CN104224636A - Natural herbal whitening mask and preparation method thereof - Google Patents
Natural herbal whitening mask and preparation method thereof Download PDFInfo
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- CN104224636A CN104224636A CN201410517451.2A CN201410517451A CN104224636A CN 104224636 A CN104224636 A CN 104224636A CN 201410517451 A CN201410517451 A CN 201410517451A CN 104224636 A CN104224636 A CN 104224636A
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Abstract
The invention belongs to the field of daily use chemical products and particularly relates to a natural herbal whitening mask and a preparation method thereof. According to the invention, natural Chinese herbal medicines including semen coicis, spreading hedyotis herb, salvia miltiorrhiza and bletilla striata are taken as the core to perform reasonable compatibility on effective purified components, and the invented formula has the synergism that the four source medicines are complementary and collaborative; both the main and the auxiliary components of the formula are made from natural animals and plants and do not contain chemosynthesis components, hormone, heavy metal or any Western medicine component, so that the mask is gentle and not irritative in cutaneous reaction and has the medical functions of whitening relatively well, removing acne and freckles, keeping moisture and the like.
Description
Technical field
The invention belongs to daily chemical product field, be specifically related to a kind of natural herb cleawhite pack and preparation method thereof.
Background technology
Along with the raising of quality of life and the progress of Technology, the kind quantity of cosmetic product is increasing, and function effect is also diversified complicated.Consumer, having more while more options, is also encountered by more problem.Such as say that a lot of cosmetics contain skin irritation composition now, a large amount of use antiseptic, some products contain hormone, also have product even containing situations such as lead, hydrargyrum exceed standard, between many cosmetics operating periods, effect is fine, once skin condition of stopping using will become poorer etc.As prerequisite, consumer is for cosmetic series products quality and its incident side-effect problem growing interest.Meanwhile, the Pure natural cosmetic based on the plant with care action becomes the new direction of cosmetic product exploitation with its higher traction and environmental friendliness.China has the long history of Chinese medicine research and use, Chinese medicine beautifying is also of long standing and well established, the degree of recognition acceptance of common people to natural Chinese medicinal herb product is high, must develop the good Chinese medicine cosmetic of effect in conjunction with these traditional resource advantages in conjunction with modern science and technology.Therefore, natural plants cosmetics have a bright future in Chinese market, and the floristics of China enriches and provides many facilities for developing this kind of cosmetics.
Semen Coicis has skin care and stays effect of appearances, and it can make skin smooth, elimination acne, freckle, senile plaque, cyasma, release-prevention, chap, pachylosis etc.Semen Coicis is rich in vitamin B1, B2, protein, and containing a large amount of to the composition coixenolide played a crucial role of improving looks.Coixenolide can accelerate the blood circulation of cortex, has the effect that check melanin is formed, can soft and smooth and conditioning skin, generally can promote effect with absorption enhancer is shared.Coixenolide and the Multiple components such as coixlacrymajobi inner ester and protein, aminoacid, vitamin, triterpenoid, to enhancing epidermis cell vigor, promote human metabolism, delay skin aging, wrinkle resistant, anticracking, anti-coarse and suppress pigmentation etc. to have positive effect.The skin care item that Semen Coicis is made, clinical confirmation has good curative effect to verruca plana, acne etc., and in addition, Semen Coicis oil has stronger Absorption to ultraviolet, therefore has sun-proof performance with the cosmetics of its preparation.
Herba Hedyotidis Diffusae has heat-clearing and toxic substances removing, and the effect of antiinflammatory, therefore may be used for anti-acne in cosmetics.These effects of Herba Hedyotidis Diffusae can be attributed to non-oxidizability and the anti-inflammatory activity of its brilliance.According to the result that relevant white-skinned face function is studied, melanic generative process and inflammatory reaction have close relationship.Take inflammation as the generation of the various signal transmission materials promotion black of medium, so there is the Herba Hedyotidis Diffusae of remarkable anti-inflammatory activity to have effect of check melanin generation, namely there is whitening effect.
Radix Salviae Miltiorrhizae has blood circulation promoting and blood stasis dispelling, refrigerant eliminating carbuncle, antioxidation, anti-fibrosis effect.Confirm that the chemical composition of Radix Salviae Miltiorrhizae is numerous through relevant report, pharmacological action is obvious, is desirable Chinese medicine cosmetic raw material.Containing abundant salvianolic acid B and tanshinone IIA in Radix Salviae Miltiorrhizae, salvianolic acid B and tanshinone IIA have significant antioxidation.The advantage that Radix Salviae Miltiorrhizae is applied in Chinese medicine cosmetic is that it has safety, stability, usability, functional.
