CN116649610B - Cigarette containing violet leaf absolute - Google Patents
Cigarette containing violet leaf absolute Download PDFInfo
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- CN116649610B CN116649610B CN202310934718.7A CN202310934718A CN116649610B CN 116649610 B CN116649610 B CN 116649610B CN 202310934718 A CN202310934718 A CN 202310934718A CN 116649610 B CN116649610 B CN 116649610B
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- China
- Prior art keywords
- violet
- cigarette
- violet leaf
- leaf absolute
- wafer
- Prior art date
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- 239000001846 viola odorata l. leaf absolute Substances 0.000 title claims abstract description 42
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 40
- 239000011324 bead Substances 0.000 claims abstract description 48
- 244000172533 Viola sororia Species 0.000 claims abstract description 41
- 238000004880 explosion Methods 0.000 claims abstract description 38
- 239000000463 material Substances 0.000 claims abstract description 38
- 238000001704 evaporation Methods 0.000 claims abstract description 24
- 239000004094 surface-active agent Substances 0.000 claims abstract description 24
- 230000008020 evaporation Effects 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 13
- 238000002386 leaching Methods 0.000 claims abstract description 10
- 239000002002 slurry Substances 0.000 claims abstract description 10
- 239000007791 liquid phase Substances 0.000 claims abstract description 7
- 238000004140 cleaning Methods 0.000 claims abstract description 6
- 238000005086 pumping Methods 0.000 claims abstract description 6
- 238000005096 rolling process Methods 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000003921 oil Substances 0.000 claims description 37
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 19
- 229930195729 fatty acid Natural products 0.000 claims description 19
- 239000000194 fatty acid Substances 0.000 claims description 19
- -1 polypropylene Polymers 0.000 claims description 14
- 239000003995 emulsifying agent Substances 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 claims description 9
- 239000003963 antioxidant agent Substances 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 239000003755 preservative agent Substances 0.000 claims description 8
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 7
- 229930006000 Sucrose Natural products 0.000 claims description 7
- 230000003078 antioxidant effect Effects 0.000 claims description 7
- 239000000787 lecithin Substances 0.000 claims description 7
- 229940067606 lecithin Drugs 0.000 claims description 7
- 235000010445 lecithin Nutrition 0.000 claims description 7
- 230000002335 preservative effect Effects 0.000 claims description 7
- 239000005720 sucrose Substances 0.000 claims description 7
- 239000004743 Polypropylene Substances 0.000 claims description 5
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims description 5
- 229920001155 polypropylene Polymers 0.000 claims description 5
- 235000010199 sorbic acid Nutrition 0.000 claims description 5
- 239000004334 sorbic acid Substances 0.000 claims description 5
- 229940075582 sorbic acid Drugs 0.000 claims description 5
- 239000000835 fiber Substances 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- 229920006221 acetate fiber Polymers 0.000 claims 1
- 150000004665 fatty acids Chemical class 0.000 claims 1
- 238000009792 diffusion process Methods 0.000 abstract description 22
- 239000003205 fragrance Substances 0.000 abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 4
- 230000009172 bursting Effects 0.000 abstract description 3
- 125000003118 aryl group Chemical group 0.000 abstract description 2
- 235000019505 tobacco product Nutrition 0.000 abstract description 2
- 238000002347 injection Methods 0.000 abstract 1
- 239000007924 injection Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 12
- 230000000694 effects Effects 0.000 description 6
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerol Substances OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 5
- 239000000600 sorbitol Substances 0.000 description 5
- CZBZUDVBLSSABA-UHFFFAOYSA-N butylated hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 description 4
- 239000002360 explosive Substances 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 4
- 235000019634 flavors Nutrition 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000000691 measurement method Methods 0.000 description 4
- IMOYOUMVYICGCA-UHFFFAOYSA-N 2-tert-butyl-4-hydroxyanisole Chemical compound COC1=CC=C(O)C=C1C(C)(C)C IMOYOUMVYICGCA-UHFFFAOYSA-N 0.000 description 3
- 241000208125 Nicotiana Species 0.000 description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 3
