CN116327618A - 清洗剂 - Google Patents
清洗剂 Download PDFInfo
- Publication number
- CN116327618A CN116327618A CN202211577645.2A CN202211577645A CN116327618A CN 116327618 A CN116327618 A CN 116327618A CN 202211577645 A CN202211577645 A CN 202211577645A CN 116327618 A CN116327618 A CN 116327618A
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- Prior art keywords
- component
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- content
- acid
- cleaning agent
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- 239000012459 cleaning agent Substances 0.000 title claims abstract description 53
- 125000004432 carbon atom Chemical group C* 0.000 claims abstract description 22
- 239000003599 detergent Substances 0.000 claims abstract description 21
- 150000004667 medium chain fatty acids Chemical class 0.000 claims abstract description 17
- 239000002280 amphoteric surfactant Substances 0.000 claims abstract description 15
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 13
- 150000004668 long chain fatty acids Chemical class 0.000 claims abstract description 10
- 239000007787 solid Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000002736 nonionic surfactant Substances 0.000 claims description 9
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 8
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 8
- 239000003906 humectant Substances 0.000 claims description 8
- 239000005639 Lauric acid Substances 0.000 claims description 4
- 235000021314 Palmitic acid Nutrition 0.000 claims description 4
- 235000021355 Stearic acid Nutrition 0.000 claims description 4
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 4
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 4
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 4
- 239000008117 stearic acid Substances 0.000 claims description 4
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 238000005187 foaming Methods 0.000 abstract description 17
- 206010040880 Skin irritation Diseases 0.000 abstract description 14
- 230000036556 skin irritation Effects 0.000 abstract description 14
- 231100000475 skin irritation Toxicity 0.000 abstract description 14
- 239000000203 mixture Substances 0.000 abstract description 6
- -1 fatty acid salt Chemical class 0.000 description 56
- 239000003921 oil Substances 0.000 description 26
- 235000019198 oils Nutrition 0.000 description 26
- 235000014113 dietary fatty acids Nutrition 0.000 description 24
- 239000000194 fatty acid Substances 0.000 description 24
- 229930195729 fatty acid Natural products 0.000 description 24
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 16
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
- 238000011156 evaluation Methods 0.000 description 14
- 239000000843 powder Substances 0.000 description 14
- 210000003491 skin Anatomy 0.000 description 14
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 12
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- 235000011187 glycerol Nutrition 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 239000004166 Lanolin Substances 0.000 description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 7
- 229960003237 betaine Drugs 0.000 description 7
- 239000000284 extract Substances 0.000 description 7
- 235000019388 lanolin Nutrition 0.000 description 7
- 229940039717 lanolin Drugs 0.000 description 7
- 229920000642 polymer Polymers 0.000 description 7
- 235000000346 sugar Nutrition 0.000 description 7
- 239000001993 wax Substances 0.000 description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 239000000049 pigment Substances 0.000 description 6
- 229920001296 polysiloxane Polymers 0.000 description 6
- ALYNCZNDIQEVRV-UHFFFAOYSA-N 4-aminobenzoic acid Chemical compound NC1=CC=C(C(O)=O)C=C1 ALYNCZNDIQEVRV-UHFFFAOYSA-N 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 5
- 239000006096 absorbing agent Substances 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- 230000003833 cell viability Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 239000000839 emulsion Substances 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000004094 surface-active agent Substances 0.000 description 5
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 4
- DSSYKIVIOFKYAU-OIBJUYFYSA-N (S)-camphor Chemical compound C1C[C@]2(C)C(=O)C[C@H]1C2(C)C DSSYKIVIOFKYAU-OIBJUYFYSA-N 0.000 description 4
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 4
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
- 235000001014 amino acid Nutrition 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 4
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 description 4
- 229920002678 cellulose Polymers 0.000 description 4
