti-wrinkle essential oil facial mask containing pink microalgae and spilanthol essence comprises the following steps:

mixing the raw materials according to the proportion to prepare the anti-wrinkle essential oil mask.

In summary, the application has the following beneficial effects:

1. the skin is softened by utilizing sucrose laurate and sucrose stearate, aged and contracted skin cells are relaxed by utilizing a skin relaxing agent, cells are repaired and protected by utilizing a cell protecting agent, the skin acid and base numbers are balanced and hyaluronic acid production is promoted by utilizing bergamot fruit oil, lime fruit oil and grapefruit peel oil, meanwhile, the components are promoted to effectively permeate into the deep layer of the skin by utilizing squalane, and the components are cooperated with each other, so that the emulsion has the effects of permanently improving wrinkles and nourishing the skin.

2. The application compounds the micromolecular hyaluronic acid and the medium-molecular hyaluronic acid, so that the skin can keep lasting wettability and recover elasticity.

3. The betaine and the hyaluronic acid are compounded, the betaine is used for supplying water molecules to skin cells in advance for absorption, and the hyaluronic acid is combined for further supplying water molecules for the skin cells to absorb, so that the skin can keep lasting wettability, and further the skin can recover elasticity and compactness.

Detailed Description

The present application will be described in further detail with reference to examples.

The raw materials in the present application are all commercially available. The molecular weight of the small molecular hyaluronic acid is 40-80 ten thousand daltons, the molecular weight of the medium molecular hyaluronic acid is 100-180 ten thousand daltons, and the small molecular hyaluronic acid of 40 ten thousand daltons and the medium molecular hyaluronic acid of 150 ten thousand daltons are selected in the embodiment of the application.

Examples

Example 1

An anti-wrinkle essential oil mask containing pink microalgae and spilanthol is prepared from the following raw materials in parts by weight: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 3.2 parts of cell protectant, 3.2 parts of skin relaxer, 1 part of anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime peel oil, 1 part of grapefruit peel oil, 8 parts of squalane and 32.6 parts of water.

Wherein the cytoprotective agent is a mixture of Dunaliella salina extract and jojoba seed oil, and the weight ratio of the Dunaliella salina extract in the cytoprotective agent is 8%; the skin relaxing agent is a mixture of spilanthus altissima extract and caprylic/capric triglyceride, and the spilanthus altissima extract accounts for 3% of the skin relaxing agent; the anti-inflammatory agent is a mixture of caper fruit extract and octyl dodecanol myristate, and the weight ratio of the caper fruit extract in the anti-inflammatory agent is 30%.

During preparation, the raw materials are uniformly mixed according to the proportion, and the anti-wrinkle essential oil mask is obtained.

Example 2

An anti-wrinkle essential oil mask containing pink microalgae and spilanthol is prepared from the following raw materials in parts by weight: 23 parts of caprylic/capric triglyceride, 15 parts of jojoba seed oil, 5 parts of glycerin, 5 parts of sucrose laurate, 5 parts of sucrose stearate, 4 parts of a cytoprotective agent, 3 parts of a skin relaxing agent, 2 parts of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane and 30 parts of water.

Wherein the cytoprotective agent is a mixture of Dunaliella salina extract and jojoba seed oil, and the weight ratio of the Dunaliella salina extract in the cytoprotective agent is 9%; the skin relaxing agent is a mixture of spilanthus altissima extract and caprylic/capric triglyceride, and the spilanthus altissima extract accounts for 4% of the skin relaxing agent; the anti-inflammatory agent is a mixture of caper fruit extract and octyl dodecanol myristate, and the weight ratio of the caper fruit extract in the anti-inflammatory agent is 40%.

Example 3

An anti-wrinkle essential oil mask containing pink microalgae and spilanthol is prepared from the following raw materials in parts by weight: 25 parts of caprylic/capric triglyceride, 10 parts of jojoba seed oil, 8 parts of glycerol, 1 part of sucrose laurate, 1 part of sucrose stearate, 6 parts of cytoprotective agent, 4 parts of skin relaxing agent, 3 parts of anti-inflammatory agent, 2 parts of bergamot fruit oil, 2 parts of lime peel oil, 2 parts of grapefruit peel oil, 7 parts of squalane and 29 parts of water.

