CN115399421A - Solid beverage for promoting bone growth and development and preparation method thereof - Google Patents
Solid beverage for promoting bone growth and development and preparation method thereof Download PDFInfo
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- CN115399421A CN115399421A CN202210902421.8A CN202210902421A CN115399421A CN 115399421 A CN115399421 A CN 115399421A CN 202210902421 A CN202210902421 A CN 202210902421A CN 115399421 A CN115399421 A CN 115399421A
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- Prior art keywords
- powder
- noni
- solid beverage
- yolk
- percent
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Links
- 235000013361 beverage Nutrition 0.000 title claims abstract description 45
- 239000007787 solid Substances 0.000 title claims abstract description 45
- 238000011161 development Methods 0.000 title claims abstract description 31
- 230000001737 promoting effect Effects 0.000 title claims abstract description 27
- 230000014461 bone development Effects 0.000 title claims abstract description 21
- 230000008468 bone growth Effects 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 167
- 210000002969 egg yolk Anatomy 0.000 claims abstract description 97
- 244000131360 Morinda citrifolia Species 0.000 claims abstract description 88
- 235000017524 noni Nutrition 0.000 claims abstract description 88
- 102000002322 Egg Proteins Human genes 0.000 claims abstract description 43
- 108010000912 Egg Proteins Proteins 0.000 claims abstract description 43
- 235000013345 egg yolk Nutrition 0.000 claims abstract description 35
- 241001474374 Blennius Species 0.000 claims abstract description 27
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000004386 Erythritol Substances 0.000 claims abstract description 23
- 235000018290 Musa x paradisiaca Nutrition 0.000 claims abstract description 23
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 claims abstract description 23
- 229940009714 erythritol Drugs 0.000 claims abstract description 23
- 235000019414 erythritol Nutrition 0.000 claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 17
- 239000002245 particle Substances 0.000 claims abstract description 15
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- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 claims description 8
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- ZIIUUSVHCHPIQD-UHFFFAOYSA-N 2,4,6-trimethyl-N-[3-(trifluoromethyl)phenyl]benzenesulfonamide Chemical compound CC1=CC(C)=CC(C)=C1S(=O)(=O)NC1=CC=CC(C(F)(F)F)=C1 ZIIUUSVHCHPIQD-UHFFFAOYSA-N 0.000 claims description 6
- 102000015439 Phospholipases Human genes 0.000 claims description 6
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- 235000020729 noni extract Nutrition 0.000 claims description 5
- 102100037883 Phospholipase B1, membrane-associated Human genes 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 102000013392 Carboxylesterase Human genes 0.000 claims description 2
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- 102000000496 Carboxypeptidases A Human genes 0.000 claims description 2
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- 150000003432 sterols Chemical class 0.000 claims description 2
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- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 7
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
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- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 description 2
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- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 description 2
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- 238000012360 testing method Methods 0.000 description 2
- 229960003495 thiamine Drugs 0.000 description 2
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 2
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- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- ODKSFYDXXFIFQN-BYPYZUCNSA-P L-argininium(2+) Chemical compound NC(=[NH2+])NCCC[C@H]([NH3+])C(O)=O ODKSFYDXXFIFQN-BYPYZUCNSA-P 0.000 description 1
- HNDVDQJCIGZPNO-YFKPBYRVSA-N L-histidine Chemical compound OC(=O)[C@@H](N)CC1=CN=CN1 HNDVDQJCIGZPNO-YFKPBYRVSA-N 0.000 description 1
- QIVBCDIJIAJPQS-VIFPVBQESA-N L-tryptophane Chemical compound C1=CC=C2C(C[C@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-VIFPVBQESA-N 0.000 description 1
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 description 1
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- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- QIVBCDIJIAJPQS-UHFFFAOYSA-N Tryptophan Natural products C1=CC=C2C(CC(N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-UHFFFAOYSA-N 0.000 description 1
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- 229930003537 Vitamin B3 Natural products 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000004931 aggregating effect Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
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- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
