CN110051553A - A kind of formula and preparation method thereof of waterproof foundation emulsion - Google Patents

A kind of formula and preparation method thereof of waterproof foundation emulsion Download PDF

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Publication number
CN110051553A
CN110051553A CN201910192725.8A CN201910192725A CN110051553A CN 110051553 A CN110051553 A CN 110051553A CN 201910192725 A CN201910192725 A CN 201910192725A CN 110051553 A CN110051553 A CN 110051553A
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dimethyl silicone
iron oxide
silicone polymer
ppg
peg
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陈礼桐
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Guangzhou Poly Cosmetics Co Ltd
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Guangzhou Poly Cosmetics Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/12Face or body powders for grooming, adorning or absorbing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

A kind of waterproof powder bottom formula of liquid and preparation method thereof, it includes following component: ring five dimethyl silicone polymer, Permethyl 99A, propylene glycol, isononyl isononanoate, trimethyl silicane alkoxy esters of silicon acis, Dimethicone Crosspolymer, phenyl trimethicone, cetyl PEG/PPG-10/1 dimethyl silicone polymer, dimethyl silicone polymer, double-PEG/PPG-14/14 dimethyl silicone polymers, silica, polymethyl methacrylate, boron nitride, glyceryl behenate/20 acid esters, magnesium sulfate, tocopherol acetate, titanium dioxide, iron oxide yellow, iron oxide red, iron oxide black, Phenoxyethanol, Sensiva SC50.Waterproof foundation emulsion of the present invention; the film of one layer of protection is formed in skin surface; has the effect of certain isolation external injury; the persistence of makeup is stronger; pore, acne print can be desalinated well, and to no skin irritation, there is good matte effect; adornment effect nature can be made lasting, while uniformly correcting the colour of skin.

Description

A kind of formula and preparation method thereof of waterproof foundation emulsion
Technical field
The present invention relates to a kind of formulas of foundation emulsion, refer in particular to the formula and system of a kind of foundation emulsion with waterproof effect Preparation Method.
Background technique
Foundation cream is the necessity of schoolgirl's makeup, is the basis of dressing, foundation emulsion is the foundation cream of liquid, it is the first of makeup The final step of step and skin care, the dust etc. obstructed in air enter skin, shield.
Existing many foundation emulsions are all inclined moist types, have certain moistening effect, but poor waterproof properties, makeup Persistence is long, the effect of concealing is inadequate, when it is high to encounter weather temperature, or perspires, the easy bellding light of face or De- adornment.
Therefore it provides a kind of concealing effect is good, the good foundation emulsion of waterproof performance is actually necessary.
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of waterproof powder bottom formula of liquid comprising following component: goes Ionized water, ring five dimethyl silicone polymer, Permethyl 99A, trimethyl silicane alkoxy esters of silicon acis, dimethyl silicone polymer crosslinking are poly- Close object, cetyl PEG/PPG-10/1 dimethyl silicone polymer, double-PEG/PPG-14/14 dimethyl silicone polymers, silica, sweet Oily behenate/20 acid esters, dimethyl silicone polymer, magnesium sulfate, titanium dioxide, iron oxide yellow, iron oxide red, iron oxide Black, Phenoxyethanol.
Can further comprise also following components in addition to above-mentioned necessary component: propylene glycol, be gathered phenyl trimethicone Methyl methacrylate, boron nitride, tocopherol acetate, Sensiva SC50.
Waterproof powder bottom of the present invention formula of liquid comprising following component (by weight ratio):
20% ∽ 30% of deionized water, 8% ∽ 15% of ring five dimethyl silicone polymer, 8% ∽ 13% of Permethyl 99A, the third two 6% ∽ 10% of alcohol, 5% ∽ 9% of isononyl isononanoate, 5% ∽ 8% of trimethyl silicane alkoxy esters of silicon acis, dimethyl silicone polymer 4.5% ∽ 7.5% of cross-linked polymer, 4% ∽ 6% of phenyl trimethicone, cetyl PEG/PPG-10/1 poly dimethyl 3% ∽ 5% of siloxanes, 2.5% ∽ 5% of dimethyl silicone polymer, double-PEG/PPG-14/14 dimethyl silicone polymers 2.5% ∽ 4.5%, 2.4% ∽ 4.3% of silica, 2.2% ∽ 4% of polymethyl methacrylate, 2% ∽ 3.6% of boron nitride, glycerol behenyl 2% ∽ 3% of acid esters/20 acid esters, 0.8% ∽ 1.2% of magnesium sulfate, 0.2% ∽ 0.5% of tocopherol acetate, titanium dioxide 3.6% ∽ 9.6%, 5% ∽ 8% of iron oxide yellow, 2% ∽ 6% of iron oxide red, 0.5% ∽ 3.3% of iron oxide black, Phenoxyethanol 0.1% ∽ 0.3%, 0.1% ∽ 0.2% of Sensiva SC50.
