CN111920710A - High-covering concealer and preparation process thereof - Google Patents
High-covering concealer and preparation process thereof Download PDFInfo
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- CN111920710A CN111920710A CN202011014044.1A CN202011014044A CN111920710A CN 111920710 A CN111920710 A CN 111920710A CN 202011014044 A CN202011014044 A CN 202011014044A CN 111920710 A CN111920710 A CN 111920710A
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- polydimethylsiloxane
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
Abstract
The invention discloses a high-covering concealer, which is characterized in that polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer are added into a product, so that the product can be pasted while keeping high covering; in order to match the using feeling of the product, a large amount of emollient such as: isononyl isononanoate, tridecyl alcohol trimellitate, octyl polymethylsiloxane, polydimethylsiloxane cross-linked polymer and the like, so that the use feeling is further improved on the whole; the toner of the product is treated by a special process, so that the product can keep high covering and is also conformable, not dry, not greasy and refreshing.
Description
Technical Field
The invention relates to a concealer with high covering power and a preparation process thereof, belonging to the technical field of cosmetics.
Background
Most of the high-covering concealer liquid on the market at present has the conditions of thick and heavy skin feel, non-fitting, difficult pushing, strong powder feel, air impermeability, easy smoldering makeup and the like; the product of the invention is a water-in-oil system product, and the obtained product has better fitting performance, keeps high covering power, is more fitting, smooth and not dry.
Disclosure of Invention
In view of the above technical problems, the present invention aims to: provides a concealer liquid with high covering power and a preparation process thereof.
The technical solution of the invention is realized as follows: a concealer with high covering power comprises the following raw material components: deionized water, 5-15 percent of cyclopentadimethylsiloxane, 3-8 percent of isononyl isononanoate, 1-7 percent of isododecane, 1-5 percent of butanediol, 1-5 percent of polydimethylsiloxane, 1-5 percent of tridecyl trimellitate, 1-5 percent of lauryl PEG-9 polydimethylsiloxane, 1-10 percent of glycerol, 1-5 percent of PEG-10 polydimethylsiloxane, 0.5-5 percent of trimethylsiloxy silicate, 1-5 percent of octyl methicone, 1-5 percent of silica, 0.5-1 percent of sodium chloride, 1-5 percent of polydimethylsiloxane/vinyl dimethicone crosspolymer, 0.1-1 percent of quaternary ammonium salt-18 bentonite, 0.5 to 5 percent of mica, 0.5 to 5 percent of talcum powder, 0.5 to 5 percent of polydimethylsiloxane cross-linked polymer, 0.3 to 0.7 percent of phenoxyethanol, 0.3 to 0.7 percent of beeswax, 1 to 5 percent of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 0.1 to 1 percent of triethoxy octyl silane, 0.01 to 0.3 percent of chlorphenesin, 0.1 to 0.5 percent of tocopherol acetate, 0.01 to 0.05 percent of ethylhexyl glycerol, 0.05 to 0.1 percent of disodium EDTA, 0.01 to 0.05 percent of glyceryl polyether-26, 0.01 to 0.05 percent of betaine, 0.01 to 0.05 percent of glucose, 0.01 to 0.05 percent of isocetyl polyether-10, 0.01 to 0.05 percent of raffinose, 0.02 to 0.1 percent of Hibiscus sculpos (Hippo Mutabilis) flower extract, 0.02 to 0.1 percent of hippophae rhamnoides (Hippo officinalis) extract, 0.005-0.01% of cyclotetrasiloxane, 0.01-0.02% of tocopherol (vitamin E), 0.02-0.1% of sodium hyaluronate, CI77891, CI77491, CI77499, CI77492 and CI 77002.
