CN116270313A - Tea seed oil facial cream and preparation process thereof - Google Patents
Tea seed oil facial cream and preparation process thereof Download PDFInfo
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- CN116270313A CN116270313A CN202211644307.6A CN202211644307A CN116270313A CN 116270313 A CN116270313 A CN 116270313A CN 202211644307 A CN202211644307 A CN 202211644307A CN 116270313 A CN116270313 A CN 116270313A
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- tea seed
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- 239000010495 camellia oil Substances 0.000 title claims abstract description 55
- 239000006071 cream Substances 0.000 title claims abstract description 43
- 230000001815 facial effect Effects 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 238000003756 stirring Methods 0.000 claims abstract description 25
- 239000003921 oil Substances 0.000 claims abstract description 19
- 235000019198 oils Nutrition 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 19
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 18
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000001816 cooling Methods 0.000 claims abstract description 14
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- -1 nicotinamide modified vanillin Chemical class 0.000 claims abstract description 10
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 8
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- 229940015975 1,2-hexanediol Drugs 0.000 claims abstract description 7
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims abstract description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 7
- 239000004166 Lanolin Substances 0.000 claims abstract description 7
- 229960000541 cetyl alcohol Drugs 0.000 claims abstract description 7
- 150000001875 compounds Chemical class 0.000 claims abstract description 7
- 229940075507 glyceryl monostearate Drugs 0.000 claims abstract description 7
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229940039717 lanolin Drugs 0.000 claims abstract description 7
- 235000019388 lanolin Nutrition 0.000 claims abstract description 7
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims abstract description 7
- 229960003966 nicotinamide Drugs 0.000 claims abstract description 7
- 235000005152 nicotinamide Nutrition 0.000 claims abstract description 7
- 239000011570 nicotinamide Substances 0.000 claims abstract description 7
- DFPAKSUCGFBDDF-UHFFFAOYSA-N nicotinic acid amide Natural products NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 claims abstract description 7
- WCVRQHFDJLLWFE-UHFFFAOYSA-N pentane-1,2-diol Chemical compound CCCC(O)CO WCVRQHFDJLLWFE-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 claims abstract description 7
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 7
- 229940068968 polysorbate 80 Drugs 0.000 claims abstract description 7
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 7
- 239000003755 preservative agent Substances 0.000 claims abstract description 7
- 230000002335 preservative effect Effects 0.000 claims abstract description 7
- 229920002545 silicone oil Polymers 0.000 claims abstract description 7
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 7
- 239000011734 sodium Substances 0.000 claims abstract description 7
- 238000010008 shearing Methods 0.000 claims abstract description 6
- 238000007599 discharging Methods 0.000 claims abstract description 4
- OEIJHBUUFURJLI-UHFFFAOYSA-N octane-1,8-diol Chemical compound OCCCCCCCCO OEIJHBUUFURJLI-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000004806 packaging method and process Methods 0.000 claims abstract description 4
- 238000005070 sampling Methods 0.000 claims abstract description 4
- 230000001954 sterilising effect Effects 0.000 claims abstract description 4
- 238000007689 inspection Methods 0.000 claims abstract description 3
- 230000001804 emulsifying effect Effects 0.000 claims description 14
- 235000011187 glycerol Nutrition 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 3
- 230000000694 effects Effects 0.000 abstract description 8
- 238000002156 mixing Methods 0.000 abstract 2
- 229940031723 1,2-octanediol Drugs 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 18
- 230000000052 comparative effect Effects 0.000 description 17
- 239000002537 cosmetic Substances 0.000 description 10
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 9
- 238000002835 absorbance Methods 0.000 description 7
- 239000003205 fragrance Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- 102000003425 Tyrosinase Human genes 0.000 description 6