The present invention also provides a kind of methods for preparing waterproof powder bottom formula of liquid comprising following steps:
Step 1) is weighed Permethyl 99A, ring five dimethyl silicone polymer, trimethyl silicane alcoxyl in oily phase by setting ratio Base esters of silicon acis is stirred at normal temperature to being completely dissolved;
Step 2) is proportionally added into Dimethicone Crosspolymer, phenyl trimethicone, cetyl again PEG/PPG-10/1 dimethyl silicone polymer, double-PEG/PPG-14/14 dimethyl silicone polymers, dimethyl silicone polymer, glycerol Behenate/20 acid esters, agitating and heating dissolution, temperature control at 90 DEG C hereinafter, until be completely dissolved, 3 ∽ of homogeneous 5 minutes, 2800 revs/min, and kept for 70-90 DEG C of constant temperature;
Step 3) weighs the deionized water in water phase, is heated to 90 DEG C, keeps the temperature 10 minutes and sterilizes, is cooled to 85 DEG C, then plus Enter propylene glycol, magnesium sulfate, stirring is kept for 85 DEG C of constant temperature to being completely dissolved;
Water phase is slowly added into oily phase, stirs 5 minutes, then 3 ∽ of homogeneous while quick stirring oily phase by step 4) 5 minutes, 2800 revs/min;
Step 5) weigh isononyl isononanoate, Permethyl 99A, ring five dimethyl silicone polymer, titanium dioxide, iron oxide yellow, Iron oxide red, iron oxide black, silica, polymethyl methacrylate, boron nitride, are uniformly mixed, and impregnate 3 hours, cross and grind 2 ∽ of machine 3 times is made the mill base of color uniformly, fine and smooth, is then added in the Material emulsified, is thoroughly mixed uniformly, then 3 ∽ of matter 5 minutes, 2800 revs/min;
Phenoxyethanol, Sensiva SC50, tocopherol acetate are added sequentially in Material by step 6), are stirred Uniformly, waterproof foundation emulsion finished product is obtained.
Compared with prior art, a kind of waterproof foundation emulsion of the present invention uses ring five dimethyl silicone polymer, Permethyl 99A Compatibility mixing is carried out Deng containing various silicon compound moisturizing raw materials, the film of one layer of protection is formed in skin surface, has certain Isolation external injury effect, the persistence of makeup is stronger, can desalinate pore, acne print well, and non-stimulated to skin Property, there is good matte effect, adornment effect nature can be made lasting, while uniformly correcting the colour of skin.
Specific embodiment
The present invention provides a kind of waterproof powder bottom formula of liquid comprising following component: deionized water, five poly dimethyl silicon of ring Oxygen alkane, Permethyl 99A, trimethyl silicane alkoxy esters of silicon acis, Dimethicone Crosspolymer, cetyl PEG/PPG-10/ 1 dimethyl silicone polymer, silica, glyceryl behenate/20 acid esters, gathers double-PEG/PPG-14/14 dimethyl silicone polymers Dimethyl siloxane, magnesium sulfate, titanium dioxide, iron oxide yellow, iron oxide red, iron oxide black, Phenoxyethanol.
Can further comprise also following components in addition to above-mentioned necessary component: propylene glycol, be gathered phenyl trimethicone Methyl methacrylate, boron nitride, tocopherol acetate, Sensiva SC50.