- 239000005433 ionosphere Substances 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
- 229920000223 polyglycerol Polymers 0.000 description 3
- ZTHYODDOHIVTJV-UHFFFAOYSA-N Propyl gallate Chemical compound CCCOC(=O)C1=CC(O)=C(O)C(O)=C1 ZTHYODDOHIVTJV-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- SKHBJDDIGYYYMJ-UHFFFAOYSA-N 2,6-ditert-butyl-6-methylcyclohexa-1,3-dien-1-ol Chemical compound CC(C)(C)C1=C(O)C(C)(C(C)(C)C)CC=C1 SKHBJDDIGYYYMJ-UHFFFAOYSA-N 0.000 description 1
- QSHVAZMOLNGWSY-UHFFFAOYSA-N 3-butyl-4-methoxyphenol Chemical group CCCCC1=CC(O)=CC=C1OC QSHVAZMOLNGWSY-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000621 bronchi Anatomy 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 239000000473 propyl gallate Substances 0.000 description 1
- 229940075579 propyl gallate Drugs 0.000 description 1
- 235000010388 propyl gallate Nutrition 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
- A24D1/042—Cigars; Cigarettes with mouthpieces or filter-tips with mouthpieces
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The application discloses a cigarette containing violet leaf absolute oil, and belongs to the technical field of tobacco products. The filter stick of the cigarette comprises a bursting bead containing clean violet leaf oil and a wafer provided with a central through hole, wherein the bursting bead is placed in the central through hole of the wafer; the violet leaf absolute is prepared by the following method: cleaning violet leaves, rolling to obtain slurry, adding water to dilute 1-3 times, adding a surfactant to mix uniformly, pumping into a flash tank for flash evaporation, adding 0.5-1 times of absolute ethyl alcohol into a liquid phase after flash evaporation to extract for 2-3 hours to obtain a leaching solution, concentrating to obtain an extract, extracting to obtain an extract, adding auxiliary materials to mix, and obtaining the violet leaf absolute oil. The clean violet leaf oil in the cigarette has aromatic fragrance, low viscosity and quick circulation, is placed in the injection explosion beads, can be basically and completely diffused at the through holes of the wafer for 10s after the explosion beads are pinched and broken at the low temperature of 5 ℃, and can smell obvious violet fragrance within 5s of diffusion.
Description
Technical Field
The application belongs to the technical field of tobacco products, and particularly relates to a cigarette containing violet leaf absolute.
Background
Cigarette flavoring is the main means for supplementing cigarette flavor and giving characteristic flavor style. In the traditional cigarette technology, essence and spice are directly sprayed on tobacco shreds or tobacco leaves, so that more loss is caused, and in recent years, slow-release materials of the essence for cigarettes and a bead-explosion aroma-enhancing technology also appear, thereby providing a new thought for the problems of insufficient cigarette aroma and difficult lasting aroma of cigarettes.
The explosion beads are embedded in the tobacco filter stick, so that a smoker can pinch and explode in the smoking process, liquid in the beads flows out, the taste of the cigarette is richer, the cigarette is more fragrant and moist, and the smoker can obtain more comfortable experience. Violet is a plant with ornamental value and medicinal value. The violet fragrance is harmless to human body and has a strong fragrance; meanwhile, the utility model has great assistance to the respiratory tract, and can condition bronchus and moisten throat. At present, no report is available on the fact that violet leaf absolute oil is made into explosion beads and placed in a cigarette filter stick.
In addition, in winter, the explosion beads are affected by low-temperature environment, so that the diffusion and the fluxion of the clean oil after being broken are poor, the fragrance is not easy to emit, and the effect of enhancing the fragrance of the cigarettes cannot be achieved.
Therefore, there is a need for a cigarette containing an ionophora leaf absolute that maintains good flowability even in winter, and which does not have a slow diffusion of flavor due to low temperature even in winter.
Disclosure of Invention
In order to solve the problems, a cigarette containing violet leaf absolute is provided, the violet leaf absolute is improved to have a flavoring effect and simultaneously has reduced viscosity, so that the liquid flow of the leaf absolute is enhanced; and the specific structure is arranged in the filter stick to further accelerate the diffusion speed of the clean violet leaf oil, so that the violet fragrance is fully diffused.