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- 238000010438 heat treatment Methods 0.000 description 1
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 description 1
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- DFPAKSUCGFBDDF-UHFFFAOYSA-N nicotinic acid amide Natural products NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
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- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000002331 protein detection Methods 0.000 description 1
- RADKZDMFGJYCBB-UHFFFAOYSA-N pyridoxal hydrochloride Natural products CC1=NC=C(CO)C(C=O)=C1O RADKZDMFGJYCBB-UHFFFAOYSA-N 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229960002477 riboflavin Drugs 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
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- 238000000926 separation method Methods 0.000 description 1
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- 235000019158 vitamin B6 Nutrition 0.000 description 1
- 239000011726 vitamin B6 Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 229940011671 vitamin b6 Drugs 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/56—Flavouring or bittering agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Botany (AREA)
- Non-Alcoholic Beverages (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention provides a solid beverage for promoting bone growth and development and a preparation method thereof, wherein the solid beverage comprises the following raw materials in parts by weight: 25 to 40 percent of noni pulp powder, 20 to 38 percent of erythritol, 22 to 40 percent of butter powder, 4 to 6 percent of banana powder, 3.5 to 6.0 percent of seaweed powder and 0.037 to 0.11 percent of hydrolyzed yolk powder; the solid beverage prepared by extracting noni pulp powder and hydrolyzed egg yolk powder by a specific method, mixing the noni pulp powder and the hydrolyzed egg yolk powder according to a proportion and scientifically matching the noni pulp powder and the hydrolyzed egg yolk powder has high content of main nutrient components, retains the main nutrient components of noni and has high content of the main nutrient components, and is mixed with the hydrolyzed egg yolk powder for particle homogenization, so that the noni pulp powder and the hydrolyzed egg yolk powder have good dispersibility and high solubility.
Description
Technical Field
The invention relates to the field of food processing, in particular to a solid beverage for promoting bone growth and development and a preparation method thereof.
Background
Noni has very powerful natural active nutrition and medical values of prevention and treatment, and provides a comprehensive nutritional basis for the growth and development of children. Modern medical research has confirmed that noni contains more than 275 nutrients. The vitamin feed is rich in 20 essential amino acids such as tryptophan, arginine, histidine and the like which are necessary for human bodies, 16 mineral substances such as potassium, zinc, calcium, iron, magnesium, selenium and the like, 14 vitamins such as vitamin B1, vitamin B2, vitamin B3, vitamin B6, folic acid, vitamin 12 and the like, and 17 antioxidants which are necessary for human bodies and rare iridoids which are very important for human health. Researches show that the main functions of the noni fruit include protecting cardiovascular system, preventing diabetes, improving sleep, enhancing immunity, maintaining acid-base balance of human body, resisting oxidation, eliminating harmful free radicals and the like. Noni is rich in various nutrients required by human bodies, and provides a comprehensive nutritional basis for the growth and development of children. The seaweed meal provides a mineral substance basis for growth and development, and the natural calcium is matched with the hydrolyzed yolk powder to jointly act, so that the growth length of the tibia can be promoted. The obtained product improves the efficacy of the raw and auxiliary materials, has the efficacy of promoting the growth and development of children, and has an important effect in the healthy growth of children.
The hydrolyzed yolk powder is produced by using egg yolk as a raw material, and carrying out protease treatment, heating, separation, drying and other steps after degreasing. Research shows that the hydrolyzed yolk powder can obviously promote the proliferation of osteocyte, effectively reduce the damage of bone eroding cells and inhibit the reduction of bone density, and can effectively promote the calcium absorption and the growth length of tibia when being matched with calcium.
The seaweed powder is prepared by taking natural seaweed as a main raw material, contains natural comprehensive mineral substances which are mainly rich in calcium and magnesium, has the absorption rate of 99 percent, and can promote the growth length of shin bones under the combined action of the natural calcium and the hydrolyzed yolk powder.
