CN116529343A - 合成*mre骨架类型的富铝分子筛的方法 - Google Patents

合成*mre骨架类型的富铝分子筛的方法 Download PDF

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Publication number
CN116529343A
CN116529343A CN202180076593.8A CN202180076593A CN116529343A CN 116529343 A CN116529343 A CN 116529343A CN 202180076593 A CN202180076593 A CN 202180076593A CN 116529343 A CN116529343 A CN 116529343A
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CN
China
Prior art keywords
sio
hydroxide
synthesis mixture
zsm
molecular sieve
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Pending
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CN202180076593.8A
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English (en)
Chinese (zh)
Inventor
M·H·安东尼斯
S·萨提皮
A·W·伯顿
S·J·韦格尔
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ExxonMobil Technology and Engineering Co
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ExxonMobil Technology and Engineering Co
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Application filed by ExxonMobil Technology and Engineering Co filed Critical ExxonMobil Technology and Engineering Co
Publication of CN116529343A publication Critical patent/CN116529343A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/703—MRE-type, e.g. ZSM-48
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/58—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins
    • C10G45/60—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used
    • C10G45/64—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G50/00—Production of liquid hydrocarbon mixtures from lower carbon number hydrocarbons, e.g. by oligomerisation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
CN202180076593.8A 2020-11-13 2021-08-26 合成*mre骨架类型的富铝分子筛的方法 Pending CN116529343A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US202063113627P 2020-11-13 2020-11-13
US63/113,627 2020-11-13
PCT/US2021/047630 WO2022103468A1 (en) 2020-11-13 2021-08-26 Method of synthesizing aluminum-rich molecular sieve of *mre framework type

Publications (1)

Publication Number Publication Date
CN116529343A true CN116529343A (zh) 2023-08-01

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Family Applications (1)

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CN202180076593.8A Pending CN116529343A (zh) 2020-11-13 2021-08-26 合成*mre骨架类型的富铝分子筛的方法

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Country Link
US (1) US20250001404A1 (enExample)
EP (1) EP4244189A1 (enExample)
JP (1) JP2023554228A (enExample)
KR (1) KR20230105682A (enExample)
CN (1) CN116529343A (enExample)
CA (1) CA3198683A1 (enExample)
WO (1) WO2022103468A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102022115156A1 (de) 2022-06-17 2023-12-28 Deutsches Zentrum für Luft- und Raumfahrt e.V. Verfahren zur Herstellung eines Zwischenprodukts für die Herstellung von Zeolithen mittels konzentrierter Solarstrahlung sowie Verfahren zur Herstellung von Zeolithen
CN115872414A (zh) * 2022-12-14 2023-03-31 化学与精细化工广东省实验室 一种动态合成低硅铝比zsm-48分子筛的方法
WO2024153436A1 (en) 2023-01-18 2024-07-25 ExxonMobil Technology and Engineering Company *mre-based catalysts for olefin skeletal isomerization
CN119581794B (zh) * 2023-09-05 2026-01-27 中国石油化工股份有限公司 一种电池隔膜及其制备方法和含有该隔膜的锂硫电池
CN119797390B (zh) * 2025-01-02 2025-11-14 大连理工大学 一种在双碱源体系中合成低硅铝比zsm-48分子筛的方法及应用

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101801848A (zh) * 2007-09-18 2010-08-11 埃克森美孚研究工程公司 高活性zsm-48的合成
US20200061593A1 (en) * 2018-08-27 2020-02-27 Exxonmobil Research And Engineering Company Molecular sieves and a process for making molecular sieves
CN111542494A (zh) * 2018-06-14 2020-08-14 雪佛龙美国公司 富铝*mre骨架类型分子筛

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4423021A (en) 1979-08-08 1983-12-27 Mobil Oil Corporation Method of preparing silico-crystal ZSM-48
US5075269A (en) 1988-12-15 1991-12-24 Mobil Oil Corp. Production of high viscosity index lubricating oil stock
FR2698863B1 (fr) * 1992-12-08 1995-01-13 Elf Aquitaine Procédé de synthèse de zolithes du type ZSM-48, produits obtenus et leur application en adsorption et catalyse.
FR2805762B1 (fr) 2000-03-02 2004-01-16 Inst Francais Du Petrole Catalyseur a base de zeolithe zsm-48 et procede pour l'amelioration du point d'ecoulement de charges paraffiniques
FR2808028B1 (fr) 2000-04-21 2003-09-05 Inst Francais Du Petrole Procede flexible de production de bases huiles avec une zeolithe zsm-48
US6923949B1 (en) 2004-03-05 2005-08-02 Exxonmobil Research And Engineering Company Synthesis of ZSM-48 crystals with heterostructural, non ZSM-48, seeding
US7482300B2 (en) 2005-12-13 2009-01-27 Exxonmobil Research And Engineering Company High activity ZSM-48 and methods for dewaxing
CN105849044B (zh) 2013-12-26 2018-10-26 埃克森美孚研究工程公司 Zsm-48晶体的合成
US10604413B2 (en) * 2018-03-09 2020-03-31 Chevron U.S.A. Inc. Synthesis of *MRE framework type molecular sieves

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101801848A (zh) * 2007-09-18 2010-08-11 埃克森美孚研究工程公司 高活性zsm-48的合成
CN111542494A (zh) * 2018-06-14 2020-08-14 雪佛龙美国公司 富铝*mre骨架类型分子筛
US20200061593A1 (en) * 2018-08-27 2020-02-27 Exxonmobil Research And Engineering Company Molecular sieves and a process for making molecular sieves

Non-Patent Citations (1)

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Title
G. GIORDANOA ET AL.: ""Zeolite synthesis in presence of hexamethonium ions"", JOURNAL OF MOLECULAR CATALYSIS A: CHEMICAL, vol. 305, 9 January 2009 (2009-01-09), pages 35 *

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JP2023554228A (ja) 2023-12-27
CA3198683A1 (en) 2022-05-19
WO2022103468A1 (en) 2022-05-19
US20250001404A1 (en) 2025-01-02
EP4244189A1 (en) 2023-09-20
KR20230105682A (ko) 2023-07-11

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