Wherein the cytoprotective agent is a mixture of Dunaliella salina extract and jojoba seed oil, and the weight ratio of the Dunaliella salina extract in the cytoprotective agent is 10%; the skin relaxing agent is a mixture of spilanthum extract and caprylic/capric triglyceride, and the spilanthum extract accounts for 5% of the skin relaxing agent; the anti-inflammatory agent is a mixture of caper fruit extract and octyl dodecanol myristate, and the weight ratio of the caper fruit extract in the anti-inflammatory agent is 50%.

Example 4

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 4 parts of a cytoprotective agent, 4 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 8 parts of squalane and 31 parts of water.

Example 5

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 6 parts of a cytoprotective agent, 4 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane and 32 parts of water.

Example 6

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 3.2 parts of cell protectant, 3.2 parts of skin relaxer, 1 part of anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 1 part of antioxidant and 34.6 parts of water.

Wherein the cytoprotective agent is a mixture of Dunaliella salina extract and jojoba seed oil, and the weight ratio of the Dunaliella salina extract in the cytoprotective agent is 8%; the skin relaxing agent is a mixture of spilanthus altissima extract and caprylic/capric triglyceride, and the spilanthus altissima extract accounts for 3% of the skin relaxing agent; the anti-inflammatory agent is a mixture of caper fruit extract and octyl dodecanol myristate, and the weight ratio of the caper fruit extract in the anti-inflammatory agent is 30%; the antioxidant is a mixture of wild soybean oil, carrot root extract and beta-carotene, and the weight ratio of the carrot root extract to the beta-carotene in the antioxidant is 15%.

Example 7

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 3.2 parts of cell protectant, 3.2 parts of skin relaxer, 1 part of anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 2 parts of antioxidant and 33.6 parts of water.

Wherein the cytoprotective agent is a mixture of Dunaliella salina extract and jojoba seed oil, and the weight ratio of the Dunaliella salina extract in the cytoprotective agent is 8%; the skin relaxing agent is a mixture of spilanthus altissima extract and caprylic/capric triglyceride, and the spilanthus altissima extract accounts for 3% of the skin relaxing agent; the anti-inflammatory agent is a mixture of caper fruit extract and octyl dodecanol myristate, and the weight ratio of the caper fruit extract in the anti-inflammatory agent is 30%; the antioxidant is a mixture of wild soybean oil, carrot root extract and beta-carotene, and the weight ratio of the carrot root extract to the beta-carotene in the antioxidant is 20%.

Example 8

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 3.2 parts of cell protectant, 3.2 parts of skin relaxer, 1 part of anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 1 part of tocopherol and 34.6 parts of water.

Example 9

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 3.2 parts of cell protectant, 3.2 parts of skin relaxer, 1 part of anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 1 part of phenoxyethanol and 34.6 parts of water.

Example 10

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 2 parts of a cytoprotective agent, 2 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 1 part of octaethylene glycol and 34.6 parts of water.

Example 11

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 2 parts of a cytoprotective agent, 2 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 3 parts of hyaluronic acid and 32.6 parts of water. Wherein the hyaluronic acid comprises small-molecule hyaluronic acid and medium-molecule hyaluronic acid with a weight ratio of 1:2.

Example 12

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 2 parts of a cytoprotective agent, 2 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 4 parts of hyaluronic acid and 31.6 parts of water. Wherein the hyaluronic acid comprises small-molecule hyaluronic acid and medium-molecule hyaluronic acid with a weight ratio of 1:2.

Example 13

The difference between this example and example 1 is that the raw materials are in weight ratio: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 2 parts of a cytoprotective agent, 2 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 5 parts of hyaluronic acid and 30.6 parts of water. Wherein the hyaluronic acid comprises small-molecule hyaluronic acid and medium-molecule hyaluronic acid with a weight ratio of 1:2.

Example 14

This example differs from example 11 in that the hyaluronic acid comprises small molecule hyaluronic acid and medium molecule hyaluronic acid in a weight ratio of 1:3.

Example 15

This example differs from example 11 in that the hyaluronic acid comprises small molecule hyaluronic acid and medium molecule hyaluronic acid in a weight ratio of 2:1.

