CN116270315A - Transparent makeup removing jelly composition and preparation method thereof - Google Patents
Transparent makeup removing jelly composition and preparation method thereof Download PDFInfo
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- CN116270315A CN116270315A CN202310068477.2A CN202310068477A CN116270315A CN 116270315 A CN116270315 A CN 116270315A CN 202310068477 A CN202310068477 A CN 202310068477A CN 116270315 A CN116270315 A CN 116270315A
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- Prior art keywords
- oil
- liquid
- transparent
- essential oil
- makeup removing
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- 239000000203 mixture Substances 0.000 title claims abstract description 64
- 235000015110 jellies Nutrition 0.000 title claims abstract description 44
- 239000008274 jelly Substances 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 239000003921 oil Substances 0.000 claims abstract description 41
- 235000019198 oils Nutrition 0.000 claims abstract description 41
- 239000000341 volatile oil Substances 0.000 claims abstract description 40
- 239000007788 liquid Substances 0.000 claims abstract description 20
- 229920001577 copolymer Polymers 0.000 claims abstract description 13
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 13
- 239000004359 castor oil Substances 0.000 claims abstract description 12
- 235000019438 castor oil Nutrition 0.000 claims abstract description 12
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims abstract description 12
- 239000007787 solid Substances 0.000 claims abstract description 11
- 239000002562 thickening agent Substances 0.000 claims abstract description 11
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 8
- 239000005058 Isophorone diisocyanate Substances 0.000 claims abstract description 7
- 239000004519 grease Substances 0.000 claims abstract description 7
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 7
- CXMXRPHRNRROMY-UHFFFAOYSA-N n-Decanedioic acid Natural products OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229920002545 silicone oil Polymers 0.000 claims abstract description 5
- 239000008158 vegetable oil Substances 0.000 claims abstract description 5
- 239000004215 Carbon black (E152) Substances 0.000 claims abstract description 4
- 229930195733 hydrocarbon Natural products 0.000 claims abstract description 4
- 150000002430 hydrocarbons Chemical class 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 22
- 238000001816 cooling Methods 0.000 claims description 18
- SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical compound CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 claims description 12
- 241000196324 Embryophyta Species 0.000 claims description 9
- -1 fatty alcohol esters Chemical class 0.000 claims description 9
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 9
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims description 8
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 7
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- 238000007710 freezing Methods 0.000 claims description 6
- 230000008014 freezing Effects 0.000 claims description 6
- 238000004806 packaging method and process Methods 0.000 claims description 6
- 239000000600 sorbitol Substances 0.000 claims description 6
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 5
- OVYMWJFNQQOJBU-UHFFFAOYSA-N 1-octanoyloxypropan-2-yl octanoate Chemical compound CCCCCCCC(=O)OCC(C)OC(=O)CCCCCCC OVYMWJFNQQOJBU-UHFFFAOYSA-N 0.000 claims description 4
- NFIHXTUNNGIYRF-UHFFFAOYSA-N 2-decanoyloxypropyl decanoate Chemical compound CCCCCCCCCC(=O)OCC(C)OC(=O)CCCCCCCCC NFIHXTUNNGIYRF-UHFFFAOYSA-N 0.000 claims description 4
- 150000002148 esters Chemical class 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000004973 liquid crystal related substance Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000004006 olive oil Substances 0.000 claims description 4
- 235000008390 olive oil Nutrition 0.000 claims description 4
- 235000020238 sunflower seed Nutrition 0.000 claims description 4
- UIVPNOBLHXUKDX-UHFFFAOYSA-N 3,5,5-trimethylhexyl 3,5,5-trimethylhexanoate Chemical compound CC(C)(C)CC(C)CCOC(=O)CC(C)CC(C)(C)C UIVPNOBLHXUKDX-UHFFFAOYSA-N 0.000 claims description 3
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims description 3
- 235000005979 Citrus limon Nutrition 0.000 claims description 3
- 244000131522 Citrus pyriformis Species 0.000 claims description 3
- 244000301850 Cupressus sempervirens Species 0.000 claims description 3
- 240000003553 Leptospermum scoparium Species 0.000 claims description 3
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 3
- 244000246386 Mentha pulegium Species 0.000 claims description 3
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 3
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 3
- 241000220317 Rosa Species 0.000 claims description 3
- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 3
- 229960000541 cetyl alcohol Drugs 0.000 claims description 3
- 235000005687 corn oil Nutrition 0.000 claims description 3
- 239000002285 corn oil Substances 0.000 claims description 3
- 239000008169 grapeseed oil Substances 0.000 claims description 3
- 235000001050 hortel pimenta Nutrition 0.000 claims description 3
- 229940100554 isononyl isononanoate Drugs 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 229940105132 myristate Drugs 0.000 claims description 3
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 3
- 229940032094 squalane Drugs 0.000 claims description 3
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 3
- JNAYPSWVMNJOPQ-UHFFFAOYSA-N 2,3-bis(16-methylheptadecanoyloxy)propyl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCC(C)C)COC(=O)CCCCCCCCCCCCCCC(C)C JNAYPSWVMNJOPQ-UHFFFAOYSA-N 0.000 claims description 2