The banana powder is added into the product, so that the quality of the product can be improved, the product with banana flavor can be more easily accepted by children, and the effects of reducing blood pressure, promoting digestion and the like are achieved; the addition of the erythritol successfully avoids the problems of obesity, tooth decay and the like caused by excessive consumption of sugar.
However, the noni pulp powder and the hydrolyzed egg yolk powder are lack of solid beverages with rich nutritional ingredients, the active ingredients extracted from the noni pulp in the market are low in content, and the egg yolk powder has the characteristic of poor heat resistance, so that the egg yolk products in the market are poor in dispersity and solubility, and are not beneficial to food processing products.
Disclosure of Invention
In view of the above, the present invention provides a solid beverage for promoting bone growth and development and a preparation method thereof, which solve the above problems.
The technical scheme of the invention is realized as follows: a solid beverage for promoting bone growth and development: comprises the following raw materials in percentage by weight: 25 to 40 percent of noni pulp powder, 20 to 38 percent of erythritol, 22 to 40 percent of butter powder, 4 to 6 percent of banana powder, 3.5 to 6.0 percent of seaweed powder and 0.037 to 0.11 percent of hydrolyzed egg yolk powder.
Further, the solid beverage for promoting bone growth and development comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder.
Further, the preparation method of the solid beverage for promoting the growth and development of the bone comprises the following steps:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting into slices of 1-3 cm, drying in the sun, adding sodium bisulfite and ascorbic acid, stirring, soaking for 20-25 min, filtering, adjusting the pH value of filter residues to 7-9, pulping at 300-500 rpm for 2-5 min, pulping at 800-1200 rpm for 5-8 min to obtain noni pulp, placing the noni pulp in an ethanol solution of which the volume is 5-8 times that of the noni pulp, performing strong electric field extraction, extracting for 40-50 min to obtain an extract, concentrating, performing spray drying to obtain a noni extract, and sieving with a sieve of 80-120 meshes to obtain noni pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh eggs, separating egg white and yolk, collecting yolk, stirring at the stirring speed of 200-400 rpm, filtering to remove impurities to obtain yolk liquid, and performing ultrasonic treatment at the field intensity of 100-200W/cm 2 Ultrasonic treatment for 30-50 min, centrifugal filtration after ultrasonic treatment to remove upper suspended matter to obtain defatted yolk liquid, adding protease, phospholipase and lipase, stirring and enzymolysis at 40-60 deg.c and pH 6-7 for 20-45 min to obtain enzymolysis liquid, spray dryingObtaining hydrolyzed yolk powder;
and S3, mixing the noni pulp powder, the erythritol, the banana powder, the seaweed powder and the hydrolyzed egg yolk powder according to the parts by weight, and homogenizing the mixture to obtain solid beverage powder with particles of 1-3mm in size.
Furthermore, the electric field intensity of the S1 is 2.0-2.3 kV, and the pulse frequency is 2000-2200 Hz.
Furthermore, the mass ratio of the egg yolk liquid, the protease, the phospholipase and the lipase in the S2 is (100).
Further, the protease in the S2 is selected from one or a combination of more of neutral protease, carboxypeptidase A, carboxypeptidase B and papain.
Further, the phospholipase in S2 is selected from one or more of phospholipase A1, phospholipase A2, phospholipase B and phospholipase C.
Further, the lipase in S2 is selected from one or more of phosphatase, sterol enzyme and carboxylesterase.
Further, the air inlet temperature is set to be 140-200 ℃, the air outlet temperature is set to be 60-80 ℃ and the flow rate of the material liquid is set to be 80-100 mL/min in the S2 spray drying.
Compared with the prior art, the invention has the beneficial effects that:
(1) The noni pulp powder is rich in various nutrients required by human bodies, and provides a comprehensive nutritional basis for the growth and development of children.
(2) The seaweed powder can provide various seaweed-derived minerals and provide a mineral basis for growth and development.
