CN115595004A - Preparation method and application of plant pigment for inner painting - Google Patents
Preparation method and application of plant pigment for inner painting Download PDFInfo
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- CN115595004A CN115595004A CN202211265054.1A CN202211265054A CN115595004A CN 115595004 A CN115595004 A CN 115595004A CN 202211265054 A CN202211265054 A CN 202211265054A CN 115595004 A CN115595004 A CN 115595004A
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- pigment
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- plant pigment
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- 239000000049 pigment Substances 0.000 title claims abstract description 52
- 238000010422 painting Methods 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims abstract description 16
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims abstract description 16
- 229940037003 alum Drugs 0.000 claims abstract description 11
- 238000007789 sealing Methods 0.000 claims abstract description 11
- KZNIFHPLKGYRTM-UHFFFAOYSA-N apigenin Chemical compound C1=CC(O)=CC=C1C1=CC(=O)C2=C(O)C=C(O)C=C2O1 KZNIFHPLKGYRTM-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229940117893 apigenin Drugs 0.000 claims abstract description 10
- XADJWCRESPGUTB-UHFFFAOYSA-N apigenin Natural products C1=CC(O)=CC=C1C1=CC(=O)C2=CC(O)=C(O)C=C2O1 XADJWCRESPGUTB-UHFFFAOYSA-N 0.000 claims abstract description 10
- 235000008714 apigenin Nutrition 0.000 claims abstract description 10
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims abstract description 9
- LTTQKYMNTNISSZ-MWTRTKDXSA-N (2S)-(-)-kurarinone Chemical compound C1([C@H]2OC=3C(C[C@@H](CC=C(C)C)C(C)=C)=C(O)C=C(C=3C(=O)C2)OC)=CC=C(O)C=C1O LTTQKYMNTNISSZ-MWTRTKDXSA-N 0.000 claims abstract description 8
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 8
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims abstract description 8
- XQVFLLMCNGKXSM-UHFFFAOYSA-N kurarinone Natural products COc1cc(O)c(C(CC=C(C)C)C(=C)C)c2OC(CC(=O)c12)c3ccc(O)cc3O XQVFLLMCNGKXSM-UHFFFAOYSA-N 0.000 claims abstract description 8
- KDADHLPROOOPIC-UHFFFAOYSA-N neokurarinol Natural products COc1cc(O)ccc1C1CC(=O)c2c(OC)cc(O)c(CC(CCC(C)(C)O)C(C)=C)c2O1 KDADHLPROOOPIC-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 238000007605 air drying Methods 0.000 claims abstract description 6
- 238000004140 cleaning Methods 0.000 claims abstract description 6
- 238000005360 mashing Methods 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 241000196324 Embryophyta Species 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 9
- 241000220317 Rosa Species 0.000 claims description 7
- 230000000844 anti-bacterial effect Effects 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 244000178870 Lavandula angustifolia Species 0.000 claims description 4
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 4
- 239000001102 lavandula vera Substances 0.000 claims description 4
- 235000018219 lavender Nutrition 0.000 claims description 4
- 235000013311 vegetables Nutrition 0.000 claims 1
- 230000007797 corrosion Effects 0.000 abstract description 5
- 238000005260 corrosion Methods 0.000 abstract description 5
- 239000003086 colorant Substances 0.000 abstract description 4
- 238000010428 oil painting Methods 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- XVPBINOPNYFXID-JARXUMMXSA-N 85u4c366qs Chemical compound C([C@@H]1CCC[N@+]2(CCC[C@H]3[C@@H]21)[O-])N1[C@@H]3CCCC1=O XVPBINOPNYFXID-JARXUMMXSA-N 0.000 description 5
- 229930015582 oxymatrine Natural products 0.000 description 5
- 239000000463 material Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 244000181025 Rosa gallica Species 0.000 description 2
- 235000000533 Rosa gallica Nutrition 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000001052 yellow pigment Substances 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 240000001548 Camellia japonica Species 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 241001494479 Pecora Species 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 239000006004 Quartz sand Substances 0.000 description 1
- 241000109329 Rosa xanthina Species 0.000 description 1
- 235000004789 Rosa xanthina Nutrition 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000001055 blue pigment Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 235000018597 common camellia Nutrition 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 210000004209 hair Anatomy 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 229940095050 propylene Drugs 0.000 description 1
- 239000001054 red pigment Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
Abstract
The invention discloses a preparation method and application of a plant pigment for an inner painting, and belongs to the technical field of inner painting research. The preparation method of the plant pigment comprises the following steps: cleaning fresh petals, air drying, and mashing; adding alum and apigenin or kurarinone and propylene into the mashed fresh petals, uniformly mixing, sealing and standing for 25-30 days, wherein the adding amount of alum in 100g of the mashed fresh petals is 8-12g, the adding amount of apigenin or kurarinone is 10-15g and the adding amount of propylene is 40-50ml; the resulting mixture is ground again and sealed for future use. The plant pigment is convenient to use, can be matched with tin powder, gold powder and silver powder to prepare different colors, has the advantages of strong corrosion resistance, large color change and good environmental protection performance compared with the conventional traditional Chinese painting pigment and oil painting pigment, and has beautiful and bright color in terms of color.
Description
Technical Field
The invention relates to a preparation method and application of a plant pigment for an inner painting, belonging to the technical field of inner painting pigment research.
Background
After the cigarette is happy, the snuff does not fall. The worker is careful to make transparent materials such as colored glaze (glass), agate, crystal and the like into a pot, and after the pot is taken out, small steel balls, quartz sand and a small amount of water are added into the pot to shake back and forth, so that the smooth inner wall is frosted into a fine grain surface, and the pigment ink color is easy to adhere. Then, the bamboo, copper and aluminum with hooks are used as materials, the materials are cut and ground into fine materials like a needle point and the hooks like a moon, and wools and sheep hair are bound to prepare the painting brush. The color reflection painting for taking ink according to the painting drawing skill gradually becomes the art of painting inside the snuff bottle which is viewed and spread to the present.
The modern art school of the snuff bottle with the inner picture originates from Beijing, and the history of Beijing is the most distant. Beijing is the emperor of the dynasty of the Ming and Qing dynasties of China, is also the auspicious place of the inside-painted snuff bottle, is a salty collection of people with prosperous professions in all trades, has developed economic culture, has certain necessity for cultivating the inside-painted snuff bottle art, and draws the deep culture base of the Beijing by the inside-painted artists to gradually form the Beijing style of art with poetry, writing and painting printing. Wherein, the Yunnan Pai inner painting has a characteristic of Yunnan.
The traditional inner painting pigment is generally prepared by directly selecting traditional Chinese painting pigment and oil painting pigment; in addition, ceramic pigments are selected for the baked color inner painting, and the traditional inner painting pigments are low in corrosion resistance and difficult to preserve for a long time, and are a technical bottleneck of the inner painting technology.
Disclosure of Invention
The invention aims to provide a preparation method of a plant pigment for inner painting, which comprises the following steps:
(1) Cleaning fresh petals, air drying, and mashing.
(2) Adding alum and apigenin or kurarinone and propylene into the mashed fresh petals, uniformly mixing, sealing and standing for 25-30 days, wherein the adding amount of alum in 100g of the mashed fresh petals is 8-12g, the adding amount of apigenin or kurarinone is 10-15g and the adding amount of propylene is 40-50ml.
(3) And (3) grinding the mixture obtained in the step (2) again, and sealing for later use.
Preferably, the fresh petals of the invention are antibacterial fresh petals.
Preferably, the fresh petals are red petals of a rose, and the obtained plant pigment is red.
Preferably, the fresh petals of the invention are petals of yellow roses, and the obtained plant pigment is yellow.
Preferably, the fresh petals are lavender petals, and the obtained plant pigment is blue.
The invention can also select other petals to prepare the plant pigment, and the red, yellow and blue are basic colors and can be matched to obtain different colors.
The plant pigment is mixed with one or more of gold powder, silver powder and tin powder, propylene is added for color matching, and the adding amount of each pigment is adjusted according to actual needs. The addition of the gold powder, the silver powder and the tin powder can enable the color to be more textured, and if the gold powder and the silver powder are added in some mines, stones and the like during drawing, pictures can flash and shine, so that the pictures are more vivid and stereoscopic.
The invention has the advantages of
(1) The plant pigment prepared by the method takes fresh petals as a raw material, can be independently used as a raw material for painting the petals, is bright and vivid in color, is stable in color and cannot fade. The prepared plant pigment can be stored in the air for a long time without color change, the pigment is changed into a block from a paste state along with the increase of the using time, the original color can be changed after propylene is added, and the use and the storage are very convenient.
(2) The plant pigment prepared by the method can be stored in the air for a long time without fading, probably because the fresh petals have antibacterial performance and react with alum to generate an antiseptic new substance, and the apigenin or the kurarinone has the effect of stabilizing the color.
(3) The plant pigment is convenient to use, can be matched with mineral raw materials, tin powder and gold powder to prepare different colors, has the advantages of strong corrosion resistance, large color change and good environmental protection performance compared with the conventional traditional Chinese painting pigment and oil painting pigment, and is more beautiful and bright in color and very beautiful.
Detailed Description
The present invention is further described in detail with reference to the following specific examples, but the scope of the present invention is not limited to the above description.
Example 1
A preparation method of a plant pigment for inner painting specifically comprises the following steps:
(1) Cleaning fresh red rose petals, air drying, and mashing.
(2) Adding alum, apigenin and propylene into mashed fresh red rose petals, uniformly mixing, sealing, and standing for 25 days, wherein the addition amount of alum in 100g of the mashed fresh rose petals is 10g, the addition amount of apigenin is 15g, and the addition amount of propylene is 45ml.
(3) And (3) grinding the mixture obtained in the step (2) again, and sealing for later use.
Example 2
A preparation method of a plant pigment for inner painting specifically comprises the following steps:
(1) Cleaning fresh yellow rose petals, air drying, and mashing.
(2) Adding Alumen, oxymatrine, and propylene into mashed fresh yellow rose petal, mixing, sealing, and standing for 28 days, wherein the amount of Alumen added in 100g of mashed fresh rose petal is 12g, the amount of oxymatrine added is 10g, and the amount of propylene added is 50ml.
(3) And (3) grinding the mixture obtained in the step (2) again, and sealing for later use.
Example 3
A preparation method of a plant pigment for inner painting specifically comprises the following steps:
(1) Cleaning fresh Lavender petal, air drying, and mashing.
(2) Adding Alumen, oxymatrine, and propylene into mashed fresh Lavender petal, mixing, sealing, and standing for 30 days, wherein 100g of the mashed fresh petal contains Alumen 8g, oxymatrine 13g, and propylene 40ml.
(3) And (3) grinding the mixture obtained in the step (2) again, and sealing for later use.
Comparative example 1
The conditions of this example were the same as example 1 except that apigenin or kurarinone was not added.
Comparative example 2
The conditions of this example were the same as example 1, except that no alum was added.
Plant pigments can be obtained in examples 1 and 3, red pigments can be obtained in example 1, yellow pigments can be obtained in example 2, and blue pigments can be obtained in example 3, and the pigments are bright and can be stored in air for a long time and do not change color for 2 to 3 years.
The plant pigment provided by the embodiment of the invention can be matched with gold powder, silver powder and tin powder for color matching in the using process, for example, camellia can be prepared by red plant pigment, tin powder and propylene, the color of a mine can be prepared by yellow pigment, gold powder and silver powder, and after the gold powder, the silver powder or the tin powder is added, the texture of a picture can be better.
The corrosivity, the fluency, the uniformity, the chromatic aberration and the antibacterial property of the pigments obtained in the examples 1 to 3 are tested by a conventional method, wherein the corrosion resistance test method comprises the following steps: the inner painting drawn by the pigment is placed in salt fog, the change of color is observed, and the experimental effect is shown in table 1.
TABLE 1
As can be seen from Table 1, the pigments prepared in examples 1 to 3 have better uniformity, antibacterial property, corrosion resistance and stability, and the addition of alum and oxymatrine is beneficial to improving the performance of the pigment.
Claims (7)
1. A preparation method of a plant pigment for inner painting is characterized by comprising the following steps:
(1) Cleaning fresh petals, air drying, and mashing;
(2) Adding alum and apigenin or kurarinone and propylene into the mashed fresh petals, uniformly mixing, sealing and standing for 25-30 days, wherein the adding amount of alum in 100g of the mashed fresh petals is 8-12g, the adding amount of apigenin or kurarinone is 10-15g and the adding amount of propylene is 40-50ml;
(3) And (3) grinding the mixture obtained in the step (2) again, and sealing for later use.
2. The method for preparing a plant pigment for interior painting according to claim 1, characterized in that: and (3) placing the mixture in the step (2) at a reaction temperature of 25-30 ℃.
3. The method for preparing a plant pigment for interior painting according to claim 1, characterized in that: the fresh petals are antibacterial fresh petals.
4. The method for preparing a plant pigment for interior painting according to claim 3, characterized in that: the fresh petals are red petals of rose, and the obtained plant pigment is red.
5. The method for preparing a plant pigment for interior painting according to claim 3, characterized in that: the fresh petals are petals of yellow rose, and the obtained plant pigment is yellow.
6. The method for preparing a plant pigment for interior painting according to claim 3, characterized in that: the fresh petals are petals of lavender, and the obtained plant pigment is blue.
7. Use of a vegetable pigment obtained by the process according to claim 1, wherein: the plant pigment is mixed with one or more of gold powder, silver powder and tin powder, propylene is added for color matching, and the adding amount of each pigment is adjusted according to actual needs.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211265054.1A CN115595004B (en) | 2022-10-17 | 2022-10-17 | Preparation method and application of plant pigment for interior painting |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211265054.1A CN115595004B (en) | 2022-10-17 | 2022-10-17 | Preparation method and application of plant pigment for interior painting |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115595004A true CN115595004A (en) | 2023-01-13 |
| CN115595004B CN115595004B (en) | 2024-04-05 |
Family
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| Application Number | Title | Priority Date | Filing Date |
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| CN202211265054.1A Active CN115595004B (en) | 2022-10-17 | 2022-10-17 | Preparation method and application of plant pigment for interior painting |
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| Country | Link |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5780060A (en) * | 1994-02-02 | 1998-07-14 | Centre National De La Recherche Scientifique | Microcapsules with a wall of crosslinked plant polyphenols and compositions containing them |
| CN102690530A (en) * | 2012-06-07 | 2012-09-26 | 南通恒隆化工有限公司 | Environment-friendly pigment red |
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-
2022
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| CN113801495A (en) * | 2021-09-29 | 2021-12-17 | 浙江理工大学 | Preparation method of antibacterial composite pigment juice green based on high-energy ball milling method and freeze drying technology |
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| CN115595004B (en) | 2024-04-05 |
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