- 241000218645 Cedrus Species 0.000 claims description 2
- 235000005976 Citrus sinensis Nutrition 0.000 claims description 2
- 240000002319 Citrus sinensis Species 0.000 claims description 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 2
- 244000178870 Lavandula angustifolia Species 0.000 claims description 2
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 2
- 235000018330 Macadamia integrifolia Nutrition 0.000 claims description 2
- 240000000912 Macadamia tetraphylla Species 0.000 claims description 2
- 235000003800 Macadamia tetraphylla Nutrition 0.000 claims description 2
- 235000019082 Osmanthus Nutrition 0.000 claims description 2
- 241000333181 Osmanthus Species 0.000 claims description 2
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000001693 citrus decumana extract Substances 0.000 claims description 2
- 239000003240 coconut oil Substances 0.000 claims description 2
- 235000019864 coconut oil Nutrition 0.000 claims description 2
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 2
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 claims description 2
- 239000000194 fatty acid Substances 0.000 claims description 2
- 229930195729 fatty acid Natural products 0.000 claims description 2
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 claims description 2
- 229940119170 jojoba wax Drugs 0.000 claims description 2
- 239000001102 lavandula vera Substances 0.000 claims description 2
- 235000018219 lavender Nutrition 0.000 claims description 2
- 229940057995 liquid paraffin Drugs 0.000 claims description 2
- 239000010466 nut oil Substances 0.000 claims description 2
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 2
- 229920001921 poly-methyl-phenyl-siloxane Polymers 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 abstract description 7
- 238000012360 testing method Methods 0.000 description 32
- 239000006071 cream Substances 0.000 description 23
- 230000000052 comparative effect Effects 0.000 description 18
- 239000002994 raw material Substances 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 230000000694 effects Effects 0.000 description 10
- 239000001993 wax Substances 0.000 description 9
- 239000002537 cosmetic Substances 0.000 description 6
- 230000007794 irritation Effects 0.000 description 6
- 239000007933 dermal patch Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 2
- AGNTUZCMJBTHOG-UHFFFAOYSA-N 3-[3-(2,3-dihydroxypropoxy)-2-hydroxypropoxy]propane-1,2-diol Chemical compound OCC(O)COCC(O)COCC(O)CO AGNTUZCMJBTHOG-UHFFFAOYSA-N 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 210000000245 forearm Anatomy 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 231100000430 skin reaction Toxicity 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- 230000037072 sun protection Effects 0.000 description 2
- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 1
- SFAAOBGYWOUHLU-UHFFFAOYSA-N 2-ethylhexyl hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(CC)CCCC SFAAOBGYWOUHLU-UHFFFAOYSA-N 0.000 description 1
- 239000005635 Caprylic acid (CAS 124-07-2) Substances 0.000 description 1
- 240000000560 Citrus x paradisi Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 235000004443 Ricinus communis Nutrition 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 206010040914 Skin reaction Diseases 0.000 description 1
- BHEOSNUKNHRBNM-UHFFFAOYSA-N Tetramethylsqualene Natural products CC(=C)C(C)CCC(=C)C(C)CCC(C)=CCCC=C(C)CCC(C)C(=C)CCC(C)C(C)=C BHEOSNUKNHRBNM-UHFFFAOYSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000000222 aromatherapy Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 230000002996 emotional effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 210000000887 face Anatomy 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 230000000774 hypoallergenic effect Effects 0.000 description 1
- ASKIVFGGGGIGKH-UHFFFAOYSA-N isostearic acid monoglyceride Natural products CC(C)CCCCCCCCCCCCCCC(=O)OCC(O)CO ASKIVFGGGGIGKH-UHFFFAOYSA-N 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 229940070765 laurate Drugs 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000004200 microcrystalline wax Substances 0.000 description 1
- 235000019808 microcrystalline wax Nutrition 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 229960002446 octanoic acid Drugs 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 230000035483 skin reaction Effects 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 239000000516 sunscreening agent Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention provides a transparent makeup removing jelly composition and a preparation method thereof, wherein the transparent makeup removing jelly composition comprises the following components in percentage by mass: 50-90 parts of liquid grease, 7-30 parts of emulsifying agent, 3-15 parts of thickening agent and 0.1-5 parts of skin care essential oil; wherein the liquid oil comprises natural vegetable oil, synthetic oil, hydrocarbon oil and silicone oil; the emulsifier is one or a combination of a plurality of nonionic surfactants with liquid-state to semi-solid HLB values of 6-10; the thickener is one or two of castor oil/IPDI copolymer, hydrogenated castor oil/sebacic acid copolymer; the skin care essential oil is plant essential oil. The transparent makeup removing jelly composition is strong in makeup removing force, transparent in jelly-like appearance, convenient to carry, free of dropping liquid, free of wax-based components, instant in oil application and free of residual feel of oil film after cleaning.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to a transparent makeup removing jelly composition and a preparation method thereof.