- 239000001913 cellulose Substances 0.000 description 4
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000010445 mica Substances 0.000 description 4
- 229910052618 mica group Inorganic materials 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 229960004063 propylene glycol Drugs 0.000 description 4
- 239000003760 tallow Substances 0.000 description 4
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 3
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 239000002202 Polyethylene glycol Substances 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
- 229920002472 Starch Polymers 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 description 3
- 239000010495 camellia oil Substances 0.000 description 3
- 235000019864 coconut oil Nutrition 0.000 description 3
- 239000003240 coconut oil Substances 0.000 description 3
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 150000004665 fatty acids Chemical class 0.000 description 3
- 239000006260 foam Substances 0.000 description 3
- MTNDZQHUAFNZQY-UHFFFAOYSA-N imidazoline Chemical compound C1CN=CN1 MTNDZQHUAFNZQY-UHFFFAOYSA-N 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- ZQBAKBUEJOMQEX-UHFFFAOYSA-N phenyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OC1=CC=CC=C1 ZQBAKBUEJOMQEX-UHFFFAOYSA-N 0.000 description 3
- 229920001223 polyethylene glycol Polymers 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 235000010356 sorbitol Nutrition 0.000 description 3
- 239000000600 sorbitol Substances 0.000 description 3
- 239000008107 starch Substances 0.000 description 3
- 235000019698 starch Nutrition 0.000 description 3
- YBJHBAHKTGYVGT-ZKWXMUAHSA-N (+)-Biotin Chemical compound N1C(=O)N[C@@H]2[C@H](CCCCC(=O)O)SC[C@@H]21 YBJHBAHKTGYVGT-ZKWXMUAHSA-N 0.000 description 2
- WQZGKKKJIJFFOK-SVZMEOIVSA-N (+)-Galactose Chemical compound OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-SVZMEOIVSA-N 0.000 description 2
- GHOKWGTUZJEAQD-ZETCQYMHSA-N (D)-(+)-Pantothenic acid Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-ZETCQYMHSA-N 0.000 description 2
- 229940058020 2-amino-2-methyl-1-propanol Drugs 0.000 description 2
- ZPVFWPFBNIEHGJ-UHFFFAOYSA-N 2-octanone Chemical compound CCCCCCC(C)=O ZPVFWPFBNIEHGJ-UHFFFAOYSA-N 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 2