- 108060008724 Tyrosinase Proteins 0.000 description 6
- 230000005764 inhibitory process Effects 0.000 description 6
- 235000006708 antioxidants Nutrition 0.000 description 5
- 230000003020 moisturizing effect Effects 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical class COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 3
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 239000002199 base oil Substances 0.000 description 2
- 230000006870 function Effects 0.000 description 2
- 238000000338 in vitro Methods 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 1
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 241000209507 Camellia Species 0.000 description 1
- 206010008570 Chloasma Diseases 0.000 description 1
- 208000032544 Cicatrix Diseases 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- AHMIDUVKSGCHAU-UHFFFAOYSA-N Dopaquinone Natural products OC(=O)C(N)CC1=CC(=O)C(=O)C=C1 AHMIDUVKSGCHAU-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- WTDRDQBEARUVNC-LURJTMIESA-N L-DOPA Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C(O)=C1 WTDRDQBEARUVNC-LURJTMIESA-N 0.000 description 1
- AHMIDUVKSGCHAU-LURJTMIESA-N L-dopaquinone Chemical compound [O-]C(=O)[C@@H]([NH3+])CC1=CC(=O)C(=O)C=C1 AHMIDUVKSGCHAU-LURJTMIESA-N 0.000 description 1
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 description 1
- 208000003351 Melanosis Diseases 0.000 description 1
- 206010070834 Sensitisation Diseases 0.000 description 1
- BHEOSNUKNHRBNM-UHFFFAOYSA-N Tetramethylsqualene Natural products CC(=C)C(C)CCC(=C)C(C)CCC(C)=CCCC=C(C)CCC(C)C(=C)CCC(C)C(C)=C BHEOSNUKNHRBNM-UHFFFAOYSA-N 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 235000018597 common camellia Nutrition 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000008099 melanin synthesis Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 description 1
- 235000019645 odor Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 231100000241 scar Toxicity 0.000 description 1
- 230000037387 scars Effects 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000008313 sensitization Effects 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Birds (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses tea seed oil facial cream and a preparation process thereof, comprising the following steps: mixing raw materials of tea seed oil, cetyl alcohol, glyceryl monostearate, lanolin, polysorbate-80 and silicone oil, heating and stirring to obtain oil phase; mixing and stirring raw materials of glycerol, EDTA-2Na, 1, 2-pentanediol, 1, 2-hexanediol, octanediol and deionized water to obtain a water phase; heating the oil phase and the water phase respectively to fully dissolve the raw materials, adding the oil phase into the water phase under the condition of continuous stirring, and simultaneously shearing, homogenizing and cooling; cooling with cold water, maintaining stirring and proper vacuum, raising temperature, adding nicotinamide modified vanillin, sodium antioxidant and GPL compound preservative, stirring to make it uniform, sterilizing, and discharging; then cooling to room temperature, sampling and detecting, packaging after the inspection is qualified, and obtaining tea seed oil facial cream; the skin care effect of the cream is improved, and the stability is higher.
Description
Technical Field
The invention relates to the field of tea seed oil application, in particular to tea seed oil face cream and a preparation process thereof.
Background
The tea seed oil belongs to nondrying oil, is clear and pure in quality, rich in nutrition, fragrant and mellow in taste and extremely strong in palatability, and is high-quality edible oil. Many of the characteristics of tea seed oil are suitable for use in cosmetics. The tea seed oil is natural and mild, has no greasy feeling, has stronger permeability and good affinity with skin, is a good base oil tea seed oil for cosmetics, contains various physiological active substances such as street alcohol, tocopherol, keratene, camellia nutrient and the like, can be used as base oil for cosmetics, can prevent corrosion and sterilize, can balance the secretion of grease, has good heat stability, is not easy to oxidize and deteriorate, and is safe and free of toxic and side effects. According to the ultraviolet absorption experiment on tea seed oil, the tea seed oil has strong absorption on medium wave ultraviolet rays at the wavelength, and is used as a high-quality natural high-grade cosmetic skin care product raw material, and the performance of the tea seed oil is superior to that of the anti-substance oil.