(3) The hydrolyzed egg yolk powder can promote the proliferation of osteoblast, and can promote the growth length of tibia under the combined action of the hydrolyzed egg yolk powder and seaweed calcium.
(4) The banana-flavored product can be accepted by children more easily and has the effects of helping digestion and the like; the addition of the erythritol successfully avoids the problems of obesity, tooth decay and the like caused by excessive consumption of sugar.
Detailed Description
In order to better understand the technical content of the invention, specific examples are provided below to further illustrate the invention.
The experimental methods used in the examples of the present invention are all conventional methods unless otherwise specified.
The materials, reagents and the like used in the examples of the present invention can be obtained commercially without specific description.
Example 1
A solid beverage for promoting bone growth and development: comprises the following raw materials in percentage by weight: 40% of noni pulp powder, 20% of erythritol, 22% of butter powder, 4% of banana powder, 3.5% of seaweed powder and 0.037% of hydrolyzed yolk powder.
Example 2
A solid beverage for promoting bone growth and development: comprises the following raw materials in percentage by weight: 25% of noni pulp powder, 20% of erythritol, 22% of butter powder, 4% of banana powder, 3.5% of seaweed powder and 0.037% of hydrolyzed yolk powder.
Example 3
A solid beverage for promoting bone growth and development comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder;
the above examples 1 to 3 were carried out by the following preparation methods:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting into slices of 1-3 cm, drying in the sun, adding sodium bisulfite and ascorbic acid, stirring, soaking for 22min, filtering, adjusting the pH value of filter residues to 8, pulping at 400rpm for 3min, pulping at 1000rpm for 7min to obtain noni pulp, placing the noni pulp in an ethanol solution with the volume 7 times that of the noni pulp, performing strong electric field extraction, wherein the electric field intensity is 2.2kV, the pulse frequency is 2200Hz, extracting for 45min to obtain an extract, concentrating, spray drying to obtain noni fruit extract, and sieving with a 100-mesh sieve to obtain noni fruit pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh fowl egg, separating egg white and yolk, collecting yolk, stirring at 300rpm, filtering to remove impurities to obtain yolk liquid, and ultrasonic treating at field strength of 150W/cm 2 Carrying out ultrasonic treatment for 40min, carrying out centrifugal filtration after ultrasonic treatment, removing suspended matters on the upper layer to obtain degreased yolk liquid, adding neutral protease, phospholipase A1 and phosphatase, wherein the mass ratio of the yolk liquid to the neutral protease to the phospholipase A1 to the phosphatase is 0.5, stirring and carrying out enzymolysis for 35min under the conditions of 50 ℃ and pH value of 6, and carrying out spray drying on the obtained enzymolysis liquid, wherein the air inlet temperature is 170 ℃, the air outlet temperature is 70 ℃, and the flow rate of feed liquid is 90mL/min to obtain hydrolyzed yolk powder;
and S3, mixing the noni pulp powder, the erythritol, the banana powder, the seaweed powder and the hydrolyzed egg yolk powder according to the parts by weight, and homogenizing the mixture to obtain solid beverage powder with particles of 1-3mm in size.