- 229920000178 Acrylic resin Polymers 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 241000416162 Astragalus gummifer Species 0.000 description 2
- ZCTQGTTXIYCGGC-UHFFFAOYSA-N Benzyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OCC1=CC=CC=C1 ZCTQGTTXIYCGGC-UHFFFAOYSA-N 0.000 description 2
- QFOHBWFCKVYLES-UHFFFAOYSA-N Butylparaben Chemical compound CCCCOC(=O)C1=CC=C(O)C=C1 QFOHBWFCKVYLES-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
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- 108010035532 Collagen Proteins 0.000 description 2
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- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 2
- ZAQJHHRNXZUBTE-UHFFFAOYSA-N D-threo-2-Pentulose Natural products OCC(O)C(O)C(=O)CO ZAQJHHRNXZUBTE-UHFFFAOYSA-N 0.000 description 2
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- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 description 2
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Abstract
本发明提供起泡优异、皮肤刺激性低的清洗剂。使用下述清洗剂,其包含:(A)碳数为8以上且12以下的中链脂肪酸、(B)碳数为14以上且22以下的长链脂肪酸、(C)中和剂、以及(D)两性表面活性剂,其中,前述(A)成分和前述(B)成分的总含量相对于前述清洗剂的总量为15.0质量%以上且45.0质量%以下,前述(A)成分的含量相对于前述(A)成分和前述(B)成分的总含量为9.0质量%以上且小于20.0质量%,前述(A)成分的含量相对于前述(D)成分的含量的质量比为3.0以下。
Description
技术领域
本发明涉及清洗剂。更详细而言,涉及皮肤清洗剂。
背景技术
从清洗力、起泡的观点出发,用于洗脸等的清洗剂中通常混配高级脂肪酸盐。进而,除了清洗力、起泡以外,为了改善使用感、保湿性等,还研究了在清洗剂中组合表面活性剂、保湿剂和其他添加剂。
但是,清洗剂中使用的高级脂肪酸盐存在对皮肤的刺激性强这一缺点。针对这样的课题,专利文献1提出了一种糊状清洗剂组合物,其含有(A)磷酸酯系表面活性剂、(B)高级脂肪酸盐、(C)熔点为50℃以上的固体脂。另外,专利文献2提出了一种皮肤清洗剂组合物,其含有(A)表面活性剂和(B)两亲性酯,前述(A)成分的含量为0.025~2重量%。
现有技术文献
专利文献
专利文献1:日本特开平10-183194号公报
专利文献2:日本特开2020-7303号公报
发明内容
但是,在中链脂肪酸盐的含量相对于高级脂肪酸盐整体的比例高的情况下,皮肤刺激性增高。而且,在专利文献1记载的清洗剂中,中链脂肪酸盐(月桂酸盐)的含量相对于高级脂肪酸盐整体的比例高,皮肤刺激性未充分降低。另外,专利文献2记载的清洗剂为液态,以雾状态而非泡沫状态喷出的形态来使用,因而不会起泡。因此,依然要求一种起泡优异、皮肤刺激性低的清洗剂。
本发明人等为了解决上述课题而进行了深入研究,结果发现,通过在清洗剂中同时混配(A)碳数为8以上且12以下的中链脂肪酸、(B)碳数为14以上且22以下的长链脂肪酸、(C)中和剂以及(D)两性表面活性剂,进而调节(A)成分和(B)成分的总含量、(A)成分的含量相对于(A)成分和(B)成分的总含量的比例、以及(A)成分的含量相对于(D)成分的含量的质量比,能够解决上述课题,从而完成了本发明。
根据本发明,提供以下的发明。
[1]一种清洗剂,其包含:
(A)碳数为8以上且12以下的中链脂肪酸、
(B)碳数为14以上且22以下的长链脂肪酸、
(C)中和剂、以及
(D)两性表面活性剂,
其中,前述(A)成分和前述(B)成分的总含量相对于前述清洗剂的总量为15.0质量%以上且45.0质量%以下,
前述(A)成分的含量相对于前述(A)成分和前述(B)成分的总含量为9.0质量%以上且小于20.0质量%,
前述(A)成分的含量相对于前述(D)成分的含量的质量比为3.0以下。
[2]根据[1]所述的清洗剂,其中,所述(A)碳数为8以上且12以下的中链脂肪酸为月桂酸。
[3]根据[1]或[2]所述的清洗剂,其中,(B)碳数为14以上且22以下的长链脂肪酸为选自由肉豆蔻酸、棕榈酸和硬脂酸组成的组中的至少1种。
[4]根据[1]~[3]中任一项所述的清洗剂,其中,前述(A)成分的含量相对于前述(A)成分和前述(B)成分的总含量为9质量%以上且小于20质量%。