Cosmetics generally refer to daily chemical industry products which are spread on the skin, hair, nails, lips and the like on any part of the surface of a human body by rubbing, spraying or other similar methods to achieve the purposes of cleaning, eliminating bad odors, protecting skin, beautifying and finishing. The industry has long expected that bio-functional cosmetics which use natural substances as main matrixes and integrate modern life science and pharmacology will be the most promising cosmetics and will be the main stream of century cosmetics. Therefore, the natural tea seed oil with a plurality of excellent characteristics is applied to cosmetics and has wide development space.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the tea seed oil facial cream and the preparation process thereof, so as to at least improve the skin care effect of the facial cream and have higher stability.
The aim of the invention is realized by the following technical scheme: a tea seed oil facial cream comprising, in mass fraction:
10-15% of tea seed oil;
3-5% of cetyl alcohol;
4-6% of glyceryl monostearate;
1-3% of lanolin;
2-4% of polysorbate-80;
2-4% of silicone oil;
EDTA-2Na 0.02-0.07％；
1.5-4.5% of 1, 2-pentanediol;
0.3-0.8% of 1, 2-hexanediol;
0.02-0.10% of octyl glycol;
3-5% of glycerol;
50-70% of deionized water;
0.1-0.5% of nicotinamide modified vanillin;
0.1-0.2% of antioxidant sodium acid;
GPL compound preservative 0.05-0.1%.
A preparation process of tea seed oil face cream comprises the following technical steps:
s1, adding 10-15% of raw material tea seed oil, 3-5% of cetyl alcohol, 4-6% of glyceryl monostearate, 1-3% of lanolin, 2-4% of polysorbate-80 and 2-4% of silicone oil into an oil phase pot of an emulsifying pot, stirring, heating, and preserving heat to obtain an oil phase;
s2, adding 3-5% of raw material glycerin, 0.02-0.07% of EDTA-2Na, 1.5-4.5% of 1, 2-pentanediol, 0.3-0.8% of 1, 2-hexanediol, 0.02-0.10% of octanediol and 50-70% of deionized water into a water phase pot of an emulsifying pot, fully stirring until the materials are uniform, heating, and preserving heat to obtain a water phase;
s3, heating the oil phase and the water phase respectively to fully dissolve the raw materials, adding the oil phase into the water phase under the condition of continuous stirring, and simultaneously shearing, homogenizing and cooling;
s4, cooling with cold water, keeping stirring and proper vacuum, raising the temperature in the emulsifying pot, stopping stirring, adding raw materials of 0.1-0.5% of nicotinamide modified vanillin, 0.1-0.2% of antioxidant sodium acid and 0.05-0.1% of GPL compound preservative into the emulsifying pot, stirring to make the raw materials fully uniform, and then sterilizing and discharging;
s5, cooling to room temperature, sampling and detecting, and packaging after the inspection is qualified to obtain the tea seed oil facial cream.
Further, in the step S1, the temperature is raised to 70-80 ℃ and the temperature is kept for 10-20 minutes.
Further, in the step S2, the temperature is raised to 70-80 ℃ and the temperature is kept for 10-20 minutes.
Further, both the oil phase and the water phase are heated to 80 ℃ to 85 ℃.
Further, in the step S3, shearing and homogenizing time is 5min, and cooling to 40-45 ℃.
Further, in the step S5, the temperature of the emulsifying pot is raised to 50 ℃, and the stirring time is 15-25min.
The beneficial effects of the invention are as follows:
(1) The tea seed oil facial cream provided by the invention contains high-component squalene, so that the facial cream has biological oxidation resistance, can prevent ultraviolet rays from damaging skin, nourish skin, strengthen skin resistance, and reduce wrinkles and skin diseases.
(2) The tea seed oil facial cream has the function of scavenging free radicals, can promote the moderate crosslinking of collagen, and can prevent skin from wrinkling and vesicular; in addition, the cream can accelerate the removal of damaged cells and aging cells, and has the function of delaying aging.
(3) The face cream has certain effects on eliminating scars, acne mask, color spots, chloasma and the like on the skin, can accelerate the metabolism of the skin and accelerate the updating speed of the skin; the skin epidermis cells and the new cells are protected, the skin moisture is protected, and the skin moisturizing effect is achieved.
(4) The tea seed oil facial cream provided by the invention is a natural component, and has the advantages of good skin care effect, no toxic or side effect, good safety and no sensitization phenomenon.
