CN114848540A - Double-continuous-phase makeup removing composition for cleaning and tendering skin, makeup removing gel and preparation method of makeup removing composition - Google Patents
Double-continuous-phase makeup removing composition for cleaning and tendering skin, makeup removing gel and preparation method of makeup removing composition Download PDFInfo
- Publication number
- CN114848540A CN114848540A CN202210375814.8A CN202210375814A CN114848540A CN 114848540 A CN114848540 A CN 114848540A CN 202210375814 A CN202210375814 A CN 202210375814A CN 114848540 A CN114848540 A CN 114848540A
- Authority
- CN
- China
- Prior art keywords
- water
- bicontinuous
- makeup removing
- skin
- phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/03—Liquid compositions with two or more distinct layers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Abstract
The invention discloses a double-continuous-phase makeup removing composition with clean and tender skin, makeup removing gel and a preparation method of the makeup removing composition, wherein the double-continuous-phase makeup removing composition with clean and tender skin comprises an emollient, diethoxyethyl succinate, PEG-7 glyceryl cocoate, a surfactant, deionized water, vegetable oil, a water-soluble solvent and other auxiliary materials; the composition has cleaning effect of cleansing oil to make cleansing stronger, and skin feel of cleansing water to make skin refreshing and comfortable; the problems that the existing makeup remover oil is too greasy after makeup removal, the makeup remover water is poor in makeup removal effect, and cleaning is not thorough are solved; and even if the palm has water, the makeup removing effect is not influenced. According to the preparation method of the bicontinuous phase makeup removing composition with the functions of cleaning and tendering skin, the water phase and the oil phase can be bicontinuous through simple control and can stably exist, and the preparation process does not need complex processes and equipment, so that the preparation method is suitable for large-scale production.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a clean and tender skin bicontinuous makeup removing composition, a makeup removing gel and a preparation method of the makeup removing composition.
Background
Along with the development of times, consumers pay more and more attention to makeup, particularly millennium generation pursuit of makeup, so that the market of the makeup cosmetics is gradually increased, makeup removal also becomes a popular product of the cosmetics, and in addition, in recent years, the anti-pollution concept is deep in mind, the deep cleaning requirement is strong, the makeup removal product is deeply dug, and the makeup removal product becomes one of the cosmetics for cleaning and protecting the skin of the consumers at night.
With the increasing requirements of people on makeup removing products, the skin feel is more important, the traditional makeup removing oil has good makeup removing effect, but is too greasy, and the palm has moisture during use, so that the makeup removing effect is reduced. The makeup remover is very fresh, but has poor makeup removing effect. Therefore, the double-continuous-phase cleansing gel which is clean and refreshing, has no greasy skin feel and good cleansing effect and meets the market demand is needed to be developed.
Disclosure of Invention
In order to overcome the defects of the prior art, the first object of the invention is to provide a bicontinuous makeup removing composition with clean and tender skin, the composition has bicontinuous direction, after the heavy makeup of the makeup remover is removed, the skin feel is not greasy, the makeup removing effect is good, the makeup remover is warm and non-irritant, and the makeup removing effect is not influenced because palms are water.
The second purpose of the invention is to provide a preparation method of the bicontinuous phase makeup removing composition with clean and tender skin.
The third purpose of the invention is to provide a bicontinuous phase makeup removing gel with clean and tender skin, which comprises the bicontinuous phase makeup removing composition with clean and tender skin.
One of the purposes of the invention can be achieved by adopting the following technical scheme:
a bicontinuous phase makeup removing composition with clean and tender skin comprises the following components in percentage by mass:
15-25% of an emollient; 1-5% of diethoxyethyl succinate; 5-15% of PEG-7 glycerol cocoate; 10-15% of surfactant; 5-30% of deionized water; 0.5-5% of vegetable oil; 20-35% of water-soluble solvent; 0.31 to 0.85 percent of other auxiliary materials.