[5]根据[1]~[4]中任一项所述的清洗剂,其中,前述(A)成分的含量相对于前述(D)成分的含量的质量比为0.8以上且2.0以下。
[6]根据[1]~[5]中任一项所述的清洗剂,其还包含(E)非离子性表面活性剂。
[7]根据[1]~[6]中任一项所述的清洗剂,其还包含(F)保湿剂。
[8]根据[1]~[7]中任一项所述的清洗剂,其还包含(G)固体油分。
[9]根据[1]~[8]中任一项所述的清洗剂,其为皮肤清洗剂。
根据本发明,可提供起泡优异、皮肤刺激性低的清洗剂。
具体实施方式
[清洗剂]
本发明的清洗剂包含:(A)碳数为8以上且12以下的中链脂肪酸、(B)碳数为14以上且22以下的长链脂肪酸、(C)中和剂、以及(D)两性表面活性剂作为必须成分。进而,根据目的,本发明的清洗剂还可以包含(E)非离子性表面活性剂、(F)保湿剂、(G)固体油分以及其他成分。本发明的清洗剂的起泡优异、皮肤刺激性低。
((A)碳数为8以上且12以下的中链脂肪酸)
作为碳数为8以上且12以下的中链脂肪酸,可以为直链、支链、饱和、不饱和中的任意种。具体而言,作为碳数为8以上且12以下的高级脂肪酸,可举出辛酸、癸酸和月桂酸等。这些之中可以将1种或2种以上组合混配。其中,特别优选混配月桂酸。
((B)碳数为14以上且22以下的长链脂肪酸)
作为碳数为14以上且22以下的中链脂肪酸,可以为直链、支链、饱和、不饱和中的任意种。具体而言,作为碳数为14以上且22以下的高级脂肪酸,可举出肉豆蔻酸、棕榈酸、硬脂酸、油酸、亚油酸、花生酸和山嵛酸等。这些之中可以将1种或2种以上组合混配。其中,特别优选混配选自由肉豆蔻酸、棕榈酸和硬脂酸组成的组中的至少1种。
(A)成分和(B)成分的总含量相对于清洗剂的总量为15.0质量%以上且45.0质量%以下,优选为17.0质量%以上且42.0质量%以下、更优选为20.0质量%以上且40.0质量%以下。
(A)成分的含量相对于(A)成分和(B)成分的总含量为9.0质量%以上且小于20.0质量%,优选为9.5质量%以上且19.0质量%以下、进一步优选为10.0质量%以上且18.0质量%以下。
(A)成分的含量相对于(D)成分的含量的质量比为3.0以下,优选为0.8以上且2.0以下、更优选为0.9以上且1.5以下。
通过使各成分的含量满足上述数值范围,可得到起泡优异、皮肤刺激性低的清洗剂。
((C)中和剂)
作为中和剂,没有特别限定,只要是通常作为脂肪酸皂的材料使用的中和剂就没有特别限定。作为中和剂,例如可举出:氢氧化钾、氢氧化钠等碱金属盐的氢氧化物;氢氧化镁、氢氧化钙等碱土金属的氢氧化物;2-氨基-2-甲基-1-丙醇、单乙醇胺、二乙醇胺、三乙醇胺等烷醇胺;L-精氨酸、赖氨酸、鸟氨酸等碱性氨基酸;氨水、氢氧化铵、碳酸氢钠等。这些之中可以将1种或2种以上组合混配。这些之中,从使在水中的溶解性、清洗效果良好的观点出发,优选为选自氢氧化钠、氢氧化钾、氢氧化钙、氢氧化镁、氢氧化铝、氨水、单乙醇胺、二乙醇胺和三乙醇胺中的1种或2种以上,更优选为选自氢氧化钠、氢氧化钾、氨水、单乙醇胺、二乙醇胺和三乙醇胺中的1种或2种以上。特别优选混配选自氢氧化钠和氢氧化钾中的1种或2种。
上述中链/长链脂肪酸的盐例如通过用中和剂中和中链/长链脂肪酸来制造。但是,通常不会被完全中和,产物也会包含未反应的中链/长链脂肪酸。在本发明中,中链/长链脂肪酸的中和率没有特别限定,优选为60~90摩尔%、更优选为70~85摩尔%。因此,在本发明的清洗剂中,包含优选60~90摩尔%、更优选70~85摩尔%的中链/长链脂肪酸盐与优选10~40摩尔%、更优选15~30摩尔%的中链/长链脂肪酸。中和剂的含量没有特别限定,可以适当调节以达到上述中和率。
((D)两性表面活性剂)
两性表面活性剂没有特别限定,可以使用通常作为清洗剂的材料使用的两性表面活性剂。作为两性表面活性剂,例如可举出:椰油酰胺丙基甜菜碱、烷基甜菜碱、咪唑啉鎓甜菜碱、月桂基二甲基氨基乙酸甜菜碱、酰胺甜菜碱、磺基甜菜碱等甜菜碱系表面活性剂;2-十一烷基-N,N,N-(羟乙基羧甲基)-2-咪唑啉钠、2-椰油酰基-2-咪唑啉鎓氢氧化物-1-羧基乙氧基二钠盐等咪唑啉系两性表面活性剂等。这些之中可以将1种或2种以上组合混配。特别是,其中优选甜菜碱系表面活性剂,优选混配选自由椰油酰胺丙基甜菜碱、烷基甜菜碱和咪唑啉鎓甜菜碱组成的组中的至少1种。
本发明中,不受理论束缚,推测通过在清洗剂中以特定的比例混配中链脂肪酸盐和两性表面活性剂,中链脂肪酸盐与两性表面活性剂形成复合体,由此中链脂肪酸盐难以被细胞摄取,皮肤刺激性降低。
两性表面活性剂的含量相对于清洗剂的总量为1.0质量%以上且10质量%以下,优选为1.5质量%以上且8.0质量%以下、更优选为2.0质量%以上且6.0质量%以下。若两性表面活性剂的含量在上述数值范围内,则可得到起泡优异、皮肤刺激性低的清洗剂。
((E)非离子性表面活性剂)
作为非离子性表面活性剂,没有特别限定,可以使用通常作为清洗剂的材料使用的非离子性表面活性剂。作为非离子性表面活性剂,例如可举出:蔗糖脂肪酸酯、乙二醇脂肪酸酯、聚乙二醇脂肪酸酯、丙二醇脂肪酸酯、聚丙二醇脂肪酸酯、甘油脂肪酸酯、聚甘油脂肪酸酯和山梨糖醇酐脂肪酸酯等脂肪酸酯型非离子性表面活性剂。这些之中可以将1种或2种以上组合混配。
非离子性表面活性剂的含量相对于清洗剂的总量优选为0.1质量%以上且10质量%以下、更优选为1质量%以上且7质量%以下。
((F)保湿剂)