Background
Make-up removal products are a class of cosmetics aimed at removing make-up from the surface of the skin. Make-up removal products, from a safety point of view, cannot bring irritation to the skin, including physical irritation and chemical irritation; from a functional point of view, it is desirable to dissolve the dirt such as oily film formers, toners and oils secreted by the skin; from the convenience point of view, the portable multifunctional medical device is convenient to carry and does not drip when in use; from the viewpoint of usability, the product cannot have obvious oil film feel after use, and is easy to clean and has no residue.
The cosmetic makeup remover mainly comprises makeup remover, makeup remover oil, makeup remover cream and the like. The cleansing water is used for removing light makeup by adding a nonionic surfactant and wiping with the aid of cleansing cotton, has poor cleansing effect on concentrated makeup and is not friendly to sensitive muscles. The cleansing oil has better cleansing effect on the concentrated makeup by using a cleansing mechanism of oil-soluble oil, but has the use problems of inconvenient carrying, difficult quantification during taking, easy dropping and the like. The makeup removing cream system is required to be added with a higher content of wax base so as to achieve paste texture, and the problems of difficulty in pushing away, eye pasting, difficulty in cleaning and the like are caused on the makeup removing using feel due to the existence of wax components, and meanwhile, the appearance of the oil wax base makeup removing cream is white paste, so that the transparent appearance of crystal clear cannot be realized.
Patent CN 111110599A is directed at the thick sense problem and the opaque outward appearance problem that wax component that current makeup removal exists, has innovatively developed a transparent makeup removal cream, mixes with the gel of amino acid system and the gel of nylon system, produces the pasty makeup removal article of transparency, and this kind of transparent makeup removal cream elasticity is good, nevertheless brings new problem: the face mask is difficult to melt, inconvenient to take and use, limited in use, not suitable for being used on the whole face and difficult to popularize.
Therefore, a new makeup removal product needs to be developed, has the characteristics of excellent makeup removal effect, convenience in carrying, easiness in use, no liquid drop, easiness in cleaning, no residue and the like, is transparent in appearance, increases pleasure of consumers in makeup removal, and meets the demands of consumers pursuing the transparent appearance.
Disclosure of Invention
Based on the above problems, the present invention aims to provide a transparent makeup removing jelly composition which solves the problems of the makeup removing preparations and ensures excellent makeup removing effect, and a preparation method thereof.
Aiming at the problems, the following technical scheme is provided: a transparent makeup removing jelly composition comprises the following components in percentage by mass: 50-90 parts of liquid grease, 7-30 parts of emulsifying agent, 3-15 parts of thickening agent and 0.1-5 parts of skin care essential oil; wherein, the liquid crystal display device comprises a liquid crystal display device,
the liquid oil comprises natural vegetable oil, synthetic oil, hydrocarbon oil and silicone oil;
the emulsifier is one or a combination of a plurality of nonionic surfactants with the HLB value of 6-10 from liquid state to semi-solid state, or a combination of the nonionic surfactants with the HLB value of 6-10 from liquid state to semi-solid state and the nonionic surfactants with the HLB value of 12-17 from liquid state to semi-solid state;
the thickener is one or two of castor oil/IPDI copolymer, hydrogenated castor oil/sebacic acid copolymer;
the skin care essential oil is one or more of grapefruit peel oil, lemon essential oil, sweet orange essential oil, cypress essential oil, rose essential oil, tea tree essential oil, lavender essential oil, osmanthus essential oil, peppermint essential oil and cedar essential oil in the plant essential oil.