The specific technical scheme of the application is as follows:
the filter stick of the cigarette comprises explosion beads containing the clean violet leaf oil and a wafer provided with a central through hole, wherein the radial plane of the wafer is perpendicular to the central axis of the cigarette, and the explosion beads are placed in the central through hole of the wafer;
the diameter of the central through hole is the same as that of the explosion bead;
the violet leaf absolute is prepared by the following method:
cleaning violet leaves, rolling to obtain slurry, adding water to dilute 1-3 times, adding a surfactant to mix uniformly, pumping into a flash tank for flash evaporation, adding 0.5-1 times of organic solvent into the liquid phase after flash evaporation to extract for 2-3 hours to obtain extract, concentrating to obtain extract, extracting to obtain extract, adding auxiliary materials to mix, and obtaining the violet leaf absolute oil.
Preferably, the contact part of the wafer and the explosion bead is in a sawtooth shape, a circular tooth shape, a tooth strip shape, a burr shape, a spiral shape, a prismatic shape, a round shape or a spiral shape.
Preferably, the material of the wafer and the material of the filter stick are fiber tows; the fiber tows include, but are not limited to, acetate tows, polypropylene tows.
Preferably, the thickness of the wafer is 1/3-2/3 of the diameter of the explosion beads.
Preferably, the thickness of the wafer is 2/3 of the diameter of the bursting beads.
Preferably, in the preparation process of the violet leaf absolute, the addition mass fraction of the auxiliary materials is 0.8-2.8%; the auxiliary materials comprise the following components:
0.05-1 part of preservative, 0.5-5 parts of emulsifier and 3-4 parts of antioxidant.
Preferably, in the preparation process of the violet leaf absolute, the adding mass fraction of the auxiliary materials is 1.0-2.5%; the auxiliary materials comprise the following components:
0.05-1 part of preservative, 0.5-4 parts of emulsifier and 3-4 parts of antioxidant.
Such preservatives include, but are not limited to, sodium benzoate, sorbic acid, and parabens;
the emulsifying agent comprises, but is not limited to, polyglycerol stearate, mono-diglyceride fatty acid ester, tween;
such antioxidants include, but are not limited to, 2,6 di-t-butyl cresol, t-butyl p-hydroxy anisole, propyl gallate.
Preferably, the surfactant in the preparation process of the violet leaf absolute comprises sucrose fatty acid ester and lecithin in a weight ratio of 2-4:1, more preferably, 2:1.
preferably, the addition weight of the surfactant in the preparation process of the violet leaf absolute accounts for 0.1-2% of the weight of the violet leaf, and more preferably, 0.5-2%.
Preferably, in the preparation process of the violet leaf absolute, the flash evaporation conditions are as follows: flash evaporation is carried out for 15-30s under the pressure of-1 to-0.09 MPa; the flash evaporation temperature is 45-50 ℃.
More preferably, in the preparation process of the violet leaf absolute, the flash evaporation conditions are as follows: flash evaporation is carried out for 15-30s under the pressure of-1 to-0.5 MPa; the flash evaporation temperature is 45-50 ℃.
Preferably, the extraction conditions in the preparation process of the violet leaf absolute oil are as follows: the extraction temperature is 20-30 ℃, the extraction pressure is 10-15MPa, and the extraction time is 0.5-0.8h.
The beneficial effects of the application include, but are not limited to:
1. the violet leaf absolute oil with low viscosity and aromatic flavor and no choke is obtained by combining a flash evaporation process after the surfactant is added, the viscosity is reduced because flash evaporation creates a low-pressure environment for the surfactant, the compactness of surfactant aggregates in a liquid phase is enhanced, the capability of the surfactant for reducing the surface tension of slurry liquid is further enhanced, oily substances in the violet leaf are better dissolved, and the viscosity of the leaf absolute oil is reduced;
in order to further enhance the circulation of the leaf absolute with reduced viscosity in a low-temperature environment, the application adds an emulsifying agent to further emulsify and solubilize the leaf absolute, and when the emulsifying agent is a single-glycerol fatty acid ester and a diglycerol fatty acid ester through screening, the viscosity reduction effect is best, and the emulsifying agent, an antioxidant and a preservative are added into the extracted violet leaf absolute together as auxiliary materials, so that the leaf absolute with further reduced viscosity is obtained.
2. According to the application, a special structure is arranged in the cigarette filter stick, the explosion beads containing the clean violet leaf oil are placed at the through holes, and after the explosion beads are pinched, liquid matters in the explosion beads are diffused into the wafer, so that the diffusion speed of the clean violet leaf oil in the cigarette filter stick is remarkably improved, and the fragrance diffusion time is improved by about 4.9 times; furthermore, the application sets a special contact surface, a prismatic shape, a burr shape, a saw tooth shape and the like at the contact position of the explosion beads and the wafer, thereby accelerating the diffusion speed of leaf absolute oil in the wafer, and the fragrance emission time is rapid, and the strong violet fragrance can be smelled within 5 seconds.