Example 4
A solid beverage for promoting bone growth and development comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder;
the solid beverage is prepared by the following preparation method:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting into slices of 1-3 cm, drying in the sun, adding sodium bisulfite and ascorbic acid, stirring, soaking for 20min, filtering, adjusting the pH value of filter residues to 7, pulping at 300rpm for 2min, pulping at 800rpm for 5min to obtain noni pulp, placing the noni pulp in an ethanol solution of 5 times of volume, performing strong electric field extraction, wherein the electric field intensity is 2.0kV, the pulse frequency is 2000Hz, extracting for 40min to obtain an extract, concentrating, spray drying to obtain noni fruit extract, and sieving with a 80-mesh sieve to obtain noni fruit pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh fowl egg, separating egg white and yolk, collecting yolk, stirring at 200rpm, filtering to remove impurities to obtain yolk liquid, and ultrasonic treating at field strength of 100W/cm 2 Carrying out ultrasonic treatment for 30min, carrying out centrifugal filtration after ultrasonic treatment, removing upper-layer suspended matters to obtain degreased egg yolk liquid, and adding neutral protease, phospholipase A1 and phosphatase, wherein the mass ratio of the egg yolk liquid to the neutral protease to the phospholipase A1 to the phosphatase is 100:1, 0.2Stirring and performing enzymolysis for 20min under the condition of a value of 6 to obtain an enzymolysis liquid, and performing spray drying on the enzymolysis liquid, wherein the air inlet temperature is 140 ℃, the air outlet temperature is 60 ℃, and the flow rate of the feed liquid is 80mL/min to obtain hydrolyzed yolk powder;
and S3, mixing the noni pulp powder, the erythritol, the banana powder, the seaweed powder and the hydrolyzed yolk powder according to the parts by weight, and performing particle homogenization on the mixture to prepare solid beverage powder with particles of 1-3mm in size.
Example 5
A solid beverage for promoting bone growth and development comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder;
the solid beverage is prepared by the following preparation method:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting into slices of 1-3 cm, drying in the sun, adding sodium bisulfite and ascorbic acid, stirring, soaking for 25min, filtering, adjusting the pH value of filter residues to 9, pulping at 500rpm for 5min, pulping at 800-1200 rpm for 8min to obtain noni pulp, placing the noni pulp in an ethanol solution of which the volume is 5-8 times that of the noni pulp, performing strong electric field extraction, wherein the electric field intensity is 2.3kV, the pulse frequency is 2200Hz, extracting for 50min to obtain an extract, concentrating, spray drying to obtain a noni extract, and sieving with a 120-mesh sieve to obtain noni pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh egg, separating egg white and yolk, collecting yolk, stirring at 400rpm, filtering to remove impurities to obtain yolk liquid, and ultrasonic treating at 200W/cm field strength 2 Carrying out ultrasonic treatment for 30-50 min, carrying out centrifugal filtration after ultrasonic treatment, removing suspended matters on the upper layer to obtain degreased egg yolk liquid, adding neutral protease, phospholipase A1 and phosphatase, wherein the mass ratio of the egg yolk liquid to the neutral protease to the phospholipase A1 to the phosphatase is (100) 0.8;
and S3, mixing the noni pulp powder, the erythritol, the banana powder, the seaweed powder and the hydrolyzed yolk powder according to the parts by weight, and performing particle homogenization on the mixture to prepare solid beverage powder with particles of 1-3mm in size.
1. The solid beverages obtained in examples 1 to 5 were measured to determine the nutritional ingredients
Protein detection standards: first method of GB 5009.5-2016;
and (3) detection standard of total content of amino acid: GB 5009.124-2016;
vitamin C detection standard: GB 5009.86-2016;
vitamin B1 detection standard: GB 5009.84-2016;
fat detection standard: a second method of GB 5009.6-2016;
total carbohydrate: GB 28050-2011.
The test results were as follows:
the above results show that the solid beverage of the present invention contains high content of main nutrients, which indicates that the solid beverage obtained by the extraction method of morinda citrifolia and the mixing of the raw materials in proportion of the present invention can retain the main nutrients of morinda citrifolia at a high level.
2. The dispersibility and solubility of the polymer were measured
(1) Dispersibility: 2g of the solid beverage obtained in examples 1 to 5 was dissolved in 50ml of deionized water, and the solution was placed in a stirring flask at a stirring speed of 400rpm, and the time required from the start of stirring to the complete dissolution of the powder was counted after 30 seconds of stirring.
(2) Solubility: 20g of the solid beverage powder obtained in examples 1 to 5 was dissolved in 100mL of the above solid beverage powder at 22 ℃, the dissolved solution was centrifuged at 5000rpm for 10min, the supernatant was dried and weighed, and the solubility was calculated according to the following formula:
solubility (S) = (m) 0 -m 1 )/m 0 X 100%; in the formula m 0 M is the original powder mass 1 The mass of the supernatant after drying;
the measurement results are as follows:
from the above results, it can be seen that the solid beverage having good dispersibility and high solubility can be obtained by mixing the respective raw materials and homogenizing them with microparticles according to the method for extracting noni puree powder and hydrolyzed egg yolk powder of the present invention.
Comparative example 1
The comparative example differs from example 3 in that: the strong electric field extraction is replaced by supercritical CO in the process of preparing noni pulp powder 2 Extracting; in particular to a solid beverage for promoting the growth and development of bones, which comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder;
the preparation method comprises the following steps:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting into 1-3 cm slices, sun-drying, adding sodium bisulfite and ascorbic acid, stirring, soaking for 22min, filtering, adjusting pH of the filter residue to 8, pulping at 400rpm for 3min, pulping at 1000rpm for 7min to obtain noni pulp, placing the noni pulp in 7 times volume of ethanol solution, and performing supercritical CO 2 Extracting under 20Mpa at 40 deg.C for 30min to obtain extractive solution, concentrating, spray drying to obtain Morinda citrifolia extract, and sieving with 100 mesh sieve to obtain Morinda citrifolia pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh fowl egg, separating egg white and yolk, collecting yolk, stirring at 300rpm, filtering to remove impurities to obtain yolk liquid, and ultrasonic treating at field strength of 150W/cm 2 Ultrasonic treating for 40min, centrifuging after ultrasonic treatment, removing upper layer suspended matter to obtain defatted egg yolk liquid, adding neutral proteaseThe mass ratio of phospholipase A1 to phosphatase, the mass ratio of yolk liquid to neutral protease to phospholipase A1 to phosphatase is 0.5, the mass ratio is 0.3;
and S3, mixing the noni pulp powder, the erythritol, the banana powder, the seaweed powder and the hydrolyzed yolk powder according to the parts by weight, and performing particle homogenization on the mixture to prepare solid beverage powder with particles of 1-3mm in size.
The above results show that the present invention sufficiently increases the active ingredients in the noni extract by electric field extraction, thereby increasing the extraction efficiency.
Comparative example 2
This comparative example differs from example 3 in that the hydrolyzed egg yolk powder was prepared without ultrasonic treatment; in particular to a solid beverage for promoting the growth and development of bones, which comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder;
the preparation method comprises the following steps:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting into slices of 1-3 cm, drying in the sun, adding sodium bisulfite and ascorbic acid, stirring, soaking for 22min, filtering, adjusting the pH value of filter residues to 8, pulping at 400rpm for 3min, pulping at 1000rpm for 7min to obtain noni pulp, placing the noni pulp in an ethanol solution with the volume 7 times that of the noni pulp, performing strong electric field extraction, wherein the electric field intensity is 2.2kV, the pulse frequency is 2200Hz, extracting for 45min to obtain an extract, concentrating, spray drying to obtain noni fruit extract, and sieving with a 100-mesh sieve to obtain noni fruit pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh poultry eggs, separating egg white and yolk, collecting yolk, stirring at the stirring speed of 300rpm, filtering to remove impurities to obtain yolk liquid, adding neutral protease, phospholipase A1 and phosphatase, stirring and performing enzymolysis for 35min under the conditions that the mass ratio of the yolk liquid to the neutral protease to the phospholipase A1 to the phosphatase is 100;
and S3, mixing the noni pulp powder, the erythritol, the banana powder, the seaweed powder and the hydrolyzed yolk powder according to the parts by weight, and performing particle homogenization on the mixture to prepare solid beverage powder with particles of 1-3mm in size.
