CN115554236A - Preparation method of swelling-diminishing and pain-relieving ointment - Google Patents
Preparation method of swelling-diminishing and pain-relieving ointment Download PDFInfo
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- 208000002193 Pain Diseases 0.000 title claims abstract description 23
- 239000002674 ointment Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 79
- 239000000341 volatile oil Substances 0.000 claims abstract description 55
- 239000003921 oil Substances 0.000 claims abstract description 46
- 235000019198 oils Nutrition 0.000 claims abstract description 46
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 44
- 238000001914 filtration Methods 0.000 claims abstract description 41
- 238000002156 mixing Methods 0.000 claims abstract description 31
- 238000010438 heat treatment Methods 0.000 claims abstract description 27
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- 235000015912 Impatiens biflora Nutrition 0.000 claims abstract description 25
- 235000006679 Mentha X verticillata Nutrition 0.000 claims abstract description 20
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- 238000003756 stirring Methods 0.000 claims abstract description 16
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- 238000001816 cooling Methods 0.000 claims abstract description 9
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 claims abstract description 9
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 claims abstract description 9
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims abstract description 9
- 229940043351 ethyl-p-hydroxybenzoate Drugs 0.000 claims abstract description 9
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000012467 final product Substances 0.000 claims abstract description 4
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- 230000000202 analgesic effect Effects 0.000 claims description 4
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- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 1
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- QMAYBMKBYCGXDH-UHFFFAOYSA-N alpha-amorphene Natural products C1CC(C)=CC2C(C(C)C)CC=C(C)C21 QMAYBMKBYCGXDH-UHFFFAOYSA-N 0.000 description 1
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- YOCDGWMCBBMMGJ-UHFFFAOYSA-N delta-cadinene Natural products C1C=C(C)CC2C(C(C)C)CCC(=C)C21 YOCDGWMCBBMMGJ-UHFFFAOYSA-N 0.000 description 1
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- 230000000552 rheumatic effect Effects 0.000 description 1
- USDOQCCMRDNVAH-UHFFFAOYSA-N sigma-cadinene Natural products C1C=C(C)CC2C(C(C)C)CC=C(C)C21 USDOQCCMRDNVAH-UHFFFAOYSA-N 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
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- 150000003505 terpenes Chemical class 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/06—Ointments; Bases therefor; Other semi-solid forms, e.g. creams, sticks, gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/21—Amaranthaceae (Amaranth family), e.g. pigweed, rockwort or globe amaranth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/25—Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
- A61K36/258—Panax (ginseng)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/758—Zanthoxylum, e.g. pricklyash
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/82—Theaceae (Tea family), e.g. camellia
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/16—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing nitrogen, e.g. nitro-, nitroso-, azo-compounds, nitriles, cyanates
- A61K47/18—Amines; Amides; Ureas; Quaternary ammonium compounds; Amino acids; Oligopeptides having up to five amino acids
- A61K47/183—Amino acids, e.g. glycine, EDTA or aspartame
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0014—Skin, i.e. galenical aspects of topical compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The scheme relates to a preparation method of a swelling and pain relieving ointment, which comprises the following steps: 5-10 parts of a small fig old vine juice, 25-40 parts of a achyranthes root stem juice, 5-10 parts of a pseudo-ginseng flower juice, 5-10 parts of a impatiens balsamina stem juice, 5-10 parts of glycerol and 1-3 parts of cocoyl disodium glutamate, and mixing and heating the materials according to a proportion until the materials are melted; preparing an oil phase: 1-2 parts of pepper volatile oil and 1-2 parts of mint volatile oil; 6-10 parts of vaseline; 6-9 parts of beeswax; 8-15 parts of tea seed oil; mixing according to the proportion, heating in water bath; filtering the melted oil phase, and removing residues; heating the oil phase and the water phase to the same temperature, slowly pouring the water phase into the oil phase, slowly stirring, adding 0.1-0.3 part by mass of ethyl p-hydroxybenzoate, and cooling to paste to obtain the final product. The ointment prepared by the invention has the effects of relieving swelling and pain, and activating blood circulation to dissipate blood stasis. The product has simple preparation process, and is convenient and safe for use.