Detailed Description
The present application is described in detail below with reference to examples, but the present application is not limited to these examples.
Example 1
The filter stick of the cigarette comprises explosion beads containing the clean violet leaf oil and a circular sheet provided with a central through hole, wherein the radial plane of the circular sheet is perpendicular to the central axis of the cigarette, and the explosion beads are placed in the central through hole of the circular sheet;
the material of the wafer is the same as that of the cigarette filter stick, and the wafer is polypropylene tows; the contact part of the wafer and the explosion beads is in a corner shape; the thickness of the wafer is 2/3 of the diameter of the explosion beads.
The diameter of the central through hole is the same as the diameter of the explosion bead.
The violet leaf absolute is prepared by the following method:
cleaning violet leaves, rolling to obtain slurry, adding water to dilute 1.5 times, adding surfactant accounting for 0.5% of the weight of the violet leaves, uniformly mixing, pumping into a flash tank with the pressure of-0.4 MPa, flash evaporating for 30s at 45 ℃, adding absolute ethyl alcohol with the volume of 0.7 times into the liquid phase after flash evaporation, leaching for 2h to obtain leaching liquor, concentrating to obtain extract, extracting for 0.8h at 20 ℃ and 12MPa to obtain extract, adding auxiliary materials with the mass fraction of 1.5%, and mixing to obtain the violet leaf absolute oil.
The auxiliary materials are prepared from the following components: the preservative comprises, by weight, 0.05 part of sorbic acid, 2 parts of an emulsifier mono-diglycerol fatty acid ester, and 3 parts of an antioxidant tert-butyl p-hydroxyanisole.
The surfactant is prepared from sucrose fatty acid ester and lecithin according to different weight proportions, the proportions of the surfactant are optimally screened in the embodiment, the influence of the sucrose fatty acid ester and the lecithin under different weight proportions on the clean violet leaf oil is studied, and the specific proportions and the results are shown in the table 1 below.
The viscosity measurement method comprises the following steps:
the viscosity measurement method is a capillary method: at a constant temperature of 25 ℃, a volume of sample is loaded into the capillary, and the time t for the sample to flow through the capillary under the force of gravity is observed and recorded. The time t is then multiplied by the viscometer constant, resulting in the viscosity values shown in Table 1.
TABLE 1 influence of different surfactant ratios on Violet leaf absolute
As can be seen from the data in the table, the weight ratio of sucrose fatty acid ester to lecithin is 2-4:1, the prepared violet leaf absolute has relatively lower viscosity and better fluxion, wherein the violet leaf absolute is prepared by the following components in weight ratio of 2: the effect is best at 1.
Example 2
The filter stick of the cigarette comprises explosion beads containing the clean violet leaf oil and a circular sheet provided with a central through hole, wherein the radial plane of the circular sheet is perpendicular to the central axis of the cigarette, and the explosion beads are placed in the central through hole of the circular sheet;
the material of the wafer is the same as that of the cigarette filter stick, and the wafer is polypropylene tows; the contact part of the wafer and the explosion beads is in a corner shape; the thickness of the wafer is 2/3 of the diameter of the explosion beads.
The diameter of the central through hole is the same as the diameter of the explosion bead.
The violet leaf absolute is prepared by the following method:
cleaning violet leaves, rolling to obtain slurry, adding water to dilute 3 times, adding surfactant accounting for 0.1% of the weight of the violet leaves, uniformly mixing, pumping into a flash tank with the pressure of-0.09 MPa, flash evaporating for 15s at 50 ℃, adding absolute ethyl alcohol with the volume of 0.5 times into the liquid phase after flash evaporation to extract for 2h to obtain extract, concentrating to obtain extract, extracting for 0.5h at 20 ℃ and 10MPa to obtain extract, adding auxiliary materials with the mass fraction of 1.0%, and mixing to obtain the violet leaf absolute oil.