作为保湿剂,没有特别限定,可以使用通常作为清洗剂的材料使用的保湿剂。作为保湿剂,例如可举出:聚乙二醇、丙二醇、一缩二丙二醇、甘油、二甘油、1,3-丁二醇、异戊二醇、丙二醇、1,2-己二醇、木糖醇、山梨糖醇、麦芽糖醇、硫酸软骨素、透明质酸、硫酸粘液素、卡洛宁酸、去端肽胶原、乳酸钠、胆汁酸盐、dl-吡咯烷酮羧酸盐、短链可溶性胶原、二聚甘油(EO)PO加成物、刺梨果提取物、西洋蓍草提取物、草木犀提取物等。这些之中可以将1种或2种以上组合混配。特别是,这些之中,优选混配选自由聚乙二醇、丙二醇、一缩二丙二醇、甘油、二甘油、1,3-丁二醇、木糖醇、山梨糖醇和麦芽糖醇组成的组中的至少1种,更优选混配选自由一缩二丙二醇、甘油和山梨糖醇组成的组中的至少1种。
保湿剂的含量相对于清洗剂的总量优选为1质量%以上且45质量%以下、更优选为10质量%以上且40质量%以下、进一步优选为15质量%以上且35质量%以下。
((G)固体油分)
作为固体油分,没有特别限定,可以使用通常作为清洗剂的材料使用的固体油分。固体油分是指常温(25℃)下为固态或半固态的油分。作为这样的油分,例如可举出:可可脂、椰油、马油、氢化椰油、棕榈油、牛脂、羊油、氢化牛脂、棕榈仁油、猪油、牛骨油、日本蜡仁油、氢化油、牛蹄脂、野漆果蜡、氢化蓖麻油等固体油脂;蜜蜡、小烛树蜡、棉蜡、巴西棕榈蜡、杨梅蜡、虫蜡、鲸蜡、褐煤蜡、米糠蜡、羊毛脂、木棉蜡、乙酰化羊毛脂、甘蔗蜡、羊毛脂酸异丙酯、月桂酸己酯、氢化羊毛脂、霍霍巴蜡、硬质羊毛脂、虫胶蜡、POE羊毛脂醇醚、POE羊毛脂醇乙酸酯、POE胆甾醇醚、POE氢化羊毛脂醇醚等蜡类;聚乙烯蜡、石蜡、地蜡、凡士林、微晶蜡、微结晶蜡(lunacera)等烃系蜡;单硬脂基甘油醚(鲨肝醇)等脂肪酸甘油醚;乙酰甘油酯、甘油三(2-庚基十一烷酸)酯等脂肪酸甘油酯等。这些之中可以将1种或2种以上组合混配。
固体油分的含量相对于清洗剂的总量优选为0.01质量%以上且10质量%以下、更优选为0.1质量%以上且5质量%以下、进一步优选为0.2质量%以上且2质量%以下。
(水)
作为清洗剂中混配的水,没有特别限定,可以使用化妆品、准药品等中使用的水,例如可以使用纯化水、离子交换水、自来水等。
水的含量可以根据除水以外的成分的含量而适当调节。例如,水的含量相对于清洗剂的总量优选为20质量%以上且80质量%以下、更优选为30质量%以上且70质量%以下。
(其他成分)
本发明的清洗剂除了上述成分以外,还可以混配以往公知的清洗剂中所使用的成分。作为其他成分,可举出下述这样的成分。其他成分只要发挥本发明的效果,则可以进一步混配下述成分中的1种或2种以上来制造。
作为粉末成分,例如可举出:无机粉末(例如,滑石、高岭土、云母、绢云母(sericite)、白云母、金云母、合成云母、红云母、黑云母、蛭石、碳酸镁、碳酸钙、硅酸铝、硅酸钡、硅酸钙、硅酸镁、硅酸锶、钨酸金属盐、镁、二氧化硅、沸石、硫酸钡、煅烧硫酸钙(烧石膏)、磷酸钙、氟磷灰石、羟基磷灰石、陶瓷粉、金属皂(例如,肉豆蔻酸锌、棕榈酸钙、硬脂酸铝)、氮化硼等);有机粉末(例如,聚酰胺树脂粉末(尼龙粉末)、聚乙烯粉末、聚甲基丙烯酸甲酯粉末、聚苯乙烯粉末、苯乙烯与丙烯酸的共聚物树脂粉末、苯并胍胺树脂粉末、聚四氟乙烯粉末、纤维素粉末等);无机白色颜料(例如,二氧化钛、氧化锌等);无机红色系颜料(例如,氧化铁(氧化铁红)、钛酸铁等);无机褐色系颜料(例如,γ-氧化铁等);无机黄色系颜料(例如,氧化铁黄、黄土等);无机黑色系颜料(例如,氧化铁黑、低阶氧化钛等);无机紫色系颜料(例如,锰紫、钴紫等);无机绿色系颜料(例如,氧化铬、氢氧化铬、钛酸钴等);无机蓝色系颜料(例如,群青、普鲁士蓝等);珠光颜料(例如,氧化钛被覆云母、氧化钛被覆氯氧化铋、氧化钛被覆滑石、着色氧化钛被覆云母、氯氧化铋、鱼鳞箔等);金属粉末颜料(例如,铝粉、铜粉等);锆、钡或铝色淀等的有机颜料(例如,红色201号、红色202号、红色204号、红色205号、红色220号、红色226号、红色228号、红色405号、橙色203号、橙色204号、黄色205号、黄色401号以及青色404号等有机颜料;红色3号、红色104号、红色106号、红色227号、红色230号、红色401号、红色505号、橙色205号、黄色4号、黄色5号、黄色202号、黄色203号、绿色3号以及蓝色1号等);天然色素(例如,叶绿素、β-胡萝卜素等)等。
液态油分是指室温下为液态的油分。作为这样的油分,例如可举出:鳄梨油、月见草油、山茶油、鳖油、澳洲坚果油、向日葵油、杏仁油、玉米油、貂油、橄榄油、菜籽油、卵黄油、芝麻油、桃仁油、小麦胚芽油、山茶花油、蓖麻油、亚麻籽油、红花油、棉籽油、紫苏子油、大豆油、花生油、茶籽油、椰子油、米糠油、中国桐油、日本桐油、霍霍巴油、胚芽油等液态油脂;辛酸鲸蜡酯、鲸蜡基2-乙基己酸酯、二甲基辛酸己基癸酯、月桂酸乙酯、月桂酸己酯、肉豆蔻酸异丙酯、肉豆蔻酸2-己基癸酯、肉豆蔻酸肉豆蔻酯、肉豆蔻酸辛基十二烷基酯、棕榈酸异丙酯、2-乙基己基棕榈酸酯、棕榈酸2-己基癸酯、棕榈酸2-庚基十一烷基酯、硬脂酸丁酯、硬脂酸异鲸蜡酯、异硬脂酸异鲸蜡酯、油酸癸酯、油酸十二烷基酯、油酸油酯、乳酸肉豆蔻酯、乳酸鲸蜡酯、苹果酸二异硬脂酯、12-羟基硬脂酸胆甾醇酯、蓖麻油脂肪酸甲酯、琥珀酸2-乙基己酯、己二酸二异丁酯、己二酸2-己基癸基酯、己二酸二2-庚基十一烷基酯、癸二酸二异丙酯、癸二酸二-2-乙基己酯、二-2-乙基己酸乙二醇酯、二癸酸新戊二醇酯、二辛酸新戊二醇酯、乙酸甘油酯、二-2-庚基十一烷酸甘油酯、三辛酸甘油酯、三-2-乙基己酸甘油酯、三肉豆蔻酸甘油酯、三异棕榈酸甘油酯、三-2-庚基十一烷酸甘油酯、三-2-乙基己酸三羟甲基丙烷酯、三异硬脂酸三羟甲基丙烷酯、四辛酸季戊四醇酯、四-2-乙基己酸季戊四醇酯等酯油;液体石蜡、角鲨烯、姥鲛烷、聚丁烯等烃油;二甲基聚硅氧烷、甲基苯基聚硅氧烷、二苯基聚硅氧烷等链状聚硅氧烷;八甲基环四硅氧烷、十甲基环五硅氧烷、十二甲基环六硅氧烷等环状聚硅氧烷;氨基改性聚硅氧烷、聚醚改性聚硅氧烷、烷基改性聚硅氧烷、氟改性聚硅氧烷等各种改性聚硅氧烷等硅油。可以使用这些中的1种或组合使用2种以上。
