CN115595708A - 一种锦纶石墨烯抗静电面料的制备方法 - Google Patents

一种锦纶石墨烯抗静电面料的制备方法 Download PDF

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CN115595708A
CN115595708A CN202211119690.3A CN202211119690A CN115595708A CN 115595708 A CN115595708 A CN 115595708A CN 202211119690 A CN202211119690 A CN 202211119690A CN 115595708 A CN115595708 A CN 115595708A
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李伟春
仇云斌
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Wujiang Yurun Textile Co ltd
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Abstract

本发明公开了一种锦纶石墨烯抗静电面料的制备方法，包括，织造、染整、压光、涂层、水洗和成型；使用15D‑70D锦纶纤维和锦纶石墨烯混纺纤维原料进行织造，本发明加入锦纶石墨烯纤维，减少静电压半衰期、表面电阻率、摩擦电荷面密度和摩擦带点电压，有效防止静电产生，从而消除静电现象，多次水洗后，抗静电数值保持很好，使得面料手感柔软舒适，抗皱，轻薄，防漏绒，耐久抗静电性能。

Description

一种锦纶石墨烯抗静电面料的制备方法
技术领域
本发明涉及纺织技术领域，尤其涉及一种锦纶石墨烯抗静电面料的制备方法。
背景技术
秋冬季节，特别是冬季，空气干燥寒冷，使静电无处不在，甚至给我们的生活带来较大的安全隐患。比如加油站等场所，静电积聚后引发火灾等诸如此类的情况不在少数。还比如，人们穿着的服装，到冬季就特别容易产生静电，经常会给人带来静电恐惧的烦恼。有时碰到衣服或门把手等金属物体，会被电一下，特别难受。还有，穿脱衣服时经常会产生噼里啪啦的小火花，令人感到非常不适和恐惧。随着国家的发展进步，人民的生活水平越来越高，消除和防止因服装静电对一些场合产生的安全危害，对广大人们来说，是个非常重要的事情。
对于服装防静电面料而言，既要使面料细腻，美观，高档，还要和日常实用性相适合；要保持优异，耐久的防静电功能性，还要有很好的手感和质感，防泼水和防绒这些性能，是目前很大的空白市场。普通面料的防静电性能，一种采用加助剂，达到暂时防静电的功能，水洗后防静电功能就很快下降，防静电不耐久。第二种，用普通的导电丝达到防静电功能，但面料往往是70D以上，密度低，支纱粗，不适合用于档次高的服装上，有的布料虽薄，但纹路不美观，就只是横条，不宜做日常服装面料。在此基础上发明了这款新型防静电美观功能面料。
我们创造性开发了以锦纶和石墨烯组合的面料，利用锦纶很好的公定回潮率，使服装对人体更加舒适，采用特别的格子和黑色横条的组合织造工艺，这种新型创造使面料美观高档，增加了3倍的石墨烯材料，使面料的防静电效果非常理想，而且是耐久防静电，所以可以彻底解决了困扰人们服装静电引发的一系列问题。石墨烯的抗菌抑菌，防紫外线和远红外发热等功能，也为面料增加了很多实用功能。
发明内容
本发明目的就是为了弥补已有技术普通防静电面料，有的支纱粗密度低，有的密度高支纱细，但不美观，有的美观了但不耐久抗静电的缺陷，提供一种锦纶石墨烯抗静电面料的制备方法。本发明使锦纶纤维和石墨烯纤维混纺运用到 15D-70D锦纶面料上，加入石墨烯纤维，减少静电压半衰期、表面电阻率、摩擦电荷面密度和摩擦带点电压，有效防止静电产生，从而消除静电现象，多次水洗后，抗静电数值保持很好，使面料的抗静电功能和面料的轻薄高密美观，防泼水和防绒这些功能很好的结合在一起，抗静电功能和防泼水性能和防绒性能都达到了国标的检测合格要求。使很多场合可以避免因服装静电产生的安全隐患。
本发明是通过以下技术方案实现的：
一种锦纶石墨烯抗静电面料的制备方法，包括有织造、染整、压光、涂层、水洗和成型；
选择经向15D-70D锦纶纤维、纬向15D-70D锦纶*3加上15D-70D锦纶石墨烯纤维混纺黑丝*2为原料进行织造；所用原料中，石墨烯抗静电锦纶纤维重量占比为1～10％；本发明实现了锦纶石墨烯黑丝与格子，条子的美学结合，看上去既有条感又有格子，很好的避免了黑丝过于明显单调的尴尬。布料美观，轻薄，柔软，防绒，高效耐久抗静电，不易起皱，石墨烯的特殊抗菌抑菌，远红外发热等这些优良功能良好结合，使冬季服装免受静电的痛苦干扰。
所述织造采用了格子和黑色条子的美学结合。
所述染整包括如下工艺：染色、脱水、第一次定型、第二次定型加强防泼水；
所述染色工艺采用的染料的组成及质量份为：酸性黑4.0质量份,酸性黄0.8 质量份，酸性红0.5质量份、98％冰醋酸0.5质量份。所述染色工艺的温度控制为：起始温度为30℃，以0.5℃/min加热至60℃，保温10min，再以0.5℃ /min加热至85℃，保温10min，再以0.5℃/min加热至105℃，保温60min，最后以0.8℃/min降温至70℃。
所述第一次定型温度为100～180℃；
所述第二次定型加强防泼水如下：防水剂(此助剂为行业内通用的产品)按 40g/L调配，烘箱温度调整为第一节140℃预烘，其余均为165℃焙烘，车速为80 码，出烘箱经过冷却风吹降温，使温度降至30℃稳定形态。
所述压光采用镜面棍压制；温度160℃，车速度30y/h，压力10kg。
所述涂层采用两次PU涂层；每次5节烘箱，第一节烘箱159℃，第二节烘箱160℃，第三节烘箱温度160℃，第四季烘箱温度159℃，第五节烘箱温度160℃，车速40y/h。