Example 16

The difference between this example and example 11 is that the raw materials are in weight proportions: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 2 parts of a cytoprotective agent, 2 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 3 parts of hyaluronic acid, 2 parts of betaine and 30.6 parts of water. In this example, the mass ratio of betaine to hyaluronic acid is 1:1.5.

example 17

The difference between this example and example 11 is that the raw materials are in weight proportions: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 2 parts of a cytoprotective agent, 2 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 3 parts of hyaluronic acid, 3 parts of betaine and 29.6 parts of water. In this example, the mass ratio of betaine to hyaluronic acid is 1:1.

example 18

The difference between this example and example 11 is that the raw materials are in weight proportions: 20 parts of caprylic/capric triglyceride, 13 parts of jojoba seed oil, 10 parts of glycerin, 3 parts of sucrose laurate, 3 parts of sucrose stearate, 2 parts of a cytoprotective agent, 2 parts of a skin relaxing agent, 1 part of an anti-inflammatory agent, 1 part of bergamot fruit oil, 1 part of lime fruit peel oil, 1 part of grapefruit peel oil, 5 parts of squalane, 4 parts of hyaluronic acid, 2 parts of betaine and 29.6 parts of water. In this example, the mass ratio of betaine to hyaluronic acid is 2:1.

comparative example

Comparative example 1

This comparative example differs from example 1 in that sucrose laurate is replaced with an equal amount of water.

Comparative example 2

This comparative example differs from example 1 in that sucrose stearate is replaced with an equal amount of water.

Comparative example 3

This comparative example differs from example 1 in that the cytoprotective agent is replaced with an equal amount of water.

Comparative example 4

This comparative example differs from example 1 in that the skin relaxant was replaced with an equal amount of water.

Comparative example 5

This comparative example differs from example 1 in that the anti-inflammatory agent is replaced with an equal amount of water.

Comparative example 6

This comparative example differs from example 1 in that bergamot fruit oil was replaced with an equal amount of water.

Comparative example 7

This comparative example differs from example 1 in that the lime peel oil was replaced with an equal amount of water.

Comparative example 8

This comparative example differs from example 1 in that the grapefruit peel oil was replaced with an equal amount of water.

Comparative example 9

This comparative example differs from example 1 in that squalane was replaced with an equal amount of water.

Comparative example 10

This comparative example differs from example 1 in that the skin relaxant was replaced with an equivalent amount of cytoprotective agent.

Comparative example 11

This comparative example differs from example 1 in that squalane was replaced with an equivalent amount of skin relaxant.

Comparative example 12

This comparative example differs from example 1 in that the cytoprotective agent was replaced by an equivalent amount of squalane.

Performance test

300 female volunteers with ages of 30-50 years were randomly selected, and were randomly divided into 30 groups, and the masks in each example and each comparative example were used once per night for 28 days.

The skin elasticity R2 value, the face wrinkle area, the skin brightness L value and the skin smoothness SEsm of the volunteer are detected in advance before the volunteer uses the mask, and an average value is calculated for each group; the volunteers were then checked again for skin elasticity R2 value, face wrinkle area, skin brightness L value and skin smoothness SEsm after 14 days and 28 days of continuous use of the mask, and after each group calculated the average value and the corresponding rate of change.

Table 1 test results of test one, test two, test three

Referring to table 1, the masks of examples 1 to 3 showed superior moisturizing and wrinkle removing effects compared to comparative examples 1 to 9, showing that the present application, when sucrose laurate, sucrose stearate, bergamot fruit oil, lime fruit oil, grapefruit fruit oil and squalane were used in combination, the skin was made to relax and soft, and at the same time skin pores were made to open so that the emulsion active ingredient was absorbed by the cells inside the skin, so that the skin could be kept permanently moist, and the skin wrinkles were effectively improved.

In combination with examples 1, 4 and 5, the weight ratio of cytoprotective agent, squalane and skin relaxant in example 1 was 1:2.5:1, the weight ratio of cytoprotective agent, squalane to skin relaxant in example 4 was 1:2:1, the weight ratio of cytoprotective agent, squalane to skin relaxant in example 5 was 1:1.17:1.25, the mask of example 4 had better moisturizing, anti-wrinkle, skin tightening effects. It is considered by analysis that squalane can promote skin to open pores and promote emulsion components to permeate into deep layers of skin, but when the amount of squalane is increased, the possibility of excessively opening pores may be raised, so that the skin irritation caused by emulsion is increased, the skin is easily damaged, and the effect of improving the skin state cannot be achieved. The insufficient amount of squalane can affect the absorption of effective components of emulsion by deep skin and improve deep skin. Even if the amount of the skin relaxant is increased as in example 5, when the amount of squalane used is insufficient, skin pores cannot be effectively opened, so that the skin relaxant and the emulsion active ingredient cannot act on the deep layer of the skin but tend to act on the surface layer of the skin, and thus the effect of improving the skin state cannot be sustained, which is manifested as poor overall effect of improving the skin state.