The invention further provides that the natural vegetable oil and fat is one or more of sunflower seed oil, olive oil, coconut oil, jojoba oil, white pool flower seed oil, corn oil, macadamia nut oil and grape seed oil.
The invention further provides that the synthetic oil ester is one or a combination of a plurality of fatty alcohol esters or fatty acid esters.
The invention further provides that the synthetic oil ester is one or a combination of a plurality of cetyl alcohol ethyl caproate, propylene glycol dicaprylate/dicaprate, isononyl isononanoate, glycerol tri (ethyl caproate), caprylic acid/capric acid triglyceride, pentaerythritol tetra (ethyl caproate), ethylhexyl palmitate and isopropyl palmitate.
The invention further provides a composition of one or more of squalane, C15-19 alkane and liquid paraffin.
The invention further provides that the silicone oil is one or a combination of more than one of polydimethylsiloxane, polymethylphenylsiloxane and cyclopentadimethylsiloxane.
The invention further provides that the liquid-to-semisolid surfactant with the HLB value of 6-10 is one or two of PEG-20 glycerol triisostearate and sorbitol polyether-30 tetraoleate.
The invention further provides that the composition of the liquid-to-semi-solid nonionic surfactant with the HLB value of 6-10 and the liquid-to-semi-solid nonionic surfactant with the HLB value of 12-17 is a composition of sorbitol polyether-30 tetraoleate and PEG-7 caprylic/capric triglyceride, or a composition of PEG-20 triisostearate and PEG-8 triisostearate, or a composition of polyglycerol-6 dicaprate and polyglycerol-10 myristate.
The preparation method of the transparent makeup removing jelly composition comprises the following steps:
(1) Mixing liquid grease and a thickening agent, heating to 88-95 ℃ while stirring, and keeping the temperature, stirring and dissolving until the liquid grease and the thickening agent are completely uniform and transparent to obtain a mixture;
(2) Cooling to 65-75deg.C, sequentially adding emulsifying agent, maintaining temperature, and stirring;
(3) Cooling to 60-65deg.C, sequentially adding plant essential oil, maintaining temperature, and stirring;
(4) Cooling to 50-60deg.C, preserving heat, packaging into corresponding container, standing, and freezing.
The invention has the beneficial effects that:
1, the transparent makeup removing jelly composition adopts a pure oil system aiming at makeup removing water, so that makeup can be easily dissolved, and the makeup removing force is strong;
2, the transparent cleansing jelly composition adopts transparent jelly-like appearance texture aiming at cleansing oil, is convenient to carry and can not drip when being taken;
the transparent makeup removing jelly composition does not contain wax-based components aiming at the property that makeup removing cream is not easy to push away, and the components forming a formula structure have shear-alkene characteristics, are taken by a spoon, are simply rubbed off by hands at the palm, are used for instantly changing oil once being smeared, are used for all faces, are used for dissolving makeup dirt in the face in a looping way, are cleaned by clear water, are emulsified in one second when meeting water, have no oil film feel after being cleaned, and have no residual feel;
4, the transparent makeup removing jelly composition is added with plant essential oil, so that immersive aromatherapy experience is brought during makeup removal, emotional stress is relieved, and the skin is moisturized and nourished.
Detailed Description
The following describes the embodiments of the present invention in further detail with reference to examples. The following examples are illustrative of the invention and are not intended to limit the scope of the invention.