Further, the emollient is one or a composition of more than two of ethylhexyl palmitate, cetyl ethyl hexanoate and isononyl isononanoate.
Further, the water-soluble solvent is polyhydric alcohol, and the polyhydric alcohol is one or a combination of more than two of glycerol, dipropylene glycol, propylene glycol, butanediol and 1, 3-propanediol.
Further, the surfactant is one or a composition of more than two of sorbitol polyether-30 tetraoleate, PEG-20 glycerol triisostearate and PEG-8 diisostearate.
Further, the vegetable oil is one or a composition of more than two of sweet almond oil, grape seed oil and olive fruit oil.
Further, the other auxiliary materials comprise essence and preservative;
the essence is at least one of fruit fragrance and flower fragrance, and the mass percentage content of the essence is 0.01-0.5%;
the preservative is at least one of phenoxyethanol and ethylhexyl glycerin, and the preservative accounts for 0.3-0.8% by mass.
The second purpose of the invention can be achieved by adopting the following technical scheme:
a preparation method of a bicontinuous phase makeup removing composition with clean and tender skin comprises the following steps:
step S1, heating, preserving heat and cooling deionized water, adding a water-soluble solvent, diethoxyethyl succinate and PEG-7 glyceryl cocoate, and uniformly stirring to obtain a water phase substance;
and S2, adding the emollient, the surfactant and the vegetable oil into the main pot, uniformly stirring to obtain an oil phase substance, slowly adding the water phase substance obtained in the step S1 into the oil phase substance, and uniformly stirring while keeping the temperature to obtain the clean and tender skin bicontinuous phase makeup removing composition.
Further, in step S1, the heating-maintaining-cooling process includes: heating to 85-95 deg.C, keeping the temperature for 5-15min, and naturally cooling to 40-50 deg.C;
also comprises adding antiseptic when preparing water phase material in step S1, and adding essence when preparing oil phase material in step S2.
The third purpose of the invention can be achieved by adopting the following technical scheme:
a bicontinuous phase makeup removing gel with clean and tender skin comprises the bicontinuous phase makeup removing composition with clean and tender skin.
Further, the bicontinuous phase makeup removing gel with clean and tender skin directly serves as the bicontinuous phase makeup removing gel with clean and tender skin.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention discloses a bicontinuous phase makeup removing composition with clean and tender skin, which comprises a water-soluble organic solvent, hydrophilic skin grease, a hydrophilic oleophilic emollient, an oily emollient, vegetable grease and a surfactant, wherein an oil phase and a water phase are continuous phases, namely the stable existence of the three phases of the water phase, the oil phase and the surfactant in the same system is taken as a coexistent makeup removing system, and both water-soluble components and oil-soluble components in cosmetics can be dissolved by the makeup removing system, so that the makeup removing efficiency is higher compared with that of traditional makeup removing water or makeup removing oil; the cleansing power of the cleansing oil is considered, so that the cleansing is stronger, and the skin feel of the cleansing water makes the skin clean and comfortable; and even if the palm has water, the makeup removing effect is not influenced.
2. According to the preparation method of the bicontinuous phase makeup removing composition with the functions of cleaning and tendering skin, the water phase and the oil phase can be bicontinuous through simple control and can stably exist, and the preparation process does not need complex processes and equipment, so that the preparation method is suitable for large-scale production.
3. The bicontinuous phase makeup removing composition gel with the functions of cleaning and tendering skin can be directly used and can be compounded with other substances; and has the effects of cleansing oil and cleansing water.