Play the component of waterproof efficacy: ring five dimethyl silicone polymer, Permethyl 99A, trimethyl silicane alkoxy esters of silicon acis, Dimethicone Crosspolymer, cetyl PEG/PPG-10/1 dimethyl silicone polymer, double-PEG/PPG-14/14 are poly- Dimethyl siloxane, silica, glyceryl behenate/20 acid esters, dimethyl silicone polymer.
A kind of waterproof powder bottom formula of liquid comprising following component (by weight ratio):
20% ∽ 30% of deionized water, 8% ∽ 15% of ring five dimethyl silicone polymer, 8% ∽ 13% of Permethyl 99A, the third two 6% ∽ 10% of alcohol, 5% ∽ 9% of isononyl isononanoate, 5% ∽ 8% of trimethyl silicane alkoxy esters of silicon acis, dimethyl silicone polymer 4.5% ∽ 7.5% of cross-linked polymer, 4% ∽ 6% of phenyl trimethicone, cetyl PEG/PPG-10/1 poly dimethyl 3% ∽ 5% of siloxanes, dimethyl silicone polymer 2.5% ∽ 5%, double 2.5% ∽ of-PEG/PPG-14/14 dimethyl silicone polymer 4.5%, 2.4% ∽ 4.3% of silica, 2.2% ∽ 4% of polymethyl methacrylate, 2% ∽ 3.6% of boron nitride, glycerol behenic acid 2% ∽ 3% of ester/20 acid esters, 0.8% ∽ 1.2% of magnesium sulfate, 0.2% ∽ 0.5% of tocopherol acetate, titanium dioxide 3.6% ∽ 9.6%, 5% ∽ 8% of iron oxide yellow, 2% ∽ 6% of iron oxide red, 0.5% ∽ 3.3% of iron oxide black, Phenoxyethanol 0.1% ∽ 0.3%, 0.1% ∽ 0.2% of Sensiva SC50.
Wherein, emollients, thickener and solvent of the ring five dimethyl silicone polymer as foundation emulsion are volatility silicon Oil has good compatibility, gas permeability and spreadability, so that manufactured foundation emulsion soft-touch, smooth and salubrious.
Permethyl 99A has volatility as splendid solvent, can promote smear, improves texture, Permethyl 99A is one Kind colorless and odorless transparency liquid, has excellent physical chemistry and toxicological security, aromatic hydrocarbons and sulphur is practically free of, to eyes and skin Skin is non-stimulated, sensitization, also without side-effects to blackhead.Permethyl 99A is volatilization class oil, is widely used as volatilizing in America and Europe The substituent of property silicone oil (D4, D5), skin sense are extremely salubrious.There are good dissolubility and compatibility to various raw material active matters and grease Property, excellent powder dispersibility, surface tension is low, easily sprawls and is emulsified, and can be widely used for various: sun-proof, color make-up unloads Adornment, in the products such as hair care and basic skin care;Also it can be used as the oil-soluble carrier of both effectiveness substance, can dissolve Victoria C and be directly used in Skin is easier to directly play the effect of Victoria C and avoids being oxidized.
Propylene glycol adjusts the humidity and lubricity of foundation emulsion as moisturizer, promotes the moisturizing waterproof effect of foundation emulsion.
Isononyl isononanoate: unique more methyl branch structures, silk-like feeling, dry and comfortable and extremely soft feel are splendid Emollient, have good dispersibility to colorant, be commonly called as synthesis silk oil.
Trimethyl silicane alkoxy esters of silicon acis: organic siliconresin has excellent film forming, waterproofness, promotes color make-up product Persistence.
Dimethicone Crosspolymer: silicone elastomer can be used as oil phase thickeners, provide silky tactile impression, improve Sense is smeared, dry and comfortable, smooth, non-greasy the skin sense of product is assigned.
Phenyl trimethicone: high refractive index, compatibility is good, lubrication, softness, salubrious non-greasy
Cetyl PEG/PPG-10/1 dimethyl silicone polymer: water-in-oil emulsifier has splendid application characteristic, skin sense Lubrication, compatibility is good, and stability is good.
Double-PEG/PPG-14/14 dimethyl silicone polymers: silicon water-in-oil emulsifier.
Dimethyl silicone polymer: moist type silicone oil has the characteristics that low surface tension and high spreading coefficient, can be in skin table Face forms hydrophobic and ventilative protective film.
