CN1057196A - A kind of preparation method of Chinese medicine fresh Succus Bambusae - Google Patents
A kind of preparation method of Chinese medicine fresh Succus Bambusae Download PDFInfo
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- CN1057196A CN1057196A CN 90105836 CN90105836A CN1057196A CN 1057196 A CN1057196 A CN 1057196A CN 90105836 CN90105836 CN 90105836 CN 90105836 A CN90105836 A CN 90105836A CN 1057196 A CN1057196 A CN 1057196A
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- succus bambusae
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- bamboo stem
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Abstract
A kind of preparation method of Chinese medicine fresh Succus Bambusae, be to be raw material with bright bamboo stalk, its chopping is soaked in water at normal temperatures or contains in the water of 10-50% alcohol (in methanol, ethanol, propanol, the n-butyl alcohol any), carry 50-120 ℃ of following heat again, filter, get faint yellow to light red brown fresh Succus Bambusae (extracting solution that contains alcohol is answered heating recovery alcohol).This method has the yield height, quality is good, production cost is low, equipment investment is few, method is easy, be convenient to characteristics such as batch production production and control of product quality, and the bamboo fibre behind the extracted from bamboo juice also can fully utilize, and bigger economic and social benefit is arranged.
Description
The present invention is a kind of preparation method of Chinese medicine fresh Succus Bambusae.
Fresh Succus Bambusae is a Chinese medicine, has the effect of removing heat-phlegm.Be used for the treatment of illness such as cough due to lung-heat's abundant expectoration, uncomfortable in chest, the apoplexy stiff tongue of asthma, accumulation and obstruction of sputum, the hot infantile convulsion of children's's expectorant clinically.Commercially available fresh Succus Bambusae is to be that raw material adopts traditional method that scorches [being Pharmacopoeia of People's Republic of China (an one) version regulation in 1977] to produce with the Phyllostachys bamboo.The method method that bamboo in addition alive is got Succus Bambusae except that scorching method for preparing fresh Succus Bambusae (is seen " Zhejiang Chinese medicine " the 1st phase in 1976, " production process of phyllostachys nigra (lodd.ex lindl.) munro var.henonis (miff.) spapf et rendle liquid and process introduction " one literary composition and see " Chinese Hospitals pharmaceutical journal " 2 phases in 1987 " Sucus bambusae is followed the example of " literary composition) and the report of percolation (seeing " Shandong medical industry " 2 phases in 1987, " discussion of fresh Succus Bambusae extraction process " literary composition) extraction Succus Bambusae.The method of scorching is that bright bamboo stem is cut into 30~50cm length, and joint is removed at two ends, rives, and erects, and the middle part scorches with fire, and the faint yellow extremely light red brown liquid that the two ends drop goes out promptly is a fresh Succus Bambusae.This legal system is got Succus Bambusae yield low (be about former bamboo weight 3%), and the production cost height is not easy to quality control and batch production production, needs to cut down a large amount of bamboos aborning, and the waste bamboo resource has destroyed bamboo fibre, is not easy to bamboo resource is fully utilized.It is in boring on the bamboo that lives or after removing a joint bamboo tail bamboo to be stooped the method for getting fresh Succus Bambusae that the bamboo that lives is got the Succus Bambusae method.This genealogy of law dispersibility manual operations, get Succus Bambusae be subjected to multiple condition restriction (as rain, the Heavenly Stems, hot summer and severe winter all can not get Succus Bambusae), its gained fresh Succus Bambusae yield is low, be not easy to batch production production and control of product quality and management.Percolation is to be contained in the percolation pipe after bright bamboo stem is cut into slices, and with cold water soak and percolation, collects a certain amount of percolate and is fresh Succus Bambusae.It is to carry out at normal temperatures that this legal system is got fresh Succus Bambusae, and preparation time is long, and product is easily corrupt rotten, and uncontrollable quality, so this method only is in the laboratory test stage can not drop into batch production and produce and implement.
The objective of the invention is the shortcoming that exists at existing fresh Succus Bambusae preparation method, propose a kind of yield height, quality is good, method for making is easy, cost the is low method for preparing fresh Succus Bambusae.
The present invention realizes by following approach, with the bright bamboo stem of grass is raw material, after chopping, be soaked in water or contain 10~15% alcohol (methanol, ethanol, propanol, in the n-butyl alcohol any) in the water, bright bamboo stem raw material and water or the solid-liquid weight ratio that contains the water of above-mentioned alcohol are 1: 1.5~8, after it is soaked 0.5~2 hour at normal temperatures, heat again to 50~120 ℃ of following heat and carry 2~8 hours, thereafter filter bright bamboo stem extracting solution (should reclaim alcohol with heating means according to the boiling point of alcohol) to the extracting solution that contains above-mentioned alcohol, again through adding cold clear water dilution or heating concentrated extracting solution, the weight that makes this solution is 1~3 times of bright bamboo stem raw material weight, obtains having faint yellow to light red brown fresh Succus Bambusae at last.