The beauty functions of the Pseudobulbus Bletillae (Rhizoma Bletillae) has whitening and speckle dispelling, and detumescence and promoting granulation has Acne treatment, effect of acne removing print.The compositions such as Pseudobulbus Bletillae (Rhizoma Bletillae) rich in starch, glucose, volatile oil and phlegmatic temperament, enjoy the good reputation of " whitening fairy maiden " always.Effect and the effect of the Pseudobulbus Bletillae (Rhizoma Bletillae) are various, and the cosmetic result of the Pseudobulbus Bletillae (Rhizoma Bletillae) just receives praise greatly in ancient times, pursue as beauty treatment good medicine by people always." property of medicine opinion " cloud its " control skin ulcer on face, make us flesh sliding ".Compendium of Material Medica cloud its " wash one's face black, speckle dispelling ".Experiment proves that bletilla striata extract has significant antioxidant activity.Nowadays the Pseudobulbus Bletillae (Rhizoma Bletillae) is widely used in modern Chinese medicine and daily use chemicals industry, especially has the favor that good water retention property and certain anti-aging effects are more and more subject to cosmetic industry.
No matter above-mentioned four kinds of Chinese medicines are recorded or modern pharmacology research based on tradition, all prove that it has effective beauty functions respectively, if add relevant auxiliary element and form scientific and reasonable prescription, the deficiency of single ingredient will be made up, reach double whitening, anti-acne, speckle dispelling and moistening effect, great exploitation potential for its.
Summary of the invention
The object of this invention is to provide a kind of natural herb cleawhite pack and preparation method thereof, under the prerequisite of not adding any artificial synthetic chemistry composition, exploitation has the plant mask of whitening, anti-acne, speckle dispelling and moisture-keeping functions, and facial film stability, thickening degree, color and luster and smear dispersibility the best.
The present invention is for solving the problem, the technical scheme taked is: a kind of natural herb cleawhite pack, described facial film is by Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, Semen Coicis filtrate, tea tree ethereal oil, glycerol, soil temperature-60, Arlacel-60, stearic acid, lanoline, hexadecanol, aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae is made, and the parts by weight preparing each component needed for facial film are respectively Herba Hedyotidis Diffusae filtrate 1 part, Radix Salviae Miltiorrhizae filtrate 1 part, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate 1 part, Semen Coicis filtrate 28.5 parts, tea tree ethereal oil 29 parts, glycerol 4 parts, soil temperature-60 3 parts, Arlacel-60 3 parts, stearic acid 3.5 parts, lanoline 4 parts, hexadecanol 3.5 parts, aloe stoste 0.165 part, Herba Rosmarini Officinalis hydrosol 0.165 part, Kaolin 0.55 part, vitamin E 0.5 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, Jojoba oil 1 part, Oleum Vitis viniferae 2 parts.
The preparation method of described natural herb cleawhite pack, comprises the following steps:
Prepared by step one, medicinal material extract
1) Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and Pseudobulbus Bletillae (Rhizoma Bletillae) powder are broken to 300 orders, for subsequent use;
2) Herba Hedyotidis Diffusae after step 1) being pulverized, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) put into respectively volumetric concentration be 70% ethanol soak 48 hours, and ethanol contend corresponding to every gram of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) is 10mL, between soak period every 60min frequency be the ultrasonic Treatment 5min of 40kHz;
3) after immersion terminates, by step 2) be the filter paper filtering of 20 μm immersed with the ethanol aperture of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae), obtained Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate and Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, filtrate by put into that Rotary Evaporators is concentrated into original volume after the weight ratio mixing of 1:1:1 1/10th, afterwards the liquid after concentrated is put into baking oven, after drying, obtained mixture, for subsequent use;
4) Semen Coicis powder is broken to 300 orders, then put into deionized water to soak 24 hours, and deionized water volume corresponding to every gram of Semen Coicis is 10mL, between soak period every 60 min frequencies be the ultrasonic Treatment 5min of 40kHz, be the filter paper filtering of 20 μm afterwards by the deionized water aperture being soaked with Semen Coicis, collect Semen Coicis filtrate, for subsequent use;
5) add tea tree ethereal oil in the Semen Coicis filtrate of collecting to step 4), and the corresponding tea tree ethereal oil 1g of every 1mL Semen Coicis filtrate, obtained mixed liquor, afterwards mixed liquor being put into temperature is that the cold room of 4-8 DEG C is for subsequent use;
Prepared by step 2, facial film
get two containers, and be labeled as container A, container B respectively;
in container A, add the mixed liquor that glycerol and step 5) are obtained, and the weight ratio of mixed liquor and glycerol is 57:4, after stirring, container A is placed in the water-bath 30-35min that temperature is 90 DEG C, for subsequent use;
soil temperature-60, Arlacel-60, stearic acid and lanoline is added in container B, its weight ratio is 3:3:3.5:4, after stirring, container B is placed in the water-bath 25-30min that temperature is 90 DEG C, take out container B afterwards, and the material in container B is heated, is stirred to and melts completely, pour the liquid after melting into step
container A in, for subsequent use;
4. by step
container A to be placed on temperature be 90 DEG C, rotating speed is stir 10min in the motor stirrer of 500r/min, adds hexadecanol during stirring, the corresponding hexadecanol 0.04g of the every mL of liquid in container A, then 5min is stirred with the motor stirrer that rotating speed is 500 r/min, after being cooled to 60 DEG C, for subsequent use;
the obtained mixture of aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin and step 3) is added in step container A 4., and the weight ratio that aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, mixture and container A have liquid is 3:3:10:5.5:77.5, it is 60 DEG C in temperature afterwards, rotating speed is stir 5min in the motor stirrer of 500 r/min, for subsequent use;
by step
container A be cooled to 45 DEG C, and vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae and tea tree ethereal oil is added in container A, and the weight ratio of existing liquid is 0.5:1:1:2:0.5:99 in vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae, tea tree ethereal oil and container A, temperature be 45 DEG C, rotating speed is stir 5min in the motor stirrer of 500r/min, the liquid in container naturally cooled to room temperature i.e. obtained facial film.