Example 1
The embodiment provides a transparent makeup removing jelly composition, which comprises the following components in percentage by mass:
TABLE 1 Components and mass percent content tables for example 1
| Sequence number | Composition of the components | Mass percent% |
| 1 | Caprylic/capric triglyceride | 32 |
| 2 | Propylene glycol dicaprylate/dicaprate | 25 |
| 3 | Sunflower seed oil | 20 |
| 4 | Castor oil/IPDI copolymer | 5 |
| 5 | Hydrogenated castor oil/sebacic acid copolymer | 3 |
| 6 | Sorbitol polyether-30 tetraoleate | 12 |
| 7 | PEG-7 caprylic/capric triglyceride | 2 |
| 8 | Grapefruit essential oil | 0.9 |
| 9 | Peppermint essential oil | 0.1 |
The preparation method of the transparent makeup removing jelly composition comprises the following steps:
(1) Mixing the raw materials with the serial numbers of 1-5 according to the content of the formula, heating to 88-95 ℃ while stirring, and keeping the temperature, stirring and dissolving until the raw materials are completely uniform and transparent;
(2) Cooling to 65-75deg.C, sequentially adding 6,7 # raw materials, maintaining temperature, and stirring;
(3) Cooling to 60-65deg.C, sequentially adding raw materials No. 8 and No. 9, maintaining temperature, and stirring;
(4) Cooling to 50-60deg.C, preserving heat, packaging into corresponding container, standing, and freezing.
Example 2
The embodiment provides a transparent makeup removing jelly composition, which comprises the following components in percentage by mass:
TABLE 2 Components and mass percent content tables for example 2
| Sequence number | Composition of the components | Mass percent% |
| 1 | Cetyl alcohol ethylhexyl ester | 53.5 |
| 2 | Isononyl isononanoate | 25 |
| 3 | Castor oil/IPDI copolymer | 8 |
| 4 | PEG-20 Triglycerol isostearate | 12 |
| 5 | Polyglycerol-10 laurate | 0.5 |
| 6 | Lemon essential oil | 0.8 |
| 7 | Tea tree essential oil | 0.2 |
The preparation method of the transparent makeup removing jelly composition comprises the following steps:
(1) Mixing the raw materials with the serial numbers of 1-3 according to the content of the formula, heating to 88-95 ℃ while stirring, and keeping the temperature, stirring and dissolving until the raw materials are completely uniform and transparent;
(2) Cooling to 65-75deg.C, sequentially adding the materials No. 4 and No. 5, maintaining the temperature, and stirring;
(3) Cooling to 60-65deg.C, sequentially adding 6,7 # raw materials, maintaining temperature, and stirring;
(4) Cooling to 50-60deg.C, preserving heat, packaging into corresponding container, standing, and freezing.
Example 3
The embodiment provides a transparent makeup removing jelly composition, which comprises the following components in percentage by mass:
TABLE 3 Components and mass percent content tables for example 3
| Sequence number | Composition of the components | Mass percent% |
| 1 | Olive oil | 37 |
| 2 | Ethylhexyl palmitate | 25 |
| 3 | Cyclopentadimethicone | 5 |
| 4 | C15-19 alkane | 5 |
| 5 | Castor oil/IPDI copolymer | 4 |
| 6 | Hydrogenated castor oil/sebacic acid copolymer | 2 |
| 7 | PEG-20 Triglycerol isostearate | 12 |
| 8 | PEG-8 Glycerol isostearate | 8 |
| 9 | Rose essential oil | 2 |
The preparation method of the transparent makeup removing jelly composition comprises the following steps:
(1) According to the content of the formula, the raw materials with the serial numbers of 1-6 are mixed and heated to 88-95 ℃ while stirring, and the mixture is stirred and dissolved until the mixture is completely uniform and transparent;
(2) Cooling to 65-75deg.C, sequentially adding raw materials No. 7 and No. 8, maintaining temperature, and stirring;
(3) Cooling to 60-65deg.C, sequentially adding raw material No. 9, maintaining temperature, and stirring;
(4) Cooling to 50-60deg.C, preserving heat, packaging into corresponding container, standing, and freezing.
Example 4
The embodiment provides a transparent makeup removing jelly composition, which comprises the following components in percentage by mass:
TABLE 4 Components and mass percent content tables for example 4
| Sequence number | Composition of the components | Mass percent% |
| 1 | Olive oil | 23 |
| 2 | Corn oil | 20 |
| 3 | Grape seed oil | 15 |
| 4 | Squalane (Squalene) | 10 |
| 5 | Castor oil-IPDI copolymer | 2 |
| 6 | Hydrogenated castor oil/sebacic acid copolymer | 6 |
| 7 | Polyglycerol-6-dicaprate | 15 |
| 8 | Polyglycerol-10 myristate | 4 |
| 9 | Cypress essential oil | 5 |
The preparation method of the transparent makeup removing jelly composition comprises the following steps:
(1) According to the content of the formula, the raw materials with the serial numbers of 1-6 are mixed and heated to 88-95 ℃ while stirring, and the mixture is stirred and dissolved until the mixture is completely uniform and transparent;
(2) Cooling to 65-75deg.C, sequentially adding raw materials No. 7 and No. 8, maintaining temperature, and stirring;
(3) Cooling to 60-65deg.C, sequentially adding raw material No. 9, maintaining temperature, and stirring;
(4) Cooling to 50-60deg.C, preserving heat, packaging into corresponding container, standing, and freezing.