According to the optimization parameters obtained in example 1, the surfactant is set as follows: the sucrose fatty acid ester and lecithin are prepared from the following components in parts by weight: 1, the composition is as follows; the auxiliary materials are prepared from components of preservative (sorbic acid), emulsifying agent and antioxidant (tertiary butyl p-hydroxy anisole) according to a certain weight ratio, the auxiliary material ratio is screened, and the influence of different auxiliary material ratios on the clean violet leaf oil is explored, wherein the specific ratio is shown in the table 2 below.
The viscosity measurement method was the same as in example 1.
TABLE 2 influence of different adjuvant formulation conditions on Violet leaf absolute
As can be seen from table 2, the viscosity of the clean violet leaf oil prepared from the auxiliary materials comprising sorbitol, mono-, di-glycerol fatty acid ester and t-butyl p-hydroxyanisole is lower than that of the clean violet leaf oil prepared from the auxiliary materials comprising sorbitol, polyglycerol stearate and t-butyl p-hydroxyanisole, because the polyglycerol stearate has more glyceryl groups, more hydrophilic groups and more oleophobic groups than the mono-, di-glycerol fatty acid ester does not dissolve the oily components in the clean violet leaf oil in the slurry better than the mono-, di-glycerol fatty acid ester. According to the application, when optimized proportion is carried out among sorbitol, mono-, di-glycerin fatty acid ester and tert-butyl p-hydroxy anisole, according to the table 2, when 0.05-1 part of sorbic acid serving as a preservative, 0.5-4 parts of mono-di-glycerin fatty acid ester serving as an emulsifier and 3-4 parts of tert-butyl p-hydroxy anisole serving as an antioxidant are added, the viscosity of the clean violet leaf oil can be further reduced, wherein the proportion of sorbitol is 0.05: mono-, di-glycerol fatty acid ester 2: the best effect is obtained when tert-butyl is blended with hydroxyanisole 3.
Example 3
The surfactant and the auxiliary materials of the embodiment adopt the optimal technological parameters obtained by screening in the embodiment 1-2, and the method is as follows:
the filter stick of the cigarette comprises explosion beads containing the clean violet leaf oil and a circular sheet provided with a central through hole, wherein the radial plane of the circular sheet is perpendicular to the central axis of the cigarette, and the explosion beads are placed in the central through hole of the circular sheet;
the material of the wafer is the same as the material of the tow of the cigarette filter stick, and the wafer is polypropylene tow; the contact part of the wafer and the explosion beads is in a corner shape; the thickness of the wafer is 2/3 of the diameter of the explosion beads.
The diameter of the central through hole is the same as that of the explosion bead.
The violet leaf absolute is prepared by the following method:
cleaning violet leaves, rolling to obtain slurry, adding water to dilute 1 time, adding surfactant accounting for 2% of the weight of the violet leaves, uniformly mixing, pumping into a flash tank with the pressure of-1 MPa, flash evaporating for 30s at 48 ℃, adding absolute ethyl alcohol with the volume of 1 time into the liquid phase after flash evaporation to leach for 3h to obtain leaching liquor, concentrating to obtain extract, extracting for 0.8h at 30 ℃ and 15MPa to obtain extract, adding auxiliary materials with the mass fraction of 2.5%, and mixing to obtain the violet leaf absolute oil.
The surfactant is prepared from sucrose fatty acid ester and lecithin in a weight ratio of 2:1.
The auxiliary materials comprise 0.05 part of sorbitol, 2 parts of mono-diglycerol fatty acid ester and 3 parts of tert-butyl p-hydroxy anisole according to parts by weight.
The prepared clean violet leaf oil has a viscosity of 41cp, has a strong violet fragrance and is free from nose choking, and the viscosity measurement method is the same as that of example 2.
Comparative example 1 differs from example 3 in that violet leaf absolute is prepared by the following method: directly adding organic solvent into violet leaves for leaching, concentrating the leaching solution to obtain extract, and extracting to obtain violet leaf absolute.
Comparative example 2 differs from example 3 in that violet leaf absolute is prepared by the following method: directly adding organic solvent into violet leaves for leaching, concentrating the leaching solution to obtain extract, extracting to obtain extract, adding auxiliary materials and mixing to obtain violet leaf absolute.
Comparative example 3 differs from example 3 in that no disc device was provided in the cigarette filter rod.
Comparative example 4 differs from example 3 in that the contact of the disc with the bead in the cigarette filter rod is smoothly curved.