作为天然的水溶性高分子,例如可举出:植物系高分子(例如,阿拉伯胶、黄蓍胶、半乳聚糖、瓜尔胶、角豆胶、刺梧桐树胶、角叉莱胶、果胶、琼脂、榅桲籽(marmelo)、海藻胶(褐藻提取物)、淀粉(大米、玉米、马铃薯、小麦)、甘草酸);微生物系高分子(例如,黄原胶、葡聚糖、琥珀酰聚糖、普鲁兰多糖等);动物系高分子(例如,胶原、酪蛋白、白蛋白、明胶等)等。
作为半合成的水溶性高分子,例如可举出:淀粉系高分子(例如,羧甲基淀粉、甲基羟丙基淀粉等);纤维素系高分子(甲基纤维素、乙基纤维素、甲基羟丙基纤维素、羟乙基纤维素、纤维素硫酸钠、羟丙基纤维素、羧甲基纤维素、羧甲基纤维素钠、结晶纤维素、纤维素粉末等);藻酸系高分子(例如,藻酸钠、藻酸丙二醇酯等)等。
作为紫外线吸收剂,例如可举出:苯甲酸系紫外线吸收剂(例如,对氨基苯甲酸(以下简称为PABA)、PABA单甘油酯、N,N-二丙氧基PABA乙酯、N,N-二乙氧基PABA乙酯、N,N-二甲基PABA乙酯、N,N-二甲基PABA丁酯、N,N-二甲基PABA乙酯等);邻氨基苯甲酸系紫外线吸收剂(例如,高孟基-N-乙酰邻氨基苯甲酸酯等);水杨酸系紫外线吸收剂(例如,水杨酸戊酯、水杨酸薄荷酯、胡莫柳酯、水杨酸辛酯、水杨酸苯酯、水杨酸苄酯、水杨酸对异丙醇苯酯等);肉桂酸系紫外线吸收剂(例如,肉桂酸辛酯、4-异丙基肉桂酸乙酯、2,5-二异丙基肉桂酸甲酯、2,4-二异丙基肉桂酸乙酯、2,4-二异丙基肉桂酸甲酯、对甲氧基肉桂酸丙酯、对甲氧基肉桂酸异丙酯、对甲氧基肉桂酸异戊酯、对甲氧基肉桂酸辛酯(对甲氧基肉桂酸2-乙基己酯)、对甲氧基肉桂酸2-乙氧基乙酯、对甲氧基肉桂酸环己酯、α-氰基-β-苯基肉桂酸乙酯、α-氰基-β-苯基肉桂酸2-乙基己酯、单-2-乙基己酰基-二对甲氧基肉桂酸甘油酯等);二苯甲酮系紫外线吸收剂(例如,2,4-二羟基二苯甲酮、2,2’-二羟基-4-甲氧基二苯甲酮、2,2’-二羟基-4,4’-二甲氧基二苯甲酮、2,2’,4,4’-四羟基二苯甲酮、2-羟基-4-甲氧基二苯甲酮、2-羟基-4-甲氧基-4’-甲基二苯甲酮、2-羟基-4-甲氧基二苯甲酮-5-磺酸盐、4-苯基二苯甲酮、2-乙基己基-4’-苯基-二苯甲酮-2-甲酸酯、2-羟基-4-正辛氧基二苯甲酮、4-羟基-3-羧基二苯甲酮等);3-(4’-甲基亚苄基)-d,l-樟脑、3-亚苄基-d,l-樟脑、2-苯基-5-甲基苯并噁唑、2,2’-羟基-5-甲基苯基苯并三唑、2-(2’-羟基-5’-叔辛基苯基)苯并三唑、2-(2’-羟基-5’-甲基苯基)苯并三唑、二苯并吖嗪、二茴香酰甲烷、4-甲氧基-4’-叔丁基二苯甲酰甲烷、5-(3,3-二甲基-2-亚降冰片基)-3-戊烷-2-酮等。
作为金属离子掩蔽剂,例如可举出:1-羟基乙烷-1,1-二膦酸、1-羟基乙烷-1,1-二膦酸四钠盐、依地酸二钠、依地酸三钠、依地酸四钠、柠檬酸钠、多聚磷酸钠、偏磷酸钠、葡糖酸、磷酸、柠檬酸、抗坏血酸、琥珀酸、依地酸、乙二胺羟乙基三乙酸三钠等。
作为低级醇,例如可举出:乙醇、丙醇、异丙醇、异丁醇、叔丁醇等。
作为单糖,例如可举出:三碳糖(例如,D-甘油醛、二羟基丙酮等);四碳糖(例如,D-赤藓糖、D-赤藓酮糖、D-苏糖、赤藓糖醇等);五碳糖(例如,L-阿拉伯糖、D-木糖、L-来苏糖、D-阿拉伯糖、D-核糖、D-核酮糖、D-木酮糖、L-木酮糖等);六碳糖(例如,D-葡萄糖、D-塔罗糖、D-阿洛酮糖、D-半乳糖、D-果糖、L-半乳糖、L-甘露糖、D-塔格糖等);七碳糖(例如,庚醛糖、庚酮糖等);八碳糖(例如,辛酮糖等);脱氧糖(例如,2-脱氧-D-核糖、6-脱氧-L-半乳糖、6-脱氧-L-甘露糖等);氨基糖(例如,D-葡糖胺、D-半乳糖胺、唾液酸、氨基糖醛酸、胞壁酸等);糖醛酸(例如,D-葡糖醛酸、D-甘露糖醛酸、L-古罗糖醛酸、D-半乳糖醛酸、L-艾杜糖醛酸等)等。
作为低聚糖,例如可举出:蔗糖、龙胆三糖、伞形糖、乳糖、车前三糖(Planteose)、异剪秋罗糖类、α,α-海藻糖、棉子糖、剪秋罗糖类、Umbilicin(3-O-β-D-呋喃半乳糖-D-阿拉伯醇、3-O-β-D-Galactofuranosyl-D-Arabinitol)、水苏糖、毛蕊花糖类等。
作为氨基酸,例如可举出:中性氨基酸(例如,苏氨酸、半胱氨酸等);碱性氨基酸(例如,羟基赖氨酸等)等。另外,作为氨基酸衍生物,例如可举出:酰基肌氨酸钠(月桂酰基肌氨酸钠)、酰基谷氨酸盐、酰基β-丙氨酸钠、谷胱甘肽、吡咯烷酮羧酸等。
作为有机胺,例如可举出:单乙醇胺、二乙醇胺、三乙醇胺、吗啉、三异丙醇胺、2-氨基-2-甲基-1,3-丙二醇、2-氨基-2-甲基-1-丙醇等。
作为高分子乳液,例如可举出:丙烯酸系树脂乳液、聚丙烯酸乙酯乳液、丙烯酸系树脂液、聚丙烯酸烷基酯乳液、聚乙酸乙烯酯树脂乳液、天然橡胶胶乳等。
作为pH调节剂,例如可举出:氢氧化钠、氢氧化钾、乳酸-乳酸钠、柠檬酸-柠檬酸钠、琥珀酸-琥珀酸钠等。
作为维生素类,例如可举出:维生素A、B1、B2、B6、C、E及其衍生物、泛酸及其衍生物、生物素等。