Silica: spherical silicon powder has smooth surface, assigns product soft and smooth sense of touch.
Polymethyl methacrylate: spherical powder, skin sense is smooth, improves the spreadability of product.
Boron nitride: soft smooth, property are stablized, and provide fabulous soft and smooth texture, glossiness and patch skin.
Glyceryl behenate/20 acid esters: W/O emulsion stabilizer has thickening effect.
Magnesium sulfate: stabilizer.
Tocopherol acetate: vitamin E can be used as antioxidant, have moisture-keeping efficacy.
Phenoxyethanol: preservative.
Sensiva SC50: moisturizer
Embodiment one
A kind of waterproof powder bottom formula of liquid, raw material include following component (by weight ratio):
Ring five dimethyl silicone polymer 8%, Permethyl 99A 9%, propylene glycol 7%, isononyl isononanoate 5%, trimethyl silicane Trimethylsiloxysilicate 6%, Dimethicone Crosspolymer 5.5%, phenyl trimethicone 4%, cetyl PEG/PPG-10/1 dimethyl silicone polymer 5%, dimethyl silicone polymer 2.5%, double-PEG/PPG-14/14 poly dimethyls Siloxanes 3%, silica 2.4%, polymethyl methacrylate 2.3%, boron nitride 2%, glyceryl behenate/20 acid esters 2.5%, magnesium sulfate 0.8%, tocopherol acetate 0.3%, titanium dioxide 5.5%, iron oxide yellow 6%, iron oxide red 4%, oxygen Change iron oxide black 2.5%, Phenoxyethanol 0.15%, Sensiva SC50 0.1%, deionized water surplus.
Embodiment two
A kind of waterproof powder bottom formula of liquid, raw material include following component (by weight ratio):
Ring five dimethyl silicone polymer 12%, Permethyl 99A 11%, propylene glycol 8%, isononyl isononanoate 7%, trimethyl Siloxy esters of silicon acis 6%, Dimethicone Crosspolymer 5.5%, phenyl trimethicone 4%, cetyl PEG/PPG-10/1 dimethyl silicone polymer 3.5%, dimethyl silicone polymer 3.5%, double poly- diformazans of-PEG/PPG-14/14 Radical siloxane 3%, silica 3.4%, polymethyl methacrylate 3%, boron nitride 2.5%, glyceryl behenate/20 acid esters 2.5%, magnesium sulfate 1%, tocopherol acetate 0.4%, titanium dioxide 5.6%, iron oxide yellow 6%, iron oxide red 4%, oxidation Iron oxide black 2.5%, Phenoxyethanol 0.15%, Sensiva SC50 0.1%, deionized water surplus.
Embodiment three
A kind of waterproof powder bottom formula of liquid, raw material include following component (by weight ratio):
Ring five dimethyl silicone polymer 15%, Permethyl 99A 13%, propylene glycol 10%, isononyl isononanoate 5%, trimethyl Siloxy esters of silicon acis 6%, Dimethicone Crosspolymer 6%, phenyl trimethicone 6%, cetyl PEG/PPG-10/1 dimethyl silicone polymer 5%, dimethyl silicone polymer 4%, double-PEG/PPG-14/14 polydimethylsiloxanes Alkane 5%, silica 4%, polymethyl methacrylate 3.8%, boron nitride 3.6%, glyceryl behenate/20 acid esters 3%, sulfuric acid Magnesium 0.8%, tocopherol acetate 0.5%, titanium dioxide 9.6%, iron oxide yellow 7%, iron oxide red 5%, iron oxide black 3%, Phenoxyethanol 0.1%, Sensiva SC50 0.2%.Deionized water surplus.
The present invention also provides a kind of preparation methods of waterproof powder bottom formula of liquid comprising following steps:
Step 1) is weighed Permethyl 99A, ring five dimethyl silicone polymer, trimethyl silicane alcoxyl in oily phase by setting ratio Base esters of silicon acis is stirred at normal temperature to being completely dissolved;
Step 2) is proportionally added into Dimethicone Crosspolymer, phenyl trimethicone, cetyl again PEG/PPG-10/1 dimethyl silicone polymer, double-PEG/PPG-14/14 dimethyl silicone polymers, dimethyl silicone polymer, glycerol Behenate/20 acid esters, agitating and heating dissolution, temperature control at 90 DEG C hereinafter, until be completely dissolved, 3 ∽ of homogeneous 5 minutes, 2800 revs/min, and kept for 70-90 DEG C of constant temperature, it is preferable that constant temperature is at 80 DEG C;
Step 3) weighs the deionized water in water phase, is heated to 90 DEG C, keeps the temperature 10 minutes and sterilizes, is cooled to 85 DEG C, then plus Enter propylene glycol, magnesium sulfate, stirring is kept for 85 DEG C of constant temperature to being completely dissolved;
Water phase is slowly added into oily phase, stirs 5 minutes, then 3 ∽ of homogeneous while quick stirring oily phase by step 4) 5 minutes, 2800 revs/min;
Step 5) weigh isononyl isononanoate, Permethyl 99A, ring five dimethyl silicone polymer, titanium dioxide, iron oxide yellow, Iron oxide red, iron oxide black, silica, polymethyl methacrylate, boron nitride, are uniformly mixed, and impregnate 3 hours, cross and grind 2 ∽ of machine 3 times is made the mill base of color uniformly, fine and smooth, is then added in the Material emulsified, is thoroughly mixed uniformly, then 3 ∽ of matter 5 minutes, 2800 revs/min;
Phenoxyethanol, Sensiva SC50, tocopherol acetate are added sequentially in Material by step 6), are stirred Uniformly, waterproof foundation emulsion finished product is obtained.
The above has been described in detail, described above, is only a preferred embodiment of the present invention, when cannot Limit the application practical range, i.e., it is all according to the made equivalent changes and modifications of the application range, it should still belong to covering scope of the present invention It is interior.

Claims (7)

1. a kind of waterproof powder bottom formula of liquid, it is characterised in that: including following component: deionized water, ring five dimethyl silicone polymer, Permethyl 99A, trimethyl silicane alkoxy esters of silicon acis, Dimethicone Crosspolymer, cetyl PEG/PPG-10/1 are poly- Dimethyl siloxane, double-PEG/PPG-14/14 dimethyl silicone polymers, silica, glyceryl behenate/20 acid esters, poly- two Methylsiloxane, magnesium sulfate, titanium dioxide, iron oxide yellow, iron oxide red, iron oxide black, Phenoxyethanol.
2. a kind of waterproof powder bottom formula of liquid according to claim 1, which is characterized in that can also further comprise with the following group Point: propylene glycol, phenyl trimethicone, polymethyl methacrylate, boron nitride, tocopherol acetate, ethylhexyl are sweet Oil.
3. a kind of waterproof powder bottom formula of liquid according to claim 2, which is characterized in that can also further comprise with the following group Point: (by weight ratio):
20% ∽ 30% of deionized water, 8% ∽ 15% of ring five dimethyl silicone polymer, 8% ∽ 13% of Permethyl 99A, propylene glycol 6% ∽ 10%, 5% ∽ 9% of isononyl isononanoate, 5% ∽ 8% of trimethyl silicane alkoxy esters of silicon acis, dimethyl silicone polymer are handed over 4.5% ∽ 7.5% of linked polymer, 4% ∽ 6% of phenyl trimethicone, cetyl PEG/PPG-10/1 poly dimethyl silicon 3% ∽ 5% of oxygen alkane, dimethyl silicone polymer 2.5% ∽ 5%, double 2.5% ∽ of-PEG/PPG-14/14 dimethyl silicone polymer 4.5%, 2.4% ∽ 4.3% of silica, 2.2% ∽ 4% of polymethyl methacrylate, 2% ∽ 3.6% of boron nitride, glycerol behenic acid 2% ∽ 3% of ester/20 acid esters, 0.8% ∽ 1.2% of magnesium sulfate, 0.2% ∽ 0.5% of tocopherol acetate, titanium dioxide 3.6% ∽ 9.6%, 5% ∽ 8% of iron oxide yellow, 2% ∽ 6% of iron oxide red, 0.5% ∽ 3.3% of iron oxide black, Phenoxyethanol 0.1% ∽ 0.3%, 0.1% ∽ 0.2% of Sensiva SC50.
4. a kind of waterproof powder bottom formula of liquid according to claim 3, which is characterized in that its raw material includes that following component (is pressed Weight proportion):
Ring five dimethyl silicone polymer 8%, Permethyl 99A 9%, propylene glycol 7%, isononyl isononanoate 5%, trimethyl silicane alcoxyl Base esters of silicon acis 6%, Dimethicone Crosspolymer 5.5%, phenyl trimethicone 4%, cetyl PEG/ PPG-10/1 dimethyl silicone polymer 5%, dimethyl silicone polymer 2.5%, double-PEG/PPG-14/14 polydimethylsiloxanes Alkane 3%, silica 2.4%, polymethyl methacrylate 2.3%, boron nitride 2%, glyceryl behenate/20 acid esters 2.5%, sulphur Sour magnesium 0.8%, tocopherol acetate 0.3%, titanium dioxide 5.5%, iron oxide yellow 6%, iron oxide red 4%, iron oxide black 2.5%, Phenoxyethanol 0.15%, Sensiva SC50 0.1%, deionized water surplus.
5. a kind of waterproof powder bottom formula of liquid according to claim 3, which is characterized in that its raw material includes that following component (is pressed Weight proportion):
Ring five dimethyl silicone polymer 12%, Permethyl 99A 11%, propylene glycol 8%, isononyl isononanoate 7%, trimethyl silane Oxygroup esters of silicon acis 6%, Dimethicone Crosspolymer 5.5%, phenyl trimethicone 4%, cetyl PEG/ PPG-10/1 dimethyl silicone polymer 3.5%, dimethyl silicone polymer 3.5%, double-PEG/PPG-14/14 poly dimethyl silicon Oxygen alkane 3%, silica 3.4%, polymethyl methacrylate 3%, boron nitride 2.5%, glyceryl behenate/20 acid esters 2.5%, Magnesium sulfate 1%, tocopherol acetate 0.4%, titanium dioxide 5.6%, iron oxide yellow 6%, iron oxide red 4%, iron oxide black 2.5%, Phenoxyethanol 0.15%, Sensiva SC50 0.1%, deionized water surplus.
6. a kind of waterproof powder bottom formula of liquid according to claim 3, which is characterized in that its raw material includes that following component (is pressed Weight proportion):
Ring five dimethyl silicone polymer 15%, Permethyl 99A 13%, propylene glycol 10%, isononyl isononanoate 5%, trimethyl silane Oxygroup esters of silicon acis 6%, Dimethicone Crosspolymer 6%, phenyl trimethicone 6%, cetyl PEG/ PPG-10/1 dimethyl silicone polymer 5%, dimethyl silicone polymer 4%, double-PEG/PPG-14/14 dimethyl silicone polymers 5%, silica 4%, polymethyl methacrylate 3.8%, boron nitride 3.6%, glyceryl behenate/20 acid esters 3%, magnesium sulfate 0.8%, tocopherol acetate 0.5%, titanium dioxide 9.6%, iron oxide yellow 7%, iron oxide red 5%, iron oxide black 3%, benzene Oxyethanol 0.1%, Sensiva SC50 0.2%.Deionized water surplus.
7. a kind of method for preparing waterproof powder bottom formula of liquid, it is characterised in that the following steps are included:
Step 1) is weighed Permethyl 99A, ring five dimethyl silicone polymer, trimethyl silicane alkoxy silicon in oily phase by setting ratio Acid esters is stirred at normal temperature to being completely dissolved;
Step 2) is proportionally added into Dimethicone Crosspolymer, phenyl trimethicone, cetyl PEG/ again PPG-10/1 dimethyl silicone polymer, double-PEG/PPG-14/14 dimethyl silicone polymers, dimethyl silicone polymer, glycerol behenyl Acid esters/20 acid esters, agitating and heating dissolution, temperature control is at 90 DEG C hereinafter, until being completely dissolved, 3 ∽ of homogeneous 5 minutes, 2800 Rev/min, and kept for 70-90 DEG C of constant temperature;
Step 3) weighs the deionized water in water phase, is heated to 90 DEG C, keeps the temperature 10 minutes and sterilizes, is cooled to 85 DEG C, adds third Glycol, magnesium sulfate, stirring are kept for 85 DEG C of constant temperature to being completely dissolved;
Water phase is slowly added into oily phase, stirs 5 minutes, then 3 ∽ 5 of homogeneous divides while quick stirring oily phase by step 4) Clock, 2800 revs/min;
Step 5) weighs isononyl isononanoate, Permethyl 99A, ring five dimethyl silicone polymer, titanium dioxide, iron oxide yellow, oxidation Iron oxide red, iron oxide black, silica, polymethyl methacrylate, boron nitride, are uniformly mixed, and impregnate 3 hours, cross 2 ∽ of grinder 3 times, the mill base of color uniformly, fine and smooth is made, is then added in the Material emulsified, is thoroughly mixed uniformly, then 3 ∽ of homogeneous 5 minutes, 2800 revs/min;
Phenoxyethanol, Sensiva SC50, tocopherol acetate are added sequentially in Material by step 6), are uniformly mixed, Obtain waterproof foundation emulsion finished product.
CN201910192725.8A 2019-03-13 2019-03-13 A kind of formula and preparation method thereof of waterproof foundation emulsion Pending CN110051553A (en)

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CN112386544A (en) * 2020-12-03 2021-02-23 中山市美源化妆品有限公司 Liquid foundation and preparation method thereof
CN113181091A (en) * 2021-04-20 2021-07-30 上海应用技术大学 Spot-fading foundation liquid and preparation method thereof
CN114224753A (en) * 2021-12-31 2022-03-25 广东柏俐臣生物科技有限公司 Water-in-oil type emulsified composition, foundation liquid and preparation method thereof
CN114748371A (en) * 2022-04-14 2022-07-15 莹特丽科技(苏州工业园区)有限公司 Moisturizing and skin-sticking makeup powder base solution and preparation method thereof
CN115836994A (en) * 2022-06-20 2023-03-24 科丝美诗(中国)化妆品有限公司 Make-up-holding acne-removing foundation liquid and preparation method thereof

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CN111184669A (en) * 2020-02-28 2020-05-22 广东密尚生物科技有限公司 Waterproof moisturizing composition, preparation method thereof and liquid foundation
CN111184669B8 (en) * 2020-02-28 2022-09-09 广州云联科技开发有限公司 Waterproof moisturizing composition, preparation method thereof and liquid foundation
CN111671673A (en) * 2020-06-23 2020-09-18 泉后(广州)生物科技研究院有限公司 Long-acting makeup holding powder base solution and preparation method thereof
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CN111956527A (en) * 2020-08-19 2020-11-20 广州艾蓓生物科技有限公司 Moisturizing concealer
CN112237553A (en) * 2020-10-13 2021-01-19 广州艾蓓生物科技有限公司 Waterproof liquid eye shadow and preparation method thereof
CN112263489A (en) * 2020-10-29 2021-01-26 广东雅丽诗科技有限公司 Water dispersible powder and preparation process thereof
CN112274448A (en) * 2020-11-03 2021-01-29 广州葆妍生物科技有限公司 Spray liquid foundation and preparation method thereof
CN112386544A (en) * 2020-12-03 2021-02-23 中山市美源化妆品有限公司 Liquid foundation and preparation method thereof
CN113181091A (en) * 2021-04-20 2021-07-30 上海应用技术大学 Spot-fading foundation liquid and preparation method thereof
CN114224753A (en) * 2021-12-31 2022-03-25 广东柏俐臣生物科技有限公司 Water-in-oil type emulsified composition, foundation liquid and preparation method thereof
CN114224753B (en) * 2021-12-31 2023-10-20 广东柏俐臣生物科技有限公司 Water-in-oil type emulsified composition, foundation liquid and preparation method thereof
CN114748371A (en) * 2022-04-14 2022-07-15 莹特丽科技(苏州工业园区)有限公司 Moisturizing and skin-sticking makeup powder base solution and preparation method thereof
CN114748371B (en) * 2022-04-14 2023-10-20 莹特丽科技(苏州工业园区)有限公司 Moisturizing skin-care foundation cream and preparation method thereof
CN115836994A (en) * 2022-06-20 2023-03-24 科丝美诗(中国)化妆品有限公司 Make-up-holding acne-removing foundation liquid and preparation method thereof

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