Detailed Description
The invention will be further described with reference to specific embodiments:
traditional makeup removing products can be divided into makeup removing oil, makeup removing water, makeup removing cream, makeup removing gel, makeup removing milk and the like according to dosage forms. The more the content of oily substances in the product is, the stronger the makeup removing capability or the makeup removing effect is; the makeup removing ability is from strong to weak as follows: the cleansing lotion, the cleansing cream, the cleansing gel, the cleansing milk and the cleansing water can be removed from common light makeup by using the cleansing water, the cleansing milk or the cleansing gel. Modern color cosmetics generally contain water and oil components, a large amount of grease, powder, solid wax, a film-forming agent and the like, are waterproof and sweat-resistant, and have strong skin-adhering property, so that a plurality of face cleaning products (soap-based face cleaning cream) cannot be thoroughly cleaned, and make-up removing oil and make-up removing cream can be dissolved in oil and can be fused by finger massage, and are emulsified and removed by water during washing, so that the purpose of make-up removal is achieved. However, the cleansing oil or the cleansing cream also has certain disadvantages that the cleansing oil or the cleansing cream is too greasy to use, and the cleansing effect is reduced due to moisture in the palm when the cleansing cream or the cleansing cream is used. Therefore, a makeup removing product which is clean and refreshing, has no greasy skin feel and has good makeup removing effect needs to be developed.
A bicontinuous phase makeup removing composition with clean and tender skin comprises the following components in percentage by mass:
15-25% of an emollient; 1-5% of diethoxyethyl succinate; 5-15% of PEG-7 glycerol cocoate; 10-15% of surfactant; 5-30% of deionized water; 0.5-5% of vegetable oil; 20-35% of water-soluble solvent; 0.31 to 0.85 percent of other auxiliary materials.
Different from the traditional water-in-oil or oil-in-water emulsification structure, the water phase and the oil phase in the bicontinuous phase are respectively continuous, and the emulsifier or the surfactant is distributed on the membrane interface of the water and the oil to form a stable system. When the makeup remover is used for makeup removal, the three components are still in a relative state, wherein the oil phase dissolves the makeup substances, and because of the bicontinuous property of the water phase and the oil phase, the dissolved oily substances in the makeup remover can not enter the water phase, so that the water phase still keeps high water solubility. When the cleansing is carried out by water in the early stage, the compatibility of the water phase and the water for rinsing enables the double-continuous makeup remover product to be rinsed off more easily, so that the dissolved makeup remover can be removed without residual feeling.
In the invention, PEG-7 glyceryl cocoate ester is hydrophilic emollient oil, and diethoxyethyl succinate is hydrophilic lipophilic emollient, so that the emollient effect can be achieved after makeup removal; wherein the water-soluble solvent and water form a water phase, the emollient and the vegetable oil form an oil phase, and the water phase, the oil phase and the surfactant form a stable state under the reuse of the surfactant.
As an embodiment of the present invention, the emollient is one or a combination of two or more of ethylhexyl palmitate, cetyl ethylhexanoate, and isononyl isononanoate.
In one embodiment of the present invention, the water-soluble solvent is a polyhydric alcohol, and the polyhydric alcohol is one or a combination of two or more of glycerin, dipropylene glycol, propylene glycol, butylene glycol, and 1, 3-propanediol.
In one embodiment of the present invention, the surfactant is one or a combination of two or more of sorbitan polyether-30 tetraoleate, PEG-20 glyceryl triisostearate, and PEG-8 diisostearate.
Sorbitol polyether-30 tetraoleate, PEG-20 glyceryl triisostearate and PEG-8 diisostearate are used as surfactants with good performance, and can maintain the stability of the interface of a water phase and an oil phase, so that a bicontinuous phase is stable.
In one embodiment of the present invention, the vegetable oil or fat is one or a combination of two or more of sweet almond oil, grape seed oil, and olive fruit oil.
The vegetable oil is close to the sebum of a human body, has good compatibility with the skin, is easy to be absorbed by the skin, has high nutritive value, can inhibit water evaporation, has relatively moist skin feel and softens the skin, and therefore, can moisten and maintain the skin after makeup removal.
As an embodiment of the present invention, the other adjuvants include essence and preservative;
the essence is at least one of fruit fragrance and flower fragrance, and the mass percentage content of the essence is 0.01-0.5%;
the preservative is at least one of phenoxyethanol and ethylhexyl glycerin, and the preservative accounts for 0.3-0.8% by mass.