作为抗氧化剂,例如可举出:生育酚类、二丁基羟基甲苯、丁基羟基茴香醚、没食子酸酯类、亚硫酸盐、亚硫酸氢盐等。作为抗氧化助剂,例如可举出:磷酸、柠檬酸、抗坏血酸、马来酸、丙二酸、琥珀酸、富马酸、脑磷脂、六偏磷酸盐(酯)、植酸、乙二胺四乙酸等。
作为其他可混配成分,例如可举出:防腐剂(对羟基苯甲酸乙酯、对羟基苯甲酸丁酯等);消炎剂(例如,甘草酸衍生物、甘草次酸衍生物、水杨酸衍生物、桧木醇、氧化锌、尿囊素等);美白剂(例如,胎盘提取物、草莓虎耳草提取物、熊果苷等);各种提取物(例如,黄柏、黄连、紫草根、芍药、獐牙菜、桦木、鼠尾草、枇杷、胡萝卜、芦荟、欧锦葵叶粉、鸢尾、葡萄、薏苡仁、丝瓜、白花百合鳞茎、番红花、日本川穹根、生姜、小连翘、红芒柄花、大蒜、辣椒、陈皮、当归、海藻等);活化剂(例如,蜂王浆、光敏剂、胆甾醇衍生物等);血液循环促进剂(例如,壬酸香草酰胺、烟酸苄基酯、烟酸β-丁氧基乙基酯、辣椒素、姜油酮、斑蝥酊、鱼石脂、单宁酸、α-冰片、烟酸生育酚、烟酸肌醇酯、环扁桃酯、桂利嗪、妥拉唑林、乙酰胆碱、维拉帕米、千金藤素、γ-谷维素等);抗脂溢剂(例如,硫、二甲噻蒽等);抗炎剂(例如,氨甲环酸、硫代牛磺酸、亚牛磺酸等)等。
(用途)
本发明的清洗剂可以用于以往公知的清洗用途,特别是可以适合用作皮肤清洗剂。例如,可以以填充于以往公知的清洗剂用泵起泡器的形态来使用。具体而言,适合以洗面奶、沐浴露、洗手液等形态来提供。
实施例
基于以下的例子对本发明进行具体说明,但本发明并不限定于这些例子。只要没有特别说明,混配量以质量%表示。
[实施例1~4、比较例1~5]
<清洗剂的制备例>
按照表1所示的配方制备各实施例和比较例的清洗剂。需要说明的是,表1中,各成分的混配率为质量%。
<清洗剂的评价>
对如上述制备的清洗剂,按照以下的基准来评价皮肤刺激性和起泡。将评价结果示于表1。
[皮肤刺激性]
(评价方法)
使用各清洗剂,通过依据OECD收录的试验法的试验方法,将各清洗剂添加至人三维培养表皮(Labcyte Epi-model),求出24小时后的细胞存活率。其后,将基准清洗剂(比较例1)的细胞存活率设为100,与各清洗剂的细胞存活率进行比较,从而利用下式算出皮肤负担减轻评分,利用下述评价基准来评价对皮肤的刺激性。皮肤负担减轻评分的值越低,表示皮肤负担越少。
<皮肤负担减轻评分的计算式>
皮肤负担减轻评分=基准清洗剂(比较例1)的细胞存活率/各清洗剂的细胞存活率
<评价基准>
A:皮肤负担减轻评分为1以上且小于30
B:皮肤负担减轻评分为30以上且小于60
C:皮肤负担减轻评分为60以上且小于90
D:皮肤负担减轻评分为90以上且小于110
E:皮肤负担减轻评分为110以上
[起泡]
(评价方法)
让30多岁~40多岁的人接受感官评价的训练,选定3名能够以一定基准进行评价的专业评审员。这3名专业评审员在手中取各清洗剂1.5g并使其起泡,评价起泡的快慢。具体而言,通过下述绝对评价以5个等级进行评价,基于评审员全员的各清洗剂的评价分数总和,算出其平均值,进行判定。若评价结果为A~C评价,则为合格。
<评价分数>
5分:起泡非常快。
4分:起泡快。
3分:起泡稍快。
2分:起泡一般。
1分:起泡慢。
<评价基准>
A:平均分数为4.0分以上
B:平均分数为3.5分以上且小于4.0分
C:平均分数为3.0分以上且小于3.5分
D:平均分数为2.0分以上且小于3.0分
E:平均分数小于2.0分
[表1]
由上述结果可知,本发明的清洗剂起泡优异,皮肤刺激性低。另外,一并考虑比较例的结果可知,在本发明的清洗剂中,通过同时混配(A)碳数为8以上且12以下的中链脂肪酸、(B)碳数为14以上且22以下的长链脂肪酸、(C)中和剂以及(D)两性表面活性剂,进而调节(A)成分和(B)成分的总含量、(A)成分的含量相对于(A)成分和(B)成分的总含量的比例、以及(A)成分的含量相对于(D)成分的含量的质量比,从而实现了优异的效果。
Claims (9)
1.一种清洗剂,其包含:
(A)碳数为8以上且12以下的中链脂肪酸、
(B)碳数为14以上且22以下的长链脂肪酸、
(C)中和剂、以及
(D)两性表面活性剂,
其中,所述(A)成分和所述(B)成分的总含量相对于所述清洗剂的总量为15.0质量%以上且45.0质量%以下,
所述(A)成分的含量相对于所述(A)成分和所述(B)成分的总含量为9.0质量%以上且小于20.0质量%,
所述(A)成分的含量相对于所述(D)成分的含量的质量比为3.0以下。
2.根据权利要求1所述的清洗剂,其中,所述(A)碳数为8以上且12以下的中链脂肪酸为月桂酸。
3.根据权利要求1或2所述的清洗剂,其中,(B)碳数为14以上且22以下的长链脂肪酸为选自由肉豆蔻酸、棕榈酸和硬脂酸组成的组中的至少1种。
4.根据权利要求1或2所述的清洗剂,其中,所述(A)成分的含量相对于所述(A)成分和所述(B)成分的总含量为9.5质量%以上且19.0质量%以下。
5.根据权利要求1或2所述的清洗剂,其中,所述(A)成分的含量相对于所述(D)成分的含量的质量比为0.8以上且2.0以下。
6.根据权利要求1或2所述的清洗剂,其还包含(E)非离子性表面活性剂。
7.根据权利要求1或2所述的清洗剂,其还包含(F)保湿剂。
8.根据权利要求1或2所述的清洗剂,其还包含(G)固体油分。
9.根据权利要求1或2所述的清洗剂,其为皮肤清洗剂。
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