CN116509746A - Moisturizing and repairing mask and preparation method thereof - Google Patents

Moisturizing and repairing mask and preparation method thereof Download PDF

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Publication number
CN116509746A
CN116509746A CN202310381033.4A CN202310381033A CN116509746A CN 116509746 A CN116509746 A CN 116509746A CN 202310381033 A CN202310381033 A CN 202310381033A CN 116509746 A CN116509746 A CN 116509746A
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parts
phase
raw materials
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water
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CN116509746B (en
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徐妍
马应柳
马应珍
周如进
黄剑强
鲁正海
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Guangzhou Hengfang Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4953Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention discloses a moisturizing and repairing mask, which comprises an A-phase component, a B-phase component, a C-phase component and a D-phase component, wherein the A-phase component comprises the following raw materials: water, butylene glycol, thickening stabilizer, glyceryl polyether-26, allantoin, glycerin, sodium hyaluronate, panthenol; the phase B component comprises the following raw materials: 1, 2-hexanediol, p-hydroxyacetophenone; the C phase component comprises the following raw materials: water, tetrahydropyrimidine carboxylic acid, betaine; the phase D component comprises the following raw materials: triethanolamine, gelai, demin, and Magnetitum; the moisturizing and repairing mask and the preparation method thereof can enter into the horny layer tissue gaps of the face, and the nutritional ingredients can enter into the fixed layer, so that the mask has high absorptivity, good utilization rate and stable product activity.

Description

Moisturizing and repairing mask and preparation method thereof
Technical Field
The invention relates to a moisturizing and repairing mask and a preparation method thereof.
Background
The prior market whitening cosmetics generally have the minimum molecules above 500 nanometers, and the keratin tissue gaps of the face are about 50-100 nanometers, so that the nutrients cannot enter into the fixed layer, the absorptivity is less than thousandths, the utilization rate is poor, the product activity is unstable, and the like.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the moisturizing and repairing mask which can enter into the keratin tissue gaps of the face, can enter into the fixed layer of the face, has high absorption rate and good utilization rate, and has stable product activity, and the preparation method thereof.
The technical scheme adopted for solving the technical problems is as follows:
a moisturizing and repairing facial mask comprises an A phase component, a B phase component, a C phase component and a D phase component, wherein,
the phase A component comprises the following raw materials: water, butylene glycol, thickening stabilizer, glyceryl polyether-26, allantoin, glycerin, sodium hyaluronate, panthenol;
the phase B component comprises the following raw materials: 1, 2-hexanediol, p-hydroxyacetophenone;
the C phase component comprises the following raw materials: water, tetrahydropyrimidine carboxylic acid, betaine;
the phase D component comprises the following raw materials: triethanolamine, gelai Keyin, demin Shu, and Magnetitum.
Preferably, the phase A component comprises the following raw materials in parts by weight: 70-80 parts of water, 1-10 parts of butanediol, 0.1-0.3 part of thickening stabilizer, 0.1-0.3 part of glycerin polyether-261-5 part of allantoin, 1-10 parts of glycerin, 0.05-0.2 part of sodium hyaluronate and 0.5-2 parts of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.1-1 part of 1, 2-hexanediol and 0.1-1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 1-5 parts of water, 0.5-2 parts of tetrahydropyrimidine carboxylic acid and 0.5-2 parts of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.1-0.3 part of triethanolamine, 0.5-2 parts of Gliocarpin, 0.1-0.5 part of Demin and 0.5-3 parts of water-locking magnetite;
preferably, the phase A component comprises the following raw materials in parts by weight: 70 parts of water, 1 part of butanediol, 0.1 part of thickening stabilizer, 0.1 part of glycerin polyether-261 part, 1 part of glycerin, 0.05 part of sodium hyaluronate and 0.5 part of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.1 part of 1, 2-hexanediol and 0.1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 1 part of water, 0.5 part of tetrahydropyrimidine carboxylic acid and 0.5 part of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.1 part of triethanolamine, 0.5 part of Gliocarpin, 0.1 part of Demin and 0.5 part of water-locking magnetite.