A preparation method of a bicontinuous phase makeup removing composition with clean and tender skin comprises the following steps:
step S1, heating, preserving heat and cooling deionized water, adding a water-soluble solvent, diethoxyethyl succinate and PEG-7 glyceryl cocoate, and uniformly stirring to obtain an aqueous phase substance;
and S2, adding the emollient, the surfactant and the vegetable oil into the main pot, uniformly stirring to obtain an oil phase substance, slowly adding the water phase substance obtained in the step S1 into the oil phase substance, and uniformly stirring while keeping the temperature to obtain the clean and tender skin bicontinuous phase makeup removing composition.
In one embodiment of the present invention, in step S1, the heating-keeping-cooling process includes: heating to 85-95 deg.C, keeping the temperature for 5-15min, and naturally cooling to 40-50 deg.C;
also comprises adding antiseptic when preparing water phase material in step S1, and adding essence when preparing oil phase material in step S2.
A bicontinuous phase makeup removing gel with clean and tender skin comprises the bicontinuous phase makeup removing composition with clean and tender skin.
Further, the bicontinuous phase makeup removing gel with clean and tender skin directly serves as the bicontinuous phase makeup removing gel with clean and tender skin.
The invention is further illustrated by the following specific examples.
Example 1:
adding 25.65% of deionized water into a water kettle, heating and stirring to 90 ℃, preserving heat for 10min, cooling to 45 ℃, then adding 28% of water-soluble solvent, 3% of diethoxyethyl succinate, 10% of PEG-7 glyceryl cocoate and 0.6% of preservative into water, and uniformly stirring to obtain a water phase substance; adding 20% of an emollient, 12% of a surfactant, 0.5% of vegetable oil and 0.25% of essence into a main pot, uniformly stirring to obtain an oil phase substance, slowly adding a water phase substance into the oil phase substance, and stirring for 12min at a constant temperature until the mixture is uniformly stirred to obtain the clean and tender bicontinuous phase makeup removing composition; wherein the water-soluble solvent is a mixture of glycerol, butanediol, propylene glycol and the like in mass ratio; the preservative is phenoxyethanol; the emollient is a mixture of ethylhexyl palmitate, cetyl ethyl hexanoate, isononyl isononanoate and the like in a mass ratio; the surfactant is a mixture of sorbitol polyether-30 tetraoleate, PEG-20 glycerol triisostearate and the like in a mass ratio; the vegetable oil is grape seed oil; the essence is one of fruit essence.
Example 2:
adding 26.19% of deionized water into a water kettle, heating and stirring to 85 ℃, preserving heat for 15min, cooling to 40 ℃, then adding 20% of water-soluble solvent, 1% of diethoxyethyl succinate, 15% of PEG-7 glyceryl cocoate and 0.3% of preservative into water, and uniformly stirring to obtain a water phase substance; adding 25% of an emollient, 10% of a surfactant, 2.5% of vegetable oil and fat and 0.01% of essence into a main pot, uniformly stirring to obtain an oil phase substance, slowly adding a water phase substance into the oil phase substance, and stirring for 15min at a constant temperature until the mixture is uniformly stirred to obtain the clean and tender bicontinuous phase makeup removing composition; wherein the water-soluble solvent is dipropylene glycol and butanediol according to the mass ratio of 1: 3; the preservative is a mixture of phenoxyethanol and ethylhexyl glycerol in equal mass ratio; the emollient is ethylhexyl palmitate or isononyl isononanoate according to the mass ratio of 1: 2; the surfactant is a mixture of sorbitol polyether-30 tetraoleate, PEG-8 diisostearate and the like in a mass ratio; the vegetable oil is a mixture of sweet almond oil, olive fruit oil and the like in a mass ratio; the essence is one of flower fragrance essences.