(5) The tea seed oil cream reduces the viscosity of tea oil from 64mPas to 49mPas, has good emulsion stability, and does not delaminate at 50 ℃ for 48 hours and at 0 ℃ for 48 hours.
Detailed Description
The technical scheme of the present invention is described in further detail below with reference to examples, but the scope of the present invention is not limited to the following.
Examples
A tea seed oil facial cream comprising, in mass fraction:
10-15% of tea seed oil;
3-5% of cetyl alcohol;
4-6% of glyceryl monostearate;
1-3% of lanolin;
2-4% of polysorbate-80;
2-4% of silicone oil;
EDTA-2Na 0.02-0.07％；
1.5-4.5% of 1, 2-pentanediol;
0.3-0.8% of 1, 2-hexanediol;
0.02-0.10% of octyl glycol;
3-5% of glycerol;
50-70% of deionized water;
0.1-0.5% of nicotinamide modified vanillin;
0.1-0.2% of antioxidant sodium acid;
GPL compound preservative 0.05-0.1%;
which comprises the following steps:
s1, adding 10-15% of raw material tea seed oil, 3-5% of cetyl alcohol, 4-6% of glyceryl monostearate, 1-3% of lanolin, 2-4% of polysorbate-80 and 2-4% of silicone oil into an oil phase pot of an emulsifying pot, stirring, heating to 70-80 ℃, and preserving heat for 10-20 minutes to obtain an oil phase;
s2, adding 3-5% of raw material glycerin, 0.02-0.07% of EDTA-2Na, 1.5-4.5% of 1, 2-pentanediol, 0.3-0.8% of 1, 2-hexanediol, 0.02-0.10% of octanediol and 50-70% of deionized water into a water phase pot of an emulsifying pot, fully stirring uniformly, heating to 70-80 ℃, and preserving heat for 10-20 minutes to obtain a water phase;
s3, heating the oil phase and the water phase to 80-85 ℃ respectively, keeping the temperature to enable the raw materials to be fully dissolved, adding the oil phase into the water phase under continuous stirring, shearing and homogenizing for 5min, and cooling to 40-45 ℃;
s4, cooling with cold water, keeping stirring and proper vacuum, stopping stirring when the temperature in the emulsifying pot reaches 50 ℃, adding raw materials of 0.1-0.5% of nicotinamide modified vanillin, 0.1-0.2% of sodium antioxidant and 0.05-0.1% of GPL compound preservative into the emulsifying pot, stirring for 15-25 minutes to make the raw materials fully uniform, and then sterilizing and discharging;
and S5, cooling to room temperature, sampling and detecting, and packaging after the detection is qualified to obtain the tea seed oil facial cream.
The individual components and the corresponding parts by weight of the tea seed oil creams of examples 1-3 are shown in Table 1.
Table 1: examples 1-3 tea seed oil creams each component and mass fraction thereof
Based on example 1, a comparative example was set, and the composition of the comparative example is shown in table 2.
Table 2: the tea seed oil face cream of comparative examples 1-2 comprises the following components in percentage by mass
The preparation method of comparative examples 1-2 differs from example 1 in that: the nicotinamide-modified vanillin component was replaced or deleted accordingly, with the other steps being the same as in example 1.
(1) Stability test
The testing method comprises the following steps: 2g of the tea seed oil creams prepared in examples 1-3 and comparative examples 1-2 were respectively dripped on fragrance smelling papers; and 20 fragrance smelling staff are selected, the group of fragrance smelling staff can easily distinguish deionized water, acetic acid with the mass concentration of 1% and beta-phenethyl alcohol with the mass concentration of 1%, the fragrance smelling staff can respectively smell and score tea seed oil facial cream on fragrance smelling paper every 1h in rooms with the same temperature and humidity conditions (the score is 0-10, and the score is 10 is the highest), and the average number of each time period is calculated.