Comparative example 5 differs from example 3 in that no auxiliary material was added.
The clean ionosphere oils prepared in example 3 and comparative examples 1-5 were injected into the explosive beads, 100 explosive beads were prepared, each, placed at 5 ℃ for 30 minutes, taken out, placed in a central through-hole disc, the explosive beads were pinched apart, and the diffusion rate of the clean ionosphere oil in each 100 explosive beads (time from when the clean ionosphere oil starts to contact the disc to when it completely diffuses to the edge) was examined, and the specific results are shown in the table below.
The viscosity test method was the same as in example 1.
TABLE 3 comparison of the clean Violet leaf oils of comparative examples 1-5 and example 3
As can be seen from the above table, the prepared violet leaf absolute oil is injected into the explosion beads and the explosion beads are placed in the through holes in the center of the wafer, the example 3 is subjected to surfactant+flash evaporation treatment, the diffusion speed of the violet leaf absolute oil prepared by adding auxiliary materials is fastest, the violet leaf absolute oil is completely diffused to the edge of the wafer for only about 10s, and the diffusion time of the leaf absolute oil without the auxiliary materials is 32s; the complete diffusion time without surfactant+flash evaporation treatment is about 170 s; the complete diffusion time without surfactant plus flash evaporation and auxiliary material treatment is about 220s, and the diffusion speed is far lower than 10s.
In addition, it can be seen that the bead explosion diffusion in the embodiment 3 of the application is rapid and durable diffusion, and the total diffusion can reach about 98% within 10s and 100% within 30s; this is not achieved by comparative examples 1, 2, 5. Compared with comparative example 5, the surfactant and flash evaporation treatment of the application in example 3 can obviously reduce the viscosity of the leaf absolute while the leaf absolute has strong and non-nasal-choking violet fragrance, and the components such as the emulsifier in the auxiliary materials can emulsify oily components in the extract by adding the auxiliary materials, so that the viscosity of the leaf absolute is further reduced.
As can be seen from the above table, the shape/area of the contact between the wafer and the bead has an important effect on the diffusion rate of the leaf absolute oil, and the angular contact surface in example 3 can further increase the diffusion rate of the leaf absolute oil in the blade compared with the smooth arc contact surface in comparative example 4, because the angular contact surface has a guiding property for the diffusion of the leaf absolute oil, and thus increases the diffusion rate. Compared with the comparative example 3 without the disc device, after the explosion beads are broken, the fragrance emission time of the leaf absolute in the comparative example 3 is about 4.9 times that of the example 3, which shows that the disc device greatly quickens the diffusion speed of the leaf absolute, further quickens the diffusion of the fragrance, and can smell the intense violet fragrance within 5 seconds.
The above description is only an example of the present application, and the scope of the present application is not limited to the specific examples, but is defined by the claims of the present application. Various modifications and variations of the present application will be apparent to those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the technical idea and principle of the present application should be included in the protection scope of the present application.
Claims (5)
1. The cigarette containing the violet leaf absolute is characterized in that a filter rod of the cigarette comprises explosion beads containing the violet leaf absolute and a circular sheet provided with a central through hole, the radial plane of the circular sheet is perpendicular to the central axis of the cigarette, and the explosion beads are placed in the central through hole of the circular sheet;
the diameter of the central through hole is the same as that of the explosion bead;
the contact part of the wafer and the explosion bead is in a sawtooth shape, a circular tooth shape, a tooth strip shape, a burr shape, a spiral shape, a prismatic shape, a round shape or a spiral shape;
the material of the wafer and the material of the filter stick are fiber tows; the fiber tows comprise acetate fiber tows and polypropylene tows;
the violet leaf absolute is prepared by the following method:
cleaning violet leaves, rolling to obtain slurry, adding water to dilute the slurry by 1-3 times, adding a surfactant to mix uniformly, pumping the slurry into a flash tank, carrying out flash evaporation for 15-30s at the temperature of 45-50 ℃ under the pressure of-1 to-0.09 MPa, adding an organic solvent with the volume of 0.5-1 times into a liquid phase after flash evaporation to leach for 2-3 hours to obtain a leaching solution, concentrating the leaching solution to obtain an extract, extracting the extract to obtain an extract, adding auxiliary materials to mix, and obtaining the clean violet leaves oil;
the surfactant is prepared from sucrose fatty acid ester and lecithin in a weight ratio of 2-4:1, mixing and preparing;
the adding mass fraction of the auxiliary materials is 0.8-2.8%; the auxiliary materials comprise the following components:
the preservative sorbic acid 0.05-1 weight portions, emulsifier mono-or diglyceride fatty acid cool 0.5-4 weight portions, antioxidant tert-butyl p-light Miao Xiang ether 3-4 weight portions.
