CN115753274B - A rapid sampling platform and method for columnar sediment samples - Google Patents
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Abstract
Description
技术领域technical field
本发明属于海洋地质勘探技术领域,具体涉及一种用于海洋地质领域柱状沉积物样品的准确剖分和快速分样平台及分样方法。The invention belongs to the technical field of marine geological exploration, and in particular relates to an accurate subdivision and rapid sampling platform and a sampling method for columnar sediment samples in the marine geological field.
背景技术Background technique
取样测试和原位测试是进行海洋沉积环境研究的两种常见手段,测试的内容主要包括测年、沉积物粒度、矿物、常微量元素、有机碳氮等。Sampling test and in-situ test are two common methods for marine sedimentary environment research. The test contents mainly include dating, sediment grain size, minerals, normal and trace elements, organic carbon and nitrogen, etc.
取样测试需要先从现场取得沉积物柱状样品,然后在实验室按一定间距对样品进行切分测试,切分操作不当可能会带来扰动加剧、外源污染等问题,影响测试结果的准确性。原位测试是在沉积物原来位置或基本上在原位状态条件下对沉积物进行的测试,可以有效避免取样、保存、切分等过程对样品的扰动或污染,更为准确地反应沉积物实际状态性质。由于技术条件、测试成本、测试仪器等因素的限制,加上影响原位测试成果的因素较为复杂,原位测试应用较为局限,取样测试仍是现阶段海洋沉积环境研究的主要手段。Sampling tests need to obtain sediment columnar samples from the field first, and then cut the samples at a certain interval in the laboratory for testing. Improper cutting operations may cause problems such as increased disturbance and external pollution, which will affect the accuracy of the test results. In-situ testing is to test the sediment at its original position or basically under the condition of in-situ state, which can effectively avoid the disturbance or pollution of the sample during the process of sampling, storage, cutting, etc., and reflect the sediment more accurately The nature of the actual state. Due to the limitations of technical conditions, testing costs, testing instruments and other factors, and the complex factors affecting the results of in-situ testing, the application of in-situ testing is relatively limited. Sampling testing is still the main means of marine sedimentary environment research at this stage.
目前,还没有考虑如何减小扰动和外源污染并能对沉积物柱状样品快速准确切分的装置,也没有从取样阶段出发考虑如何进行样品准确切分的方法。常规的沉积物柱状样品的切分主要依靠手工进行,一般先将取得的沉积物柱状样品纵向剖成两个半圆形柱状样,然后利用切土刀等工具比对标尺按照需求进行样品切分。At present, there is no device that considers how to reduce disturbance and external pollution and can quickly and accurately segment sediment columnar samples, nor does it consider how to accurately segment samples from the sampling stage. The segmentation of conventional sediment columnar samples is mainly carried out manually. Generally, the obtained sediment columnar samples are longitudinally cut into two semicircular columnar samples, and then the samples are segmented according to the requirements using tools such as soil cutters and comparison scales. .
一般对沉积物柱状样品的切分往往直接垂直柱长方向切分,这一前提是采集的柱状样品是与沉积层垂直的。实际上,柱状样采集时受现场条件和地层分布影响,柱状样与沉积层之间存在一个不确定的角度关系,尤其是进行高分辨率小间距精细切分时,这种切分准确性是值得商榷的。此外,手动切分存在误差大、效率低、易引入碎屑污染、振动扰动等问题。如何减小切分过程对样品的污染和扰动,快速、准确切分沉积物柱状样品,是海洋沉积物研究需要解决的技术问题。Generally, the segmentation of sediment columnar samples is often directly vertical to the column length, and this premise is that the collected columnar samples are perpendicular to the sedimentary layer. In fact, the collection of columnar samples is affected by field conditions and stratum distribution, and there is an uncertain angle relationship between columnar samples and sedimentary layers. Especially when finely segmenting with high resolution and small spacing, the accuracy of this segmentation is Debatable. In addition, manual segmentation has problems such as large errors, low efficiency, easy introduction of debris pollution, and vibration disturbance. How to reduce the pollution and disturbance of samples during the cutting process, and quickly and accurately cut sediment columnar samples are technical problems that need to be solved in marine sediment research.