Table 3: stability test results
According to Table 3, compared with the comparative example, the tea seed oil cream prepared in the embodiment of the invention still has a certain tea seed oil fragrance after volatilizing for 5 hours, and has good stability, but the fragrance component is volatilized when the comparative example without adding nicotinamide-modified vanillin is in 4-5 hours, so that the effect of stabilizing the tea seed oil component in the formula is demonstrated by the nicotinamide-modified vanillin added in the invention.
(2) Tyrosinase inhibition rate test
The tyrosinase inhibition rate of the tea seed oil cream was determined by an in vitro method [1], with 3 replicates per group. The calculation formula is as follows:
wherein, A1 is the absorbance of the test group, A2 is the absorbance of the control group 1, B1 is the absorbance of the control group 2, and B2 is the absorbance of the control group 3;
the results of the inhibition ratios of tyrosinase for examples 1-3 and comparative examples 1-2 are shown in Table 4 below.
Table 4: inhibition rate of tyrosinase
| Inhibition of tyrosinase (%) | |
| Example 1 | 86.1 |
| Example 2 | 73.5 |
| Example 3 | 69.3 |
| Comparative example 1 | 84.3 |
| Comparative example 2 | 83.6 |
As can be seen from Table 4, compared with the comparative example, the tea seed oil cream prepared in example 1 of the present invention has a higher tyrosinase inhibition rate, and can effectively inhibit tyrosine from forming dopaquinone in dopa and inhibit melanin production.
(3) DPPH clearance test
DPPH clearance of tea seed oil creams was determined by an in vitro method [1], with 3 replicates per group. The calculation formula is as follows:
wherein A0 is the absorbance of the test group, A1 is the absorbance of the comparison group, and A2 is the absorbance of the blank group;
the DPPH clearance results of examples 1 to 3 and comparative examples 1 to 2 are shown in Table 5 below.
Table 5: DPPH clearance rate
| DPPH clearance (%) | |
| Example 1 | 85.3 |
| Example 2 | 71.5 |
| Example 3 | 67.9 |
| Comparative example 1 | 82.1 |
| Comparative example 2 | 81.9 |
As can be seen from Table 5, the tea seed oil cream prepared in example 1 of the present invention has DPPH clearance of up to 85.3% as compared with the comparative example, which is probably because the tea seed oil contains vitamin E and antioxidant components which have a strong DPPH clearance; the effect of the effective substances on DPPH is enhanced, so that the clearance rate of DPPH is improved.
(4) Moisture retention test of creams
Examples 1-3 and comparative examples 1-2 were tested for moisturizing performance in an environment at 22 ℃ and a relative humidity of 60% with reference to the standard QB/T4256-2011 cosmetic moisturizing efficacy evaluation guidelines. The results are shown in Table 6.
Table 6: moisture retention test
As can be seen from Table 5, the tea seed oil cream prepared in example 1 of the present invention had the highest skin moisture content, which was 53.9% at the beginning, 56.1 after 1 hour of application and 51.2% after 8 hours of application, as compared with the comparative example, probably due to the moisture-retaining components such as caprylyl glycol contained in the cream inhibiting the loss of water on the skin surface and increasing the moisture content in the skin.
[1] Zhong Xueyun, tang Saisai A moisturizing facial cream with anti-aging effect [ P ]. Shanghai city: CN114259448A,2022-04-01.
The foregoing is merely a preferred embodiment of the invention, and it is to be understood that the invention is not limited to the form disclosed herein but is not to be construed as excluding other embodiments, but is capable of numerous other combinations, modifications and environments and is capable of modifications within the scope of the inventive concept, either as taught or as a matter of routine skill or knowledge in the relevant art. And that modifications and variations which do not depart from the spirit and scope of the invention are intended to be within the scope of the appended claims.
Claims (7)
1. A tea seed oil facial cream, characterized in that the tea seed oil facial cream comprises, in mass fraction:
10-15% of tea seed oil;
3-5% of cetyl alcohol;
4-6% of glyceryl monostearate;
1-3% of lanolin;
2-4% of polysorbate-80;
2-4% of silicone oil;
EDTA-2Na 0.02-0.07％；
1.5-4.5% of 1, 2-pentanediol;
0.3-0.8% of 1, 2-hexanediol;
0.02-0.10% of octyl glycol;
3-5% of glycerol;
50-70% of deionized water;
0.1-0.5% of nicotinamide modified vanillin;
0.1-0.2% of antioxidant sodium acid;
GPL compound preservative 0.05-0.1%.