Preferably, the phase A component comprises the following raw materials in parts by weight: 80 parts of water, 10 parts of butanediol, 0.3 part of thickening stabilizer, 265 parts of glycerin polyether, 0.3 part of allantoin, 10 parts of glycerin, 0.2 part of sodium hyaluronate and 2 parts of panthenol;
the phase B component comprises the following raw materials in parts by weight: 1 part of 1, 2-hexanediol and 1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 5 parts of water, 2 parts of tetrahydropyrimidine carboxylic acid and 2 parts of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.3 part of triethanolamine, 2 parts of Gliocarpin, 0.5 part of Demin, and 3 parts of water-locking magnetite.
Preferably, the phase A component comprises the following raw materials in parts by weight: 76.62 parts of water, 5 parts of butanediol, 0.14 part of thickening stabilizer, 263 parts of glycereth-2 parts of allantoin, 5 parts of glycerol, 0.1 part of sodium hyaluronate and 1 part of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 3 parts of water, 1 part of tetrahydropyrimidine carboxylic acid and 1 part of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.14 part of triethanolamine, 1 part of Gliocarpin, 0.3 part of Demin, and 1.5 parts of water-locking magnetite.
Preferably, the thickening stabilizer is an acrylic ester/C10-30 alkanol acrylate cross-linked polymer.
Preferably, the gliclazide comprises glucosyl glycoside, water, 1, 2-pentanediol.
Preferably, the desmethylose comprises 1, 2-pentanediol, butanediol, hydroxyphenyl propionamide benzoic acid, ascorbyl palmitate.
Preferably, the water-locking magnetite comprises saccharide isomer, water, citric acid and sodium citrate.
The invention provides a preparation method of a moisturizing and repairing mask, which comprises the following steps:
sequentially weighing the phase A components, adding into an emulsifying pot, heating to 80-85deg.C, starting a homogenizer, homogenizing for 3-5min, homogenizing and dissolving completely, maintaining the temperature for 20-40min, and vacuum cooling;
when the temperature is reduced to 70 ℃, adding the dissolved phase B which is stirred by a container outside in advance, and stirring uniformly;
when the temperature is reduced to below 38 ℃, all components of the phase C are respectively added, all components of the phase D are respectively added, the mixture is stirred uniformly, then sampling and inspection are carried out, and after the mixture is qualified, filtering and discharging are carried out by using a filter cloth with 150-250 meshes.
The beneficial effects of the invention are as follows:
multiple active ingredients are adopted, so that the skin is subjected to multiple moisturizing from inside to outside, and deep repairing is realized, wherein the core ingredients of the long-acting moisturizing are as follows: saccharide isomer and glyceroglycosides, which are the only enantiomer of the glyceroglycosides on the market, are the main active ingredients of the honey Luo Mu which survive in a long-term drought environment, can be produced by salt-tolerant blue-green algae, have natural super-strong vitality and protect organisms from osmotic pressure injury; the collocation of the isomer and the glyceroglycosides has several functions: enhancing cell viability and metabolism, activating regenerative skin cells, accelerating synthesis of type I collagen precursors in aging cells, increasing skin moisture retention, elasticity, smoothness and skin thickness, accelerating wound healing and tissue repair, deeply locking water for more than 24 hours, reversing several phenomena of dry skin: coarse, dull, desquamated, tight, reddish; the core components of deep repair are: tetrahydropyrimidine carboxylic acid and hydroxyphenylpropionamide benzoic acid, which combine several effects: reducing itching of the skin, strengthening skin barrier and helping repair, reducing erythema and skin irritation; visible transition of dry, scaling and rough skin to healthy, moist, smooth and soft skin; long-acting skin hydration, comprehensive pollution resistance and reduction of skin stress caused by blue light.
Detailed Description
The principles and features of the present invention are described below with examples given for the purpose of illustration only and are not intended to limit the scope of the invention. The invention is more specifically described by way of example in the following paragraphs. Advantages and features of the invention will become more apparent from the following description and from the claims.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used herein in the description of the invention is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. The term "and/or" as used herein includes any and all combinations of one or more of the associated listed items.