Example 3:
adding 18.7% of deionized water into a water kettle, heating and stirring to 95 ℃, preserving heat for 5min, cooling to 45 ℃, then adding 35% of water-soluble solvent, 5% of diethoxyethyl succinate, 5% of PEG-7 glyceryl cocoate and 0.8% of preservative into water, and uniformly stirring to obtain a water phase substance; adding 15% of an emollient, 15% of a surfactant, 5% of vegetable oil and fat and 0.5% of essence into a main pot, uniformly stirring to obtain an oil phase substance, slowly adding a water phase substance into the oil phase substance, and stirring for 12min at a constant temperature until the mixture is uniformly stirred to obtain the clean and tender bicontinuous phase makeup removing composition; wherein the water-soluble solvent is butanediol; the preservative is ethylhexyl glycerol; the emollient is cetyl ethylhexanoate; the surfactant is PEG-20 glycerol triisostearate; the vegetable oil is olive fruit oil; the essence is one of fruit essence.
Example 4:
adding 15.75% of deionized water into a water kettle, heating and stirring to 87 ℃, preserving heat for 7min, cooling to 42 ℃, then adding 32% of water-soluble solvent, 4% of diethoxyethyl succinate, 12% of PEG-7 glyceryl cocoate and 0.4% of preservative into water, and uniformly stirring to obtain a water phase substance; adding 22% of an emollient, 13.5% of a surfactant, 4% of vegetable oil and fat and 0.35% of essence into a main pot, uniformly stirring to obtain an oil phase substance, slowly adding a water phase substance into the oil phase substance, and stirring for 12min at a constant temperature until the mixture is uniformly stirred to obtain the clean and tender bicontinuous phase makeup removing composition; wherein the water-soluble solvent is a mixture of glycerol, dipropylene glycol and 1, 3-propylene glycol according to the mass ratio of 1:1: 2; the preservative is ethylhexyl glycerol; the emollient is ethylhexyl palmitate; the surfactant is PEG-20 glyceryl triisostearate and PEG-8 diisostearate according to the mass ratio of 1: 5 with a mixture of; the vegetable oil is a mixture of grape seed oil and olive fruit oil according to a mass ratio of 2: 1; the essence is one of flower fragrance essences.
Example 5:
adding 29% of deionized water into a water kettle, heating and stirring to 92 ℃, preserving heat for 7min, cooling to 47 ℃, then adding 24% of water-soluble solvent, 2% of diethoxyethyl succinate, 7.5% of PEG-7 glyceryl cocoate and 0.4% of preservative into the water, and uniformly stirring to obtain a water phase substance; adding 22% of an emollient, 13.5% of a surfactant, 1.5% of vegetable oil and fat and 0.1% of essence into a main pot, uniformly stirring to obtain an oil phase substance, slowly adding a water phase substance into the oil phase substance, and stirring for 12min at a constant temperature until the mixture is uniformly stirred to obtain the clean and tender bicontinuous phase makeup removing composition; wherein the water-soluble solvent is a mixture of glycerol, dipropylene glycol and 1, 3-propylene glycol according to the mass ratio of 1:1: 2; the preservative is ethylhexyl glycerol; the emollient is ethylhexyl palmitate; the surfactant is a mixture of sorbitol polyether-30 tetraoleate, PEG-20 glycerol triisostearate and PEG-8 diisostearate in a mass ratio of 5:1: 2; the vegetable oil is a mixture of grape seed oil and olive fruit oil according to a mass ratio of 2: 1; the essence is one of flower fragrance essences.
Comparative example 1
Comparative example 1 differs from claim 1 in that no surfactant is added.
In a comparative example 2,
comparative example 2 differs from claim 1 in that diethoxyethyl succinate and PEG-7 glyceryl cocoate were not added.
Comparative example 3
Comparative example 3 differs from example 1 in that the water-soluble solvent is ethanol.