2. The preparation process of the tea seed oil facial cream is characterized by comprising the following technical steps of:
s1, adding 10-15% of raw material tea seed oil, 3-5% of cetyl alcohol, 4-6% of glyceryl monostearate, 1-3% of lanolin, 2-4% of polysorbate-80 and 2-4% of silicone oil into an oil phase pot of an emulsifying pot, stirring, heating, and preserving heat to obtain an oil phase;
s2, adding 3-5% of raw material glycerin, 0.02-0.07% of EDTA-2Na, 1.5-4.5% of 1, 2-pentanediol, 0.3-0.8% of 1, 2-hexanediol, 0.02-0.10% of octanediol and 50-70% of deionized water into a water phase pot of an emulsifying pot, fully stirring until the materials are uniform, heating, and preserving heat to obtain a water phase;
s3, heating the oil phase and the water phase respectively to fully dissolve the raw materials, adding the oil phase into the water phase under the condition of continuous stirring, and simultaneously shearing, homogenizing and cooling;
s4, cooling with cold water, keeping stirring and proper vacuum, raising the temperature in the emulsifying pot, stopping stirring, adding raw materials of 0.1-0.5% of nicotinamide modified vanillin, 0.1-0.2% of antioxidant sodium acid and 0.05-0.1% of GPL compound preservative into the emulsifying pot, stirring to make the raw materials fully uniform, and then sterilizing and discharging;
s5, cooling to room temperature, sampling and detecting, and packaging after the inspection is qualified to obtain the tea seed oil facial cream.
3. The process for preparing tea seed oil cream according to claim 2, which is characterized in that: in the step S1, the temperature is raised to 70-80 ℃ and the temperature is kept for 10-20 minutes.
4. The process for preparing tea seed oil cream according to claim 2, which is characterized in that: and in the step S2, the temperature is raised to 70-80 ℃ and the temperature is kept for 10-20 minutes.
5. The process for preparing tea seed oil cream according to claim 2, which is characterized in that: the oil phase and the water phase are heated to 80-85 ℃.
6. The tea seed oil facial cream and the preparation process thereof according to claim 1, wherein: in the step S3, shearing and homogenizing time is 5min, and cooling to 40-45 ℃.
7. The tea seed oil facial cream and the preparation process thereof according to claim 1, wherein: and (5) heating the temperature of the emulsifying pot to 50 ℃ in the step (S5), and stirring for 15-25min.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107496278A (en) * | 2017-10-23 | 2017-12-22 | 合肥卡迪尔化妆品有限公司 | Carnosine snow face frost |
| CN107648088A (en) * | 2017-11-08 | 2018-02-02 | 泉州医学高等专科学校 | A kind of anti-oxidant skin cream and preparation method thereof |
| CN113143798A (en) * | 2021-02-09 | 2021-07-23 | 常山百顺农业开发有限公司 | Tea oil cream and preparation method thereof |
| CN114557922A (en) * | 2022-03-16 | 2022-05-31 | 全芯生物科技(澳门)有限公司 | Rosemary essential oil face cream and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107496278A (en) * | 2017-10-23 | 2017-12-22 | 合肥卡迪尔化妆品有限公司 | Carnosine snow face frost |
| CN107648088A (en) * | 2017-11-08 | 2018-02-02 | 泉州医学高等专科学校 | A kind of anti-oxidant skin cream and preparation method thereof |
| CN113143798A (en) * | 2021-02-09 | 2021-07-23 | 常山百顺农业开发有限公司 | Tea oil cream and preparation method thereof |
| CN114557922A (en) * | 2022-03-16 | 2022-05-31 | 全芯生物科技(澳门)有限公司 | Rosemary essential oil face cream and preparation method thereof |
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