Example 1
A moisturizing and repairing facial mask comprises an A phase component, a B phase component, a C phase component and a D phase component, wherein,
the phase A component comprises the following raw materials in parts by weight: 70 parts of water, 1 part of butanediol, 0.1 part of thickening stabilizer, 0.1 part of glycerin polyether-261 part, 1 part of glycerin, 0.05 part of sodium hyaluronate and 0.5 part of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.1 part of 1, 2-hexanediol and 0.1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 1 part of water, 0.5 part of tetrahydropyrimidine carboxylic acid and 0.5 part of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.1 part of triethanolamine, 0.5 part of Gliocarpin, 0.1 part of Demin and 0.5 part of water-locking magnetite.
The thickening stabilizer is acrylic ester/C10-30 alkanol acrylic ester cross-linked polymer, the gelatine comprises glyceroglycosides, water and 1, 2-pentanediol, the desmethylose comprises 1, 2-pentanediol, butanediol, hydroxyphenylpropionyl amide benzoic acid and ascorbyl palmitate, and the water-locking magnetite comprises saccharide isomers, water, citric acid and sodium citrate.
Example 2
A moisturizing and repairing facial mask comprises an A phase component, a B phase component, a C phase component and a D phase component, wherein,
the phase A component comprises the following raw materials in parts by weight: 80 parts of water, 10 parts of butanediol, 0.3 part of thickening stabilizer, 265 parts of glycerin polyether, 0.3 part of allantoin, 10 parts of glycerin, 0.2 part of sodium hyaluronate and 2 parts of panthenol;
the phase B component comprises the following raw materials in parts by weight: 1 part of 1, 2-hexanediol and 1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 5 parts of water, 2 parts of tetrahydropyrimidine carboxylic acid and 2 parts of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.3 part of triethanolamine, 2 parts of Gliocarpin, 0.5 part of Demin, and 3 parts of water-locking magnetite.
The thickening stabilizer is acrylic ester/C10-30 alkanol acrylic ester cross-linked polymer, the gelatine comprises glyceroglycosides, water and 1, 2-pentanediol, the desmethylose comprises 1, 2-pentanediol, butanediol, hydroxyphenylpropionyl amide benzoic acid and ascorbyl palmitate, and the water-locking magnetite comprises saccharide isomers, water, citric acid and sodium citrate.
Example 3
A moisturizing and repairing facial mask comprises an A phase component, a B phase component, a C phase component and a D phase component, wherein,
the phase A component comprises the following raw materials in parts by weight: 76.62 parts of water, 5 parts of butanediol, 0.14 part of thickening stabilizer, 263 parts of glycereth-2 parts of allantoin, 5 parts of glycerol, 0.1 part of sodium hyaluronate and 1 part of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 3 parts of water, 1 part of tetrahydropyrimidine carboxylic acid and 1 part of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.14 part of triethanolamine, 1 part of Gliocarpin, 0.3 part of Demin, and 1.5 parts of water-locking magnetite.
The thickening stabilizer is acrylic ester/C10-30 alkanol acrylic ester cross-linked polymer, the gelatine comprises glyceroglycosides, water and 1, 2-pentanediol, the desmethylose comprises 1, 2-pentanediol, butanediol, hydroxyphenylpropionyl amide benzoic acid and ascorbyl palmitate, and the water-locking magnetite comprises saccharide isomers, water, citric acid and sodium citrate.