Comparative example
This comparative example provides a cleansing cream, which differs from example 1 in that: 1. the selected thickening agents are different, and the comparative example is thickened by a wax base to form opaque cleansing cream; 2. in the comparative example, essence is added, and in the example 1, plant essential oil is selected. The other operations were the same as in example 1. The cleansing cream comprises the following components in percentage by mass:
TABLE 5 comparative examples of the components and mass percent content tables
| Sequence number | Composition of the components | Mass percent% |
| 1 | Caprylic/capric triglyceride | 34.8 |
| 2 | Propylene glycol dicaprylate/dicaprate | 25 |
| 3 | Sunflower seed oil | 20 |
| 4 | Synthetic wax | 5.5 |
| 5 | Microcrystalline wax | 0.5 |
| 6 | Sorbitol polyether-30 tetraoleate | 12 |
| 7 | PEG-7 caprylic/capric triglyceride | 2 |
| 8 | Essence | 0.2 |
Test examples of Performance test
Test object: the cleansing jelly composition obtained in examples 1 to 4, the cleansing cream obtained in comparative example, one of the commercially available cleansing water samples, and one of the commercially available cleansing oil samples.
1. Stability test
The test is carried out according to the physical and chemical index detection standard of the cleansing liquid (type II) in GB/T35914-2018 cleansing oil (liquid, cream, ointment, cream) GBT 35914-2018. The specific test results are shown in table 6:
table 6 stability test results table
As is clear from Table 6, the cleansing jelly compositions obtained in examples 1 to 4 of the present invention were better in stability.
2. Irritation test
Skin patch test: selecting 175 persons meeting the subject standard, randomly dividing the subjects into 7 groups of 25 persons, and respectively carrying out patch tests on the makeup removing jelly composition obtained in the examples 1-4, the makeup removing cream obtained in the comparative example, the commercial makeup removing water and the commercial makeup removing oil; the makeup removing products in the test objects are respectively placed in the patch tester small chambers, the dosage is about 0.03mL, and no substances are placed in the control holes; applying the patch test with the test object on the back or forearm curved side of the subject with hypoallergenic tape, and applying on skin with palm light pressure for 24 hr; the skin reaction was observed after removing the spot tester for 30min, 24h and 48h, and the observation results were recorded, the classification standard is shown in Table 7, and the test results are shown in Table 8.
TABLE 7 skin Patch test skin response grading criteria
TABLE 8 skin patch test results
As can be seen from Table 8, the cleansing jelly compositions obtained in examples 1 to 4 of the present invention were free from skin irritation, and were superior to two commercially available cleansing samples. As can be seen from the comparison of example 1 and the comparison example, the present invention uses natural plant essential oils, which have significant advantages over the comparison using fragrances.
3. Cleansing ability test
The test process comprises the following steps: selecting 140 testers meeting the test subject standard, and randomly dividing the testers into 7 groups of 20 testers; taking commercially available color cosmetics, respectively including foundation, eye shadow, lipstick and sun cream, and sequentially testing; each product was applied to the forearm (1.25 mg/cm), after waiting for 0.5h, the makeup-removing jelly composition obtained in examples 1 to 4, the makeup-removing cream obtained in comparative examples, and commercially available makeup-removing water and commercially available makeup-removing oil were applied to the makeup-coated portion, and 400mg of each test subject was wiped for 25 seconds, and then rinsed with water; skin brightness values (L) of the test areas before makeup, after makeup and after makeup removal are used for calculating the value of the makeup removing capability S, and the average value is calculated according to the following calculation formula, and the test results of different makeup are shown in tables 9-12.
The calculation formula is as follows: s= (L) After makeup removal -L After makeup )/(L Before making up -L After makeup )，
Wherein: s = cleaning power, L = brightness after washing.