Tea tree ethereal oil used in the present invention is the T36-C5 tea tree ethereal oil of Melaleuca board, and aloe stoste is your board clear, and Herba Rosmarini Officinalis hydrosol is fragrant grass collection board, and Herba Lysimachiae foenum-graeci quintessence oil is Di Xiang board, and Oleum Vitis viniferae is good and U.S. board.
Effect of each component in invention:
One, quintessence oil and base oil:
1 Herba Lysimachiae foenum-graeci quintessence oil: had by effect that we know: anti-bacteria; Promote Skin Cell regeneration, accelerating wound healing, desalination cicatrix, to burning, having tanned severely special effect; Improve acne, abscess, eczema.More because the feature of its " bidirectional balanced " skin oil and fat, almost various skin can feel at ease to accept the grace of Herba Lysimachiae foenum-graeci quintessence oil, is the quintessence oil that current global sales is the highest.
2 tea tree ethereal oils: tea tree ethereal oil has antiinflammatory, antibacterial effect.Use in cosmetics is its anti-acne, sun-proof result.And tea tree ethereal oil has antimicrobial acivity, biocidal efficacies, antibacterial activity, the nonirritant of All Pure Nature.Therefore be preservative substance with it in natural plants cosmetics.Tea tree ethereal oil has special, and strong abnormal smells from the patient can use as spice.
3 Jojoba oil: based on oil, Jojoba oil is the base oil that permeability is the strongest, and pole is absorbed by the skin, salubrious non-greasy, can recover skin PH equilibrium valve, remove wrinkle, pore refining, improves oily skin.
4 Oleum Vitis viniferaes: Semen Vitis viniferae has antioxidative effect, add it as antioxidant.Be usually used in skin whitening desalination mottle, slow down aging, desalination wrinkle.
Two, surfactant:
5 soil temperatures-60 and Arlacel-60: soil temperature-60 and Arlacel-60 all belong to non-ionic surface active agent, are characterized in safety, gentle to skin, nonirritant, has good emulsibility, and stability is equally very high.
Three, antioxidant:
6 vitamin Es: vitamin E uses as antioxidant in cosmetics, can be anti-aging in advance, prevention sunburn, the generation of pre-sun-proof rear red seal.And vitamin E has effect of sterilization, the effect of antiseptic also can be played.
Four, wetting agent:
7 lanolines: its maximum feature derives from animal bodies non-chemically to synthesize safety very high, and being used in cosmetics non-stimulated to skin gentleness, is good cosmetics additive.
8 glycerol and aloe stoste: aloe stoste has the effect of moisturizing, sun-proof, antibacterial, antiinflammatory, and the effect with cancellation pox print and desalination cicatrix.Glycerol can prevent chapped skin, skin care, is good wetting agent.Its moistening effect equals to hyaluronic acid, and cheap.
Five, antiseptic:
9 tea tree ethereal oils: tea tree ethereal oil can be used as natural antiseptic agent and is its good bactericidal and bacteriostatic effect.In facial film, add tea tree ethereal oil can well play antisepsis.
Six, other:
10 stearic acid: stearic acid is substrate, have the effect of emulsifying, because it is nontoxic, use in harmless cosmetics of being everlasting.Stearic acid can extract in animals and plants.
11 hexadecanol: for the manufacture of spice, cosmetics, detergent, plasticizer etc., be applicable in all kinds of cosmetics, as substrate, are particularly suitable for cream acid and emulsion; In medicine, W/O emulsifying agent mastic can be directly used in, ointment base etc.; For defoamer, water and soil heat preserving agent, colour coupler, GC stationary liquid
beneficial effect
The present invention for core with natural Chinese medicinal herb Semen Coicis, Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae), is effectively purified to it and point has carried out reasonable compatibility, and the formula invented serves the potentiation collaborative to four taste source medicine complementations.Main and auxiliary element in formula all derives from natural animal-plant, without chemosynthesis composition, without hormone, and heavy metal or any western medicine composition, non-stimulated to dermoreaction gentleness, and there is the pharmacodynamic features such as stronger whitening, anti-acne, speckle dispelling and moisturizing.
Accompanying drawing explanation
Fig. 1 is experiment No. 1-3 obtained product;
Fig. 2 is experiment No. 4-6 obtained product;
Fig. 3 is experiment No. 7-9 obtained product;
Fig. 4 for placing 24 hours under temperature is 40 DEG C of conditions, and nine group of formula mastic are without oil-water separation phenomenon;
Fig. 5 returns to room temperature nine group of formula mastic without oil-water separation phenomenon for place 24 hours under temperature is 5 DEG C of conditions after.
Detailed description of the invention
A kind of natural herb cleawhite pack, described facial film is by Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, Semen Coicis filtrate, tea tree ethereal oil, glycerol, soil temperature-60, Arlacel-60, stearic acid, lanoline, hexadecanol, aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae is made, and the parts by weight preparing each component needed for facial film are respectively Herba Hedyotidis Diffusae filtrate 1 part, Radix Salviae Miltiorrhizae filtrate 1 part, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate 1 part, Semen Coicis filtrate 28.5 parts, tea tree ethereal oil 29 parts, glycerol 4 parts, soil temperature-60 3 parts, Arlacel-60 3 parts, stearic acid 3.5 parts, lanoline 4 parts, hexadecanol 3.5 parts, aloe stoste 0.165 part, Herba Rosmarini Officinalis hydrosol 0.165 part, Kaolin 0.55 part, vitamin E 0.5 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, Jojoba oil 1 part, Oleum Vitis viniferae 2 parts.
The preparation method of described natural herb cleawhite pack, comprises the following steps:
Prepared by step one, medicinal material extract
1) Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and Pseudobulbus Bletillae (Rhizoma Bletillae) powder are broken to 300 orders, for subsequent use;
2) Herba Hedyotidis Diffusae after step 1) being pulverized, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) put into respectively volumetric concentration be 70% ethanol soak 48 hours, and ethanol contend corresponding to every gram of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) is 10mL, between soak period every 60min frequency be the ultrasonic Treatment 5min of 40kHz;
3) after immersion terminates, by step 2) be the filter paper filtering of 20 μm immersed with the ethanol aperture of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae), obtained Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate and Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, filtrate by put into that Rotary Evaporators is concentrated into original volume after the weight ratio mixing of 1:1:1 1/10th, afterwards the liquid after concentrated is put into baking oven, after drying, obtained mixture, for subsequent use;
4) Semen Coicis powder is broken to 300 orders, then put into deionized water to soak 24 hours, and deionized water volume corresponding to every gram of Semen Coicis is 10mL, between soak period every 60 min frequencies be the ultrasonic Treatment 5min of 40kHz, be the filter paper filtering of 20 μm afterwards by the deionized water aperture being soaked with Semen Coicis, collect Semen Coicis filtrate, for subsequent use;
5) add tea tree ethereal oil in the Semen Coicis filtrate of collecting to step 4), and the corresponding tea tree ethereal oil 1g of every 1mL Semen Coicis filtrate, obtained mixed liquor, afterwards mixed liquor being put into temperature is that the cold room of 4-8 DEG C is for subsequent use;
Prepared by step 2, facial film
get two containers, and be labeled as container A, container B respectively;
in container A, add the mixed liquor that glycerol and step 5) are obtained, and the weight ratio of mixed liquor and glycerol is 57:4, after stirring, container A is placed in the water-bath 30-35min that temperature is 90 DEG C, for subsequent use;
soil temperature-60, Arlacel-60, stearic acid and lanoline is added in container B, its weight ratio is 3:3:3.5:4, after stirring, container B is placed in the water-bath 25-30min that temperature is 90 DEG C, take out container B afterwards, and the material in container B is heated, is stirred to and melts completely, pour the liquid after melting into step
container A in, for subsequent use;
4. by step
container A to be placed on temperature be 90 DEG C, rotating speed is stir 10min in the motor stirrer of 500r/min, adds hexadecanol during stirring, the corresponding hexadecanol 0.04g of the every mL of liquid in container A, then 5min is stirred with the motor stirrer that rotating speed is 500 r/min, after being cooled to 60 DEG C, for subsequent use;
the obtained mixture of aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin and step 3) is added in step container A 4., and the weight ratio that aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, mixture and container A have liquid is 3:3:10:5.5:77.5, it is 60 DEG C in temperature afterwards, rotating speed is stir 5min in the motor stirrer of 500 r/min, for subsequent use;
by step
container A be cooled to 45 DEG C, and vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae and tea tree ethereal oil is added in container A, and the weight ratio of existing liquid is 0.5:1:1:2:0.5:99 in vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae, tea tree ethereal oil and container A, temperature be 45 DEG C, rotating speed is stir 5min in the motor stirrer of 500r/min, the liquid in container naturally cooled to room temperature i.e. obtained facial film.
Embodiment 1
A kind of natural herb cleawhite pack, described facial film is by Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, Semen Coicis filtrate, tea tree ethereal oil, glycerol, soil temperature-60, Arlacel-60, stearic acid, lanoline, hexadecanol, aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae is made, and the parts by weight preparing each component needed for facial film are respectively Herba Hedyotidis Diffusae filtrate 1 part, Radix Salviae Miltiorrhizae filtrate 1 part, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate 1 part, Semen Coicis filtrate 28.5 parts, tea tree ethereal oil 29 parts, glycerol 4 parts, soil temperature-60 3 parts, Arlacel-60 3 parts, stearic acid 3.5 parts, lanoline 4 parts, hexadecanol 3.5 parts, aloe stoste 0.165 part, Herba Rosmarini Officinalis hydrosol 0.165 part, Kaolin 0.55 part, vitamin E 0.5 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, Jojoba oil 1 part, Oleum Vitis viniferae 2 parts.
The preparation method of described natural herb cleawhite pack, comprises the following steps:
Prepared by step one, medicinal material extract
1) Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and Pseudobulbus Bletillae (Rhizoma Bletillae) powder are broken to 300 orders, for subsequent use;
2) Herba Hedyotidis Diffusae after step 1) being pulverized, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) put into respectively volumetric concentration be 70% ethanol soak 48 hours, and ethanol contend corresponding to every gram of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) is 10mL, between soak period every 60min frequency be the ultrasonic Treatment 5min of 40kHz;
3) after immersion terminates, by step 2) be the filter paper filtering of 20 μm immersed with the ethanol aperture of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae), obtained Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate and Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, filtrate by put into that Rotary Evaporators is concentrated into original volume after the weight ratio mixing of 1:1:1 1/10th, afterwards the liquid after concentrated is put into baking oven, after drying, obtained mixture, for subsequent use;
4) Semen Coicis powder is broken to 300 orders, then put into deionized water to soak 24 hours, and deionized water volume corresponding to every gram of Semen Coicis is 10mL, between soak period every 60 min frequencies be the ultrasonic Treatment 5min of 40kHz, be the filter paper filtering of 20 μm afterwards by the deionized water aperture being soaked with Semen Coicis, collect Semen Coicis filtrate, for subsequent use;
5) add tea tree ethereal oil in the Semen Coicis filtrate of collecting to step 4), and the corresponding tea tree ethereal oil 1g of every 1mL Semen Coicis filtrate, obtained mixed liquor, afterwards mixed liquor being put into temperature is that the cold room of 4-8 DEG C is for subsequent use;
Prepared by step 2, facial film
get two containers, and be labeled as container A, container B respectively;
in container A, add the mixed liquor that glycerol and step 5) are obtained, and the weight ratio of mixed liquor and glycerol is 57:4, after stirring, container A is placed in the water-bath 30-35min that temperature is 90 DEG C, for subsequent use;
soil temperature-60, Arlacel-60, stearic acid and lanoline is added in container B, its weight ratio is 3:3:3.5:4, after stirring, container B is placed in the water-bath 25-30min that temperature is 90 DEG C, take out container B afterwards, and the material in container B is heated, is stirred to and melts completely, pour the liquid after melting into step
container A in, for subsequent use;
4. by step
container A to be placed on temperature be 90 DEG C, rotating speed is stir 10min in the motor stirrer of 500r/min, adds hexadecanol during stirring, the corresponding hexadecanol 0.04g of the every mL of liquid in container A, then 5min is stirred with the motor stirrer that rotating speed is 500 r/min, after being cooled to 60 DEG C, for subsequent use;
the obtained mixture of aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin and step 3) is added in step container A 4., and the weight ratio that aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, mixture and container A have liquid is 3:3:10:5.5:77.5, it is 60 DEG C in temperature afterwards, rotating speed is stir 5min in the motor stirrer of 500 r/min, for subsequent use;
by step
container A be cooled to 45 DEG C, and vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae and tea tree ethereal oil is added in container A, and the weight ratio of existing liquid is 0.5:1:1:2:0.5:99 in vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae, tea tree ethereal oil and container A, temperature be 45 DEG C, rotating speed is stir 5min in the motor stirrer of 500r/min, the liquid in container naturally cooled to room temperature i.e. obtained facial film.
Embodiment 2
A kind of natural herb cleawhite pack, described facial film is by Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, Semen Coicis filtrate, tea tree ethereal oil, glycerol, soil temperature-60, Arlacel-60, stearic acid, lanoline, hexadecanol, aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae is made, and the parts by weight preparing each component needed for facial film are respectively Herba Hedyotidis Diffusae filtrate 1 part, Radix Salviae Miltiorrhizae filtrate 1 part, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate 1 part, Semen Coicis filtrate 28.5 parts, tea tree ethereal oil 29 parts, glycerol 4 parts, soil temperature-60 3 parts, Arlacel-60 3 parts, stearic acid 3.5 parts, lanoline 4 parts, hexadecanol 3.5 parts, aloe stoste 0.165 part, Herba Rosmarini Officinalis hydrosol 0.165 part, Kaolin 0.55 part, vitamin E 0.5 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, Jojoba oil 1 part, Oleum Vitis viniferae 2 parts.
The preparation method of described natural herb cleawhite pack, comprises the following steps:
Prepared by step one, medicinal material extract
1) Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and Pseudobulbus Bletillae (Rhizoma Bletillae) powder are broken to 300 orders, for subsequent use;
2) Herba Hedyotidis Diffusae after step 1) being pulverized, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) put into respectively volumetric concentration be 70% ethanol soak 48 hours, and ethanol contend corresponding to every gram of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) is 10mL, between soak period every 60min frequency be the ultrasonic Treatment 5min of 40kHz;
3) after immersion terminates, by step 2) be the filter paper filtering of 20 μm immersed with the ethanol aperture of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae), obtained Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate and Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, filtrate by put into that Rotary Evaporators is concentrated into original volume after the weight ratio mixing of 1:1:1 1/10th, afterwards the liquid after concentrated is put into baking oven, after drying, obtained mixture, for subsequent use;
4) Semen Coicis powder is broken to 300 orders, then put into deionized water to soak 24 hours, and deionized water volume corresponding to every gram of Semen Coicis is 10mL, between soak period every 60 min frequencies be the ultrasonic Treatment 5min of 40kHz, be the filter paper filtering of 20 μm afterwards by the deionized water aperture being soaked with Semen Coicis, collect Semen Coicis filtrate, for subsequent use;
5) add tea tree ethereal oil in the Semen Coicis filtrate of collecting to step 4), and the corresponding tea tree ethereal oil 1g of every 1mL Semen Coicis filtrate, obtained mixed liquor, afterwards mixed liquor being put into temperature is that the cold room of 4-8 DEG C is for subsequent use;
Prepared by step 2, facial film
get two containers, and be labeled as container A, container B respectively;
in container A, add the mixed liquor that glycerol and step 5) are obtained, and the weight ratio of mixed liquor and glycerol is 57:4, after stirring, container A is placed in the water-bath 30-35min that temperature is 90 DEG C, for subsequent use;
soil temperature-60, Arlacel-60, stearic acid and lanoline is added in container B, its weight ratio is 3:3:3.5:4, after stirring, container B is placed in the water-bath 25-30min that temperature is 90 DEG C, take out container B afterwards, and the material in container B is heated, is stirred to and melts completely, pour the liquid after melting into step
container A in, for subsequent use;
4. by step
container A to be placed on temperature be 90 DEG C, rotating speed is stir 10min in the motor stirrer of 500r/min, adds hexadecanol during stirring, the corresponding hexadecanol 0.04g of the every mL of liquid in container A, then 5min is stirred with the motor stirrer that rotating speed is 500 r/min, after being cooled to 60 DEG C, for subsequent use;
the obtained mixture of aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin and step 3) is added in step container A 4., and the weight ratio that aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, mixture and container A have liquid is 3:3:10:5.5:77.5, it is 60 DEG C in temperature afterwards, rotating speed is stir 5min in the motor stirrer of 500 r/min, for subsequent use;
by step
container A be cooled to 45 DEG C, and vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae and tea tree ethereal oil is added in container A, and the weight ratio of existing liquid is 0.5:1:1:2:0.5:99 in vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae, tea tree ethereal oil and container A, temperature be 45 DEG C, rotating speed is stir 5min in the motor stirrer of 500r/min, the liquid in container naturally cooled to room temperature i.e. obtained facial film.
The film preparation of experiment one side
One, medicinal material extract preparation:
1) by Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae, the Pseudobulbus Bletillae (Rhizoma Bletillae), clay into power.The three kinds of Chinese medicines of immersion respectively (ratio of liquid and medical material is 10:1) 48 hours of ethanol with 70% (period certain interval of time ultrasonic 5 minutes).After 48 hours, the mixture of Chinese medicine and 70% ethanol is filtered, the filtrate after filtering is revolved steaming to about remaining 50ml.Revolving remaining liquid after steaming places with baking oven, dry for standby.2) Semen Coicis is clayed into power.24 hours (the ultrasonic 5 minutes at set intervals period) of Semen Coicis of 50g is soaked with the deionized water of 500ml.After 24 hours, the mixture of deionized water and Semen Coicis is filtered.Filtrate instillation 1.0g tea tree ethereal oil (for anticorrosion) after filtration is positioned in cold compartment of refrigerator for subsequent use.
