CN116492441A - 一种苗方推拿膏及其制备方法 - Google Patents
一种苗方推拿膏及其制备方法 Download PDFInfo
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- CN116492441A CN116492441A CN202310562190.5A CN202310562190A CN116492441A CN 116492441 A CN116492441 A CN 116492441A CN 202310562190 A CN202310562190 A CN 202310562190A CN 116492441 A CN116492441 A CN 116492441A
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- Medicines Containing Plant Substances (AREA)
Abstract
本发明公开了一种苗方推拿膏，包括以下重量份的原料：金铁锁10‑15份、黑骨藤10份、延胡索3‑6份、透骨草3‑6份、伸筋草3‑6份、乳香3份、没药3份、木瓜3份、红花3份、干姜6‑9份、花椒6‑9份、基质100份、辅料10份和抗氧剂0.1份。制备方法，具体包括以下步骤：(1)称取各原料；(2)将各中药混合打粉；(3)回流提取，倾出过滤；(4)再次回流提取，倾出过滤；(5)合并，与基质混合，加入辅料；(6)加水超声震荡，调整pH值为酸性，加入抗氧剂，再次测定pH值，即得。本发明苗方推拿膏具有温经除湿，散淤定痛的功效，适用于风湿痹痛、颈肩腰腿及关节疼患者，结合推拿手法止痛效果更好。
Description
技术领域
本发明涉及中药技术领域，更具体的说是涉及一种苗方推拿膏及其制备方法。
背景技术
推拿，为一种非药物的自然疗法、物理疗法。通常是指医者运用自己的双手作用于病患的体表、受伤的部位、不适的所在、特定的腧穴、疼痛的地方，具体运用推、拿、按、摩、揉、捏、点、拍等形式多样的手法，以期达到疏通经络、推行气血、扶伤止痛、祛邪扶正、调和阴阳的疗效。为了加强疗效，防止皮肤破损，在施推拿术时通常配用推拿膏(油)作为润滑介质进行按摩。
目前，市场上推拿膏的品牌众多，特别是各类中医养生馆内，推拿膏的种类更加繁多。但是，治疗风湿骨痛的推拿膏质量良莠不齐，迄今为止并无具有影响力的产品。
苗族聚居地终年湿度较大，光照较少，百姓深受寒湿邪气之苦，“风湿关节痛”疾病也频发，自然环境造就了苗族医药在治疗风湿骨痛疾病有独特疗效。
因此，如何开发一种苗方推拿膏是本领域技术人员亟需解决的问题。
发明内容
有鉴于此，本发明的目的在于提供一种苗方推拿膏及其制备方法，以解决现有技术中的不足。
为了实现上述目的，本发明采用如下技术方案：
一种苗方推拿膏，包括以下重量份的原料：金铁锁10-15份、黑骨藤10份、延胡索3-6份、透骨草3-6份、伸筋草3-6份、乳香3份、没药3份、木瓜3份、红花3份、干姜6-9份、花椒6-9份、基质100份、辅料10份和抗氧剂0.1份。
本发明中，
金铁锁，中药名。为石竹科植物金铁锁PsammosilenetunicoidesW.C.WuetCY.Wu的干燥根。秋季采挖，除去外皮和杂质，晒干。味苦、辛，性温。归肝经。祛风除湿，散瘀止痛，解毒消肿。用于风湿痹痛，胃脘冷痛，跌打损伤，外伤出血；外治疮疖，蛇虫咬伤。
黑骨藤，即狭叶蓬莱葛，中药材名。本品为马钱科狭叶蓬莱葛GardneriaangustifoliaWall.，以根入药。功能主治为：利湿祛风，活络健脾。主治劳伤，风湿骨痛。苦，温。利湿祛风，活络健脾。主治劳伤，风湿骨痛。
延胡索，中药名。为罂粟科植物延胡索的干燥块茎。夏初茎叶枯萎时采挖，除去须根，洗净，置沸水中煮至恰无白心时，取出，晒干。生于山地林下，或为栽培。分布河北、山东、江苏、浙江等地。辛、苦，温。归肝、脾经。具有活血，行气，止痛的功效。用于胸胁、脘腹疼痛，胸痹心痛，经闭痛经，产后瘀阻，跌扑肿痛。