Table 9 results of makeup removing ability test on foundation
| Group of | Mean value of S value |
| Example 1 | 97.5％ |
| Example 2 | 98.9％ |
| Example 3 | 97.2％ |
| Example 4 | 96.8％ |
| Comparative example | 50.5％ |
| Commercially available cleansing water | 94.6％ |
| Commercially available cleansing oil | 62.4％ |
As can be seen from the test results of Table 9, the makeup removing power of the makeup removing jelly compositions obtained in examples 1 to 4 was similar to that of the makeup removing oil sample on the market, but significantly superior to that of the makeup removing cream obtained in comparative example and that of the makeup removing oil sample on the market.
Table 10 results of makeup removing ability test for eye shadow
As can be seen from the test results of Table 10, the makeup removing power of the makeup removing jelly compositions obtained in examples 1 to 4 was significantly better than that of the makeup removing cream obtained in comparative example and that of two commercial makeup removing samples.
Table 11 results of the test for the cleansing effect on lipstick
| Group of | Mean value of S value |
| Example 1 | 95.5％ |
| Example 2 | 94.9％ |
| Example 3 | 96.2％ |
| Example 4 | 95.8％ |
| Comparative example | 55.3％ |
| Commercially available cleansing water | 62.6％ |
| Commercially available cleansing oil | 65.4％ |
As can be seen from the test results of Table 11, the makeup removing power of the makeup removing jelly compositions obtained in examples 1 to 4 on lipstick was significantly better than that of the makeup removing cream obtained in comparative example and two commercial makeup removing samples.
Table 12 results of test for cleansing effect of Sun-block milk
| Group of | Mean value of S value |
| Example 1 | 96.5％ |
| Example 2 | 96.9％ |
| Example 3 | 97.2％ |
| Example 4 | 96.8％ |
| Comparative example | 48.3％ |
| Commercially available cleansing water | 52.6％ |
| Commercially available cleansing oil | 55.4％ |
As can be seen from the test results of Table 12, the makeup removing power of the makeup removing jelly compositions obtained in examples 1 to 4 on the sun block cream was significantly better than that of the makeup removing cream obtained in comparative example and two commercial makeup removing samples.
In conclusion, the makeup removing jelly composition obtained in the embodiments 1 to 4 has strong makeup removing capability on the face, eyes, lips and other parts, and has no irritation to skin.
4. Cleansing use feel test
The test process comprises the following steps: selecting 70 testers meeting the standard of a subject, and randomly dividing the testers into 7 groups of 10 people; the commercial makeup is taken, including foundation, eye shadow, lipstick and sun protection emulsion, facial makeup is carried out according to the application sequence of foundation, eye shadow, lipstick and sun protection emulsion, after waiting for 1h, the makeup removing jelly composition obtained in examples 1-4, the makeup removing cream obtained in comparative example, seven makeup removing products of commercial makeup removing water and commercial makeup removing oil are respectively used for carrying out semi-face makeup removing treatment on each group, each group of testers scores according to the self makeup removing feeling, the score is 10-fraction full-scale, the score is 1-fraction unsatisfactory, and the score is 10-fraction satisfactory. The test dimension is set as: the comprehensive evaluation of appearance happiness, aroma happiness, convenience in taking, spreadability satisfaction, cosmetic dissolving capability satisfaction, cleaning feel satisfaction, residual satisfaction and cosmetic removing effect. The scores of each group were averaged and the results of each group are shown in table 13.
TABLE 13 cleansing use sensory test results
As can be seen from Table 13, the transparent makeup removing jelly compositions prepared in examples 1 to 4 of the present invention were higher in each dimension score, and the makeup removing effect was evaluated in combination to be significantly higher than the makeup removing cream obtained in comparative example and two commercial makeup removing samples. In addition, the cleansing cream obtained in the comparative example has a wax-based thickening effect, so that the cleansing cream is not easy to push out and has residual oil film feel caused by wax, and therefore, the satisfaction score in terms of spreading and cleaning feel is much lower than that of the transparent cleansing jelly compositions prepared in examples 1 to 4 of the present invention.
In conclusion, the transparent makeup removing jelly composition prepared by the invention has the advantages of strong stability, no irritation, convenient use, strong makeup removing capability, easy cleaning and no bad residual film feel. From the sense point of view, the transparent jelly-like texture brings pleasant and purified feeling to the user, the fragrance of the plant essential oil brings therapeutic and healed emotion value to the user, and meanwhile, the plant essential oil has skin nourishing effect and can nourish the skin after long-term lasting use.