Two, facial film preparation:
1) temperature of water-bath is adjusted to 90 degrees Celsius.2) Semen Coicis deionized water extract 57.0 g is added at a beaker, glycerol 4.0 g.A beaker is placed in the water-bath of 90 degrees Celsius.3) in No. two beakers, add soil temperature 3.0 g, span 3.0 g, stearic acid 3.5 g, lanoline 4.0 g.No. two beakers are placed in water-bath.4) heated, be stirred to and melt completely by the material in No. two beakers, the liquid after thawing is poured in a beaker.5) with motor stirrer Keep agitation (oil phase enters after aqueous phase) beaker.Period adds hexadecanol 3.0 g, and constant speed stirs 10 minutes at this temperature, stirring 5 minutes of slowing down again after 10 minutes.6) be cooled to 60 degrees Celsius after 5 minutes, add aloe stoste 3.0 g, Herba Rosmarini Officinalis hydrosol 3.0 g, Kaolin 10.0 g, Herba Hedyotidis Diffusae extract 0.5 g, bletilla striata extract 4.0 g, Radix Salviae Miltiorrhizae 1.0 g.Constant speed, constant temperature stir 5 minutes.7) be cooled to 45 degrees Celsius after 5 minutes, add vitamin E 0.5 g, Herba Lysimachiae foenum-graeci quintessence oil 1.0g, Jojoba oil 1.0g, Oleum Vitis viniferae 2.0g, tea tree ethereal oil 0.5g, at this temperature, constant speed stirs 5 minutes.(8) close water-bath, allow the facial film finished product in beaker naturally cool to room temperature.
Optimize
For making facial film present best state in outward appearance and result of use, devise nine groups of experiments further, in order to optimize face pack prescription.Four factors of experimental selection are lanoline, Kaolin, Radix Salviae Miltiorrhizae, the Pseudobulbus Bletillae (Rhizoma Bletillae) respectively.As following table:
The data gone out according to upper tabular carry out facial film preparation, the operation of concrete operating procedure refer step two.The facial film cumulative volume of each preparation be set as 100 g, in order to make cumulative volume constant, the corresponding amount changing Semen Coicis deionized water extraction liquid is as follows, the order of other raw material interpolation and mass conservation.
According to the product analysis experimental result obtained, following table is formula for a product Indexs measure.
Drawn by the above results, the formula of experiment 1,2,4 and 9 and process conditions can prepare the facial film of comparatively high-quality and effect.
About the explanation of antiseptic, the date of the facial film of first batch of preparation is (this time only with the addition of tea tree ethereal oil as natural antiseptic agent in experiment on November 27th, 2013, do not add other chemical preservative), last date of observation before leaving school is January 6, facial film is now in good condition does not have Signs of Mould, and abnormal smells from the patient is also still good.Store on June 26th, 6 months 1 at normal temperatures, the facial film deposited in face-mask sub-packaging box is in good condition, does not have Signs of Mould.Therefore, this formula facial film, room temperature 25 degrees Celsius, under sealing state, can be preserved more than 6 months when using without chemical preservation, should be placed on summer in cold compartment of refrigerator and also use as early as possible.
Claims (2)
1. a natural herb cleawhite pack, it is characterized in that: described facial film is by Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, Semen Coicis filtrate, tea tree ethereal oil, glycerol, soil temperature-60, Arlacel-60, stearic acid, lanoline, hexadecanol, aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae is made, and the parts by weight preparing each component needed for facial film are respectively Herba Hedyotidis Diffusae filtrate 1 part, Radix Salviae Miltiorrhizae filtrate 1 part, Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate 1 part, Semen Coicis filtrate 28.5 parts, tea tree ethereal oil 29 parts, glycerol 4 parts, soil temperature-60 3 parts, Arlacel-60 3 parts, stearic acid 3.5 parts, lanoline 4 parts, hexadecanol 3.5 parts, aloe stoste 0.165 part, Herba Rosmarini Officinalis hydrosol 0.165 part, Kaolin 0.55 part, vitamin E 0.5 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, Jojoba oil 1 part, Oleum Vitis viniferae 2 parts.
2. the preparation method of a kind of natural herb cleawhite pack according to claim 1, is characterized in that, comprise the following steps:
Prepared by step one, medicinal material extract
1) Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and Pseudobulbus Bletillae (Rhizoma Bletillae) powder are broken to 300 orders, for subsequent use;
2) Herba Hedyotidis Diffusae after step 1) being pulverized, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) put into respectively volumetric concentration be 70% ethanol soak 48 hours, and ethanol contend corresponding to every gram of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae) is 10mL, between soak period every 60min frequency be the ultrasonic Treatment 5min of 40kHz;
3) after immersion terminates, by step 2) be the filter paper filtering of 20 μm immersed with the ethanol aperture of Herba Hedyotidis Diffusae, Radix Salviae Miltiorrhizae and the Pseudobulbus Bletillae (Rhizoma Bletillae), obtained Herba Hedyotidis Diffusae filtrate, Radix Salviae Miltiorrhizae filtrate and Pseudobulbus Bletillae (Rhizoma Bletillae) filtrate, filtrate by put into that Rotary Evaporators is concentrated into original volume after the weight ratio mixing of 1:1:1 1/10th, afterwards the liquid after concentrated is put into baking oven, after drying, obtained mixture, for subsequent use;
4) Semen Coicis powder is broken to 300 orders, then put into deionized water to soak 24 hours, and deionized water volume corresponding to every gram of Semen Coicis is 10mL, between soak period every 60 min frequencies be the ultrasonic Treatment 5min of 40kHz, be the filter paper filtering of 20 μm afterwards by the deionized water aperture being soaked with Semen Coicis, collect Semen Coicis filtrate, for subsequent use;
5) add tea tree ethereal oil in the Semen Coicis filtrate of collecting to step 4), and the corresponding tea tree ethereal oil 1g of every 1mL Semen Coicis filtrate, obtained mixed liquor, afterwards mixed liquor being put into temperature is that the cold room of 4-8 DEG C is for subsequent use;
Prepared by step 2, facial film
1. get two containers, and be labeled as container A, container B respectively;
2. in container A, add the mixed liquor that glycerol and step 5) are obtained, and the weight ratio of mixed liquor and glycerol is 57:4, after stirring, container A is placed in the water-bath 30-35min that temperature is 90 DEG C, for subsequent use;
3. in container B, soil temperature-60, Arlacel-60, stearic acid and lanoline is added, its weight ratio is 3:3:3.5:4, after stirring, container B is placed in the water-bath 25-30min that temperature is 90 DEG C, take out container B afterwards, and the material in container B is heated, is stirred to and melts completely, liquid after melting is poured in step container A 2., for subsequent use;
4. step container A being 3. placed on temperature is 90 DEG C, rotating speed is stir 10min in the motor stirrer of 500r/min, hexadecanol is added during stirring, the corresponding hexadecanol 0.04g of the every mL of liquid in container A, then 5min is stirred with the motor stirrer that rotating speed is 500 r/min, after being cooled to 60 DEG C, for subsequent use;
5. in step container A 4., the obtained mixture of aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin and step 3) is added, and the weight ratio that aloe stoste, Herba Rosmarini Officinalis hydrosol, Kaolin, mixture and container A have liquid is 3:3:10:5.5:77.5, it is 60 DEG C in temperature afterwards, rotating speed is stir 5min in the motor stirrer of 500 r/min, for subsequent use;
6. step container A is 5. cooled to 45 DEG C, and vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae and tea tree ethereal oil is added in container A, and the weight ratio of existing liquid is 0.5:1:1:2:0.5:99 in vitamin E, Herba Lysimachiae foenum-graeci quintessence oil, Jojoba oil, Oleum Vitis viniferae, tea tree ethereal oil and container A, temperature be 45 DEG C, rotating speed is stir 5min in the motor stirrer of 500r/min, the liquid in container naturally cooled to room temperature i.e. obtained facial film.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104800136A (en) * | 2015-05-20 | 2015-07-29 | 河南中医学院 | Chinese medicine cosmetic with functions of keeping skin moisturized, whitening skin and resisting aging |
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| CN105055236A (en) * | 2015-08-13 | 2015-11-18 | 刘汉科 | Rosemary hydrosol lotion and preparation method thereof |
| CN105106064A (en) * | 2015-09-10 | 2015-12-02 | 高密市丽美化妆品有限公司 | Moisture-preserving and nourishing wash-free mask and preparing method thereof |
| CN105380840A (en) * | 2015-11-13 | 2016-03-09 | 上海辰山植物园 | Chinese herbal medicine composition for acne removal restoration and preparation method thereof |
| CN105380840B (en) * | 2015-11-13 | 2018-07-06 | 上海辰山植物园 | A kind of Chinese herbal medicine anti-acne remediation composition and preparation method thereof |
| CN105902463A (en) * | 2016-05-13 | 2016-08-31 | 太仓善融信息服务有限公司 | Preparation method of Chinese traditional medicine masks with function of removing yellowness |
| CN111870575A (en) * | 2020-08-24 | 2020-11-03 | 广州三广生物科技有限公司 | Traditional Chinese medicine composition for whitening and removing freckles and preparation method thereof |
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Application publication date: 20141224 |