透骨草，中药名。为大戟科地构叶属植物地构叶Speranskiatuberculata(Bunge)Baill.的全草。植物地构叶，分布于我国辽宁、吉林、内蒙古、河北、河南、山西、陕西、甘肃、山东、江苏、安徽、四川。味辛，性温。入肝、肾经。具有祛风除湿，舒筋活血，散瘀消肿，解毒止痛之功效。主治风湿痹痛，筋骨挛缩，寒湿脚气，腰部扭伤，瘫痪，闭经，阴囊湿疹，疮疖肿毒。
伸筋草，中药名。为石松科植物石松Lycopodium jaPonicum Thunb.的干燥全草。夏、秋二季茎叶茂盛时采收，除去杂质，晒干。味苦、微辛，性温。肝、脾、肾经。有祛风除湿，舒筋活络的功效。用于关节酸痛，屈伸不利。
乳香，中药名。为橄榄科植物乳香树Boswellia carterii Birdw.及同属植物Boswellia bhaurdajiana Birdw.树皮渗出的树脂。辛、苦，温。归心、肝、脾经。活血行气止痛，消肿生肌。用于胸痹心痛，胃脘疼痛，痛经经闭，产后瘀阻，症瘕腹痛，风湿痹痛，筋脉拘挛，跌打损伤，痈肿疮疡。
没药，中药名。为橄榄科植物地丁树Commiphora myrrha Engl.或哈地丁树Commiphora molmol Engl.的干燥树脂。分为天然没药和胶质没药。分布于索马里、埃塞俄比亚及阿拉伯半岛南部等地。味辛、苦，性平。归心、肝、脾经。具有散瘀定痛，消肿生肌之功效。常用于胸痹心痛，胃脘疼痛，痛经经闭，产后瘀阻，癥瘕腹痛，风湿痹痛，跌打损伤，痈肿疮疡等病症的治疗。
木瓜，中药名。为蔷薇科植物贴梗海棠Chaenomeles speciosa(Sweet)Nakai的干燥近成熟果实。夏、秋二季果实绿黄时采收，置沸水中烫至外皮灰白色，对半纵剖，晒干。味酸，性温。肝、脾经。有舒筋活络，和胃化湿的功效。用于治疗湿痹拘挛，腰膝关节酸重疼痛，暑湿吐泻，转筋挛痛，脚气水肿。
红花，中药名。为菊科植物红花Carthamus tinctorius L.的干燥花。夏季花由黄变红时采摘，阴干或晒干。全国各地广有栽培。味辛，性温。归心、肝经。具有活血通经，散瘀止痛之功效。用于经闭，痛经，恶露不行，症瘕痞块，胸痹心痛，瘀滞腹痛，胸胁刺痛，跌扑损伤，疮疡肿痛。
干姜，中药名。为姜科植物姜Zingiber oj-jicinale Rosc.的干燥根茎。冬季采挖，除去须根和泥沙，晒干或低温干燥。趁鲜切片晒干或低温干燥者称为“干姜片”。味辛，性热。归脾、胃、肾、心、肺经。温中散寒，回阳通脉，温肺化饮。用于脘腹冷痛，呕吐泄泻，肢冷脉微，寒饮喘咳。
花椒，中药名。为芸香科植物青椒ZanthoxylumschinifoliumSieb.etZucc.或花椒ZanthoxylumbungeanumMaxim.的干燥成熟果皮。秋季采收成熟果实，晒干，除去种子和杂质。味辛，性温。归脾、胃、肾经。温中止痛，杀虫止痒。用于脘腹冷痛，呕吐泄泻，虫积腹痛；外用：湿疹，阴痒。
进一步，上述基质包括以下重量份的原料：硬脂酸50份和凡士林50份。
进一步，上述辅料包括以下重量份的原料：甘油9.8份、氮酮0.1份和尼泊金乙酯0.1份。
进一步，上述抗氧剂为亚硫酸氢钠。
一种苗方推拿膏的制备方法，具体包括以下步骤：
(1)按上述苗方推拿膏的重量份数称取各原料；
(2)将金铁锁、黑骨藤、延胡索、透骨草、伸筋草、乳香、没药、木瓜、红花、干姜和花椒混合打粉，得到中药粉末；
(3)先向中药粉末中加入乙醇进行回流提取，然后倾出过滤，分别得到第一次提取液和滤渣；
(4)再向滤渣中加入乙醇进行回流提取，然后倾出过滤，得到第二次提取液；
(5)先将第一次提取液和第二次提取液进行合并，然后与基质进行混合后加热并搅拌均匀，最后加入辅料继续加热并搅拌均匀，得到乳膏；
(6)先向乳膏中加水进行超声震荡至完全溶解，然后调整pH值为酸性，最后加入抗氧剂，再次测定pH值，即得苗方推拿膏。
进一步，上述步骤(3)中，乙醇的质量百分数为75％，加入量为中药粉末重量的10倍量；回流提取的时间为1h。