Comparative example 4
Comparative example 4 differs from example 1 in that the emollient is 5% and isopropyl myristate is added at 15% by mass.
Comparative example 5
Comparative example 5 differs from example 1 in that the formulation ingredients are added together simultaneously for mix and stir mixing.
Test example 1 stability test
The samples of examples 1 to 5 and comparative examples 1 to 5 were contained in a transparent container, placed between two polarizing plates arranged vertically, and observed whether or not transmitted light passed through the transparent container, and if not, the samples were considered to be isotropic.
None of the compositions of examples 1-5 and comparative example 4 passed a light beam through a transparent container containing the composition, and none of the compositions of comparative examples 1-3 and comparative example 5 passed a light beam through a transparent container containing the composition. Indicating that the absence of surfactant, diethoxyethyl succinate and PEG-7 glyceryl cocoate, polyol, and the manner in which the preparation was an additive material all affected the formation of the bicontinuous phase.
The samples of examples 1 to 5 and comparative examples 1 to 5 were each frozen at-5 ℃ for 1 hour, then returned to normal temperature, and the light-passing properties were re-measured;
samples of examples 1 to 5 and comparative examples 1 to 5 were then separately incubated at 55 ℃ for 1 hour, and then returned to ambient temperature, and the light transmission was re-measured.
By the above temperature change, the compositions of examples 1 to 5 still passed no light beam and showed good cold and hot stability, while the composition of comparative example 4 did not change under cold conditions but passed light beam after heating and showed poor heat stability.
Test example 2 makeup removal effect test
Commercially available cosmetic foundation was applied on white artificial leather of 2cm × 2cm area, then the artificial leather coated with the cosmetic was dried, coated with the compositions of examples 1 to 5 and comparative examples 1 to 5, kept for 5min and rubbed with hand 20 times, then rinsed with an equal amount of water, and then grease residue on the artificial leather was measured with a colorimeter, and the measured elution results are shown in table 1:
TABLE 1 cosmetic removal effect of examples and comparative examples
As can be seen from Table 1, the compositions of examples 1-5 have a good makeup removal effect, almost 98% or more of the makeup base can be removed, and comparative examples 3 and 4 also have a good removal effect, but because the ethanol of comparative example 3 is not a polyhydric alcohol, the bicontinuous phase of the resulting composition is poor in effect, and thus the effects of examples 1-5 are not achieved. The isopropyl myristate of comparative example 4 formed a composition with poor thermal stability and thus poor stability during rubbing, resulting in poor make-up removal. Comparative examples 1-2 and comparative example 5 also have difficulty in obtaining a good removal effect.
Test example 3 safety test
According to the technical Specification for safety of cosmetics, adverse reactions of skin are graded, the skin is detected by a patch test method, and 30 healthy volunteers are selected, wherein the healthy volunteers are 18-24 years old and have no allergic history. The inner forearm of the subject was cleaned, 0.04mL of the sample of example 1 was applied to the filter paper attached to the plaque tester, and the plaque tester was applied to the inner forearm of the subject with a non-irritating adhesive tape for 48 hours for observation. The rating scale is shown in Table 2 and the results are shown in Table 3.
TABLE 2 grading Standard of adverse skin reactions
TABLE 3 Patch adverse reaction results
As can be seen from the adverse reaction results of the patch in Table 3, the adverse reaction probability and the adverse reaction level of the patch added with the composition of the example are both low, and the patch meets the relevant technical Specification for cosmetic safety.