发明内容Contents of the invention
本发明的目的是提供一种柱状沉积物样品快速分样平台,以填补目前没有可以准确、快速进行柱状沉积物样品切分的技术空白,同时提出一种沉积物柱状样品切分方法,以期提高沉积物样品切分的准确性。The purpose of the present invention is to provide a kind of columnar sediment sample rapid sampling platform, to fill up the technical blank that can not carry out columnar sediment sample segmentation accurately and rapidly at present, propose a kind of sediment columnar sample segmentation method simultaneously, in order to improve Accuracy of sediment sample segmentation.
为了实现上述目的,本发明采用的一种技术方案是:一种柱状沉积物样品的快速分样平台,包括操作台面、固定夹紧装置、剖切装置和步进分样装置;操作台面上沿长度方向间隔布置若干夹紧固定装置;所述固定夹紧装置的两侧分别设置相互平行的滑轨和齿条导轨;所述的剖切装置滑动连接在所述滑轨上;所述的步进分样装置一侧滑动连接于滑轨上,另一侧通过齿轮啮合于齿条导轨上。In order to achieve the above object, a technical scheme adopted by the present invention is: a rapid sampling platform for columnar sediment samples, including an operating table top, a fixed clamping device, a cutting device and a stepping sampling device; A number of clamping and fixing devices are arranged at intervals in the length direction; slide rails and rack guide rails parallel to each other are respectively arranged on both sides of the fixing and clamping devices; the cutting device is slidably connected on the slide rails; the step One side of the sampling device is slidably connected to the slide rail, and the other side is meshed with the rack guide rail through gears.
进一步地,所述的固定夹紧装置由固定底座、固定抱箍组成,固定底座固定于操作台面上;固定抱箍与固定底座的一侧铰接连接,固定抱箍可沿铰接轴旋转打开或闭合;固定底座与固定抱箍具有半径相同的半圆形凹槽。Further, the fixed clamping device is composed of a fixed base and a fixed hoop, the fixed base is fixed on the operating table; the fixed hoop is hingedly connected to one side of the fixed base, and the fixed hoop can be rotated along the hinge axis to open or close ; The fixed base and the fixed hoop have semicircular grooves with the same radius.
进一步地,所述固定抱箍铰接的一侧设有顶紧装置,所述顶紧装置包括顶紧螺丝和固定插销;所述固定插销的下端与操作台面连接,上端设有螺母;所述顶紧螺丝穿过所述螺母,并可沿螺母前后移动,进而将所述固定抱箍的侧面顶紧或松开。Further, the hinged side of the fixed hoop is provided with a tightening device, and the tightening device includes a tightening screw and a fixed pin; the lower end of the fixed pin is connected to the operating table, and the upper end is provided with a nut; The tightening screw passes through the nut and can move back and forth along the nut, thereby tightening or loosening the side of the fixing hoop.
进一步地,所述的固定抱箍顶部开设有长槽,所述固定插销穿过所述的长槽与操作台面固定。Further, a long slot is opened on the top of the fixing hoop, and the fixing bolt passes through the long slot and is fixed to the operating table.
进一步地,所述的剖切装置包括切割刀、T型滑轨、T型滑块和滑块,所述T型滑块的水平部装配于滑轨上;所述T型滑块的竖直部与所述T型滑轨的竖直部装配;所述T型滑轨的水平部与滑块装配;滑块的一端与电机固定,电机与切割刀连接。Further, the cutting device includes a cutting knife, a T-shaped slide rail, a T-shaped slide block and a slide block, the horizontal part of the T-shaped slide block is assembled on the slide rail; the vertical part of the T-shaped slide block The part is assembled with the vertical part of the T-shaped slide rail; the horizontal part of the T-shaped slide rail is assembled with the slider; one end of the slider is fixed with the motor, and the motor is connected with the cutting knife.
进一步地,所述步进分样装置由支架、角度器、步进手柄、分样刀片构成,所述支架横跨在滑轨和齿条导轨上方,一侧设有滑块,另一侧设有齿轮;支架的中部设有环形滑槽;环形滑槽内装配有角度器;角度器上安装竖直布置的分样刀片。Further, the step-by-step sampling device is composed of a bracket, an angler, a step handle, and a sample-dividing blade; There are gears; the middle part of the bracket is provided with an annular chute; an angler is installed in the annular chute; vertically arranged sample dividing blades are installed on the angler.
进一步地,所述的齿轮连接有手柄。Further, the gear is connected with a handle.
进一步地,所述操作台面上沿所述固定夹紧装置的布置方向标有刻度线。Further, scale lines are marked on the operating table along the arrangement direction of the fixing and clamping devices.
本发明采用的另一种技术方案是:一种柱状沉积物样品的快速分样方法,该方法利用所述的分样平台对样品进行切分,具体包括以下步骤:Another technical solution adopted in the present invention is: a method for rapid sample division of columnar sediment samples, which utilizes the described sample division platform to segment the sample, specifically comprising the following steps:
(1)首先对柱状样品进行X光影像扫描,转动柱状样品当X射线方向与沉积层布平行时,获得最清晰的层布影像,并标出不同层位的角度分布;(1) First scan the columnar sample by X-ray image, rotate the columnar sample when the X-ray direction is parallel to the deposition layer, obtain the clearest layer image, and mark the angular distribution of different layers;
(2)确定样品的剖切面,所述剖切面为一个与沉积物层布面垂直且经过柱状样品长轴的平面,将柱状样品沿所述剖切面剖开获得镜像对称的两半样品;(2) Determine the cut plane of the sample, the cut plane is a plane perpendicular to the sediment layer cloth surface and passing through the long axis of the columnar sample, and the columnar sample is cut along the cut plane to obtain two half samples of mirror symmetry;
(3)根据X光影像上对应的标记角度,沿平行于沉积层进行样品分割并记录。(3) According to the corresponding marking angle on the X-ray image, the sample is segmented and recorded parallel to the deposition layer.
与现有技术相比,本发明具有如下有益效果:Compared with the prior art, the present invention has the following beneficial effects:
本发明结构合理、操作方便、方法得当,可以很好的解决人工对沉积物柱状样品连续切分时存在切分误差、加剧扰动、外源污染、效率低等问题,可以快速、精确的对柱状沉积物进行连续分样,同时可根据实际取样情况,对切分角度进行调整校正,提高样品切分合理性和准确性。本发明的分样平台就方法是对目前柱状沉积物分样技术的一个重要补充。The invention has reasonable structure, convenient operation and proper method, and can well solve the problems of segmentation error, aggravated disturbance, external source pollution, low efficiency and the like in the continuous segmentation of sediment columnar samples manually, and can quickly and accurately analyze columnar samples. The sediment is divided continuously, and the cutting angle can be adjusted and corrected according to the actual sampling situation to improve the rationality and accuracy of the sample cutting. The sampling platform and method of the present invention is an important supplement to the current columnar sediment sampling technology.
附图说明Description of drawings
图1是本发明实施例1中的柱状沉积物样品的快速分样平台的整体结构示意图;Fig. 1 is the overall structure schematic diagram of the rapid sampling platform of columnar sediment sample in the embodiment 1 of the present invention;
图2是本发明实施例1中的柱状沉积物样品的快速分样平台的俯视图;Fig. 2 is the plan view of the fast sampling platform of the columnar sediment sample in the embodiment 1 of the present invention;
图3是实施例1中固定夹紧装置的结构示意图(闭合状态);Fig. 3 is a schematic structural view (closed state) of the fixed clamping device in Embodiment 1;
图4为实施例1中固定夹紧装置的结构示意图(打开状态);Fig. 4 is the schematic structural view (open state) of fixed clamping device in embodiment 1;
图5为实施例1中剖切装置的结构示意图;Fig. 5 is the structural representation of cutting device in embodiment 1;
图6为实施例1中剖切装置的爆炸视图;Fig. 6 is the exploded view of cutting device in embodiment 1;
图7为实施例1中步进分样装置的结构示意图;Fig. 7 is the structural representation of step-by-step sampling device in embodiment 1;
图8为实施例1中步进分样装置的正视图;Fig. 8 is the front view of step-by-step sample dividing device in embodiment 1;
图9为实施例1中支架的结构示意图;Figure 9 is a schematic structural view of the bracket in Example 1;
图10为实施例1中支架的仰视图;Fig. 10 is the bottom view of bracket in embodiment 1;
图11为实施例1中分样刀片的结构示意图;Fig. 11 is the structural representation of sample dividing blade in embodiment 1;
图12为实施例1中角度器的结构示意图;Fig. 12 is the structural representation of angler in embodiment 1;
图13为实施例2中固定夹紧装置的结构示意图(闭合状态);Fig. 13 is a schematic structural view (closed state) of the fixed clamping device in
图14为实施例2中固定夹紧装置的结构示意图(打开状态);Fig. 14 is a schematic structural view (open state) of the fixed clamping device in
图15为实施例3中柱状样中心轴与沉积层不垂直示意图;Fig. 15 is a schematic diagram showing that the central axis of the columnar sample is not perpendicular to the deposition layer in Example 3;
图16为实施例3中沿剖切面剖分后样品示意图;Fig. 16 is the schematic diagram of the sample after being divided along the cutting plane in
其中,1、支腿,2、操作台面,3、调平脚垫,4、滑轨,5、齿条导轨,6、剖切装置,7、步进分样装置,8、固定夹紧装置,9、固定底座,10、固定抱箍,11、固定插销,12、蝶形螺丝,13、电机,14、无屑切割刀,15、T型滑轨,16、T型滑块,17、支架,18、角度器,19、步进手柄,21、刀片体,22、薄壁手持板,23、窄缝,24、过刀槽,25、半圆缺口;26、第一滑块;27、齿轮;28第二滑块;29、卡块;30、环形滑槽。Among them, 1. Outrigger, 2. Operating table, 3. Leveling foot pad, 4. Slide rail, 5. Rack guide rail, 6. Cutting device, 7. Stepping sample dividing device, 8. Fixed clamping device , 9, fixed base, 10, fixed hoop, 11, fixed pin, 12, butterfly screw, 13, motor, 14, chipless cutter, 15, T-shaped slide rail, 16, T-shaped slider, 17, Bracket, 18, angler, 19, stepping handle, 21, blade body, 22, thin-walled hand-held plate, 23, narrow slit, 24, knife groove, 25, semicircle gap; 26, the first slide block; 27, Gear; 28 second slide block; 29, block; 30, annular chute.
具体实施方式Detailed ways
为了便于理解本发明,下面结合附图和具体实施例,对本发明进行更详细的说明。附图中给出了本发明的较佳的实施例。但是,本发明可以以许多不同的形式来实现,并不限于本说明书所描述的实施例。相反地,提供这些实施例的目的是使对本发明公开内容的理解更加透彻全面。In order to facilitate the understanding of the present invention, the present invention will be described in more detail below in conjunction with the accompanying drawings and specific embodiments. Preferred embodiments of the invention are shown in the accompanying drawings. However, the present invention can be implemented in many different forms and is not limited to the embodiments described in this specification. On the contrary, these embodiments are provided to make the understanding of the present disclosure more thorough and comprehensive.
实施例1本实施例提供的柱状沉积物样品的快速分样平台,整体结构如图1和图2所示,该平台主要由四部分组成,分别是操作台面2、剖切装置6、步进分样装置7、固定夹紧装置8。其中,操作台面2是整个装置的基础承载平台,由四条支腿1支撑,支腿1的底部安装有调平脚垫3,可以通过调平脚垫3调整操作台面2,使其处于平稳状态。Example 1 The rapid sampling platform for columnar sediment samples provided in this example has an overall structure as shown in Figure 1 and Figure 2. The platform is mainly composed of four parts, namely the operating table 2, the
在操作台面2上,沿长度方向设有一系列固定夹紧装置8并标有刻度线,以及一条滑轨4和一条齿条导轨5与之平行。滑轨4和齿条导轨5分别位于固定夹紧装置8的两侧。在操作台面2上,还设有剖切装置6和步进分样装置7,其中,剖切装置6装配于滑轨4上,可沿滑轨4左右移动,步进分样装置7横跨在固定夹紧装置8的两侧,一侧与滑轨4滑动连接,另一侧与齿条导轨5齿轮啮合连接。固定夹紧装置8用于将沉积物柱状样品的塑料或金属取样管外壳均匀夹持固定,剖切装置6用于对取样管外壳进行剖切,步进分样装置7用于对样品进行快速切分。On the operating table 2, a series of fixed
如图3所示,固定夹紧装置8由固定底座9、固定抱箍10、固定插销11和蝶形顶紧螺丝12构成,固定底座9采用螺栓固定于操作台面2上,固定抱箍10与固定底座9在侧面采用销轴铰接,固定抱箍10沿转轴可以旋转开合。固定底座9和固定抱箍10为具有半圆形凹槽的对称结构,当固定抱箍10沿转轴旋转闭合后,与固定底座9共同构成了内部的容纳空腔,从而容纳固定柱状样品。需要注意的是,闭合状态下,固定抱箍10和固定底座9留有一定间隙,该间隙用于使剖切装置6上的无屑切割刀通过,以便对柱状样品的取样管外壳进行剖切。As shown in Figure 3, the fixed
当固定柱状样品时,为了使固定抱箍10与固定底座9保持闭合状态,在固定抱箍10和固定底座9铰接的那一侧设有固定插销11和蝶形螺丝12,固定插销11竖直布置在操作台面2上,可与操作台面2上预设的开孔直接插拔安装,固定插销11的顶部有一个螺母,蝶形螺丝12从螺母中穿过,其末端正对固定抱箍10的侧面,通过旋转拧紧蝶形螺丝12,可使其朝着固定抱箍10移动,直至将固定抱箍顶住,使固定抱箍不能旋转打开,如图3所示。当需要打开时,可将蝶形螺丝12旋转松开,再将固定插销11从操作台面2上拨出,固定抱箍10沿轴旋转可以打开,打开状态如图4所示。When fixing the columnar sample, in order to keep the
如图5和图6所示,剖切装置6由电机13、无屑切割刀14、T型滑轨15、T型滑块16和第一滑块26构成。T型滑块16的水平部与滑轨4滑动装配,使T型滑块16可沿滑轨4左右移动,T型滑块16的竖直部与T型滑轨15的竖直部滑动装配,使T型滑轨15可沿T型滑块16在竖直方向上、下移动,T型滑轨15的水平部与第一滑块26滑动装配,使T型滑轨15可沿第一滑块26在水平方向上前、后移动。第一滑块26的前端固定电机13,电机13的轴上安装有无屑切割刀14,当电机启动后,可以驱动无屑切割刀14旋转,对柱状样品的取样管外壳进行剖切。为了固定T型滑轨15的位置,在T型滑块16的竖直部和第一滑块26上也分别设有蝶形螺丝12,拧紧螺丝,可以将T型滑轨15顶紧固定。As shown in FIGS. 5 and 6 , the
如图7和图8所示,步进分样装置7由支架17、角度器18、步进手柄19、分样刀片、齿轮27、第二滑块28、卡块29构成。支架17横跨在滑轨4和齿条导轨5上,一侧通过第二滑块28与滑轨4滑动连接,另一侧通过卡块29和齿轮27与齿条导轨5啮合,齿轮27位于卡块29内部,步进手柄19穿过卡块29与齿轮27连接。当旋转步进手柄19时,步进手柄带动齿轮27旋转,从而沿着齿条导轨5移动,步进手柄19一次最小0.5cm间隔固定步进,通过步进手柄可以精确控制步进分样装置匀速移动。As shown in FIGS. 7 and 8 , the stepping
支架17的结构如图9和图10所示,包括两侧的第二滑块28和卡块29,以及中间的环形滑槽30,环形滑槽30具有缺口。角度器18滑动装配在环形滑槽30内,可以在水平面内沿环形滑槽30旋转。缺口用于将角度器取出。The structure of the
角度器的结构如图12所示,包括窄缝23,过刀槽24、半圆缺口25,窄缝23用于固定分样刀片,过刀槽24、半圆缺口25用于使分样刀片通过。分样刀片的结构如图11所示,包括刀片体21和薄壁手持板22,其中薄壁手持板22的长度小于过刀槽24的宽度,以便使分样刀片顺利通过。The structure of the angler is shown in Figure 12, including
实施例2本实施例提供的柱状沉积物样品的快速分样平台,大体结构与实施例1相同,所不同的是,为了方便固定抱箍的固定和打开,避免反复插拔固定插销,将固定抱箍的结构进行了改进,如图13和图14所示,在固定抱箍10的顶部开设一个长槽,固定插销11从该长槽内穿过,下端与操作台面固定,上端安装蝶形顶紧螺丝12。采用此种结构,在打开固定抱箍10时,无需将固定插销取下,只需将蝶形顶紧螺丝拧下即可,避免反复插拔固定插销带来的麻烦。Example 2 The rapid sampling platform for columnar sediment samples provided in this example has the same general structure as Example 1, the difference is that, in order to facilitate the fixing and opening of the fixing hoop, and to avoid repeated insertion and extraction of the fixing pin, the fixing The structure of the hoop has been improved, as shown in Figure 13 and Figure 14, a long slot is opened on the top of the fixed
本发明的柱状沉积物样品的快速分样平台,工作原理如下描述:The rapid sampling platform for columnar sediment samples of the present invention has a working principle as follows:
将柱状样品及取样管放进固定底座9中,旋转固定抱箍10,使其与固定底座9闭合,将固定插销11上的蝶形螺丝拧紧顶在固定抱箍10的侧面,将其固定。Put the columnar sample and sampling tube into the fixed
调整T型滑轨15和T型滑块16的位置,使无屑切割刀14从固定底座和固定抱箍之间的间隙伸入,启动电机13,从而对取样管外壳进行切割,通过T型滑块16在滑轨4上移动,完成取样管外壳一侧的整体切割。将柱状样品及取样管旋转180°以上述相同方式进行对侧剖切。Adjust the position of the T-shaped
通过步进手柄19调整支架17移动到合适的位置,旋转角度器18调整角度后,取一个分样刀片通过角度器18上的窄缝23向下插入,完成对柱状样品的切分,然后,通过步进手柄19使支架17移动到下一个工位,重新调整角度,取一个新的分样刀片进行切分,直至整个柱状样品切分完毕。Move the
实施例3本实施例提供一种柱状沉积物样品的快速分样方法通常,在进行沉积物分样时往往直接将样品垂直于中心轴方向进行切分,不考虑样品层布与轴线的实际关系。这一前提是重力取样器设计足够理想,可以有效控制取样器下落姿态,保证取样轴线与地层面垂直。如图15所示,假设沉积层与面xOy平行分布,取样管中心轴为OP,当取样时取样管与地层不垂直时,OP与面xOy之间存在一定夹角∠β≠90°,OP′是OP在xOy平面上的投影。沿垂直于OP方向的面进行样品切分,这显然与实际地层沉积分布情况不符,尤其是小间距、高分辨率分样时,会将不同层位的沉积物划分到同一试样,导致测试结果混杂、特征不明显。Example 3 This example provides a rapid sampling method for columnar sediment samples. Usually, when performing sediment sampling, the sample is often directly divided perpendicular to the central axis, regardless of the actual relationship between the sample layer distribution and the axis. . This premise is that the design of the gravity sampler is ideal enough to effectively control the falling attitude of the sampler and ensure that the sampling axis is perpendicular to the ground surface. As shown in Figure 15, assuming that the sedimentary layer is distributed parallel to the surface xOy, and the central axis of the sampling pipe is OP, when the sampling pipe is not perpendicular to the formation during sampling, there is a certain angle ∠β≠90° between OP and the surface xOy, and OP ' is the projection of OP on the xOy plane. Segmenting samples along the plane perpendicular to the OP direction is obviously inconsistent with the actual distribution of stratigraphic deposits, especially when dividing samples with small spacing and high resolution, the sediments of different layers will be divided into the same sample, resulting in the test Results were mixed and uncharacterized.
针对以上问题,本发明提出一种分样方法以解决,具体为:For above problem, the present invention proposes a kind of sampling method to solve, specifically:
(1)在进行柱状样品剖分前,首先进行X光影像扫描,转动柱状样当X射线方向与沉积层布平行时,获得最清晰的层布影像,并标出不同层位的角度分布。(1) Before dissecting the columnar sample, first scan the X-ray image, rotate the columnar sample when the X-ray direction is parallel to the deposition layer distribution, obtain the clearest layer distribution image, and mark the angular distribution of different layers.
(2)据此确定样品的剖切面,是一个与沉积物层布面xOy垂直且经过轴OP的平面(图15中的面OCPP′),将柱状样品沿剖切面剖开获得镜像对称的两半样品。(2) Based on this, the section plane of the sample is determined, which is a plane perpendicular to the sediment layer distribution surface xOy and passing through the axis OP (the plane OCPP' in Fig. 15), and the columnar sample is cut along the section plane to obtain two symmetrical half sample.
(3)根据X光影像上对应的标记角度,沿平行于沉积层进行样品分割并记录。此方法能够保证切分样品与实际沉积层布保持一致,减小不同层位沉积样品混合,提高样品切分准确度。(3) According to the corresponding marking angle on the X-ray image, the sample is segmented and recorded parallel to the deposition layer. This method can ensure that the segmented samples are consistent with the actual deposition layer distribution, reduce the mixing of deposition samples at different layers, and improve the accuracy of sample segmentation.
本实施例提供的方法中对柱状样品的切分采用实施例1中的分样平台,具体切分过程如下所述:In the method provided in this embodiment, the splitting platform of the columnar sample is adopted in Example 1, and the specific splitting process is as follows:
(1)根据沉积物柱状样半径选择合适的固定底座9和固定抱箍10,根据切分间距选择合适的步进手柄,根据柱状样X射线扫描层位特性确定剖分平面,标记剖分线位置;(1) Select the appropriate fixed
(2)将柱状样品及取样管置于固定底座半圆形凹槽内,闭合固定抱箍10,将固定插销11插入操作台面的对应固定孔内,旋转蝶形螺丝12顶住固定抱箍10,将取样管外壳夹紧;(2) Place the columnar sample and sampling tube in the semicircular groove of the fixed base, close the fixed
(3)松开T型滑轨15上的蝶形螺丝12,上、下、左、右移动T型滑轨15,调整无屑切割刀14的位置,水平方向上使切割刀与柱状样品圆心处于同一高度,切入深度为切割外壳但不切透(距内壁约0.5mm为宜),拧紧蝶形螺丝12固定无屑切割刀14的位置;(3) Loosen the
(4)打开电机13电源同时缓慢推动T型滑块16沿滑轨4移动,剖切外壳;将柱状样品旋转180°以上述相同方式进行对侧剖切;沿剖切面剖分后样品如图16所示;(4) Turn on the power supply of the
(5)松开固定夹紧装置8上的蝶形螺丝12,打开固定抱箍10,用壁纸刀沿无屑切割刀剖切槽线,将剩余外壳割开去除上半圆外壳;(5) Loosen the
(6)将样品起始端、步进手柄19和起始刻度线对齐,根据需要调整角度器18角度(建议角度器18窄缝平面与X光影像显示的沉积层平行);(6) Align the starting end of the sample, the stepping
(7)转动步进手柄19使支架17向后移动一个剖分间距,取一个分样刀片,将其沿角度器18中间的窄缝插下,完成一个样品切分;(7) Turn the stepping handle 19 to move the
重复步骤(7),即可快速完成后续样品切分,工作完成后对装置进行清理和保养。Repeat step (7) to quickly complete subsequent sample segmentation, and clean and maintain the device after the work is completed.
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