This method is raw materials used to be the bright bamboo stem of the various Sinobambusas of grass, and wherein the raw material that more preferably adopts is the bright bamboo stem of Sinocalamus, bitter bamboo genus, Phyllostachys, Thorny Sinobambusa.The bright bamboo stem of above-mentioned four kinds of Sinobambusas has rich in natural resources in China, the fresh Succus Bambusae quality height that price is low, produce.This method prepares its bright bamboo stem raw material of fresh Succus Bambusae and water or contains in the water of 10-50% alcohol (in methanol, ethanol, propanol, the n-butyl alcohol any), and bright bamboo stem raw material and above-mentioned water or the preferred solid-liquid weight ratio of aqueous solvent that contains above-mentioned alcohol are 1: 2~3.To more help the amino acid whose extraction of fresh Succus Bambusae active ingredient through the bright bamboo stem soak at room temperature after the chopping in water or contain in the alcoholic acid water of 10-50% 1~2 hour and carry out heat again and carry.
Adopt this method to prepare fresh Succus Bambusae, the yield of its fresh Succus Bambusae is 100~300% of a bright bamboo weight, be to scorch 30~90 times of method yield, the active ingredient amino acids content of eliminating phlegm and stopping cough is to scorch more than the octuple of method, and other useful component guaiacol, gluconic acid etc. are also than scorching method content height.Adopt this method to prepare fresh Succus Bambusae and do not need to cut down a large amount of bamboos, production cost is low, equipment investment is few, constant product quality, impurity are few, be easy to batch production production and control of product quality and management, bamboo fibre behind the extracted from bamboo juice also can be used for making paper pulp and bamboo fiberboard etc., has improved the comprehensive utilization value and the economic benefit of bamboo resource.As add an amount of antiseptic with after the fresh Succus Bambusae dilution, boiling, checking, bottling to make fresh bamboo trickle liquid; Fresh Succus Bambusae is added adjuvant also can be made into Chinese medicine single preparation bamboo trickle paste, bamboo drop plate; Can be made into Chinese patent medicine compound recipe fresh Succus Bambusae with drug matchings such as Herba Houttuyniae, Rhizoma Pinelliae, fresh ginger, Folium Eriobotryae, Radix Platycodonis, peppermints; Can be made into Chinese patent medicine Succus Bambusae phlegm-resolving pill with drug matchings such as Radix Scutellariae, Pericarpium Citri Reticulatae, Rhizoma Pinelliae Preparatum, Lapis Micae Aureus (forging), Lignum Aquilariae Resinatum, Radix Et Rhizoma Rhei, the Rhizoma Atractylodis Macrocephalae, Radix Glycyrrhizaes.Fresh Succus Bambusae also can be used with other drug matching in prescription.
Through adopting the inventive method trial production fresh bamboo trickle liquid to prove that the production cost of producing fresh bamboo trickle liquid than the method that scorches hangs down 40 times, the efficacy component amino acids content ratio of eliminating phlegm and stopping cough scorches high ten times of methods.
Embodiment
Example 1: with the bright bar 0.5kg chopping of cizu or bitter bamboo, be 1: 2~3 by the solid-liquid weight ratio, it was soaked 1~2 hour at normal temperatures that heat and carry 2~8 hours to 50~120 ℃ of heat, filtration can get light red brown fresh Succus Bambusae 1~1.5kg with cold water.
Example 2: the bright bamboo stem 0.5kg chopping that will press from both sides bamboo or hardhead bambusa textilt in vain, is 1: 4~6 with containing 50% alcoholic acid aqueous solvent by the solid-liquid weight ratio, it was soaked 1~2 hour at normal temperatures, heat again to 50~80 ℃ of heat and carry 2~4 hours, filter, get bright bamboo stem extracting solution, heating extraction liquid can get flaxen fresh Succus Bambusae 1~1.5kg after reclaiming ethanol.
Claims (4)
1, a kind of preparation method of Chinese medicine fresh Succus Bambusae, it is characterized in that this method is a raw material with the bright bamboo stem of grass, after chopping, be soaked in water or contain 10-50% alcohol (methanol, ethanol, propanol, any in the n-butyl alcohol) in the water, bright bamboo stem raw material and water or the solid-liquid weight ratio that contains the water of above-mentioned alcohol are 1: 1.5~8, after it is soaked 0.5~2 hour at normal temperatures, heat again to 50~120 ℃ of heat and carry 2~8 hours, thereafter filter bright bamboo stem extracting solution (should reclaim alcohol with heating means according to the boiling point of alcohol) to the extracting solution that contains above-mentioned alcohol, again through adding cold clear water dilution or heating concentrated extracting solution, the weight that makes this liquid is 1~3 times of bright bamboo stem raw material weight, can have faint yellow to light red brown fresh Succus Bambusae subsequently.