进一步，上述步骤(4)中，乙醇的质量百分数为75％，加入量为滤渣重量的8倍量；回流提取的时间为1h。
进一步，上述步骤(6)中，乳膏和水的质量体积比为1g:10mL；超声震荡的时间为10min；调整pH值为5-6。
经由上述的技术方案可知，与现有技术相比，本发明的有益效果如下：
1、本发明苗方推拿膏的处方来源于黔东南民间苗医传统用药经验方，结合苗医与中医理论基础，选用当地野生药材，配以现代制药工艺精制而成。当产量大幅度提高后，能够保证野生苗药的供应。
2、本发明苗方推拿膏具有温经除湿，散淤定痛的功效，适用于风湿痹痛、颈肩腰腿及关节疼患者，结合推拿手法止痛效果更好。
具体实施方式
下面对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
实施例1
苗方推拿膏，包括以下重量的原料：金铁锁10g、黑骨藤10g、延胡索3g、透骨草3g、伸筋草3g、乳香3g、没药3g、木瓜3g、红花3g、干姜6g、花椒6g、硬脂酸50g、凡士林50g、甘油9.8g、氮酮0.1g、尼泊金乙酯0.1g和抗氧剂0.1g；
上述苗方推拿膏的制备方法，具体包括以下步骤：
(1)按上述苗方推拿膏的重量称取各原料；
(2)将金铁锁、黑骨藤、延胡索、透骨草、伸筋草、乳香、没药、木瓜、红花、干姜和花椒混合打粉，得到中药粉末；
(3)先向中药粉末中加入10倍重量、质量百分数为75％的乙醇回流提取1h，然后倾出过滤，分别得到第一次提取液和滤渣；
(4)再向滤渣中加入8倍重量质量百分数为75％的乙醇进行回流提取1h，然后倾出过滤，得到第二次提取液；
(5)先将第一次提取液和第二次提取液进行合并，然后与基质一起放入烧杯中进行混合，将烧杯放入恒温水浴锅内用电动恒速搅拌器充分加热并搅拌均匀，最后加入甘油、氮酮和尼泊金乙酯继续加热并搅拌均匀，得到乳膏；
(6)将1g乳膏放入小烧杯中加入10mL蒸馏水，超声震荡10min至完全溶解，用pH试纸测得pH值为5-6，用pH计测得pH值为6.43，最后加入亚硫酸氢钠，用pH计测得pH值为6.17，再次测定pH值，即得苗方推拿膏。
实施例2
苗方推拿膏，包括以下重量的原料：金铁锁12g、黑骨藤10g、延胡索5g、透骨草5g、伸筋草5g、乳香3g、没药3g、木瓜3g、红花3g、干姜8g、花椒8g、硬脂酸50g、凡士林50g、甘油9.8g、氮酮0.1g、尼泊金乙酯0.1g和抗氧剂0.1g；
上述苗方推拿膏的制备方法，具体包括以下步骤：
(1)按上述苗方推拿膏的重量称取各原料；
(2)将金铁锁、黑骨藤、延胡索、透骨草、伸筋草、乳香、没药、木瓜、红花、干姜和花椒混合打粉，得到中药粉末；
(3)先向中药粉末中加入10倍重量、质量百分数为75％的乙醇回流提取1h，然后倾出过滤，分别得到第一次提取液和滤渣；
(4)再向滤渣中加入8倍重量质量百分数为75％的乙醇进行回流提取1h，然后倾出过滤，得到第二次提取液；
(5)先将第一次提取液和第二次提取液进行合并，然后与基质一起放入烧杯中进行混合，将烧杯放入恒温水浴锅内用电动恒速搅拌器充分加热并搅拌均匀，最后加入甘油、氮酮和尼泊金乙酯继续加热并搅拌均匀，得到乳膏；
(6)将1g乳膏放入小烧杯中加入10mL蒸馏水，超声震荡10min至完全溶解，用pH试纸测得pH值为5-6，用pH计测得pH值为6.43，最后加入亚硫酸氢钠，用pH计测得pH值为6.17，再次测定pH值，即得苗方推拿膏。
实施例3
苗方推拿膏，包括以下重量的原料：金铁锁15g、黑骨藤10g、延胡索6g、透骨草6g、伸筋草6g、乳香3g、没药3g、木瓜3g、红花3g、干姜9g、花椒9g、硬脂酸50g、凡士林50g、甘油9.8g、氮酮0.1g、尼泊金乙酯0.1g和抗氧剂0.1g；
上述苗方推拿膏的制备方法，具体包括以下步骤：
(1)按上述苗方推拿膏的重量称取各原料；
(2)将金铁锁、黑骨藤、延胡索、透骨草、伸筋草、乳香、没药、木瓜、红花、干姜和花椒混合打粉，得到中药粉末；