The foregoing is merely a preferred embodiment of the present invention, and it should be noted that it will be apparent to those skilled in the art that modifications and variations can be made without departing from the technical principles of the present invention, and these modifications and variations should also be regarded as the scope of the invention.
Claims (9)
1. The transparent makeup removing jelly composition is characterized by comprising the following components in percentage by mass: 50-90 parts of liquid grease, 7-30 parts of emulsifying agent, 3-15 parts of thickening agent and 0.1-5 parts of skin care essential oil; wherein, the liquid crystal display device comprises a liquid crystal display device,
the liquid oil comprises natural vegetable oil, synthetic oil, hydrocarbon oil and silicone oil;
the emulsifier is one or a combination of a plurality of nonionic surfactants with the HLB value of 6-10 from liquid state to semi-solid state, or a combination of the nonionic surfactants with the HLB value of 6-10 from liquid state to semi-solid state and the nonionic surfactants with the HLB value of 12-17 from liquid state to semi-solid state;
the thickener is one or two of castor oil/IPDI copolymer, hydrogenated castor oil/sebacic acid copolymer;
the skin care essential oil is one or more of grapefruit peel oil, lemon essential oil, sweet orange essential oil, cypress essential oil, rose essential oil, tea tree essential oil, lavender essential oil, osmanthus essential oil, peppermint essential oil and cedar essential oil in the plant essential oil.
2. A transparent make-up removal jelly composition as claimed in claim 1, wherein: the natural vegetable oil is one or more of sunflower seed oil, olive oil, coconut oil, jojoba oil, white pool flower seed oil, corn oil, macadamia nut oil and grape seed oil.
3. A transparent make-up removal jelly composition as claimed in claim 1, wherein: the synthetic oil ester is one or a combination of more of fatty alcohol esters or fatty acid esters.
4. A transparent make-up removal jelly composition according to claim 3, characterized in that: the synthetic oil ester is one or more of cetyl alcohol ethyl caproate, propylene glycol dicaprylate/dicaprate, isononyl isononanoate, glycerol tri (ethyl caproate), caprylic/capric triglyceride, pentaerythritol tetra (ethyl caproate), ethylhexyl palmitate and isopropyl palmitate.
5. A transparent make-up removal jelly composition as claimed in claim 1, wherein: the hydrocarbon oil is one or more of squalane, C15-19 alkane and liquid paraffin.
6. A transparent make-up removal jelly composition as claimed in claim 1, wherein: the silicone oil is one or a combination of more of polydimethylsiloxane, polymethylphenylsiloxane and cyclopentadimethylsiloxane.
7. A transparent make-up removal jelly composition as claimed in claim 1, wherein: the liquid-state to semi-solid state nonionic surfactant with HLB value of 6-10 is one or two of PEG-20 glycerol triisostearate and sorbitol polyether-30 tetraoleate.
8. A transparent make-up removal jelly composition as claimed in claim 1, wherein: the composition of the liquid-state to semi-solid state nonionic surfactant with the HLB value of 6-10 and the liquid-state to semi-state nonionic surfactant with the HLB value of 12-17 is a composition of sorbitol polyether-30 tetraoleate and PEG-7 caprylic/capric triglyceride, or a composition of PEG-20 triisostearate and PEG-8 triisostearate, or a composition of polyglycerol-6 dicaprate and polyglycerol-10 myristate.
9. A method of preparing a transparent make-up removal jelly composition according to any one of claims 1 to 7, comprising the steps of:
(1) Mixing liquid grease and a thickening agent, heating to 88-95 ℃ while stirring, and keeping the temperature, stirring and dissolving until the liquid grease and the thickening agent are completely uniform and transparent to obtain a mixture;
(2) Cooling to 65-75deg.C, sequentially adding emulsifying agent, maintaining temperature, and stirring;
(3) Cooling to 60-65deg.C, sequentially adding plant essential oil, maintaining temperature, and stirring;
(4) Cooling to 50-60deg.C, preserving heat, packaging into corresponding container, standing, and freezing.
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| CN114712255A (en) * | 2022-04-11 | 2022-07-08 | 科思嘉(上海)生物科技有限公司 | Moisturizing essence and preparation method thereof |
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| CN114712255A (en) * | 2022-04-11 | 2022-07-08 | 科思嘉(上海)生物科技有限公司 | Moisturizing essence and preparation method thereof |
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