In combination with comparative example 10, the skin condition of the volunteer in comparative example 10 was improved to a lesser extent than in example 1, and it was analyzed that aged, contracted muscles and cells could not be effectively relaxed in the absence of the skin relaxant, so that the cells could not effectively absorb the emulsion active ingredient, while the addition amount of the cytoprotective agent was correspondingly increased, but the restoration effect by the cytoprotective agent was limited based on the inability of the cells to effectively absorb the emulsion active ingredient, thereby showing an improvement in the skin condition, but the improvement degree was weaker than in example 1.

In combination with comparative example 11, the skin condition of the volunteer in comparative example 11 was improved to a lesser extent than in example 1, and it was found by analysis that, after the permeation promoting effect of squalane was lost, the emulsion active ingredient could not penetrate into the deep skin layer effectively, and the cells in the deep skin layer could not be repaired effectively. The skin relaxing agent was added in an increased amount to promote aging of the skin surface layer, relaxation of contracted muscles and cells, and allow the cells of the skin surface layer to absorb the emulsion active ingredient, but the improvement of the skin state was not achieved in a lasting effect because it was limited to repair of the skin surface layer and the improvement of the skin deep layer was not improved effectively, which is shown to be weaker than in example 1 in the volunteer of comparative example 11.

In combination with comparative example 12, the skin condition of the volunteer in comparative example 12 was improved to a lesser extent than in example 1, and it was found that although the addition of squalane increased to promote the opening of skin pores and the penetration of the emulsion active ingredient into the deep layer of the skin, the emulsion active ingredient was less effective in improving the deep layer of the skin but the improvement effect was continued for a shorter period of time after lacking the effect of wrapping and repairing the cells with the cytoprotective agent, and therefore it was revealed that the skin improvement effect of the volunteer in comparative example 12 was weaker than in example 1.

Therefore, the inventor can effectively increase the moisturizing, anti-wrinkle and skin nourishing effects of the emulsion by compounding the cytoprotective agent, the squalane and the skin relaxing agent in a specific proportion, so that the skin state of a user can be effectively and permanently improved.

In combination with examples 1, 6 to 10, the mask of example 1 exhibited slightly lower skin improvement effect, indicating that the addition of antioxidants, tocopherols, phenoxyethanol and octylglycol to the emulsion suitably increased the skin improvement effect of the mask.

From examples 1, 11 to 13, it can be seen that the addition of hyaluronic acid to the emulsion is effective in improving the moisturization, elasticity and firmness of the skin and is effective in improving skin wrinkles. Meanwhile, the weight ratio of the sum of the weights of lime peel oil and grapefruit peel oil to hyaluronic acid in example 11 was 1:1.5, the weight ratio of the sum of the weights of lime peel oil and grapefruit peel oil to hyaluronic acid in example 12 was 1:2, the weight ratio of the sum of the weights of lime peel oil and grapefruit peel oil to hyaluronic acid in example 13 was 1:2.5, analysis shows that the effect of the mask in example 12 is optimal, and analysis shows that after hyaluronic acid is directly added into the mask, the hyaluronic acid can directly act on the inside of skin to play a role in moisturizing, when the usage amount of the hyaluronic acid is increased, for sensitive skin, red swelling of sensitive skin can be easily caused due to the good water absorption and retention effects of the hyaluronic acid, and the usage amount of the hyaluronic acid is reduced, so that the improvement effect of the emulsion on the skin state can be affected. Therefore, the inventor adjusts the proportion of the lime peel oil, the grapefruit peel oil and the hyaluronic acid, so that the hyaluronic acid plays a role in moisturizing the skin, and as the directly added hyaluronic acid is degraded, the lime peel oil and the grapefruit peel oil promote skin cells to secrete the hyaluronic acid, so that the amount of the hyaluronic acid is balanced and the moisturizing effect can be continuously played.