Description
Technical Field
The invention relates to a plaster technology, in particular to a swelling and pain relieving plaster.
Background
In activities such as daily life, production, labor, exercise and the like, people often encounter collision, subcutaneous capillary vessel rupture can occur after local skin is collided and collided, and subcutaneous congestion is caused, and a local cold compress method is mostly adopted for the situation, so that the contraction of the capillary vessel after the local cold compress can relieve the symptom of the subcutaneous congestion and relieve local swelling; can also be treated by adopting a medicinal method. In the actual activities of life, production, working, sports and the like, ice is not seen everywhere, and a plurality of people do not specially buy oral medicines for once bump.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a preparation method of a portable detumescence analgesic plaster.
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of the swelling-diminishing pain-relieving plaster comprises the following steps:
preparing an aqueous phase: 5-10 parts of a small fig old vine juice, 25-40 parts of a achyranthes root stem juice, 5-10 parts of a pseudo-ginseng flower juice, 5-10 parts of a impatiens balsamina stem juice, 5-10 parts of glycerol and 1-3 parts of cocoyl disodium glutamate, and mixing and heating the materials according to a proportion until the materials are melted;
preparing an oil phase: 1-2 parts of pepper volatile oil and 1-2 parts of mint volatile oil; 6-10 parts of vaseline; 6-9 parts of beeswax; 8-15 parts of tea seed oil; mixing according to the proportion, heating in water bath; filtering the melted oil phase, and removing residues;
heating the oil phase and the water phase to the same temperature, slowly pouring the water phase into the oil phase, mixing, slowly stirring, adding 0.1-0.3 part by mass of ethyl p-hydroxybenzoate, and cooling to paste to obtain the final product.
Furthermore, the water phase is heated to 85 ℃ in the preparation process, and the oil phase is heated to 50-95 ℃ in the preparation process.
Further, the preparation of each juice in the aqueous phase is as follows:
cleaning caulis Seu folium Ampelopsis Brevipedunculatae, air drying, cutting, pulping, and filtering with multilayer gauze to obtain the final product;
collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, air drying, cutting, pulping, and filtering with multilayer gauze to obtain impatiens balsamina stem liquid;
taking achyranthes stem liquid, namely taking achyranthes stem of 7-8 months, picking clean leaves, cleaning, drying, cutting, pulping, and filtering by adopting a plurality of layers of gauze to obtain the achyranthes stem liquid;
and (3) taking 7-8 months of the pseudo-ginseng flower, cleaning, airing, cutting, pulping, and filtering by adopting a plurality of layers of gauzes to obtain the pseudo-ginseng flower juice.
Further, in the oil phase:
herba Menthae volatile oil is prepared by cleaning folium Menthae, cutting, and steam distilling to obtain herba Menthae volatile oil;
and (3) taking the pepper volatile oil, cleaning the pepper, and obtaining the pepper volatile oil by adopting a steam distillation method.
The small flower vine is used as a medicine by root and old vine and is used for treating diseases such as blood deficiency, irregular menstruation, amenorrhea, postpartum weakness, lumbar and leg soreness and pain, traumatic fracture and the like.
The balsamine stems have the effects of expelling wind-damp, promoting blood circulation and relieving pain, and are used for treating rheumatic arthralgia and difficulty in flexion and extension.
The achyranthes root stem has the functions of removing blood stasis, stimulating the menstrual flow, tonifying liver and kidney, strengthening muscles and bones, inducing diuresis, treating stranguria and guiding blood downward.
Notoginseng radix has effects of removing blood stasis, stopping bleeding, promoting blood circulation, and relieving pain. Can be used for treating hemorrhage, traumatic injury, and swelling and pain due to blood stasis.
The chemical components of herba Menthae mainly include volatile oil, flavonoids, terpenes, phenolic acids, quinones, phenylpropanoids, etc. Modern pharmacological research shows that the mint has pharmacological activities of antibiosis, antivirus, anti-inflammation, antioxidation, antitumor and the like.
The main components of the pepper volatile oil comprise linalool, limonene, beta-myrcene, delta-cadinene and other compounds, and the pepper volatile oil has biological activities of resisting inflammation, easing pain, inhibiting bacteria, killing insects, resisting oxidation, resisting tumors, performing local anesthesia, promoting percutaneous penetration and the like.