A preparation process of a concealer with high covering power comprises the following steps:
firstly, fully and uniformly stirring deionized water, chlorphenesin, EDTA disodium and sodium chloride at the rotation speed of 600-800 rpm/min; adding glycerol, butanediol, betaine, glucose, glyceryl polyether-26, raffinose, sodium hyaluronate, fructus Hippophae extract, and flos Hibisci Mutabilis extract, stirring at 800-; finally heating to 80-85 ℃, keeping the temperature and stirring for 10-15min, and putting into a main emulsifying pot after ensuring that the water phase system is transparent, clear and free of particles;
adding dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer, vinyl dimethyl silicone polymer/polymethyl silicone silsesquioxane cross-linked polymer, isocetyl polyether-10, silica, titanium dioxide, iron yellow, iron red, iron black, triethoxy octyl siloxane and alumina into a high-speed stirrer, rotating at 900rpm/min, fully and uniformly stirring, and checking that no pigment point exists;
mixing and stirring cyclopentadimethylsiloxane, cyclotetradimethylsiloxane, isododecane and trimethylsiloxy silicate uniformly until the mixture is transparent, and stirring the mixture at the speed of 500 rpm/min; then adding beeswax into the equipment, uniformly stirring, heating to 60-65 ℃, weighing isononyl isononanoate, polydimethylsiloxane, tridecyl alcohol trimellitate, lauryl PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane, PEG-10 polydimethylsiloxane, octyl polydimethylsiloxane, quaternary ammonium salt-18 bentonite, polydimethylsiloxane cross-linked polymer and tocopherol acetate together and stirring after the beeswax is completely melted;
fourthly, adding the product obtained in the second step into the product obtained in the third step, stirring, heating to 75-80 ℃, stirring at the speed of 1500-2000rpm/min, and stirring for 10min under heat preservation;
slowly adding the product obtained in the step (III) into a main emulsifying pot in which the product obtained in the step (IV) is positioned, starting homogenization, wherein the homogenization rotation degree is 2000-2500rpm/min, and the adding time is 15min, and after the product is completely added, the homogenization rotation speed is changed to 3000rpm/min, and the homogenization time is 15-20 min;
sixthly, after the temperature is reduced to 38 ℃, adding phenoxyethanol and ethylhexyl glycerol, fully and uniformly stirring, starting stirring and homogenizing, wherein the stirring speed is 800-2500 rpm/min, and the homogenizing speed is 2000-2500-rpm/min, and the time is 5 min.
Due to the application of the technical scheme, compared with the prior art, the invention has the following advantages:
the polydimethylsiloxane/vinyl polydimethylsiloxane crosslinked polymer and the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosslinked polymer are added into the product, so that the product can be well fitted while high covering is kept; in order to match the using feeling of the product, a large amount of emollient such as: isononyl isononanoate, tridecyl alcohol trimellitate, octyl polymethylsiloxane, polydimethylsiloxane crosslinked polymer and the like, so that the use feeling is further improved on the whole.
The toner of the product is treated by a special process, so that the product can keep high covering and is also conformable, not dry, not greasy and refreshing.
Detailed Description
The present invention is further illustrated by the following examples.
The invention relates to a high-covering concealer liquid which comprises the following raw material components: deionized water, 5-15 percent of cyclopentadimethylsiloxane, 3-8 percent of isononyl isononanoate, 1-7 percent of isododecane, 1-5 percent of butanediol, 1-5 percent of polydimethylsiloxane, 1-5 percent of tridecyl trimellitate, 1-5 percent of lauryl PEG-9 polydimethylsiloxane, 1-10 percent of glycerol, 1-5 percent of PEG-10 polydimethylsiloxane, 0.5-5 percent of trimethylsiloxy silicate, 1-5 percent of octyl methicone, 1-5 percent of silica, 0.5-1 percent of sodium chloride, 1-5 percent of polydimethylsiloxane/vinyl dimethicone crosspolymer, 0.1-1 percent of quaternary ammonium salt-18 bentonite, 0.5 to 5 percent of mica, 0.5 to 5 percent of talcum powder, 0.5 to 5 percent of polydimethylsiloxane cross-linked polymer, 0.3 to 0.7 percent of phenoxyethanol, 0.3 to 0.7 percent of beeswax, 1 to 5 percent of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 0.1 to 1 percent of triethoxy octyl silane, 0.01 to 0.3 percent of chlorphenesin, 0.1 to 0.5 percent of tocopherol acetate, 0.01 to 0.05 percent of ethylhexyl glycerol, 0.05 to 0.1 percent of disodium EDTA, 0.01 to 0.05 percent of glyceryl polyether-26, 0.01 to 0.05 percent of betaine, 0.01 to 0.05 percent of glucose, 0.01 to 0.05 percent of isocetyl polyether-10, 0.01 to 0.05 percent of raffinose, 0.02 to 0.1 percent of Hibiscus sculpos (Hippo Mutabilis) flower extract, 0.02 to 0.1 percent of hippophae rhamnoides (Hippo officinalis) extract, 0.005-0.01% of cyclotetrasiloxane, 0.01-0.02% of tocopherol (vitamin E), 0.02-0.1% of sodium hyaluronate, CI77891, CI77491, CI77499, CI77492 and CI 77002.
The component contents of examples 1 to 3 are shown in the following table:
wherein, the unit of each component is percentage, and the sum of the raw materials of the formula in each embodiment is 100%.
The high hiding concealer solutions of examples 1-3 above were prepared as follows:
firstly, fully and uniformly stirring deionized water, chlorphenesin, EDTA disodium and sodium chloride at the rotation speed of 600-800 rpm/min; adding glycerol, butanediol, betaine, glucose, glyceryl polyether-26, raffinose, sodium hyaluronate, fructus Hippophae extract, and flos Hibisci Mutabilis extract, stirring at 800-; finally heating to 80-85 ℃, keeping the temperature and stirring for 10-15min, and putting into a main emulsifying pot after ensuring that the water phase system is transparent, clear and free of particles;
adding dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer, vinyl dimethyl silicone polymer/polymethyl silicone silsesquioxane cross-linked polymer, isocetyl polyether-10, silica, titanium dioxide, iron yellow, iron red, iron black, triethoxy octyl siloxane and alumina into a high-speed stirrer, rotating at 900rpm/min, fully and uniformly stirring, and checking that no pigment point exists;
mixing and stirring cyclopentadimethylsiloxane, cyclotetradimethylsiloxane, isododecane and trimethylsiloxy silicate uniformly until the mixture is transparent, and stirring the mixture at the speed of 500 rpm/min; then adding beeswax into the equipment, uniformly stirring, heating to 60-65 ℃, weighing isononyl isononanoate, polydimethylsiloxane, tridecyl alcohol trimellitate, lauryl PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane, PEG-10 polydimethylsiloxane, octyl polydimethylsiloxane, quaternary ammonium salt-18 bentonite, polydimethylsiloxane cross-linked polymer and tocopherol acetate together and stirring after the beeswax is completely melted;
fourthly, adding the product obtained in the second step into the product obtained in the third step, stirring, heating to 75-80 ℃, stirring at the speed of 1500-2000rpm/min, and stirring for 10min under heat preservation;
slowly adding the product obtained in the step (III) into a main emulsifying pot in which the product obtained in the step (IV) is positioned, starting homogenization, wherein the homogenization rotation degree is 2000-2500rpm/min, and the adding time is 15min, and after the product is completely added, the homogenization rotation speed is changed to 3000rpm/min, and the homogenization time is 15-20 min;
sixthly, after the temperature is reduced to 38 ℃, adding phenoxyethanol and ethylhexyl glycerol, fully and uniformly stirring, starting stirring and homogenizing, wherein the stirring speed is 800-2500 rpm/min, and the homogenizing speed is 2000-2500-rpm/min, and the time is 5 min.
The preparation method can obtain high-quality products and is easy for mass production.
The above-mentioned embodiments are merely illustrative of the technical idea and features of the present invention, and the purpose thereof is to enable those skilled in the art to understand the contents of the present invention and implement the present invention, and not to limit the scope of the present invention, and all equivalent changes or modifications made according to the spirit of the present invention should be covered in the scope of the present invention.
Claims (2)
1. The concealer liquid with high covering power is characterized by comprising the following raw material components: deionized water, 5-15 percent of cyclopentadimethylsiloxane, 3-8 percent of isononyl isononanoate, 1-7 percent of isododecane, 1-5 percent of butanediol, 1-5 percent of polydimethylsiloxane, 1-5 percent of tridecyl trimellitate, 1-5 percent of lauryl PEG-9 polydimethylsiloxane, 1-10 percent of glycerol, 1-5 percent of PEG-10 polydimethylsiloxane, 0.5-5 percent of trimethylsiloxy silicate, 1-5 percent of octyl methicone, 1-5 percent of silica, 0.5-1 percent of sodium chloride, 1-5 percent of polydimethylsiloxane/vinyl dimethicone crosspolymer, 0.1-1 percent of quaternary ammonium salt-18 bentonite, 0.5 to 5 percent of mica, 0.5 to 5 percent of talcum powder, 0.5 to 5 percent of polydimethylsiloxane cross-linked polymer, 0.3 to 0.7 percent of phenoxyethanol, 0.3 to 0.7 percent of beeswax, 1 to 5 percent of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 0.1 to 1 percent of triethoxy octyl silane, 0.01 to 0.3 percent of chlorphenesin, 0.1 to 0.5 percent of tocopherol acetate, 0.01 to 0.05 percent of ethylhexyl glycerol, 0.05 to 0.1 percent of disodium EDTA, 0.01 to 0.05 percent of glyceryl polyether-26, 0.01 to 0.05 percent of betaine, 0.01 to 0.05 percent of glucose, 0.01 to 0.05 percent of isocetyl polyether-10, 0.01 to 0.05 percent of raffinose, 0.02 to 0.1 percent of cotton rose hibiscus extract, 0.02 to 0.1 percent of sea buckthorn extract, 0.005-0.01% of cyclotetrasiloxane, 0.01-0.02% of tocopherol, 0.02-0.1% of sodium hyaluronate, CI77891, CI77491, CI77499, CI77492 and CI 77002.
2. A preparation process of a concealer with high covering power is characterized by comprising the following steps:
firstly, fully and uniformly stirring deionized water, chlorphenesin, EDTA disodium and sodium chloride at the rotation speed of 600-800 rpm/min; adding glycerol, butanediol, betaine, glucose, glyceryl polyether-26, raffinose, sodium hyaluronate, fructus Hippophae extract, and flos Hibisci Mutabilis extract, stirring at 800-; finally heating to 80-85 ℃, keeping the temperature and stirring for 10-15min, and putting into a main emulsifying pot after ensuring that the water phase system is transparent, clear and free of particles;
adding dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer, vinyl dimethyl silicone polymer/polymethyl silicone silsesquioxane cross-linked polymer, isocetyl polyether-10, silica, titanium dioxide, iron yellow, iron red, iron black, triethoxy octyl siloxane and alumina into a high-speed stirrer, rotating at 900rpm/min, fully and uniformly stirring, and checking that no pigment point exists;
mixing and stirring cyclopentadimethylsiloxane, cyclotetradimethylsiloxane, isododecane and trimethylsiloxy silicate uniformly until the mixture is transparent, and stirring the mixture at the speed of 500 rpm/min; then adding beeswax into the equipment, uniformly stirring, heating to 60-65 ℃, weighing isononyl isononanoate, polydimethylsiloxane, tridecyl alcohol trimellitate, lauryl PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane, PEG-10 polydimethylsiloxane, octyl polydimethylsiloxane, quaternary ammonium salt-18 bentonite, polydimethylsiloxane cross-linked polymer and tocopherol acetate together and stirring after the beeswax is completely melted;
fourthly, adding the product obtained in the second step into the product obtained in the third step, stirring, heating to 75-80 ℃, stirring at the speed of 1500-2000rpm/min, and stirring for 10min under heat preservation;
slowly adding the product obtained in the step (III) into a main emulsifying pot in which the product obtained in the step (IV) is positioned, starting homogenization, wherein the homogenization rotation degree is 2000-2500rpm/min, and the adding time is 15min, and after the product is completely added, the homogenization rotation speed is changed to 3000rpm/min, and the homogenization time is 15-20 min;
sixthly, after the temperature is reduced to 38 ℃, adding phenoxyethanol and ethylhexyl glycerol, fully and uniformly stirring, starting stirring and homogenizing, wherein the stirring speed is 800-2500 rpm/min, and the homogenizing speed is 2000-2500-rpm/min, and the time is 5 min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011014044.1A CN111920710A (en) | 2020-09-24 | 2020-09-24 | High-covering concealer and preparation process thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011014044.1A CN111920710A (en) | 2020-09-24 | 2020-09-24 | High-covering concealer and preparation process thereof |
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| CN111920710A true CN111920710A (en) | 2020-11-13 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202011014044.1A Pending CN111920710A (en) | 2020-09-24 | 2020-09-24 | High-covering concealer and preparation process thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113520983A (en) * | 2021-08-02 | 2021-10-22 | 觅方(杭州)化妆品有限公司 | Double-tube foundation essence |
| CN114053160A (en) * | 2021-12-06 | 2022-02-18 | 上海大喂科技发展有限公司 | Concealer and preparation method thereof |
| CN115707447A (en) * | 2021-08-20 | 2023-02-21 | 苏州安特化妆品股份有限公司 | Double-layer makeup fixing spray and preparation process thereof |
-
2020
- 2020-09-24 CN CN202011014044.1A patent/CN111920710A/en active Pending
Non-Patent Citations (1)
| Title |
|---|
| 苏州安特化妆品股份有限公司: "Cata.Q86 流金溢彩瓷光粉底液 N1", 《国产非特殊用途化妆品备案信息服务平台》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113520983A (en) * | 2021-08-02 | 2021-10-22 | 觅方(杭州)化妆品有限公司 | Double-tube foundation essence |
| CN115707447A (en) * | 2021-08-20 | 2023-02-21 | 苏州安特化妆品股份有限公司 | Double-layer makeup fixing spray and preparation process thereof |
| CN114053160A (en) * | 2021-12-06 | 2022-02-18 | 上海大喂科技发展有限公司 | Concealer and preparation method thereof |
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Application publication date: 20201113 |