When the weight ratio of the small-molecular hyaluronic acid to the medium-molecular hyaluronic acid in the hyaluronic acid is 1 in combination with examples 11, 14 and 15: in the range of (2-3), the micromolecular hyaluronic acid and the medium-molecular hyaluronic acid can exert better synergistic effect, after the emulsion is absorbed by the skin, the micromolecular hyaluronic acid can quickly penetrate deep into the deep layer of the skin to play a role in moisturizing, and meanwhile, the micromolecular hyaluronic acid can slightly dilate capillaries to promote the skin to absorb the macromolecular hyaluronic acid and other effective components, so that the effect of improving the skin by the emulsion is exerted optimally.

In examples 11, 16 and 17, the masks added with betaine showed more excellent moisturizing, skin tightening and wrinkle removing effects, indicating that the addition of betaine to the emulsion can enhance the retention effect of the emulsion. Meanwhile, the effect of the mask in examples 16 and 18 for improving the skin condition is more excellent, which shows that betaine and hyaluronic acid can act synergistically when added into the emulsion in a specific ratio, firstly, betaine which easily releases water molecules promotes skin cells to absorb water molecules, and secondly, hyaluronic acid is supplied to skin cells to absorb water molecules, so that the skin can maintain lasting moisture and elasticity, and thus lasting firmness and effective wrinkle improvement effect are exhibited.

The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.

Claims

1. An anti-wrinkle essential oil mask containing pink microalgae and spilanthol is characterized by comprising the following raw materials in percentage by weight: 25-30% of caprylic/capric triglyceride, 10-15% of jojoba seed oil, 5-10% of glycerol, 1-5% of sucrose laurate, 1-5% of sucrose stearate, 2-6% of cytoprotective agent, 2-4% of skin relaxing agent, 1-3% of anti-inflammatory agent, 1-2% of bergamot fruit oil, 1-2% of lime peel oil, 1-2% of grapefruit peel oil, 5-8% of squalane, 0-2% of antioxidant, 0-1% of tocopherol, 0-1% of phenoxyethanol, 0-1% of caprylyl glycol, 3-5% of hyaluronic acid, 2-3% of betaine and the balance of water;

the cytoprotective agent is a mixture of dunaliella salina extract and jojoba seed oil, and the weight ratio of the dunaliella salina extract in the cytoprotective agent is 8-10%;

the skin relaxing agent is a mixture of spilanthus altissima extract and caprylic/capric triglyceride, and the spilanthus altissima extract accounts for 3-5% of the skin relaxing agent;

the anti-inflammatory agent is a mixture of caper fruit extract and octyl dodecanol myristate;

the antioxidant is a mixture of wild soybean oil, carrot root extract and beta-carotene.

2. The wrinkle resistant essential oil mask containing pink microalgae and spilanthol essence according to claim 1, wherein the wrinkle resistant essential oil mask is characterized in that: the weight ratio of caper fruit extract in the anti-inflammatory agent is 30-50%.

3. The wrinkle resistant essential oil mask containing pink microalgae and spilanthol essence according to claim 1, wherein the wrinkle resistant essential oil mask is characterized in that: in the antioxidant, the weight ratio of the carrot root extract to the beta-carotene is 15-20%.

4. The wrinkle resistant essential oil mask containing pink microalgae and spilanthol essence according to claim 1, wherein the wrinkle resistant essential oil mask is characterized in that: the weight ratio of the cell protectant, squalane and skin relaxant is 1: (2-2.5): 1.

5. the wrinkle resistant essential oil mask containing pink microalgae and spilanthol essence according to claim 1, wherein the wrinkle resistant essential oil mask is characterized in that: the hyaluronic acid comprises the following components in percentage by weight: small molecule hyaluronic acid and medium molecule hyaluronic acid of (2-3).

6. The wrinkle resistant essential oil mask containing pink microalgae and spilanthol essence according to claim 5, wherein the wrinkle resistant essential oil mask is characterized in that: the weight ratio of the sum of the weights of the lime peel oil and the grapefruit peel oil to the hyaluronic acid is 1:2.

7. the wrinkle resistant essential oil mask containing pink microalgae and spilanthol essence according to claim 5, wherein the wrinkle resistant essential oil mask is characterized in that: the mass ratio of the betaine to the hyaluronic acid is 1: (1.5-2).

8. A preparation method of an anti-wrinkle essential oil mask containing pink microalgae and spilanthol is characterized by comprising the following steps: the method comprises the following steps: