CN115707447A - Double-layer makeup fixing spray and preparation process thereof - Google Patents

Double-layer makeup fixing spray and preparation process thereof Download PDF

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Publication number
CN115707447A
CN115707447A CN202110962628.XA CN202110962628A CN115707447A CN 115707447 A CN115707447 A CN 115707447A CN 202110962628 A CN202110962628 A CN 202110962628A CN 115707447 A CN115707447 A CN 115707447A
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polydimethylsiloxane
double
layer
spray
transparent
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CN202110962628.XA
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Chinese (zh)
Inventor
李继承
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Suzhou Ante Cosmetics Co ltd
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Suzhou Ante Cosmetics Co ltd
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Priority to CN202110962628.XA priority Critical patent/CN115707447A/en
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Abstract

The invention discloses a double-layer makeup fixing spray, wherein the upper layer is a transparent oil phase and comprises the following raw materials: acrylates/stearyl acrylate/dimethicone methacrylate copolymer, cyclopentadimethicone, dimethicone, trimethylsiloxysilicate, cyclopentadimethicone, and dimethicone/vinyl dimethicone crosspolymer, polymethylsilsesquioxane, rose essential oil; the lower layer is a transparent water phase and comprises the following raw material components: deionized water, VP/VA copolymer, 1, 3-butanediol, sodium chloride, phenoxyethanol, ethylhexyl glycerin, chlorphenesin and sodium hyaluronate; mixing the oil phase and the water phase according to a mass ratio, filling into a spray bottle to obtain a double-layer makeup fixing spray, and shaking uniformly for use; the double-layer make-up fixing spray disclosed by the invention is in a mist shape, and after the make-up fixing spray is used on the face, the spray is uniformly dispersed on the face to form a make-up fixing film, so that the effects of moisturizing and long-acting make-up fixing are achieved.

Description

Double-layer makeup fixing spray and preparation process thereof
Technical Field
The invention relates to a double-layer makeup fixing spray and a preparation process thereof, belonging to the technical field of cosmetics.
Background
The makeup color products in the current market are numerous, the problems that the makeup effect is not lasting and the makeup is easy to remove can be met when a consumer uses the makeup color product, the effect of lasting makeup effect needs to be achieved by means of other products, and the makeup fixing spray can meet the requirements; the makeup fixing spray film-forming agent used in the market at present is mainly water-soluble acrylate copolymer, and has poor compatibility with common water-in-oil makeup products, so that a good makeup fixing effect cannot be achieved.
Disclosure of Invention
In view of the above technical problems, the present invention aims to: provides a double-layer makeup fixing spray and a preparation process thereof.
The technical solution of the present invention is thus achieved; a double-layer makeup fixing spray comprises an upper layer of transparent oil phase and a lower layer of transparent water phase; the mass ratio of the water phase to the oil phase is (1-6): 1; the upper oil phase comprises the following raw material components: acrylic acid (ester)/stearyl alcohol acrylate/polydimethylsiloxane methacrylate copolymer 0.1-0.5%, cyclopentadimethylsiloxane 10-65%, polydimethylsiloxane 10-40%, trimethylsiloxysilicate 5-25%, cyclopentadimethylsiloxane and polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer 0.1-2%, polymethylsilsesquioxane 1-5%, rose essential oil 0.1-0.5%; the lower aqueous phase comprises the following raw material components: 80-95% of deionized water, 1-5% of VP/VA copolymer, 1-5% of 1, 3-butanediol, 0.5-1.5% of sodium chloride, 0.1-0.8% of phenoxyethanol, 0.01-0.08% of ethylhexyl glycerol, 0.1-0.3% of chlorphenesin and 0.05-0.15% of sodium hyaluronate.
A double-layer makeup fixing spray and a preparation process thereof comprise the following steps:
(1) the oil phase is prepared by heating acrylic acid (ester)/stearyl acrylate/polydimethylsiloxane methacrylate copolymer and cyclopenta dimethyl siloxane to 70 ℃ to be completely dissolved, adding polydimethylsiloxane, trimethylsiloxysilicate, cyclopenta dimethyl siloxane, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and polymethylsilsesquioxane, stirring at the normal temperature by a stirrer at the stirring speed of 1000r/min until the mixture is transparent, adding rose essential oil, and stirring until the mixture is transparent.
(2) Mixing deionized water, VP/VA copolymer, 1, 3-butanediol, sodium chloride, phenoxyethanol, ethylhexylglycerin, chlorphenesin and sodium hyaluronate in water phase, heating to 70 deg.C, stirring with a stirrer at a stirring speed of 1000r/min, stirring to transparent, and cooling to room temperature to obtain water phase
(3) And (3) filling the oil phase and the water phase into a spray bottle according to the mass ratio of 1-6.
Due to the application of the technical scheme, compared with the prior art, the invention has the following advantages:
the double-layer makeup fixing spray contains the oil-soluble film agent and the water-soluble film agent, is good in compatibility with makeup base products, effectively increases the makeup duration time, is efficient, and simultaneously is added with the rose essential oil and the sodium hyaluronate, so that the effects of moisturizing and nourishing skin are achieved while makeup fixing.
Detailed Description
The double-layer makeup fixing spray has the advantages that the upper layer is a transparent oil phase, and the lower layer is a transparent water phase; the upper oil phase comprises the following raw material components: 0.1-0.5% of acrylic acid (ester)/stearyl alcohol acrylate/polydimethylsiloxane methacrylate copolymer, 10-65% of cyclopentadimethylsiloxane, 10-40% of polydimethylsiloxane, 5-25% of trimethylsiloxysilicate, 0.1-2% of cyclopentadimethylsiloxane and polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 1-5% of polymethylsilsesquioxane and 0.1-0.5% of rose essential oil; the lower aqueous phase comprises the following raw material components: 87-97% of deionized water, 1-5% of VP/VA copolymer, 1-5% of 1, 3-butanediol, 0.5-1.5% of sodium chloride, 0.1-0.8% of phenoxyethanol, 0.01-0.08% of ethylhexyl glycerol, 0.1-0.3% of chlorphenesin and 0.05-0.15% of sodium hyaluronate. Mixing an oil phase and a water phase, wherein the mass of the water phase is as follows: oil phase mass = 1.
The present invention is further illustrated by the following examples.
Oil phase formulation the component contents of examples 1-3 are shown in the following table:
Figure BDA0003222805350000031
aqueous phase formulation examples 1-3 had the following composition levels:
Figure BDA0003222805350000032
Figure BDA0003222805350000041
wherein, the unit of each component is percentage, and the sum of the raw materials of the formula in each embodiment is 100%.
The preparation process of the double-layer makeup fixing spray of the embodiment 1-3 comprises the following steps:
(1) heating acrylic acid (ester)/stearyl acrylate/polydimethylsiloxane methacrylate copolymer and cyclopenta polydimethylsiloxane to 70 ℃ for complete dissolution, adding polydimethylsiloxane, trimethylsiloxysilicate, cyclopenta polydimethylsiloxane, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and polymethylsilsesquioxane, stirring by a stirrer at normal temperature at the stirring speed of 800-1200 r/min, stirring to be transparent, adding rose essential oil, and stirring to be transparent to obtain an oil phase;
(2) mixing deionized water, VP/VA copolymer, 1, 3-butanediol, sodium chloride, phenoxyethanol, ethylhexylglycerin, chlorphenesin and sodium hyaluronate, heating to 70 ℃, stirring by a stirrer at the stirring speed of 800-1200 r/min until the mixture is transparent, and cooling to room temperature to obtain a water phase;
(3) filling the oil phase and the water phase into a spray bottle according to the mass ratio, mixing to obtain the double-layer makeup fixing spray, and shaking uniformly to use.
The preparation method can obtain high-quality products and is easy for mass production.
The above-mentioned embodiments are merely illustrative of the technical idea and features of the present invention, and the purpose thereof is to enable those skilled in the art to understand the contents of the present invention and implement the present invention, and not to limit the scope of the present invention, and all equivalent changes or modifications made according to the spirit of the present invention should be covered in the scope of the present invention.

Claims (2)

1. A double-layer makeup fixing spray is characterized in that: comprises an upper layer of transparent oil phase and a lower layer of transparent water phase; the mass ratio of the water phase to the oil phase is (1-6): 1;
the upper oil phase comprises the following raw material components: acrylic acid (ester)/stearyl alcohol acrylate/polydimethylsiloxane methacrylate copolymer 0.1-0.5%, cyclopentadimethylsiloxane 10-65%, polydimethylsiloxane 10-40%, trimethylsiloxysilicate 5-25%, cyclopentadimethylsiloxane and polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer 0.1-2%, polymethylsilsesquioxane 1-5%, rose essential oil 0.1-0.5%;
the lower aqueous phase comprises the following raw material components: 80-95% of deionized water, 1-5% of VP/VA copolymer, 1-5% of 1, 3-butanediol, 0.5-1.5% of sodium chloride, 0.1-0.8% of phenoxyethanol, 0.01-0.08% of ethylhexyl glycerol, 0.1-0.3% of chlorphenesin and 0.05-0.15% of sodium hyaluronate.
2. A double-layer makeup fixing spray and a preparation process thereof are characterized by comprising the following steps:
(1) heating acrylic acid (ester)/stearyl acrylate/polydimethylsiloxane methacrylate copolymer and cyclopenta polydimethylsiloxane to 70 ℃ for complete dissolution, adding polydimethylsiloxane, trimethylsiloxysilicate, cyclopenta polydimethylsiloxane, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and polymethylsilsesquioxane, stirring by a stirrer at normal temperature at the stirring speed of 800-1200 r/min, stirring to be transparent, adding rose essential oil, and stirring to be transparent to obtain an oil phase;
(2) mixing deionized water, VP/VA copolymer, 1, 3-butanediol, sodium chloride, phenoxyethanol, ethylhexylglycerin, chlorphenesin and sodium hyaluronate, heating to 70 ℃, stirring by a stirrer at the stirring speed of 800-1200 r/min until the mixture is transparent, and cooling to room temperature to obtain a water phase;
(3) filling the oil phase and the water phase into a spray bottle according to the mass ratio, mixing to obtain the double-layer makeup fixing spray, and shaking uniformly to use.
CN202110962628.XA 2021-08-20 2021-08-20 Double-layer makeup fixing spray and preparation process thereof Pending CN115707447A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107233225A (en) * 2017-06-20 2017-10-10 广东盛美化妆品有限公司 A kind of oil-control air cushion BB frosts and preparation method thereof
CN107669515A (en) * 2017-09-19 2018-02-09 诺斯贝尔化妆品股份有限公司 It is a kind of persistently to hide flaw moisturizing air cushion BB frosts
CN111920710A (en) * 2020-09-24 2020-11-13 苏州安特化妆品股份有限公司 High-covering concealer and preparation process thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107233225A (en) * 2017-06-20 2017-10-10 广东盛美化妆品有限公司 A kind of oil-control air cushion BB frosts and preparation method thereof
CN107669515A (en) * 2017-09-19 2018-02-09 诺斯贝尔化妆品股份有限公司 It is a kind of persistently to hide flaw moisturizing air cushion BB frosts
CN111920710A (en) * 2020-09-24 2020-11-13 苏州安特化妆品股份有限公司 High-covering concealer and preparation process thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
株式会社高丝: "高丝持久定妆喷雾", pages 3 - 4, Retrieved from the Internet <URL:进口普通化妆品备案信息> *

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