The tea seed oil has effects of keeping moisture, smoothing, preventing dry wrinkle, killing bacteria, and relieving itching.
Based on the raw materials, the plaster prepared by mixing the raw materials in a proper proportion is suitable for subcutaneous hematoma caused by trauma, and the using method comprises the following steps: after the ointment is cleaned conventionally, the ointment is applied to the wound twice a day without binding.
The invention has the beneficial effects that: the ointment prepared by the invention has the effects of relieving swelling and pain, and promoting blood circulation to remove blood stasis. The product has simple preparation process and convenient and safe use.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments, and it should be apparent that the described embodiments are some, but not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Furthermore, the technical features involved in the different embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Example 1
(1) Taking materials
(1) Cleaning and air drying the old rattan juice of the raw rattan with the acid rattan, chopping and pulping the old rattan with the acid rattan juice, and filtering the filtrate with four layers of gauze to obtain the old rattan juice of the raw rattan with the acid rattan juice;
(2) collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, drying in the air, chopping and pulping, and filtering by adopting four layers of gauze to obtain filtrate to obtain juice of raw impatiens balsamina stems;
(3) taking achyranthes bidentata stem liquid, namely taking achyranthes bidentata stem of 7-8 months, picking clean leaves, cleaning, drying, chopping and pulping, and filtering by adopting four layers of gauze to obtain filtrate of raw achyranthes bidentata stem liquid;
(4) taking 7-8 months of pseudo-ginseng flower, cleaning, airing, chopping and pulping, and filtering by adopting four layers of gauze to obtain filtrate to obtain raw pseudo-ginseng flower juice;
(5) herba Menthae volatile oil is prepared by cleaning folium Menthae, cutting, and steam distilling to obtain herba Menthae volatile oil;
(6) cleaning pericarpium Zanthoxyli to obtain pericarpium Zanthoxyli volatile oil, and steam distilling to obtain pericarpium Zanthoxyli volatile oil;
(2) Make up of
(1) The composition of the water phase is as follows: 5 parts by mass of old vine juice of raw small fig vine, 40 parts by mass of achyranthes root stem juice and 10 parts by mass of pseudo-ginseng flower juice; 8 parts by mass of impatiens balsamina stem juice; 5 parts of glycerol; 2 parts by mass of coconut acyl disodium glutamate;
(2) the oil phase comprises the following components: 1 part by mass of pepper volatile oil and 2 parts by mass of mint volatile oil; 8 parts of vaseline; 8 parts of beeswax; 10 parts of tea seed oil;
(3) Preparation of pain-relieving swelling-dispersing ointment
Mixing five substances in an oil phase: mixing the volatile oil of fructus Zanthoxyli, the volatile oil of herba Menthae, vaseline, cera flava, and tea seed oil at a certain ratio, heating in water bath, and dissolving at 50 deg.C; filtering the melted oil phase, and removing residues;
mixing six substances in water phase, including caulis Seu folium Ampelopsis Brevipedunculatae solution, caulis Impatientis solution, achyranthis radix stem solution, notoginseng radix juice, glycerol, and disodium cocoyl glutamate at a certain proportion, and heating to melt.
Heating the oil phase and the water phase to the same temperature, slowly pouring the obtained water phase into the oil phase, mixing, slowly stirring, adding 0.2 parts by mass of ethyl p-hydroxybenzoate, slowly stirring, and cooling to obtain a green oily ointment.
Example 2
(1) Taking materials
(1) Cleaning and air drying the old rattan juice of the raw rattan with the acid rattan, chopping and pulping the old rattan with the acid rattan, and filtering the filtrate with three layers of gauze to obtain the old rattan juice of the raw rattan with the acid rattan;
(2) collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, air drying, chopping and pulping, and filtering with three layers of gauze to obtain filtrate to obtain juice of raw impatiens balsamina stems;
(3) taking achyranthes bidentata stem liquid, namely taking achyranthes bidentata stem of 7-8 months, picking clean leaves, cleaning, drying, cutting, pulping, and filtering by adopting three layers of gauze to obtain filtrate of raw achyranthes bidentata stem;
(4) taking 7-8 months of pseudo-ginseng flower, cleaning, airing, chopping and pulping, and filtering by adopting three layers of gauze to obtain filtrate to obtain raw pseudo-ginseng flower juice;
(5) cleaning and cutting mint leaves, and obtaining mint volatile oil by adopting a steam distillation method;
(6) cleaning pericarpium Zanthoxyli, and steam distilling to obtain pericarpium Zanthoxyli volatile oil;
(2) Make up of
(1) The composition of the water phase is as follows: 10 parts by mass of old vine juice of raw small fig vine, 36 parts by mass of achyranthes root stem juice and 5 parts by mass of pseudo-ginseng flower juice; 10 parts by mass of impatiens balsamina stem juice; 10 parts of glycerol; 1 part by mass of coconut oil acyl disodium glutamate
(2) The oil phase comprises the following components: 2 parts of pepper volatile oil and 1 part of mint volatile oil; 7 parts of vaseline; 9 parts of beeswax; 8 parts of tea seed oil;
(3) Preparation of pain-relieving swelling-dispersing ointment
Mixing five substances in an oil phase: mixing the volatile oil of fructus Zanthoxyli, the volatile oil of herba Menthae, vaseline, cera flava, and tea seed oil at a certain ratio, heating in water bath, and dissolving at 65 deg.C; filtering the melted oil phase, and removing residues;
mixing six substances in water phase, including caulis Seu folium Ampelopsis Brevipedunculatae solution, caulis Impatientis solution, achyranthis radix stem solution, notoginseng radix juice, glycerol, and disodium cocoyl glutamate at a certain proportion, and heating to melt.
Heating the oil phase and the water phase to the same temperature, slowly pouring the obtained water phase into the oil phase, mixing, slowly stirring, adding 0.3 parts by mass of ethyl p-hydroxybenzoate, slowly stirring, and cooling to obtain a green oily ointment.
Example 3
(1) Taking materials
(1) Cleaning and air drying the old rattan juice of the raw rattan with the acid rattan, chopping and pulping the old rattan with the acid rattan, and filtering the filtrate with three layers of gauze to obtain the old rattan juice of the raw rattan with the acid rattan;
(2) collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, drying, chopping and pulping, and filtering by adopting three layers of gauze to obtain filtrate to obtain juice of raw impatiens balsamina stems;
(3) taking achyranthes bidentata stem liquid, namely taking achyranthes bidentata stem of 7-8 months, picking clean leaves, cleaning, drying, cutting and pulping, and filtering by adopting four layers of gauze to obtain filtrate of raw achyranthes bidentata stem;
(4) the notoginseng flower juice is obtained by taking 7-8 months notoginseng flowers, cleaning, airing, chopping, pulping, and filtering by adopting four layers of gauze to obtain filtrate, thus obtaining raw notoginseng flower juice;
(5) cleaning and cutting mint leaves, and obtaining mint volatile oil by adopting a steam distillation method;
(6) cleaning pericarpium Zanthoxyli, and steam distilling to obtain pericarpium Zanthoxyli volatile oil;
(2) Composition of
(1) The composition of the water phase is as follows: 8 parts by mass of old vine juice of raw small fig vine, 32 parts by mass of achyranthes root stem juice and 8 parts by mass of pseudo-ginseng flower juice; 8 parts by mass of impatiens balsamina stem juice; 8 parts of glycerol; 2 parts by mass of coconut oil acyl disodium glutamate
(2) The oil phase comprises the following components: 2 parts of pepper volatile oil and 2 parts of mint volatile oil; 8 parts of vaseline; 8 parts of beeswax; 13 parts by mass of tea seed oil;
(3) Preparation of analgesic and repercussive plaster
Mixing five substances in an oil phase: mixing volatile oil of fructus Zanthoxyli, volatile oil of herba Menthae, vaseline, cera flava, and tea seed oil at a certain ratio, heating in water bath, and dissolving at 75 deg.C; filtering the melted oil phase, and removing residues;
mixing six materials in water phase, including caulis Seu folium Ampelopsis Brevipedunculatae solution, caulis Impatientis solution, achyranthis radix stem solution, notoginseng radix juice, glycerol, and disodium cocoyl glutamate at a certain proportion, and heating to melt.
Heating the oil phase and the water phase to the same temperature, slowly pouring the obtained water phase into the oil phase, mixing, slowly stirring, adding 0.2 parts by mass of ethyl p-hydroxybenzoate while stirring, slowly stirring, and cooling to obtain green oily ointment.
Example 4
(1) Taking materials
(1) Cleaning and air drying the old rattan juice of the raw rattan with the acid rattan, chopping and pulping the old rattan with the acid rattan juice, and filtering the filtrate with four layers of gauze to obtain the old rattan juice of the raw rattan with the acid rattan juice;
(2) collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, drying, chopping and pulping, and filtering by adopting three layers of gauze to obtain filtrate to obtain juice of raw impatiens balsamina stems;
(3) taking achyranthes bidentata stem liquid, namely taking achyranthes bidentata stem of 7-8 months, picking clean leaves, cleaning, drying, cutting and pulping, and filtering by adopting four layers of gauze to obtain filtrate of raw achyranthes bidentata stem;
(4) the notoginseng flower juice is obtained by taking 7-8 months notoginseng flowers, cleaning, airing, chopping, pulping, and filtering by adopting three layers of gauze to obtain filtrate, thus obtaining raw notoginseng flower juice;
(5) cleaning and cutting mint leaves, and obtaining mint volatile oil by adopting a steam distillation method;
(6) cleaning pericarpium Zanthoxyli, and steam distilling to obtain pericarpium Zanthoxyli volatile oil;
(2) Composition of
(1) The composition of the water phase is as follows: 6 parts by mass of old vine juice of raw small-flowered gambir fruits, 25 parts by mass of achyranthes root stem juice and 10 parts by mass of pseudo-ginseng flower juice; 10 parts by mass of impatiens balsamina stem juice; 8 parts by mass of glycerol; 3 parts by mass of coconut oil acyl disodium glutamate
(2) The oil phase comprises the following components: 2 parts of pepper volatile oil and 2 parts of mint volatile oil; 10 parts of vaseline; 9 parts of beeswax; 14 parts of tea seed oil;
(3) Preparation of pain-relieving swelling-dispersing ointment
Mixing five substances in an oil phase: mixing the volatile oil of fructus Zanthoxyli, the volatile oil of herba Menthae, vaseline, cera flava, and tea seed oil at a certain ratio, heating in water bath, and dissolving at 95 deg.C; filtering the melted oil phase, and removing residues;
mixing six substances in water phase, including caulis Seu folium Ampelopsis Brevipedunculatae solution, caulis Impatientis solution, achyranthis radix stem solution, notoginseng radix juice, glycerol, and disodium cocoyl glutamate at a certain proportion, and heating to melt.
Heating the oil phase and the water phase to the same temperature, slowly pouring the obtained water phase into the oil phase, mixing, slowly stirring, adding 0.2 parts by mass of ethyl p-hydroxybenzoate, slowly stirring, and cooling to obtain a green oily ointment.
Example 5
(1) Taking materials
(1) Cleaning and air drying the old rattan juice of the raw rattan with the acid rattan, chopping and pulping the old rattan with the acid rattan, and filtering the filtrate with three layers of gauze to obtain the old rattan juice of the raw rattan with the acid rattan;
(2) collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, air drying, chopping and pulping, and filtering with four layers of gauze to obtain filtrate to obtain juice of raw impatiens balsamina stems;
(3) taking achyranthes bidentata stem liquid, namely taking achyranthes bidentata stem of 7-8 months, picking clean leaves, cleaning, drying, cutting, pulping, and filtering by adopting three layers of gauze to obtain filtrate of raw achyranthes bidentata stem;
(4) the notoginseng flower juice is obtained by taking 7-8 months notoginseng flowers, cleaning, airing, chopping, pulping, and filtering by adopting four layers of gauze to obtain filtrate, thus obtaining raw notoginseng flower juice;
(5) cleaning and cutting mint leaves, and obtaining mint volatile oil by adopting a steam distillation method;
(6) cleaning pericarpium Zanthoxyli, and distilling with water vapor to obtain pericarpium Zanthoxyli volatile oil;
(2) Taking materials
(1) The composition of the water phase is as follows: 7 parts by mass of old vine juice of raw small fig vine, 34 parts by mass of achyranthes root stem juice and 9 parts by mass of pseudo-ginseng flower juice; 5 parts of impatiens balsamina stem juice; 7 parts of glycerol; 2 parts by mass of coconut oil acyl disodium glutamate
(2) The oil phase comprises the following components: 2 parts by mass of pepper volatile oil and 2 parts by mass of mint volatile oil; 10 parts of vaseline; 6 parts of beeswax; 15 parts of tea seed oil;
(3) Preparation of analgesic and repercussive plaster
Mixing five substances in an oil phase: mixing the volatile oil of fructus Zanthoxyli, the volatile oil of herba Menthae, vaseline, cera flava, and tea seed oil at a certain ratio, heating in water bath, and dissolving at 85 deg.C; filtering the melted oil phase, and removing residues;
mixing six substances in water phase, including caulis Seu folium Ampelopsis Brevipedunculatae solution, caulis Impatientis solution, achyranthis radix stem solution, notoginseng radix juice, glycerol, and disodium cocoyl glutamate at a certain proportion, and heating to melt.
Heating the oil phase and the water phase to the same temperature, slowly pouring the obtained water phase into the oil phase, mixing, slowly stirring, adding 0.1 part by mass of ethyl p-hydroxybenzoate, slowly stirring, and cooling to obtain green oily ointment.
Example 6
(1) Taking materials
(1) Cleaning and air drying the old rattan juice of the raw rattan with the acid rattan, chopping and pulping the old rattan with the acid rattan juice, and filtering the filtrate with four layers of gauze to obtain the old rattan juice of the raw rattan with the acid rattan juice;
(2) collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, air drying, chopping and pulping, and filtering with four layers of gauze to obtain filtrate to obtain juice of raw impatiens balsamina stems;
(3) taking achyranthes bidentata stem liquid, namely taking achyranthes bidentata stem of 7-8 months, picking clean leaves, cleaning, drying, cutting, pulping, and filtering by adopting three layers of gauze to obtain filtrate of raw achyranthes bidentata stem;
(4) taking 7-8 months of pseudo-ginseng flower, cleaning, airing, chopping and pulping, and filtering by adopting three layers of gauze to obtain filtrate to obtain raw pseudo-ginseng flower juice;
(5) cleaning and cutting mint leaves, and obtaining mint volatile oil by adopting a steam distillation method;
(6) cleaning pericarpium Zanthoxyli, and steam distilling to obtain pericarpium Zanthoxyli volatile oil;
(2) Composition of
(1) The composition of the water phase is as follows: 9 parts of old vine juice of raw small fig vine, 28 parts of achyranthes stem juice and 10 parts of pseudo-ginseng flower juice; 10 parts by mass of impatiens balsamina stem juice; 9 parts of glycerol; 2 parts by mass of coconut oil acyl disodium glutamate
(2) The oil phase comprises the following components: 1 part by mass of pepper volatile oil and 2 parts by mass of mint volatile oil; 9 parts of vaseline; 7 parts of beeswax; 12 parts of tea seed oil;
(3) Preparation of pain-relieving swelling-dispersing ointment
Five substances of the oil phase: mixing volatile oil of fructus Zanthoxyli, volatile oil of herba Menthae, vaseline, cera flava, and tea seed oil at a certain ratio, heating in water bath, and dissolving at 70 deg.C; filtering the melted oil phase, and removing residues;
mixing six substances in water phase, including caulis Seu folium Ampelopsis Brevipedunculatae solution, caulis Impatientis solution, achyranthis radix stem solution, notoginseng radix juice, glycerol, and disodium cocoyl glutamate at a certain proportion, and heating to melt.
Heating the oil phase and the water phase to the same temperature, slowly pouring the obtained water phase into the oil phase, mixing, slowly stirring, adding 0.1 part by mass of ethyl p-hydroxybenzoate, slowly stirring, and cooling to obtain green oily ointment.
< irritation test and allergy test >
The buttocks of the mice were cut to remove hairs, and the swelling-diminishing and pain-relieving ointments prepared in examples 1, 2, 3, 4, 5 and 6 were applied to the clipped parts and the unhaired parts, respectively, for comparison, and as a result, no irritation or allergic reaction was observed.
The ointment of the invention is used for treating 24 swelling bags (no skin damage) caused by bumping: purple or red swelling bag.
All 24 selected experimenters were people who did not suffer from skin damage due to purple swelling, red swelling or bruise caused by the bump, and the age of the experimenters was from 3 years old to 55 years old, and the average age was 36 years old. The swelling bag is divided into two parts, one half of the swelling bag is not provided with any swelling reducing measure, the other half of the pain-relieving and swelling-reducing ointment obtained according to the embodiment 3 is continuously used for one week twice a day, the swelling bag and the bruise disappear after the part coated with the swelling-relieving and pain-reducing ointment is used for one week, and no pain is caused by pressing; the part without being coated can disappear after 2-3 weeks, and the pressing is painful. The ointment of the invention has no adverse reaction when being applied.
While embodiments of the invention have been disclosed above, it is not limited to the applications listed in the description and the embodiments, which are fully applicable in all kinds of fields of application of the invention, and further modifications may readily be effected by those skilled in the art, so that the invention is not limited to the specific details without departing from the general concept defined by the claims and the scope of equivalents.
Claims (4)
1. A preparation method of the swelling-diminishing and pain-relieving paste is characterized by comprising the following steps:
preparing a water phase: 5-10 parts of a small fig old vine juice, 25-40 parts of a achyranthes root stem juice, 5-10 parts of a pseudo-ginseng flower juice, 5-10 parts of a impatiens balsamina stem juice, 5-10 parts of glycerol and 1-3 parts of cocoyl disodium glutamate, and mixing and heating the materials according to a proportion until the materials are melted;
preparing an oil phase: 1-2 parts of pepper volatile oil and 1-2 parts of mint volatile oil; 6-10 parts of vaseline; 6-9 parts of beeswax; 8-15 parts of tea seed oil; mixing according to the proportion, heating in water bath; filtering the melted oil phase, and removing residues;
heating the oil phase and the water phase to the same temperature, slowly pouring the water phase into the oil phase, slowly stirring, adding 0.1-0.3 parts by mass of ethyl p-hydroxybenzoate, and cooling to obtain a paste.
2. The method for preparing the swelling and pain relieving ointment of claim 1, wherein the water phase is heated to 85 ℃ during the preparation process, and the oil phase is heated to 50-95 ℃ during the preparation process.
3. The method of preparing an analgesic and repercussive paste as set forth in claim 1, wherein each of the juices in the aqueous phase is prepared as follows:
cleaning caulis Seu folium Ampelopsis Brevipedunculatae, air drying, cutting, pulping, and filtering with multilayer gauze to obtain the final product;
collecting 7-8 months of impatiens balsamina stems, picking clean leaves, cleaning, air drying, chopping and pulping, and filtering with multilayer gauze to obtain impatiens balsamina stem liquid;
taking achyranthes stem liquid, namely taking achyranthes stem of 7-8 months, picking clean leaves, cleaning, drying, cutting, pulping, and filtering by adopting a plurality of layers of gauze to obtain the achyranthes stem liquid;
and (3) taking 7-8 months of the pseudo-ginseng flower, cleaning, airing, cutting, pulping, and filtering by adopting a plurality of layers of gauzes to obtain the pseudo-ginseng flower juice.
4. The method of preparing a swelling and pain relieving plaster of claim 1, wherein in the oil phase:
herba Menthae volatile oil is prepared by cleaning folium Menthae, cutting, and steam distilling to obtain herba Menthae volatile oil;
and (3) taking the pepper volatile oil, cleaning the pepper, and obtaining the pepper volatile oil by adopting a steam distillation method.
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| CN202211403668.1A CN115554236A (en) | 2022-11-10 | 2022-11-10 | Preparation method of swelling-diminishing and pain-relieving ointment |
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