In conclusion, the bicontinuous makeup removing composition with the functions of cleaning and tendering skin, provided by the invention, solves the problems that the existing makeup removing oil is too greasy after makeup removal, the makeup removing water has a poor makeup removing effect, and the cleaning is not complete. When the makeup of the color makeup is removed, the cleansing power of the makeup removing oil is taken into consideration to ensure that the makeup is more powerful, and the skin feel of the makeup removing water ensures that the skin is fresh and comfortable; and even if the palm has water, the makeup removing effect is not influenced.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (10)
1. The bicontinuous phase makeup removing composition with the functions of cleaning and tendering skin is characterized by comprising the following components in percentage by mass:
15-25% of an emollient; 1-5% of diethoxyethyl succinate; 5-15% of PEG-7 glycerol cocoate; 10-15% of surfactant; 5-30% of deionized water; 0.5-5% of vegetable oil; 20-35% of water-soluble solvent; 0.31 to 0.85 percent of other auxiliary materials.
2. The bicontinuous cleansing composition with skin cleaning and tendering effects as defined in claim 1,
the emollient is one or more of ethylhexyl palmitate, cetyl ethyl hexanoate, and isononyl isononanoate.
3. The bicontinuous cleansing composition for skin care according to claim 1,
the water-soluble solvent is polyhydric alcohol, and the polyhydric alcohol is one or a composition of more than two of glycerol, dipropylene glycol, propylene glycol, butanediol and 1, 3-propylene glycol.
4. The bicontinuous cleansing composition for skin care according to claim 1,
the surfactant is one or a composition of more than two of sorbitol polyether-30 tetraoleate, PEG-20 glycerol triisostearate and PEG-8 diisostearate.
5. The bicontinuous cleansing composition for skin care according to claim 1,
the vegetable oil is one or more of sweet almond oil, grape seed oil and olive fruit oil.
6. The bicontinuous cleansing composition for skin care according to claim 1,
the other auxiliary materials comprise essence and preservative;
the essence is at least one of fruit essence and flower essence, and the essence accounts for 0.01-0.5% by mass;
the preservative is at least one of phenoxyethanol and ethylhexyl glycerin, and the preservative accounts for 0.3-0.8% by mass.
7. A preparation method of a bicontinuous phase makeup removing composition with clean and tender skin is characterized by comprising the following steps:
step S1, heating, preserving heat and cooling deionized water, adding a water-soluble solvent, diethoxyethyl succinate and PEG-7 glyceryl cocoate, and uniformly stirring to obtain a water phase substance;
and S2, uniformly stirring the emollient, the surfactant and the vegetable oil to obtain an oil phase substance, slowly adding the water phase substance obtained in the step S1 into the oil phase substance, and uniformly stirring while keeping the temperature to obtain the clean and tender skin bicontinuous phase makeup removing composition.
8. The method for preparing the bicontinuous makeup removing composition with clean and tender skin according to claim 7,
in step S1, the heating-heat-preserving-cooling process includes: heating to 85-95 deg.C, keeping the temperature for 5-15min, and naturally cooling to 40-50 deg.C;
also comprises adding antiseptic when preparing water phase material in step S1, and adding essence when preparing oil phase material in step S2.
9. A bicontinuous makeup removing gel with clean and tender skin, which is characterized by comprising the bicontinuous makeup removing composition with clean and tender skin as defined in any one of claims 1 to 6.