Example 4
A preparation method of a moisturizing and repairing mask comprises the following steps:
sequentially weighing 70 parts of water, 1 part of butanediol, 0.1 part of thickening stabilizer, 261 parts of glycereth, 0.1 part of allantoin, 1 part of glycerol, 0.05 part of sodium hyaluronate and 0.5 part of panthenol, adding into an emulsifying pot, heating to 80 ℃, starting a homogenizer, homogenizing for 3min, completely homogenizing and dissolving, preserving heat for 20min, and vacuum cooling;
when the temperature is reduced to 70 ℃, 0.1 part of 1, 2-hexanediol and 0.1 part of p-hydroxyacetophenone which are stirred and dissolved in advance by a container are added and stirred uniformly;
when the temperature is reduced below 38 ℃, 1 part of water, 0.5 part of tetrahydropyrimidine carboxylic acid and 0.5 part of betaine are respectively added, 0.1 part of triethanolamine, 0.5 part of Gliocarpin, 0.1 part of desmethyline and 0.5 part of water-locking magnetite are respectively added, the mixture is stirred uniformly, then the mixture is sampled and inspected, and after the mixture is qualified, the mixture is filtered by a 150-mesh filter cloth and discharged.
Example 5
A preparation method of a moisturizing and repairing mask comprises the following steps:
sequentially weighing 80 parts of water, 10 parts of butanediol, 0.3 part of thickening stabilizer, 265 parts of glycerolyether, 0.3 part of allantoin, 10 parts of glycerin, 0.2 part of sodium hyaluronate and 2 parts of panthenol, adding into an emulsifying pot, heating to 85 ℃, starting a homogenizer, homogenizing for 5min, homogenizing and dissolving completely, preserving heat for 40min, and vacuum cooling;
when the temperature is reduced to 70 ℃, 1 part of 1, 2-hexanediol and 1 part of p-hydroxyacetophenone which are stirred and dissolved in advance by a container are added and stirred uniformly;
when the temperature is reduced to below 38 ℃, 5 parts of water, 2 parts of tetrahydropyrimidine carboxylic acid and 2 parts of betaine are respectively added, 0.3 part of triethanolamine, 2 parts of glaucone, 0.5 part of Demin and 3 parts of water-locking magnetite are respectively added, the mixture is stirred uniformly, then sampling and inspection are carried out, and after the mixture is qualified, the mixture is filtered by a filter cloth with 250 meshes and discharged.
Example 6
A preparation method of a moisturizing and repairing mask comprises the following steps:
adding 76.62 parts of water, 5 parts of butanediol, 0.14 part of thickening stabilizer, 263 parts of glycereth-263 parts of allantoin, 5 parts of glycerin, 0.1 part of sodium hyaluronate and 1 part of panthenol into an emulsifying pot, heating to 80 ℃, starting a homogenizer, homogenizing for 4min, homogenizing and dissolving completely, preserving heat for 30min, and vacuum cooling;
when the temperature is reduced to 70 ℃, 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone which are dissolved by stirring in a container outside in advance are added and stirred uniformly;
when the temperature is reduced to below 38 ℃, 3 parts of water, 1 part of tetrahydropyrimidine carboxylic acid and 1 part of betaine are respectively added, 0.14 part of triethanolamine, 1 part of glaucone, 0.3 part of Demin and 1.5 parts of water-locking magnetite are respectively added, the mixture is stirred uniformly, then sampling and inspection are carried out, and after the mixture is qualified, filtering and discharging are carried out by using 200-mesh filter cloth.
Comparative example 1:
a preparation method of a moisturizing and repairing mask comprises the following steps:
adding 76.62 parts of water, 5 parts of butanediol, 0.14 part of thickening stabilizer, 263 parts of glycereth-263 parts of allantoin, 5 parts of glycerin, 0.1 part of sodium hyaluronate and 1 part of panthenol into an emulsifying pot, heating to 80 ℃, starting a homogenizer, homogenizing for 4min, homogenizing and dissolving completely, preserving heat for 30min, and vacuum cooling;
when the temperature is reduced to 70 ℃, 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone which are dissolved by stirring in a container outside in advance are added and stirred uniformly;
when the temperature is reduced to below 38 ℃, 3 parts of water, 1 part of tetrahydropyrimidine carboxylic acid and 1 part of betaine are respectively added, 0.14 part of triethanolamine and 0.3 part of Demin are respectively added, the mixture is stirred uniformly, then sampling and inspection are carried out, and after the mixture is qualified, 200-mesh filter cloth is used for filtering and discharging.
Comparative example 2:
a preparation method of a moisturizing and repairing mask comprises the following steps:
adding 76.62 parts of water, 5 parts of butanediol, 0.14 part of thickening stabilizer, 263 parts of glycereth-263 parts of allantoin, 5 parts of glycerin, 0.1 part of sodium hyaluronate and 1 part of panthenol into an emulsifying pot, heating to 80 ℃, starting a homogenizer, homogenizing for 4min, homogenizing and dissolving completely, preserving heat for 30min, and vacuum cooling;
when the temperature is reduced to 70 ℃, 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone which are dissolved by stirring in a container outside in advance are added and stirred uniformly;
when the temperature is reduced to below 38 ℃, 3 parts of water and 1 part of betaine are respectively added, 0.14 part of triethanolamine, 1 part of glaucone and 1.5 parts of water-locking magnetite are respectively added, the mixture is stirred uniformly, then sampling and inspection are carried out, and after the mixture is qualified, 200-mesh filter cloth is used for filtering and discharging.
Experimental example 1
The moisturizing effect test was performed on the moisturizing restoration masks prepared in the above examples 4 to 6 and blank comparative examples 1 to 2.
100 subjects, aged in the range of 20-50 years, 50 females and 50 males. The facial skin moisture content of the subject is within 18-20%, no skin disease allergy history exists, and the skin moisture content meets the volunteer selection standard of the subject. Subjects were randomized into 5 groups of 10 individuals each, each male and female, and the face was selected as the test site.
Each group of 20 subjects was shown in example 4, example 5, example 6, comparative example 1, and comparative example 2.
The test period is 15 days, various indexes are tested by using a skin tester before using a sample and at 5, 10 and 15 days after using the sample, a plurality of parts of the face are tested, and an average value is taken as data of the corresponding parts.
Test evaluation results: the evaluation results of the moisturizing effects of examples 4 to 6 and comparative examples 1 to 2 of the present invention are shown in Table 1.
TABLE 1
Group of Before use Day 5 Day 10 Day 15
Example 4 18.55 27.63 31.92 32.70
Example 5 19.61 25.71 31.61 32.08
Example 6 19.52 29.92 34.47 35.16
Comparative example 1 18.90 22.01 23.30 24.15
Comparative example 2 19.59 28.61 32.46 32.80
From the above results, it was found that the mask composition containing saccharide isomer and glyceroglycoside was more excellent in moisturizing effect on the face, and the moisture content of the skin was improved to the highest level in the composition ratio of example 6.
Experimental example 2
The moisturizing restoration masks prepared in the above examples 4 to 6 and blank comparative examples 1 to 2 were subjected to restoration effect test.
100 subjects, aged in the range of 20-50 years, 50 females and 50 males. The skin of the face of the subject has dry itching, erythema and scaling, has no skin disease allergy history and accords with the volunteer selection standard of the subject. Subjects were randomized into 5 groups of 10 individuals each, each male and female, and the face was selected as the test site.
Each group of 20 subjects was shown in example 4, example 5, example 6, comparative example 1, and comparative example 2.
The test cycle was 14 days, and the skin tester was used to test various indexes before and 7 and 14 days after the sample was used, and the dry itching, erythema and scaling parts of the face were tested.
Test evaluation results: the results of evaluating the repair effects of examples 4 to 6 and comparative examples 1 to 2 of the present invention are shown in Table 2.
TABLE 2
From the above results, it was found that the mask composition comprising tetramethylpyrimidine carboxylic acid and hydroxyphenylpropionamide benzoic acid was excellent in the effect of repairing the face, and the skin was quickly repaired, and the most excellent effect was obtained in the composition ratio of example 6.
The beneficial effects of the invention are as follows:
multiple active ingredients are adopted, so that the skin is subjected to multiple moisturizing from inside to outside, and deep repairing is realized, wherein the core ingredients of the long-acting moisturizing are as follows: saccharide isomer and glyceroglycosides, which are the only enantiomer of the glyceroglycosides on the market, are the main active ingredients of the honey Luo Mu which survive in a long-term drought environment, can be produced by salt-tolerant blue-green algae, have natural super-strong vitality and protect organisms from osmotic pressure injury; the collocation of the isomer and the glyceroglycosides has several functions: enhancing cell viability and metabolism, activating regenerative skin cells, accelerating synthesis of type I collagen precursors in aging cells, increasing skin moisture retention, elasticity, smoothness and skin thickness, accelerating wound healing and tissue repair, deeply locking water for more than 24 hours, reversing several phenomena of dry skin: coarse, dull, desquamated, tight, reddish; the core components of deep repair are: tetrahydropyrimidine carboxylic acid and hydroxyphenylpropionamide benzoic acid, which combine several effects: reducing itching of the skin, strengthening skin barrier and helping repair, reducing erythema and skin irritation; visible transition of dry, scaling and rough skin to healthy, moist, smooth and soft skin; long-acting skin hydration, comprehensive pollution resistance and reduction of skin stress caused by blue light.
The above-mentioned embodiments of the present invention are not intended to limit the scope of the present invention, and the embodiments of the present invention are not limited thereto, and all kinds of modifications, substitutions or alterations made to the above-mentioned structures of the present invention according to the above-mentioned general knowledge and conventional means of the art without departing from the basic technical ideas of the present invention shall fall within the scope of the present invention.

Claims (10)

1. The utility model provides a moisturizing restoration facial mask which characterized in that: comprises an A phase component, a B phase component, a C phase component and a D phase component, wherein,
the phase A component comprises the following raw materials: water, butylene glycol, thickening stabilizer, glyceryl polyether-26, allantoin, glycerin, sodium hyaluronate, panthenol;
the phase B component comprises the following raw materials: 1, 2-hexanediol, p-hydroxyacetophenone;
the C phase component comprises the following raw materials: water, tetrahydropyrimidine carboxylic acid, betaine;
the phase D component comprises the following raw materials: triethanolamine, gelai Keyin, demin Shu, and Magnetitum.
2. The moisturizing repair mask of claim 1, wherein:
the phase A component comprises the following raw materials in parts by weight: 70-80 parts of water, 1-10 parts of butanediol, 0.1-0.3 part of thickening stabilizer, 0.1-0.3 part of glycerin polyether-261-5 part of allantoin, 1-10 parts of glycerin, 0.05-0.2 part of sodium hyaluronate and 0.5-2 parts of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.1-1 part of 1, 2-hexanediol and 0.1-1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 1-5 parts of water, 0.5-2 parts of tetrahydropyrimidine carboxylic acid and 0.5-2 parts of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.1-0.3 part of triethanolamine, 0.5-2 parts of Gliocarpin, 0.1-0.5 part of Demin, and 0.5-3 parts of water-locking magnetite.
3. The moisturizing repair mask of claim 2, wherein:
the phase A component comprises the following raw materials in parts by weight: 70 parts of water, 1 part of butanediol, 0.1 part of thickening stabilizer, 0.1 part of glycerin polyether-261 part, 1 part of glycerin, 0.05 part of sodium hyaluronate and 0.5 part of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.1 part of 1, 2-hexanediol and 0.1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 1 part of water, 0.5 part of tetrahydropyrimidine carboxylic acid and 0.5 part of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.1 part of triethanolamine, 0.5 part of Gliocarpin, 0.1 part of Demin and 0.5 part of water-locking magnetite.
4. The moisturizing repair mask of claim 2, wherein:
the phase A component comprises the following raw materials in parts by weight: 80 parts of water, 10 parts of butanediol, 0.3 part of thickening stabilizer, 265 parts of glycerin polyether, 0.3 part of allantoin, 10 parts of glycerin, 0.2 part of sodium hyaluronate and 2 parts of panthenol;
the phase B component comprises the following raw materials in parts by weight: 1 part of 1, 2-hexanediol and 1 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 5 parts of water, 2 parts of tetrahydropyrimidine carboxylic acid and 2 parts of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.3 part of triethanolamine, 2 parts of Gliocarpin, 0.5 part of Demin, and 3 parts of water-locking magnetite.
5. The moisturizing repair mask of claim 2, wherein:
the phase A component comprises the following raw materials in parts by weight: 76.62 parts of water, 5 parts of butanediol, 0.14 part of thickening stabilizer, 263 parts of glycereth-2 parts of allantoin, 5 parts of glycerol, 0.1 part of sodium hyaluronate and 1 part of panthenol;
the phase B component comprises the following raw materials in parts by weight: 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone;
the C phase component comprises the following raw materials in parts by weight: 3 parts of water, 1 part of tetrahydropyrimidine carboxylic acid and 1 part of betaine;
the phase D component comprises the following raw materials in parts by weight: 0.14 part of triethanolamine, 1 part of Gliocarpin, 0.3 part of Demin, and 1.5 parts of water-locking magnetite.
6. The moisturizing repair mask of any one of claims 1-5, wherein: the thickening stabilizer is acrylic ester/C10-30 alkanol acrylic ester cross-linked polymer.
7. The moisturizing repair mask of any one of claims 1-5, wherein: the gliclazide comprises glyceroglycosides, water and 1, 2-pentanediol.
8. The moisturizing repair mask of any one of claims 1-5, wherein: the Desensitive comprises 1, 2-pentanediol, butanediol, hydroxyphenyl propionamide benzoic acid and ascorbyl palmitate.
9. The moisturizing repair mask of any one of claims 1-5, wherein: the water-locking magnetite comprises saccharide isomer, water, citric acid and sodium citrate.
10. The preparation method of the moisturizing and repairing mask is characterized by comprising the following steps of:
sequentially weighing the phase A components, adding into an emulsifying pot, heating to 80-85deg.C, starting a homogenizer, homogenizing for 3-5min, homogenizing and dissolving completely, maintaining the temperature for 20-40min, and vacuum cooling;
when the temperature is reduced to 70 ℃, adding the dissolved phase B which is stirred by a container outside in advance, and stirring uniformly;
when the temperature is reduced to below 38 ℃, all components of the phase C are respectively added, all components of the phase D are respectively added, the mixture is stirred uniformly, then sampling and inspection are carried out, and after the mixture is qualified, filtering and discharging are carried out by using a filter cloth with 150-250 meshes.
CN202310381033.4A 2023-04-11 2023-04-11 Moisturizing and repairing mask and preparation method thereof Active CN116509746B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109044869A (en) * 2018-10-10 2018-12-21 广州雷诺生物科技有限公司 A kind of tender skin moisturizing moisture lock mask
CN111166685A (en) * 2018-10-24 2020-05-19 福建省梦娇兰日用化学品有限公司 A children skin caring cream containing horse oil
CN111249209A (en) * 2020-03-30 2020-06-09 广东芭薇生物科技股份有限公司 Moisturizing repair cream and preparation method thereof
CN111920746A (en) * 2020-06-23 2020-11-13 广州绿人生物科技有限公司 Moisturizing and repairing mask and preparation method thereof
CN112716849A (en) * 2021-01-14 2021-04-30 澳宝化妆品(惠州)有限公司 Anti-chap skin cream containing camellia oleifera extract

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109044869A (en) * 2018-10-10 2018-12-21 广州雷诺生物科技有限公司 A kind of tender skin moisturizing moisture lock mask
CN111166685A (en) * 2018-10-24 2020-05-19 福建省梦娇兰日用化学品有限公司 A children skin caring cream containing horse oil
CN111249209A (en) * 2020-03-30 2020-06-09 广东芭薇生物科技股份有限公司 Moisturizing repair cream and preparation method thereof
CN111920746A (en) * 2020-06-23 2020-11-13 广州绿人生物科技有限公司 Moisturizing and repairing mask and preparation method thereof
CN112716849A (en) * 2021-01-14 2021-04-30 澳宝化妆品(惠州)有限公司 Anti-chap skin cream containing camellia oleifera extract

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