(3)先向中药粉末中加入10倍重量、质量百分数为75％的乙醇回流提取1h，然后倾出过滤，分别得到第一次提取液和滤渣；
(4)再向滤渣中加入8倍重量质量百分数为75％的乙醇进行回流提取1h，然后倾出过滤，得到第二次提取液；
(5)先将第一次提取液和第二次提取液进行合并，然后与基质一起放入烧杯中进行混合，将烧杯放入恒温水浴锅内用电动恒速搅拌器充分加热并搅拌均匀，最后加入甘油、氮酮和尼泊金乙酯继续加热并搅拌均匀，得到乳膏；
(6)将1g乳膏放入小烧杯中加入10mL蒸馏水，超声震荡10min至完全溶解，用pH试纸测得pH值为5-6，用pH计测得pH值为6.43，最后加入亚硫酸氢钠，用pH计测得pH值为6.17，再次测定pH值，即得苗方推拿膏。
性能测试
取实施例2制得的苗方推拿膏，分别用于治疗颈型颈椎病、慢性腰肌劳损、膝骨关节炎和腰背肌筋膜炎等疾病。
各疾病的治疗人数、年龄、性别、治愈人数、缓解人数、无效人数和总有效率如表1所示。
其中，治愈：相应症状完全消失；
缓解：相应症状基本消失；
无效：相应症状没有改善；
总有效率＝(治愈人数+缓解人数)/治疗人数×100％。
表1实施例2苗方推拿膏治疗效果
由表1可知，本发明实施例2制得的苗方推拿膏对颈型颈椎病、慢性腰肌劳损、膝骨关节炎和腰背肌筋膜炎等疾病的总有效率均高达100％。
以上试验说明，本发明苗方推拿膏具有温经除湿，散淤定痛的功效，适用于风湿痹痛、颈肩腰腿及关节疼患者，结合推拿手法止痛效果更好。
对所公开的实施例的上述说明，使本领域专业技术人员能够实现或使用本发明。对这些实施例的多种修改对本领域的专业技术人员来说将是显而易见的，本文中所定义的一般原理可以在不脱离本发明的精神或范围的情况下，在其它实施例中实现。因此，本发明将不会被限制于本文所示的这些实施例，而是要符合与本文所公开的原理和新颖特点相一致的最宽的范围。
Claims (8)
1.一种苗方推拿膏，其特征在于，包括以下重量份的原料：金铁锁10-15份、黑骨藤10份、延胡索3-6份、透骨草3-6份、伸筋草3-6份、乳香3份、没药3份、木瓜3份、红花3份、干姜6-9份、花椒6-9份、基质100份、辅料10份和抗氧剂0.1份。
2.根据权利要求1所述的一种苗方推拿膏，其特征在于，所述基质包括以下重量份的原料：硬脂酸50份和凡士林50份。
3.根据权利要求1所述的一种苗方推拿膏，其特征在于，所述辅料包括以下重量份的原料：甘油9.8份、氮酮0.1份和尼泊金乙酯0.1份。
4.根据权利要求1所述的一种苗方推拿膏，其特征在于，所述抗氧剂为亚硫酸氢钠。
5.一种苗方推拿膏的制备方法，其特征在于，具体包括以下步骤：
(1)按权利要求1-4任一项所述苗方推拿膏的重量份数称取各原料；
(2)将金铁锁、黑骨藤、延胡索、透骨草、伸筋草、乳香、没药、木瓜、红花、干姜和花椒混合打粉，得到中药粉末；
(3)先向中药粉末中加入乙醇进行回流提取，然后倾出过滤，分别得到第一次提取液和滤渣；
(4)再向滤渣中加入乙醇进行回流提取，然后倾出过滤，得到第二次提取液；
(5)先将第一次提取液和第二次提取液进行合并，然后与基质进行混合后加热并搅拌均匀，最后加入辅料继续加热并搅拌均匀，得到乳膏；
(6)先向乳膏中加水进行超声震荡至完全溶解，然后调整pH值为酸性，最后加入抗氧剂，再次测定pH值，即得所述苗方推拿膏。
6.根据权利要求1所述的一种苗方推拿膏的制备方法，其特征在于，步骤(3)中，所述乙醇的质量百分数为75％，加入量为中药粉末重量的10倍量；所述回流提取的时间为1h。
7.根据权利要求1所述的一种苗方推拿膏的制备方法，其特征在于，步骤(4)中，所述乙醇的质量百分数为75％，加入量为滤渣重量的8倍量；所述回流提取的时间为1h。
8.根据权利要求1所述的一种苗方推拿膏的制备方法，其特征在于，步骤(6)中，所述乳膏和水的质量体积比为1g:10mL；所述超声震荡的时间为10min；所述调整pH值为5-6。
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