2, preparation method according to claim 1 is characterized in that the bright bamboo stem of grass is the bright bamboo stem of Sinocalamus, Phyllostachys, bitter bamboo genus, Thorny Sinobambusa.
3, preparation method according to claim 1, the solid-liquid weight ratio that it is characterized in that bright bamboo stem raw material and water or contain the water of 10-50% alcohol (in methanol, ethanol, propanol, the n-butyl alcohol any) is 1: 2~3.
4,, it is characterized in that the bright bamboo stem after chopping is soak at room temperature in water or contains in the alcoholic acid water of 10-50% 1~2 hour and carry out heat again and carry according to claim 1 or 2 or 3 described preparation methoies.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 90105836 CN1028604C (en) | 1990-06-13 | 1990-06-13 | Prepn. of Chinese herb-fresh bamboo-juice |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 90105836 CN1028604C (en) | 1990-06-13 | 1990-06-13 | Prepn. of Chinese herb-fresh bamboo-juice |
Publications (2)
Publication Number | Publication Date |
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CN1057196A true CN1057196A (en) | 1991-12-25 |
CN1028604C CN1028604C (en) | 1995-05-31 |
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CN 90105836 Expired - Fee Related CN1028604C (en) | 1990-06-13 | 1990-06-13 | Prepn. of Chinese herb-fresh bamboo-juice |
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Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1042093C (en) * | 1993-06-09 | 1999-02-17 | 罗正都 | Bamboo juice and series nutrition health care food |
CN1052649C (en) * | 1996-07-17 | 2000-05-24 | 蒋道友 | Extraction method of Sucus bambusae |
CN1053357C (en) * | 1994-11-04 | 2000-06-14 | 张仲安 | Preparation of bamboo juice |
CN1082374C (en) * | 1997-06-04 | 2002-04-10 | 中国医学科学院药物研究所 | Traditional Chinese medicinal composition with reducing-blood-sugar activity |
EP1413208A1 (en) * | 2002-10-24 | 2004-04-28 | Adaptgen Pharmaceutical Co., Ltd. | Health food and antitumor agent |
CN1304041C (en) * | 2004-05-13 | 2007-03-14 | 湖南正清制药集团股份有限公司 | Method of PH gradient extracting bamboo juice |
WO2008044894A1 (en) * | 2006-10-12 | 2008-04-17 | Unigen, Inc. | Composition for treating atopic dermatitis comprising extracts of bamboo and scutellaria |
CN100473408C (en) * | 2005-01-21 | 2009-04-01 | 四川奥邦药业有限公司 | Heat-clearing and phlegm-resolving medicine composition, preparation and use thereof |
US8535735B2 (en) | 2002-03-01 | 2013-09-17 | Unigen, Inc. | Identification of free-B-ring flavonoids as potent COX-2 inhibitors |
US8568799B2 (en) | 2002-03-22 | 2013-10-29 | Unigen, Inc. | Isolation of a dual COX-2 and 5-lipoxygenase inhibitor from acacia |
US8652535B2 (en) | 2002-04-30 | 2014-02-18 | Unigen, Inc. | Formulation of a mixture of free-B-ring flavonoids and flavans for use in the prevention and treatment of cognitive decline and age-related memory impairments |
US8790724B2 (en) | 2003-04-04 | 2014-07-29 | Unigen, Inc. | Formulation of dual cycloxygenase (COX) and lipoxygenase (LOX) inhibitors for mammal skin care |
CN104749282A (en) * | 2015-04-07 | 2015-07-01 | 湖北端正药业股份有限公司 | Method for determining content of guaiacol in fresh bamboo juice |
US9370544B2 (en) | 2002-04-30 | 2016-06-21 | Unigen, Inc. | Formulation of a mixture of free-B-ring flavonoids and flavans as a therapeutic agent |
CN112316068A (en) * | 2020-11-04 | 2021-02-05 | 江西中竹生物质科技有限公司 | Method for extracting fresh bamboo juice by using ultrasonic waves |
CN114982950A (en) * | 2022-06-10 | 2022-09-02 | 重庆升升药业有限公司 | Preparation method of fresh bamboo juice red yeast rice oral liquid |
-
1990
- 1990-06-13 CN CN 90105836 patent/CN1028604C/en not_active Expired - Fee Related
Cited By (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1042093C (en) * | 1993-06-09 | 1999-02-17 | 罗正都 | Bamboo juice and series nutrition health care food |
CN1053357C (en) * | 1994-11-04 | 2000-06-14 | 张仲安 | Preparation of bamboo juice |
CN1052649C (en) * | 1996-07-17 | 2000-05-24 | 蒋道友 | Extraction method of Sucus bambusae |
CN1082374C (en) * | 1997-06-04 | 2002-04-10 | 中国医学科学院药物研究所 | Traditional Chinese medicinal composition with reducing-blood-sugar activity |
US8535735B2 (en) | 2002-03-01 | 2013-09-17 | Unigen, Inc. | Identification of free-B-ring flavonoids as potent COX-2 inhibitors |
US9061039B2 (en) | 2002-03-01 | 2015-06-23 | Unigen, Inc. | Identification of Free-B-Ring flavonoids as potent COX-2 inhibitors |
US9168242B2 (en) | 2002-03-22 | 2015-10-27 | Unigen, Inc. | Isolation of a dual COX-2 and 5-lipdxygenase inhibitor from Acacia |
US8568799B2 (en) | 2002-03-22 | 2013-10-29 | Unigen, Inc. | Isolation of a dual COX-2 and 5-lipoxygenase inhibitor from acacia |
US8652535B2 (en) | 2002-04-30 | 2014-02-18 | Unigen, Inc. | Formulation of a mixture of free-B-ring flavonoids and flavans for use in the prevention and treatment of cognitive decline and age-related memory impairments |
US9849152B2 (en) | 2002-04-30 | 2017-12-26 | Unigen, Inc. | Formulation of a mixture of Free-B-ring flavonoids and flavans as a therapeutic agent |
US9655940B2 (en) | 2002-04-30 | 2017-05-23 | Unigen, Inc. | Formulation of a mixture of free-B-ring flavonoids and flavans as a therapeutic agent |
US9370544B2 (en) | 2002-04-30 | 2016-06-21 | Unigen, Inc. | Formulation of a mixture of free-B-ring flavonoids and flavans as a therapeutic agent |
EP1413208A1 (en) * | 2002-10-24 | 2004-04-28 | Adaptgen Pharmaceutical Co., Ltd. | Health food and antitumor agent |
US8790724B2 (en) | 2003-04-04 | 2014-07-29 | Unigen, Inc. | Formulation of dual cycloxygenase (COX) and lipoxygenase (LOX) inhibitors for mammal skin care |
US9622964B2 (en) | 2003-04-04 | 2017-04-18 | Unigen, Inc. | Formulation of dual cycloxygenase (COX) and lipoxygenase (LOX) inhibitors for mammal skin care |
CN1304041C (en) * | 2004-05-13 | 2007-03-14 | 湖南正清制药集团股份有限公司 | Method of PH gradient extracting bamboo juice |
CN100473408C (en) * | 2005-01-21 | 2009-04-01 | 四川奥邦药业有限公司 | Heat-clearing and phlegm-resolving medicine composition, preparation and use thereof |
US8771761B2 (en) | 2006-10-12 | 2014-07-08 | Unigen, Inc. | Composition for treating atopic dermatitis comprising extracts of bamboo and scutellaria |
WO2008044894A1 (en) * | 2006-10-12 | 2008-04-17 | Unigen, Inc. | Composition for treating atopic dermatitis comprising extracts of bamboo and scutellaria |
CN101616681B (en) * | 2006-10-12 | 2013-07-10 | 株式会社优力竟 | Composition for treating atopic dermatitis comprising extracts of bamboo and scutellaria |
US9623068B2 (en) | 2006-10-12 | 2017-04-18 | Unigen, Inc. | Composition for treating atopic dermatitis comprising extracts of bamboo and scutellaria |
AU2007307427B2 (en) * | 2006-10-12 | 2013-05-09 | Unigen, Inc. | Composition for treating atopic dermatitis comprising extracts of Bamboo and Scutellaria |
US8247007B2 (en) | 2006-10-12 | 2012-08-21 | Unigen, Inc. | Composition for treating atopic dermatitis comprising extracts of bamboo and Scutellaria |
CN104749282A (en) * | 2015-04-07 | 2015-07-01 | 湖北端正药业股份有限公司 | Method for determining content of guaiacol in fresh bamboo juice |
CN112316068A (en) * | 2020-11-04 | 2021-02-05 | 江西中竹生物质科技有限公司 | Method for extracting fresh bamboo juice by using ultrasonic waves |
CN114982950A (en) * | 2022-06-10 | 2022-09-02 | 重庆升升药业有限公司 | Preparation method of fresh bamboo juice red yeast rice oral liquid |
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Publication number | Publication date |
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CN1028604C (en) | 1995-05-31 |
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