CN1162613A - Process for refining bee propolis - Google Patents
Process for refining bee propolis Download PDFInfo
- Publication number
- CN1162613A CN1162613A CN 96101682 CN96101682A CN1162613A CN 1162613 A CN1162613 A CN 1162613A CN 96101682 CN96101682 CN 96101682 CN 96101682 A CN96101682 A CN 96101682A CN 1162613 A CN1162613 A CN 1162613A
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- China
- Prior art keywords
- honeybee
- refining
- propolis
- purifying
- virgin rubber
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Abstract
A process for purifying raw propolis includes such steps as breaking off, dissolving in 90% alcohol, filtering to remove impurities, purifying to recover alcohol and cooling. The obtained propolis has purity more than 90%.
Description
The present invention relates to a kind of process for refining bee propolis.
Propolis is to be got through purifying by the honeybee virgin rubber, its honeybee virgin rubber is the resin gathered from plant materials of the worker bee of west honeybee kind and the gelatinoid with viscosity of sneaking into formation such as mandibular gland secretory product and beeswax, and it is that honeybee is used for filling up the beehive crack, reinforces honeycomb, polishing lair and be encapsulated into and soak carcase " defence material ".The every group of honeybee approximately can produce the honeybee virgin rubber of 500-1000g but also comprise a certain proportion of impurity every year, as wood chip, earth, sand, weeds etc.Contain the necessary amino acid of human body, trace element such as sugar part etc. in these honeybee virgin rubbers, therefore, for a long time, these honeybee virgin rubbers utilize problem, do not paid attention to by people, just cured or lose as refuse as the recovery honeybee.
It is simple to the purpose of this invention is to provide a kind of technology, the process for refining bee propolis that purification purity is high.
The present invention is a process for refining bee propolis, and its technical process is: the honeybee virgin rubber---pulverizing-dissolving-filtration------cooling---finished product of purifying.The present invention is used for the purification production of honeybee virgin rubber.The main ethanol that adopts honeybee virgin rubber and purity 90% was with 1: 1.5 mixed in this technology, make the dissolving of honeybee virgin rubber, through filtering, elimination impurity, be heated to 55 degree-65 degree with the pot of purifying again, make the ethanol volatilization, reclaim ethanol with vacuum pump, through overcooling, make honeybee virgin rubber be cooled to the propolis finished product through purifying.
The present invention compared with prior art has following distinguishing feature and positively effect.1. technology is reasonable, and is simple to operate.2. the product purity height of being purified; Through the propolis that technical process of the present invention is purified, propolis purity can reach more than 90%.3. output height.Adopt the present invention, honeybee virgin rubber per ton 500 kilograms of propolis of can purifying.4. turn waste into wealth, adopt the present invention, make full use of the natural resource of originally not paid attention to by people.
The present invention is described in further detail below in conjunction with embodiment.
Its technical process is: the honeybee virgin rubber---pulverizes---dissolving-filtration------cooling---finished product of purifying.
1. virgin rubber.The honeybee virgin rubber that buying comes must be that color and luster is black, brown, grey or greyish-green, sap green etc.Purity is high more good more, not obvious contain impurity such as earth, stone, weeds, wood chip solidify the shape colloid.
2. pulverize.Be ground into the blocky shape honeybee virgin rubber that solidifies Powdered with pulverizer.
3. dissolving.It is that 90% ethanol cylinder dissolves that pulverous honeybee virgin rubber is put into purity, and honeybee virgin rubber and alcoholic acid ratio are 1: 1.5.Through stirring, the honeybee virgin rubber is all dissolved, at this moment, it is transparent that lysate is black.
4. filter.At first honeybee virgin rubber lysate is carried out coarse filtration, remove undissolved foreign material, carry out press filtration with 300 orders filter yarn again, remove tiny foreign material with 80 orders filter yarn.The propolis solution of this moment is purified black transparent liquid.
5. purify.Pour the former sol solution of black honeybee into the pot of purifying and be heated to 60 ℃, make the ethanol volatilization.Use vacuum filtration again, reclaim ethanol with vacuum pump.The former sol solution of honeybee of this moment has become the colloid of chocolate.
6. cooling.Naturally cool to and solidify shape, remove the beeswax that is suspended in above the honeybee virgin rubber, propolis product, whole purification process finishes.
7. finished product.Through the propolis after purifying, be ground into Powderedly again with pulverizer, press the customer requirements weight packaging, send into the final product warehouse.
The present invention is used for the former glue of honeybee and is purified to bee glue product, can turn waste into wealth propolis Not only have antibiotic, anti-inflammatory, antipruritic, anesthesia, promote drug-treating action such as tissue regeneration grade, Also can be used as the natural auxiliary additives such as food and daily cosmetics, its economic benefit and Social benefit is obvious.
Claims (3)
1. a process for refining bee propolis is characterized in that technical process is: the honeybee virgin rubber and---pulverizes---dissolving---filtration------cooling---finished product of purifying.
2. process for refining bee propolis according to claim 1 is characterized in that alcohol concn used in the dissolution process is 90%, and honeybee virgin rubber and alcoholic acid ratio are 1: 1.5.
3. process for refining bee propolis according to claim 1, the pot Heating temperature that it is characterized in that purifying in the purifying technique is 55-65 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 96101682 CN1162613A (en) | 1996-04-16 | 1996-04-16 | Process for refining bee propolis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 96101682 CN1162613A (en) | 1996-04-16 | 1996-04-16 | Process for refining bee propolis |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1162613A true CN1162613A (en) | 1997-10-22 |
Family
ID=5117196
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 96101682 Pending CN1162613A (en) | 1996-04-16 | 1996-04-16 | Process for refining bee propolis |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1162613A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1330256C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis honey sweets and preparation process |
| CN1330296C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis soft capsule and its preparation method |
| CN101889666A (en) * | 2010-06-30 | 2010-11-24 | 李国喜 | Polypeptide propolis and production process thereof |
| ITVR20100050A1 (en) * | 2010-03-16 | 2011-09-17 | Giuseppe Maria Ricchiuto | PROCEDURE FOR OBTAINING ANALLERGIC PROPOLIS |
| CN103549249A (en) * | 2013-10-11 | 2014-02-05 | 吕明 | Purification technology for propolis |
-
1996
- 1996-04-16 CN CN 96101682 patent/CN1162613A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1330256C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis honey sweets and preparation process |
| CN1330296C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis soft capsule and its preparation method |
| ITVR20100050A1 (en) * | 2010-03-16 | 2011-09-17 | Giuseppe Maria Ricchiuto | PROCEDURE FOR OBTAINING ANALLERGIC PROPOLIS |
| WO2011114291A1 (en) | 2010-03-16 | 2011-09-22 | Giuseppe Maria Ricchiuto | Process for obtaining non-allergic propolis. |
| CN102802646A (en) * | 2010-03-16 | 2012-11-28 | 朱塞佩·马里亚·里基乌托 | Process for obtaining non-allergic propolis |
| US9072754B2 (en) | 2010-03-16 | 2015-07-07 | Mr. Giuseppe Maria Ricchiuto | Process for obtaining non-allergic propolis |
| CN101889666A (en) * | 2010-06-30 | 2010-11-24 | 李国喜 | Polypeptide propolis and production process thereof |
| CN101889666B (en) * | 2010-06-30 | 2012-10-03 | 李国喜 | Polypeptide propolis and production process thereof |
| CN103549249A (en) * | 2013-10-11 | 2014-02-05 | 吕明 | Purification technology for propolis |
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| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |