CN115531229A - Preparation method of skin-moistening plant essential oil - Google Patents
Preparation method of skin-moistening plant essential oil Download PDFInfo
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- CN115531229A CN115531229A CN202211388629.9A CN202211388629A CN115531229A CN 115531229 A CN115531229 A CN 115531229A CN 202211388629 A CN202211388629 A CN 202211388629A CN 115531229 A CN115531229 A CN 115531229A
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- plant essential
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- 238000002360 preparation method Methods 0.000 title claims abstract description 27
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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Abstract
The invention relates to the technical field of plant essential oil preparation, and discloses a preparation method of skin-moistening plant essential oil, which is characterized by comprising the following steps: s1: selecting raw materials, wherein the raw materials comprise: 25-29% of caprylic/capric triglyceride, 20-22% of olive shell oil, 16-20% of sunflower seed oil, 10-13% of safflower seed oil, 10-12% of squalane, 3-4% of borneol, 2-5% of tocopherol, 1-4% of stearyl glycyrrhetinate, 0.5-2% of alkanna tinctoria root extract, 0.05-0.1% of sophora flavescens ait root extract and 0.05-0.08% of corydalis yanhusuo extract; s2: and (3) mixing and stirring the raw materials in the S1 according to the proportion of the raw materials, namely, taking olive shell oil, sunflower seed oil, safflower seed oil, squalane and tocopherol, and uniformly stirring to form a mixture A. The added solvent is caprylic/capric triglyceride, so that the skin-care oil is excellent in moisturizing grease, has good spreadability, has a smooth but not greasy feeling, and is easy to absorb by the skin. Has good effect on the uniformity and the fineness of cosmetics and can ensure that the skin is smooth and glossy.
Description
Technical Field
The invention relates to the technical field of preparation of plant essential oil, and particularly relates to a preparation method of skin-moistening plant essential oil.
Background
The human skin has a lipid layer which is an important factor influencing the skin state and can prevent the excessive evaporation of skin moisture, moisten the skin, purify the skin, neutralize the pH value of the skin surface and keep the skin healthy. Skin surface lipids mainly originate from lipids secreted by sebaceous glands and in epidermal cells, including squalane, cholesterol, triglycerides, free fatty acids and other components, and skin problems such as dry skin and dermatitis are related to the decrease of lipid content in the cortex.
People pay more attention to skin moisturizing in daily skin care, and oil on the surface of the skin can play a role in moisturizing and water locking, so the oil is more important to be the basis of skin care, and the water-oil balance needs to be paid more attention. However, skin lipid is very easy to lose, and especially, people pay more attention to the fact that the oil control and the use of the more irritating surfactant are excessively cleaned, the cutin is excessively removed, the water is excessively supplemented, and other wrong skin care methods such as skin care methods cause facial degreasing, skin surface lipid is insufficient, the lipid secretion of the skin is serious, the proportion of water and oil is unbalanced, and skin moisture is lost. Therefore, the skin lipid supplement is an important step in the skin care step, and the plant essential oil which contains more lipid and natural moisturizing components has stronger advantages in the aspect of lipid supplement.
The plant essential oil is extracted from parts of flowers, roots, leaves, fruits and the like of plants by distillation and squeezing, generally has small molecular weight and is easily absorbed by human skin. In the above mentioned lipid loss situation, the plant essential oil as a pure oil formulation has a strong advantage in supplementing lipid, and in recent years, consumers are more and more inclined to buy natural cosmetics, and also pay more attention to products with higher safety without adding essence, pigment, hormone and preservative. Essence, pigment and hormone are not added in the cosmetics, the cosmetics are mainly composed of compounds such as water and grease, and the components provide a good environment for bacterial breeding, so that preservative is not added in the cosmetics, the essential oil is in an oil form, the product has low hydration degree and natural bacteriostatic effect, the preservative is not added easily, the plant essential oil can better inherit the natural safe idea to protect the skin, and the plant essential oil is more easily accepted by public consumers.
Common essential oil products are sticky and not easy to absorb, oil films are easy to form on the surface of skin and are easy to rub off, and the moisturizing and water locking effects are reduced.
In order to meet the requirement that people hope to supplement oil and fat without risk components such as preservative, essence, pigment and the like due to water-oil imbalance of the public skin at present, the preparation method of the skin-moistening plant essential oil is provided.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of a skin-moistening plant essential oil.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme: a preparation method of skin-moistening plant essential oil comprises the following steps:
s1: selecting the raw materials, mixing the raw materials,
the raw materials comprise: 25-29% of caprylic/capric triglyceride, 20-22% of olive shell oil, 16-20% of sunflower seed oil, 10-13% of safflower seed oil, 10-12% of squalane, 3-4% of borneol, 2-5% of tocopherol, 1-4% of stearyl glycyrrhetinate, 0.5-2% of alkanna tinctoria root extract, 0.05-0.1% of sophora flavescens ait root extract and 0.05-0.08% of corydalis yanhusuo extract; on the premise of ensuring the skin care requirement, no burden is added to the skin, and no hormone, pigment, essence, preservative and mineral oil are added.
S2: mixing and stirring the raw materials in the S1 according to the proportion, namely, taking olive shell oil, sunflower seed oil, safflower seed oil, squalane and tocopherol, and uniformly stirring to form a mixture A; by adding three natural oils including olive shell oil, sunflower seed oil and safflower seed oil, and compounding ingredients such as caprylic/capric triglyceride, squalane, tocopherol and stearyl glycyrrhetinate, the moisture degree is improved, and the effects of supplementing water and locking water are achieved;
s3: mixing the raw materials in the step S1 according to the proportion, taking caprylic/capric triglyceride and stearyl alcohol glycyrrhetinate, adding the mixture A, and uniformly stirring to form a mixture B;
s4: adding the raw materials in the step S1 into the mixture B according to the proportion, and stirring;
s5: and (4) cooling the stirred substances of the product in the step (S4), discharging after the detection indexes are qualified, and subpackaging the materials into a spray pump to realize storage. Through using the jet pump, spun finish is the linearity, does not drip and spatters, and the weeping is not guaranteed that the bottleneck is clean and tidy, and it is more convenient to use, spouts promptly and uses.
Preferably, in the step S2, the mixing and stirring time is 30min, and the rotating speed is 30-40r/min.
Preferably, in the step S3, the mixing is performed under the condition of heating to 40 ℃.
Preferably, in S3, the mixing and stirring time is 30min, and the rotating speed is 30-40r/min.
Preferably, in the step S4, the stirring time is 60min, the temperature in the stirrer is set to be 30 ℃, and the rotating speed is 30-40r/min.
Preferably, in S5, the temperature is reduced to 20 ℃ for detection.
(III) advantageous effects
Compared with the prior art, the invention provides a preparation method of skin-moistening plant essential oil, which has the following beneficial effects:
1. according to the preparation method of the skin-moistening plant essential oil, the added solvent is caprylic/capric triglyceride, so that the skin-moistening plant essential oil is excellent in moistening grease, has good spreadability, enables the skin to have a smooth but not greasy feeling, and is easy to absorb by the skin. Has good effect on the uniformity and the fineness of cosmetics and can ensure that the skin is smooth and glossy.
2. According to the preparation method of the skin-moistening plant essential oil, the added olive shell oil is natural skin-moistening oil, has fragrant and elegant fragrance, can deeply nourish the skin, enables the skin to become soft and smooth, has a humidity-regulating effect, has no sticky feeling, shows excellent ductility on the skin, can be used as a solvent for dissolving other components, and can also increase the moisture-keeping performance of a skin care product.
3. The preparation method of the plant essential oil for moistening skin comprises adding sunflower seed oil containing ceramide 1, ceramide 2, cerebroside and cholesterol, etc., and can regulate skin state, improve water-oil imbalance, and lubricate skin; the sunflower seed oil contains a large amount of linoleic acid, has very strong permeability, can help other components in the skin care product to permeate into skin, and promotes other nutritional/repair components to better exert effects on the skin; the sunflower seed oil has activating effect on peroxidase-activated receptor, and can promote skin repair; has certain inhibition effect on tyrosinase and certain brightening effect.
4. According to the preparation method of the skin moistening plant essential oil, the added safflower seed oil is high in vitamin E and A contents and rich in linoleic acid, and is used as a skin conditioner, so that other plant extraction components in essential oil can be better brought into play; the safflower oil also has the function of moistening skin, can improve rough skin and make skin smooth and moist.
5. The preparation method of the skin-moistening plant essential oil has the advantages that the added stearyl glycyrrhetinate introduces lipophilic higher alkanol, improves the solubility of grease, has good compatibility with various lipids and higher alkanol, can be used for relieving and resisting allergy, and can also alleviate the toxic and side effects of cosmetics or other factors on skin.
6. According to the preparation method of the skin-moistening plant essential oil, the added squalane and tocopherol have certain moisture-preserving effect and antioxidant effect, and can deeply permeate into the skin, repair the bottom of the skin, moisten the skin, enhance the elasticity of the skin and improve the luster.
7. The plant essential oil for moistening skin is prepared by adding the alkanna tinctoria root extract, the sophora flavescens root extract, the borneol and the corydalis yanhusuo extract, has the active ingredients for relieving, calming the skin, conditioning the skin and moisturizing and repairing the skin.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:
FIG. 1 is a first representative graph of the first test result of the soothing efficacy of the present invention;
FIG. 2 is a second representative graph of the results of the soothing efficacy test of the present invention;
FIG. 3 is a third representative graph of the results of the soothing efficacy test of the present invention;
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Examples of which are illustrated in the accompanying drawings, wherein like reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are illustrative and intended to be illustrative of the invention and are not to be construed as limiting the invention.
In the description of the present invention, it is to be understood that the terms "central," "longitudinal," "lateral," "length," "width," "thickness," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," "clockwise," "counterclockwise," "axial," "radial," "circumferential," and the like are used in the orientations and positional relationships indicated in the drawings for convenience in describing the invention and to simplify the description, and are not intended to indicate or imply that the referenced device or element must have a particular orientation, be constructed and operated in a particular orientation, and are not to be considered limiting of the invention.
In the present invention, unless otherwise explicitly stated or limited, the terms "mounted," "connected," "fixed," and the like are to be construed broadly, e.g., as being permanently connected, detachably connected, or integral; can be mechanically or electrically connected; either directly or indirectly through intervening media, either internally or in any other relationship. The specific meanings of the above terms in the present invention can be understood according to specific situations by those of ordinary skill in the art.
Example 1
A preparation method of skin-moistening plant essential oil comprises the following steps:
s1: selecting the raw materials, mixing the raw materials,
the raw materials comprise: caprylic/capric triglyceride 25%, olive shell oil 20%, sunflower seed oil 20%, safflower seed oil 13%, squalane 12%, borneol 4%, tocopherol 4%, stearyl glycyrrhetinate 1%, alkanna tinctoria root extract 0.9%, sophora flavescens root extract 0.05%, and corydalis repens extract 0.05%;
s2: mixing and stirring the raw materials in the S1 according to the proportion, namely, taking olive shell oil, sunflower seed oil, safflower seed oil, squalane and tocopherol, uniformly stirring for 30min at the rotating speed of 30-40r/min to form a mixture A;
s3: mixing the raw materials in the step S1 according to the proportion, taking caprylic/capric triglyceride and stearyl alcohol glycyrrhetinate, heating to 40 ℃ for mixing, adding the mixture A, mixing and stirring for 30min at the rotating speed of 30-40r/min, and uniformly stirring to form a mixture B;
s4: mixing the raw materials in S1 at a certain ratio, adding Borneolum Syntheticum, radix Arnebiae extract, radix Sophorae Flavescentis extract, and rhizoma corydalis extract into mixture B, stirring for 60min, setting the temperature in the stirrer at 30 deg.C and rotating at 30-40r/min;
s5: and (4) cooling the stirred substances of the product in the step (S4) to 20 ℃, discharging after the detection indexes are qualified, and subpackaging the materials into a spray pump to realize storage.
Example 2
A preparation method of skin-moistening plant essential oil comprises the following steps:
s1: selecting the raw materials, mixing the raw materials,
the raw materials comprise: caprylic/capric triglyceride 27%, olive shell oil 21%, sunflower seed oil 18%, safflower seed oil 12%, squalane 12%, borneol 4%, tocopherol 4%, stearyl glycyrrhetinate 1%, alkanna tinctoria root extract 0.85%, sophora flavescens root extract 0.07%, and corydalis repens extract 0.08%;
s2: mixing and stirring the raw materials in the S1 according to the proportion, namely mixing and stirring olive shell oil, sunflower seed oil, safflower seed oil, squalane and tocopherol for 30min at the rotating speed of 30-40r/min to form a mixture A;
s3: mixing the raw materials in the step S1 according to the proportion, taking caprylic/capric triglyceride and stearyl alcohol glycyrrhetinate, heating to 40 ℃ for mixing, adding the mixture A, mixing and stirring for 30min at the rotating speed of 30-40r/min, and uniformly stirring to form a mixture B;
s4: adding the raw materials in the step S1 into the mixture B according to the proportion, stirring for 60min while stirring, setting the temperature in the stirrer at 30 ℃ and the rotating speed at 30-40r/min;
s5: and (5) cooling the stirred substance of the product in the step (S4) to 20 ℃, discharging after the detection index is qualified, and subpackaging the discharged material into a spray pump to realize storage.
Example 3
A preparation method of skin-moistening plant essential oil comprises the following steps:
s1: selecting the raw materials, mixing the raw materials,
the raw materials comprise: 29% of caprylic/capric triglyceride, 22% of olive shell oil, 16% of sunflower seed oil, 11% of safflower seed oil, 12% of squalane, 4% of borneol, 4% of tocopherol, 1% of stearyl glycyrrhetinate, 0.85% of alkanna tinctoria root extract, 0.07% of sophora flavescens root extract and 0.08% of corydalis yanhusuo extract;
s2: mixing and stirring the raw materials in the S1 according to the proportion, namely mixing and stirring olive shell oil, sunflower seed oil, safflower seed oil, squalane and tocopherol for 30min at the rotating speed of 30-40r/min to form a mixture A;
s3: mixing the raw materials in the step S1 according to the proportion, taking caprylic/capric triglyceride and stearyl alcohol glycyrrhetinate, heating to 40 ℃ for mixing, adding the mixture A, mixing and stirring for 30min at the rotating speed of 30-40r/min, and uniformly stirring to form a mixture B;
s4: adding the raw materials in the step S1 into the mixture B according to the proportion, stirring for 60min while stirring, setting the temperature in the stirrer at 30 ℃ and the rotating speed at 30-40r/min;
s5: and (5) cooling the stirred substance of the product in the step (S4) to 20 ℃, discharging after the detection index is qualified, and subpackaging the discharged material into a spray pump to realize storage.
The product from the above example was taken for soothing effect: inhibition of aggregation of zebrafish embryonic neutrophils the neutrophils from the zebrafish embryos and human neutrophils are highly similar in morphology, biochemical and physiological function. Neutrophils, the first leukocytes to appear at the site of injury or pathogen invasion, act to eliminate infectious or harmful substances. The model of the neutrophil aggregation caused by the damage of the neural cumulus cells in the side line area of the zebra fish embryo is applied to test, the quantity change of the neutrophil in the side line area of the fish embryo of the tested object treatment group and the model control group is compared, and the neutrophil inhibition rate is calculated to evaluate the relieving efficacy of the raw material, the formula or the product.
The test is carried out by using a neutrophil aggregation model caused by the copper sulfate induced neural cumulus cell injury in the lateral line region of the zebra fish embryo. And (3) exposing the 24 fish embryos to a 0.16mg/L copper sulfate pentahydrate and 5g/L arnebia euchroma (Royle) Johnston multielement soothing essence 1 sample solution, setting a model control group, fixing the fish embryos after exposure for 40min, dyeing the fish embryos with Sudan black, counting the number of neutrophils in a lateral line area, and performing statistical analysis.
And (3) testing results:
the following can be seen in combination with the attached drawings:
in the first panel, the dark spots are stained neutrophils. Control group: the soothing effect was not significant (0% inhibition of neutrophil aggregation);
in fig. two, positive control group exemplifies: 0.0036mg/L indometacin has obvious effect of relieving (30% of neutrophil aggregation inhibition rate);
in fig. three, the test sample groups: the plant essential oil has a remarkable relieving effect (51% of neutrophil aggregation inhibition rate).
The above test results show that the present invention has a soothing effect.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising a reference structure" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
Claims (6)
1. The preparation method of the skin-moistening plant essential oil is characterized by comprising the following steps:
s1: selecting the raw materials, mixing the raw materials,
the raw materials comprise: 25-29% of caprylic/capric triglyceride, 20-22% of olive shell oil, 16-20% of sunflower seed oil, 10-13% of safflower seed oil, 10-12% of squalane, 3-4% of borneol, 2-5% of tocopherol, 1-4% of stearyl glycyrrhetinate, 0.5-2% of alkanna tinctoria root extract, 0.05-0.1% of sophora flavescens ait root extract and 0.05-0.08% of corydalis yanhusuo extract;
s2: mixing and stirring the raw materials in the S1 according to the proportion, namely, taking olive shell oil, sunflower seed oil, safflower seed oil, squalane and tocopherol, and uniformly stirring to form a mixture A;
s3: mixing the raw materials in the S1 according to the proportion, taking caprylic/capric triglyceride and stearyl glycyrrhetinate, adding the mixture A, and uniformly stirring to form a mixture B;
s4: adding the raw materials in the step S1 into the mixture B according to the proportion, and stirring;
s5: and (4) cooling the stirred substances of the product in the step (S4), discharging after the detection indexes are qualified, and subpackaging the materials into a spray pump to realize storage.
2. The preparation method of the skin-moistening plant essential oil according to claim 1, characterized by comprising the following steps: in the S2, the mixing and stirring time is 30min, and the rotating speed is 30-40r/min.
3. The preparation method of the skin-moistening plant essential oil as claimed in claim 1, wherein the preparation method comprises the following steps: in the S3, the mixing condition is that the mixture is heated to 40 ℃ for mixing.
4. The preparation method of the skin-moistening plant essential oil according to claim 1, characterized by comprising the following steps: in the S3, the mixing and stirring time is 30min, and the rotating speed is 30-40r/min.
5. The preparation method of the skin-moistening plant essential oil according to claim 1, characterized by comprising the following steps: and in the step S4, when stirring is carried out, the stirring time is 60min, the temperature in the stirrer is set to be 30 ℃, and the rotating speed is 30-40r/min.
6. The preparation method of the skin-moistening plant essential oil as claimed in claim 1, wherein the preparation method comprises the following steps: and in the S5, cooling to 20 ℃ for detection.
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