所述水洗为加柔顺水洗。助剂配比工艺：膨松剂3％，柔软剂3％，平滑剂 3％，过水浸轧，使助剂充分渗透到面料，再经过两节80℃烘箱热风烘干。
所述成型为冷却成型。
所述原料的具体规格为：经向A为15D-70D锦纶，纬向A为15D-70D锦纶，纬向B为15D-70D锦纶*3，纬向C为15D-70D锦纶石墨烯纤维混纺黑丝*2；经密 902根/10cm，纬密610根/10cm，总经丝数14041根；经向A为33g/m，纬向A 为22.5g/m，纬向B为1.67g/m，纬向C为3.34g/m。
染色时采用的柔软剂采用鞣酸处理。
本发明的优点是：本发明创新性使锦纶纤维和石黑烯混纺纤维运用到15D-70D锦纶面料上，采用石墨烯黑丝和格子结合，使面料的耐久防静电功能和轻薄高密美观很好结合，再加上防泼水，防绒，不易起皱，还加上石墨烯抗菌抑菌，远红外发热等功能，使这款面料功能和优势突出，抗静电功能和防泼水性能和防绒性能都达到了国标的检测优品要求，实用性广泛，是解决静电问题很好解决方案。
本发明将锦纶和石墨烯结合，使面料对人体的舒适性更好；因为锦纶的公定回潮率很优异。
织造上，本发明布料格子和黑丝横条风格，设计美观实用，和高效防静电功能很好的结合。
附图说明
图1为本发明制得面料的实物图。
具体实施方式
一种锦纶石墨烯抗静电面料的制备方法，包括有织造、染整、压光、涂层、水洗和成型；
选择经向15D-70D低弹DTY半光锦纶纤维、纬向15D-70D半光锦纶DTY*3 加上15D-70D锦纶石墨烯纤维混纺黑丝*2为原料进行织造；所用原料中，石墨烯抗静电锦纶纤维重量占比为1～10％；织造纹理采用格子和横条相结合，使横条的石墨烯黑丝和格子可以保留各自的优势，避免了横条黑丝的突兀感，使格子中有条子，条子间有格子，使面料美学设计和强防静电功能良好组合。使实用范围更广，为更多服装带来功能与价值。
所述原料的具体规格为：经向A为15D-70D半光锦纶DTY，纬向A为15D-70D 半光锦纶DTY，纬向B为15D-70D半光锦纶DTY*3，纬向C为15D-70D锦纶石墨烯纤维混纺黑丝*2；经密902根/10cm，纬密610根/10cm，总经丝数14041根；经向A为33g/m，纬向A为22.5g/m，纬向B为1.67g/m，纬向C为3.34g/m。
鉴于锦纶的公定回潮率是化纤领域里很优异的，故而对人体而言也是更舒适的，本发明采用锦纶纤维和锦纶石墨烯纤维材料混纺纤维以梭织的方式，条子加格子的工艺织造而成，就是为了解决高效耐久防静电功能和面料细腻柔软美观等问题之间的难点，更能解决冬天服装的静电烦恼。布面微皱，格子和条子的合理结合，使面料更符合大众审美，感官更舒适。做到高效防静电，高效防绒，布面美观，高效防泼水，还有石墨烯抗菌抑菌，防紫外线，远红外发热等功能结合于一体。
所述的织造的纹理采用格子和锦纶石墨烯纤维混纺黑丝横条相结合。
所述染整包括如下工艺：染色、脱水、第一次定型、第二次定型加强防泼水；
所述染色工艺采用的染料的组成及质量份为：酸性黑4.0质量份,酸性黄0.8 质量份，酸性红0.5质量份、98％冰醋酸0.5质量份。所述染色工艺的温度控制为：起始温度为30℃，以0.5℃/min加热至60℃，保温10min，再以0.5℃ /min加热至85℃，保温10min，再以0.5℃/min加热至105℃，保温60min，最后以0.8℃/min降温至70℃。
所述第一次定型温度为160℃；
所述第二次定型加强防泼水如下：调配防水剂，防水剂为40g/L。烘箱温度调整为第一节140℃预烘，其余均为165℃焙烘，车速为80码，出烘箱经过冷却风吹和冷水锡林降温，使温度降至30℃稳定形态；二次定型同时上强防泼水，使防泼水功能出色。
锦纶纤维制成的面料，具有原材料易得、可再生、韧性好、强度高、抗拉伸性好、耐磨性好等特点，广泛应用与服装、鞋帽、箱包等领域。而使用锦纶纤维的另一个重要原因是锦纶纤维的吸潮率表现优异，使服装穿着更加舒适。故而本发明用锦纶和石墨烯混纺纤维制成的面料抗静电功能更强大，穿着舒适性更优异。
所述压光的温度为160℃，车速30y/h，压力10kg。采用油面压辊压制，车速使布面能够更加紧致细腻。
所述涂层采用两次涂层，每次5节烘箱，第一节烘箱159℃，第二节烘箱 160℃，第三节烘箱温度160℃，第四季烘箱温度159℃，第五节烘箱温度160℃，车速40y/h，两次涂层，使面料增加质感和恢复性，还具有很好的防绒性能。
所述水洗为加柔顺剂水洗。助剂配比工艺：膨松剂3％，柔软剂3％，平滑剂3％，过水浸轧，使助剂充分渗透到面料，再经过两节80℃烘箱热风烘干。通过水洗使面料彻底收缩，使成衣不缩水，同时改善手感和爽滑度，使手感更好。
本发明将锦纶和石墨烯结合，使面料对人体的舒适性更好；因为锦纶的公定回潮率很优异。如表1所示：
表1
Figure RE-GDA0003974535550000051
织造上，布料格子和黑丝横条风格，设计美观实用，和高效防静电功能很好的结合；如表2所示：
表2
Figure RE-GDA0003974535550000061
本发明制得产品如图1所示，各项检测指标具体如下：
织物电晕充电法的测定GB/T12703.1-2021(温度：20±2℃，湿度40±4％)，水洗前峰值电压(千伏):-0.21。半衰期(秒)：0.13。抗静电性能评价：优异。
静电性能(手动摩擦法)(uc/㎡)GB/T12703.2-2021，温度：20±2℃，湿度40±4％，水洗前结果为1.2，合格。具体如表3所示：
表3
Figure RE-GDA0003974535550000071
面料防绒检测报告，按GB/T14272-2011,测试结果为5根，符合防绒要求。
如表4所示：
表4
Figure RE-GDA0003974535550000072

Claims (4)

1.一种锦纶石墨烯抗静电面料的制备方法，其特征在于：包括有织造、染整、压光、涂层、水洗和成型；
选择经向15D-70D锦纶纤维、纬向15D-70D锦纶DTY*3加上15D-70D锦纶石墨烯纤维混纺黑丝*2为原料进行织造；
所述原料中，锦纶石墨烯纤维混纺黑丝重量占比为0.1～10％；
所述染整包括如下工艺：染色、脱水、第一次定型、第二次定型加强防泼水；
所述染色工艺采用的染料的组成及质量份为：酸性黑4.0质量份,酸性黄0.8质量份，酸性红0.5质量份、98％冰醋酸0 .5质量份；
所述染色工艺的温度控制为：起始温度为30℃，以0.5℃/min加热至60℃，保温10min，再以0.5℃/min加热至85℃，保温10min，再以0.5℃/min加热至105℃，保温60min，最后以0.8℃/min降温至70℃ ；
所述第一次定型温度为100～180℃；
所述第二次定型加强防泼水如下：防水剂按40g/L调配，烘箱温度调整为第一节140℃预烘，其余均为165℃焙烘，车速为 80码，出烘箱经过冷却风吹降温，使温度降至30℃稳定形态；
所述压光采用油面压辊，温度160℃，车速30y/h，压力10kg；
所述涂层采用两次涂层，每次 5节烘箱，第一节烘箱159℃，第二节烘箱160℃，第三节烘箱温度160℃，第四季烘箱温度159℃，第五节烘箱温度160℃，车速40y/h；
所述水洗工艺：加蓬松剂3%、柔软剂3%和平滑剂3%，过水再经浸轧，烘干，过两节烘箱，温度80℃，烘干成型。
2.根据权利要求1所述的一种锦纶石墨烯抗静电面料的制备方法，其特征在于：所述的织造的纹理采用格子和锦纶石墨烯纤维混纺黑丝相结合。
3.根据权利要求1所述的一种锦纶石墨烯抗静电面料的制备方法，其特征在于：所述原料的具体规格为：经向A为15D-70D锦纶，纬向A为15D-70D锦纶，纬向B为15D-70D锦纶*2，纬向C为15D-70D锦纶石墨烯纤维混纺黑丝*2；经密902根/10cm，纬密610根/10cm，总经丝数14041根；经向A为33g/m，纬向A为22.5g/m，纬向B为1.67g/m，纬向C为3.34g/m。
4.根据权利要求1所述的一种锦纶石墨烯抗静电面料的制备方法，其特征在于：染色时采用的柔软剂采用鞣酸处理。
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CN117535984A (zh) * 2023-11-15 2024-02-09 波司登羽绒服装有限公司 一种抗菌抗静电面料及其制备方法和应用

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117535984A (zh) * 2023-11-15 2024-02-09 波司登羽绒服装有限公司 一种抗菌抗静电面料及其制备方法和应用

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