10. The bicontinuous skin rejuvenation cream as claimed in claim 9 wherein said bicontinuous skin rejuvenation composition is applied directly as said bicontinuous skin rejuvenation cream.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210375814.8A CN114848540A (en) | 2022-04-11 | 2022-04-11 | Double-continuous-phase makeup removing composition for cleaning and tendering skin, makeup removing gel and preparation method of makeup removing composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210375814.8A CN114848540A (en) | 2022-04-11 | 2022-04-11 | Double-continuous-phase makeup removing composition for cleaning and tendering skin, makeup removing gel and preparation method of makeup removing composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114848540A true CN114848540A (en) | 2022-08-05 |
Family
ID=82630076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210375814.8A Pending CN114848540A (en) | 2022-04-11 | 2022-04-11 | Double-continuous-phase makeup removing composition for cleaning and tendering skin, makeup removing gel and preparation method of makeup removing composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114848540A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115581631A (en) * | 2022-11-02 | 2023-01-10 | 广州卡迪莲化妆品科技有限公司 | Mild and efficient face cleaning and makeup removing composition and preparation method thereof |
| CN117357407A (en) * | 2023-10-27 | 2024-01-09 | 广州果壳生物科技有限公司 | Soapberry-containing cleaning compound composition and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014152108A (en) * | 2013-02-05 | 2014-08-25 | Asanuma Corporation | Transparent cleansing cosmetic |
| US20210059916A1 (en) * | 2018-03-30 | 2021-03-04 | Amorepacific Corporation | Cosmetic composition for makeup removal comprising water-soluble surfactant and oil-soluble surfactant |
| CN113230170A (en) * | 2021-05-21 | 2021-08-10 | 上海新高姿化妆品有限公司 | Double-continuous-phase cleansing oil with effects of cleaning and nourishing skin and preparation method thereof |
-
2022
- 2022-04-11 CN CN202210375814.8A patent/CN114848540A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014152108A (en) * | 2013-02-05 | 2014-08-25 | Asanuma Corporation | Transparent cleansing cosmetic |
| US20210059916A1 (en) * | 2018-03-30 | 2021-03-04 | Amorepacific Corporation | Cosmetic composition for makeup removal comprising water-soluble surfactant and oil-soluble surfactant |
| CN113230170A (en) * | 2021-05-21 | 2021-08-10 | 上海新高姿化妆品有限公司 | Double-continuous-phase cleansing oil with effects of cleaning and nourishing skin and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 冯年平等: "《中药经皮给药与功效性化妆品》", 中国医药科技出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115581631A (en) * | 2022-11-02 | 2023-01-10 | 广州卡迪莲化妆品科技有限公司 | Mild and efficient face cleaning and makeup removing composition and preparation method thereof |
| CN117357407A (en) * | 2023-10-27 | 2024-01-09 | 广州果壳生物科技有限公司 | Soapberry-containing cleaning compound composition and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4368187A (en) | Sensitive-skin care regime | |
| CN114848540A (en) | Double-continuous-phase makeup removing composition for cleaning and tendering skin, makeup removing gel and preparation method of makeup removing composition | |
| JP2004519482A (en) | Gelled two-phase cosmetic composition | |
| JPH08245367A (en) | Lipid composition for fragrances and cosmetics and its preparation | |
| EP2493447B1 (en) | Human sebum mimetics derived from botanical sources and methods for making the same | |
| JP4335003B2 (en) | Ultrastable composition comprising wasabi oil and its derivatives and uses thereof | |
| CN105434291A (en) | Refreshing and non-greasy type makeup removing paste and preparation method thereof | |
| JP2004500368A (en) | Highly unsaponifiable matter and method of using the same | |
| CN105411993A (en) | Makeup removing cream and preparation method thereof | |
| US7223423B2 (en) | Skin treatment composition | |
| KR102114084B1 (en) | Treatment Cosmetics Composition for Hair and Scalp Care | |
| JP2895607B2 (en) | Transparent skin cosmetics | |
| JPS6127094B2 (en) | ||
| KR102173530B1 (en) | Manufacturing method of cleansing oil | |
| JPH0699275B2 (en) | Non-water cleansing fee | |
| JPS6253910A (en) | Liquid crystal-type oily cosmetic | |
| JPS6335517A (en) | Stabilized clathrate compound and cosmetic containing same | |
| JP3891982B2 (en) | Self-emulsifying oily liquid cosmetic | |
| JPS6026086B2 (en) | cosmetics | |
| JP2001206817A (en) | Oil-in-polyhydric alcohol type thermal substrate | |
| JP3110203B2 (en) | Hair cosmetics with hot feeling | |
| JPH05208905A (en) | Gel composition for skin cleansing | |
| JPH01238518A (en) | Oil-containing composition | |
| JPH07215834A (en) | Cosmetic | |
| CN114983838A (en) | Bicontinuous phase cleansing lotion and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |