CN110693738A - Gilding lasting and leisure foundation liquid and preparation method thereof - Google Patents

Gilding lasting and leisure foundation liquid and preparation method thereof Download PDF

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Publication number
CN110693738A
CN110693738A CN201911202607.7A CN201911202607A CN110693738A CN 110693738 A CN110693738 A CN 110693738A CN 201911202607 A CN201911202607 A CN 201911202607A CN 110693738 A CN110693738 A CN 110693738A
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polydimethylsiloxane
stirring
lasting
foundation
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李继承
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Suzhou Ante Cosmetics Ltd By Share Ltd
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Suzhou Ante Cosmetics Ltd By Share Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20Halogens; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29Titanium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/12Face or body powders for grooming, adorning or absorbing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • General Health & Medical Sciences (AREA)
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  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a gilding lasting and pure foundation solution and a preparation process thereof, the foundation solution can instantly brighten the whole skin by adding bismuth oxychloride slurry, compared with the traditional foundation solution in which grease with high refractive index is added in the formula, the brightening effect is more lasting, the makeup is natural and not fake, and powder can not float and block after makeup; the foundation liquid has creamy texture, the smearing feeling is silky and not greasy, the foundation liquid is lasting and not oily after being made up, and the foundation liquid is natural and attractive in luster; the vegetable oil and natural ingredients are added in the formula, so that the effects of moisturizing, restoring skin elasticity, slowing down skin aging and the like can be achieved; the preparation process can realize large-scale mass production.

Description

Gilding lasting and leisure foundation liquid and preparation method thereof
Technical Field
The invention relates to the field of cosmetics, in particular to a gilding lasting and pure foundation liquid and a preparation method thereof.
Background
The foundation liquid products sold in the market at present are various, and most products have the effects of being light and thin, concealing, controlling oil, preventing water, preserving moisture, moistening, keeping makeup, decorating skin color and the like, but the products with the characteristics are few, and the using requirements of customers cannot be met.
Therefore, there is a need to design a gilding lasting and unpure foundation solution, which has multiple effects of nourishing skin, moisturizing, concealing blemishes, brightening and maintaining makeup, is light in texture, natural and fitting, has natural makeup feeling, strong oil control capability, enough concealing force, lasting makeup for a long time, is breathable, fresh and non-greasy after makeup, good spreadability, smooth and silky touch feeling brought by light silicone oil in the formula, and meanwhile, the product has a good makeup effect and does not block powder and float powder.
Disclosure of Invention
In view of the above technical problems, the present invention aims to: provides a golden lasting and pure foundation fluid and a preparation method thereof.
The technical solution of the invention is realized as follows: a gilding lasting and pureness foundation solution comprises the following raw material components in percentage by mass: 8-15% of cyclopentadimethylsiloxane, 8-15% of trisiloxane, 5-10% of diphenylsiloxyphenyl trimethicone, 3-7% of titanium dioxide, 3-6% of glycerol, 2-6% of talcum powder, 3-7% of polydimethylsiloxane, 3-10% of butanediol, 2-6% of ethylhexyl methoxycinnamate, 2-6% of ethanol, 0.5-3% of lauryl PEG-9 polydimethylsiloxane, 0.5-3% of PEG-10 polydimethylsiloxane, 0.5-2% of polyglycerol-2 diisostearate, 0.5-1% of disteardimonium hectorite, 1-4% of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 0.5-2% of sodium chloride, 0.05 to 0.2 percent of chlorphenesin, 0.5 to 5 percent of bismuth oxychloride slurry, 1 to 4 percent of polydimethylsiloxane PEG-10/15 cross-linked polymer, 0.01 to 0.02 percent of aluminum hydroxide, 0.2 to 0.5 percent of p-hydroxyacetophenone, 0.4 to 0.7 percent of phenoxyethanol, 0.01 to 0.02 percent of stearic acid, 0.05 to 0.1 percent of EDTA disodium, 0.1 to 0.5 percent of tocopherol and 0.1 to 10 percent of colorant in balance.
The preparation process of the gilding lasting and purplish foundation solution comprises the following steps:
① water phase, premixing butanediol and p-hydroxyacetophenone, stirring and heating properly until the mixture is dissolved and transparent, sequentially adding glycerol, EDTA disodium, chlorphenesin and ultrapure humectant into a water phase pot, heating and heating, controlling the temperature to be 80-85 ℃ for dissolving and transparent, controlling the stirring speed to be 450-500r/min, and keeping the temperature for 15-20 min;
② adding cyclopentadimethylsiloxane, polydimethylsiloxane, diphenylsiloxyphenyl trimethicone, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, PEG-10 polydimethylsiloxane, lauryl PEG-9 polydimethylsiloxane ethyl, polyglycerol-2 diisostearate, ethylhexyl methoxycinnamate and bentonite into an oil phase pot, stirring at 900 plus 1000rpm/min for 10-15min, sequentially adding color paste CI77891, CI77492, CI77491 and CI77499 into the oil phase pot, uniformly stirring, heating to 80-82 ℃ for complete dissolution, controlling the stirring speed at 900 plus 1000rpm/min, and keeping the temperature for 15-20 min;
③ emulsification, wherein the oil phase and water phase raw materials are completely dispersed before emulsification, the material body is uniform, the emulsification pot is started to stir and is kept at 1800 plus 2000rpm/min and homogenized at 2500rpm/min, the water phase is slowly pumped into the emulsification pot, the water pumping time is controlled to be about 10-15min, the high-speed homogenization is carried out for 10-12min after pumping is finished, and the stirring is carried out at 2200 plus 2500 rpm/min;
④, stirring and cooling to 40-45 ℃, observing the color of the material body, comparing the material body with the standard sample, gradually adding the product obtained in step ② until the color of the material body is the same as that of the standard sample, and homogenizing at constant speed for 2.5-3 min;
⑤ adding low temperature phase after color matching, and homogenizing at medium speed for 2.5-3 min;
⑥ stirring at low speed, cooling to below 38 deg.C, and discharging after passing detection.
Due to the application of the technical scheme, compared with the prior art, the invention has the following advantages:
according to the gilding lasting and leisure foundation solution, the bismuth oxychloride slurry is added, so that the whole skin can be instantly brightened, compared with the traditional foundation solution in which high-refractive-index grease is added in the formula, the brightening effect is more lasting, the natural and fake makeup is realized, and the powder can not float or block after makeup.
The foundation liquid has creamy texture, the smearing feeling is silky and not greasy, the foundation liquid is lasting and not oily after being made up, and the foundation liquid is natural and attractive in luster; the vegetable oil and natural ingredients are added in the formula, so that the effects of moisturizing, restoring skin elasticity, slowing down skin aging and the like can be achieved.
Detailed Description
The present invention is further illustrated by the following examples.
The gilding lasting and pureness liquid foundation of the invention comprises the following raw material components calculated by mass fraction: 8-15% of cyclopentadimethylsiloxane, 8-15% of trisiloxane, 5-10% of diphenylsiloxyphenyl trimethicone, 3-7% of titanium dioxide, 3-6% of glycerol, 2-6% of talcum powder, 3-7% of polydimethylsiloxane, 3-10% of butanediol, 2-6% of ethylhexyl methoxycinnamate, 2-6% of ethanol, 0.5-3% of lauryl PEG-9 polydimethylsiloxane, 0.5-3% of PEG-10 polydimethylsiloxane, 0.5-2% of polyglycerol-2 diisostearate, 0.5-1% of disteardimonium hectorite, 1-4% of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 0.5-2% of sodium chloride, 0.05 to 0.2 percent of chlorphenesin, 0.5 to 5 percent of bismuth oxychloride slurry, 1 to 4 percent of polydimethylsiloxane PEG-10/15 cross-linked polymer, 0.01 to 0.02 percent of aluminum hydroxide, 0.2 to 0.5 percent of p-hydroxyacetophenone, 0.4 to 0.7 percent of phenoxyethanol, 0.01 to 0.02 percent of stearic acid, 0.05 to 0.1 percent of EDTA disodium, 0.1 to 0.5 percent of tocopherol and 0.1 to 10 percent of colorant in balance. .
Wherein, chlorphenesin can resist bacteria, diminish inflammation, relieve itching, protect skin and relieve skin pain.
Cyclopenta dimethyl siloxane, dimethyl silicone polymer, diphenyl siloxy phenyl trimethyl silicone polymer, dimethyl silicone polymer/vinyl dimethyl silicone polymer cross-linked polymer are added in the formula, so that the product is light, thin, soft and moist in texture, easy to apply makeup, refreshing, non-sticky and stable in state.
The bismuth oxychloride slurry can improve the luster of the skin and instantly and naturally brighten the whole skin.
The polyglycerol-2 diisostearate and the tocopherol acetate are natural vegetable oil and fat, have natural oxidation resistance and moistening property, can slow down skin aging and effectively heal skin wounds, and the vitamin E helps cell membranes resist free radicals.
The talcum powder brings silky touch feeling, so that the product is natural and fitting.
The component contents of examples 1 to 6 are shown in the following table:
Figure BDA0002296233780000041
Figure BDA0002296233780000051
wherein, the unit of each component is percentage, the sum of the raw materials of the formula in each embodiment is 100%, and the component content is that the component is not added.
The gilding permanent and flawless vanishing liquids of the above examples 1-6 were all prepared as follows:
① mixing butanediol and p-hydroxyacetophenone, stirring, heating to dissolve, heating to transparent, adding other raw materials (glycerol, disodium EDTA, chlorphenesin, and ultrapure humectant) ST-ultra-mol-moist into water phase pot, heating, dissolving at 80-85 deg.C, stirring at 500r/min, and keeping the temperature for 20 min;
② adding cyclopentadimethylsiloxane, polydimethylsiloxane, diphenylsiloxyphenyl trimethicone, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, PEG-10 polydimethylsiloxane, lauryl PEG-9 polydimethylsiloxane ethyl, polyglycerol-2 diisostearate, ethylhexyl methoxycinnamate and bentonite into an oil phase pot, stirring at 900 plus 1000rpm/min for 10-15min, sequentially adding color pastes CI77891, CI77492, CI77491 and CI77499 into the oil phase pot, uniformly stirring, heating to 80-82 ℃ for complete dissolution, controlling the stirring speed at 960rpm/min, and keeping the temperature for 15-20 min;
③ emulsifying, wherein the oil phase and water phase are completely dispersed before emulsification, the material is uniform, the emulsifying pot is started to stir at 2000rpm/min, the mixture is homogenized at 2500rpm/min, the water phase is slowly pumped into the emulsifying pot, the pumping speed is controlled to ensure the emulsification of the water phase, the water pumping time is controlled to be about 10-15min, after pumping, the mixture is homogenized at 3000rpm for 12min, and the mixture is stirred at 2500 rpm/min;
④ stirring and cooling to 45 ℃, observing the color of the material body, comparing the material body with the standard sample, gradually adding the oil phase product obtained in step ②, wherein the color difference is obvious, 5-10%, the difference is not obvious but has color difference, 2-5% color matching, until the color of the material body is the same as that of the standard sample, and homogenizing at a uniform speed of 2000rpm for 3 min;
⑤ adding low temperature phase such as ethanol and phenoxyethanol sequentially after color matching, and homogenizing at 2000rpm for 3 min;
⑥ stirring at low speed, cooling to below 38 deg.C, and discharging after passing detection.
The above-mentioned embodiments are merely illustrative of the technical idea and features of the present invention, and the purpose thereof is to enable those skilled in the art to understand the contents of the present invention and implement the present invention, and not to limit the scope of the present invention, and all equivalent changes or modifications made according to the spirit of the present invention should be covered in the scope of the present invention.

Claims (3)

1. A gilding lasting and pureness foundation solution is characterized by comprising the following raw material components in parts by mass: 8-15% of cyclopentadimethylsiloxane, 8-15% of trisiloxane, 5-10% of diphenylsiloxyphenyl trimethicone, 3-7% of titanium dioxide, 3-6% of glycerol, 2-6% of talcum powder, 3-7% of polydimethylsiloxane, 3-10% of butanediol, 2-6% of ethylhexyl methoxycinnamate, 2-6% of ethanol, 0.5-3% of lauryl PEG-9 polydimethylsiloxane, 0.5-3% of PEG-10 polydimethylsiloxane, 0.5-2% of polyglycerol-2 diisostearate, 0.5-1% of disteardimonium hectorite, 1-4% of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 0.5-2% of sodium chloride, 0.05 to 0.2 percent of chlorphenesin, 0.5 to 5 percent of bismuth oxychloride slurry, 1 to 4 percent of polydimethylsiloxane PEG-10/15 cross-linked polymer, 0.01 to 0.02 percent of aluminum hydroxide, 0.2 to 0.5 percent of p-hydroxyacetophenone, 0.4 to 0.7 percent of phenoxyethanol, 0.01 to 0.02 percent of stearic acid, 0.05 to 0.1 percent of EDTA disodium, 0.1 to 0.5 percent of tocopherol and 0.1 to 10 percent of colorant in balance.
2. The gilding durable smoothy base of claim 1, wherein: the balance of the colorant is one or a combination of more of CI77891, CI77492, CI77499, CI77491, disodium stearyl glutamate, triethoxy octyl silane and triethoxy silyl ethyl dimethyl silicone ethyl hexyl dimethyl silicone.
3. A preparation process of gilding lasting and pure foundation liquid is characterized by comprising the following steps:
① water phase, premixing butanediol and p-hydroxyacetophenone, stirring and heating properly until the mixture is dissolved and transparent, sequentially adding glycerol, EDTA disodium, chlorphenesin and ultrapure humectant into a water phase pot, heating and heating, controlling the temperature to be 80-85 ℃ for dissolving and transparent, controlling the stirring speed to be 450-500r/min, and keeping the temperature for 15-20 min;
② adding cyclopentadimethylsiloxane, polydimethylsiloxane, diphenylsiloxyphenyl trimethicone, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, PEG-10 polydimethylsiloxane, lauryl PEG-9 polydimethylsiloxane ethyl, polyglycerol-2 diisostearate, ethylhexyl methoxycinnamate and bentonite into an oil phase pot, stirring at 900 plus 1000rpm/min for 10-15min, sequentially adding color paste CI77891, CI77492, CI77491 and CI77499 into the oil phase pot, uniformly stirring, heating to 80-82 ℃ for complete dissolution, controlling the stirring speed at 900 plus 1000rpm/min, and keeping the temperature for 15-20 min;
③ emulsification, wherein the oil phase and water phase raw materials are completely dispersed before emulsification, the material body is uniform, the emulsification pot is started to stir and is kept at 1800 plus 2000rpm/min and homogenized at 2500rpm/min, the water phase is slowly pumped into the emulsification pot, the water pumping time is controlled to be about 10-15min, the high-speed homogenization is carried out for 10-12min after pumping is finished, and the stirring is carried out at 2200 plus 2500 rpm/min;
④, stirring and cooling to 40-45 ℃, observing the color of the material body, comparing the material body with the standard sample, gradually adding the product obtained in step ② until the color of the material body is the same as that of the standard sample, and homogenizing at constant speed for 2.5-3 min;
⑤ adding low temperature phase after color matching, and homogenizing at medium speed for 2.5-3 min;
⑥ stirring at low speed, cooling to below 38 deg.C, and discharging after passing detection.
CN201911202607.7A 2019-11-29 2019-11-29 Gilding lasting and leisure foundation liquid and preparation method thereof Pending CN110693738A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112274448A (en) * 2020-11-03 2021-01-29 广州葆妍生物科技有限公司 Spray liquid foundation and preparation method thereof
CN113908105A (en) * 2021-11-30 2022-01-11 广东金丝燕化妆品有限公司 Lasting matte dry-air-cushion foundation cream and preparation method thereof
CN115607472A (en) * 2022-10-31 2023-01-17 上海臻臣化妆品有限公司 Liquid foundation for dry skin and preparation method thereof

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CN107997993A (en) * 2017-12-30 2018-05-08 广州市中通生化制品有限公司 A kind of low viscosity foundation emulsion and preparation method thereof
CN109662935A (en) * 2019-01-26 2019-04-23 广州蔻丝恩化妆品科技有限公司 Frivolous flawless foundation emulsion of one kind and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN107997993A (en) * 2017-12-30 2018-05-08 广州市中通生化制品有限公司 A kind of low viscosity foundation emulsion and preparation method thereof
CN109662935A (en) * 2019-01-26 2019-04-23 广州蔻丝恩化妆品科技有限公司 Frivolous flawless foundation emulsion of one kind and preparation method thereof

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电子凭证-国产非特殊用途化妆品备案信息服务平台: "花迷时光鎏金逆颜粉底液 02 自然色", 《FTBA.NMPA.GOV.CN:8181/FTBAN/ITOWNET/HZP_BA/FW/PZ.JSP?PROCESSID=20180710142423YXYTH&NID=20180710142423YXYTH》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112274448A (en) * 2020-11-03 2021-01-29 广州葆妍生物科技有限公司 Spray liquid foundation and preparation method thereof
CN113908105A (en) * 2021-11-30 2022-01-11 广东金丝燕化妆品有限公司 Lasting matte dry-air-cushion foundation cream and preparation method thereof
CN115607472A (en) * 2022-10-31 2023-01-17 上海臻臣化妆品有限公司 Liquid foundation for dry skin and preparation method thereof

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