2. The cigarette of claim 1, wherein the disc has a thickness of 1/3 to 2/3 of the bead diameter.
3. The cigarette according to claim 1, wherein the adding mass fraction of the auxiliary materials in the preparing process of the violet leaf absolute is 1.0-2.5%.
4. The cigarette of claim 1, wherein the surfactant is added in an amount of 0.1-2% by weight of the violet leaf in the preparation of the violet leaf absolute.
5. The cigarette of claim 1, wherein the extraction conditions during the preparation of the clean violet leaf oil are: the extraction temperature is 20-30 ℃, the extraction pressure is 10-15MPa, and the extraction time is 0.5-0.8h.
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003268397A (en) * | 2002-03-20 | 2003-09-25 | Asama Chemical Co Ltd | Stabilized perfume composition and method for stabilizing perfume |
| WO2010103832A1 (en) * | 2009-03-12 | 2010-09-16 | ライオン株式会社 | Flavor particles and granular detergent composition comprising same |
| CN103215121A (en) * | 2013-04-25 | 2013-07-24 | 防城港市防城区那梭香料厂 | Extraction process of cinnamon oil |
| CN104004589A (en) * | 2013-10-31 | 2014-08-27 | 菏泽中禾健元生物科技有限公司 | Producing method of peony essential oil |
| CN108913361A (en) * | 2018-07-26 | 2018-11-30 | 云南中烟新材料科技有限公司 | A kind of purification tea extract, quick-fried pearl and its preparation method and application |
| CN208242829U (en) * | 2018-05-29 | 2018-12-18 | 云南中烟工业有限责任公司 | A kind of the cigarette quick-fried pearl component of packet water and filter tip |
| CN112450486A (en) * | 2020-11-23 | 2021-03-09 | 山东中烟工业有限责任公司 | Ginger juice lemon flavor essence for cigarette bead blasting and application device thereof |
| CN113845985A (en) * | 2021-10-25 | 2021-12-28 | 朗格斯酒庄（秦皇岛）有限公司 | Pretreatment method for brewing wine by adopting flash evaporation process and wine |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050172976A1 (en) * | 2002-10-31 | 2005-08-11 | Newman Deborah J. | Electrically heated cigarette including controlled-release flavoring |
-
2023
- 2023-07-28 CN CN202310934718.7A patent/CN116649610B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003268397A (en) * | 2002-03-20 | 2003-09-25 | Asama Chemical Co Ltd | Stabilized perfume composition and method for stabilizing perfume |
| WO2010103832A1 (en) * | 2009-03-12 | 2010-09-16 | ライオン株式会社 | Flavor particles and granular detergent composition comprising same |
| CN103215121A (en) * | 2013-04-25 | 2013-07-24 | 防城港市防城区那梭香料厂 | Extraction process of cinnamon oil |
| CN104004589A (en) * | 2013-10-31 | 2014-08-27 | 菏泽中禾健元生物科技有限公司 | Producing method of peony essential oil |
| CN208242829U (en) * | 2018-05-29 | 2018-12-18 | 云南中烟工业有限责任公司 | A kind of the cigarette quick-fried pearl component of packet water and filter tip |
| CN108913361A (en) * | 2018-07-26 | 2018-11-30 | 云南中烟新材料科技有限公司 | A kind of purification tea extract, quick-fried pearl and its preparation method and application |
| CN112450486A (en) * | 2020-11-23 | 2021-03-09 | 山东中烟工业有限责任公司 | Ginger juice lemon flavor essence for cigarette bead blasting and application device thereof |
| CN113845985A (en) * | 2021-10-25 | 2021-12-28 | 朗格斯酒庄（秦皇岛）有限公司 | Pretreatment method for brewing wine by adopting flash evaporation process and wine |
Non-Patent Citations (1)
| Title |
|---|
| 天然香精油的萃取方法及其应用;陈世珍;;精细与专用化学品(第10期);全文 * |
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