Comparative example 3
The difference between the comparative example and the example 3 is that the hydrolyzed egg yolk powder is prepared without adding lipase, and the solid beverage for promoting the growth and development of bones comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder;
the preparation method comprises the following steps:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting into slices of 1-3 cm, drying in the sun, adding sodium bisulfite and ascorbic acid, stirring, soaking for 22min, filtering, adjusting the pH value of filter residues to 8, pulping at 400rpm for 3min, pulping at 1000rpm for 7min to obtain noni pulp, putting the noni pulp in an ethanol solution with the volume of 7 times of that of the noni pulp, performing strong electric field extraction, wherein the electric field strength is 2.2kV, the pulse frequency is 2200Hz, extracting for 45min to obtain an extract, concentrating, spray-drying to obtain a noni extract, and sieving with a 100-mesh sieve to obtain noni pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh fowl egg, separating egg white and yolk, collecting yolk, stirring at 300rpm, filtering to remove impurities to obtain yolk liquid, and ultrasonic treating at field strength of 150W/cm 2 Carrying out ultrasonic treatment for 40min, carrying out centrifugal filtration after ultrasonic treatment, removing suspended matters on the upper layer to obtain degreased egg yolk liquid, adding neutral protease and phospholipase A1, wherein the mass ratio of the egg yolk liquid to the neutral protease to the phospholipase A1 is 100min, carrying out spray drying on the obtained enzymolysis liquid, and setting the air inlet temperature to be 170 ℃, the air outlet temperature to be 70 ℃ and the flow rate of the feed liquid to be 90mL/min to obtain hydrolyzed yolk powder;
and S3, mixing the noni pulp powder, the erythritol, the banana powder, the seaweed powder and the hydrolyzed yolk powder according to the parts by weight, and performing particle homogenization on the mixture to prepare solid beverage powder with particles of 1-3mm in size.
The above comparative examples 1 to 3 and example 3 were measured for dispersibility and solubility
The test results were as follows:
the results show that the ultrasonic treatment of the invention can avoid the yolk liquid from deforming or aggregating to generate solidified pedicel, can also effectively remove partial yolk lipid substances, the addition of lipase can effectively remove the yolk lipid substances, prevent the lipid substances from influencing the absorption of yolk components, and simultaneously, the enzymolysis can further disperse the yolk hydrolysate to form stable and uniform yolk powder.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and should not be taken as limiting the scope of the present invention, which is intended to cover any modifications, equivalents, improvements, etc. within the spirit and scope of the present invention.
Claims (9)
1. A solid beverage for promoting bone growth and development is characterized in that: comprises the following raw materials in percentage by weight: 25 to 40 percent of noni pulp powder, 20 to 38 percent of erythritol, 22 to 40 percent of butter powder, 4 to 6 percent of banana powder, 3.5 to 6.0 percent of seaweed powder and 0.037 to 0.11 percent of hydrolyzed yolk powder.
2. The solid beverage for promoting bone growth and development as claimed in claim 1, wherein: comprises the following raw materials in percentage by weight: 30% of noni pulp powder, 30% of erythritol, 28% of butter powder, 5% of banana powder, 4.8% of seaweed powder and 0.05% of hydrolyzed yolk powder.
3. The method for preparing a solid beverage for promoting bone growth and development according to claim 1, wherein: the method comprises the following steps:
s1, preparing noni pulp powder: picking fresh noni fruits, cutting the noni fruits into slices of 1-3 cm, drying the noni fruits, adding sodium bisulfite and ascorbic acid, stirring and soaking for 20-25 min, filtering, adjusting the pH value of filter residues to 7-9, pulping for 2-5 min at 300-500 rpm, pulping for 5-8 min at 800-1200 rpm to obtain noni pulp, placing the noni pulp in an ethanol solution of which the volume is 5-8 times that of the noni pulp, performing strong electric field extraction, extracting for 40-50 min to obtain an extract liquid, concentrating, performing spray drying to obtain a noni extract, and sieving by a sieve of 80-120 meshes to obtain noni pulp powder;
s2, preparing hydrolyzed egg yolk powder: selecting fresh eggs, separating egg white and yolk, collecting yolk, stirring at the stirring speed of 200-400 rpm, filtering to remove impurities to obtain yolk liquid, carrying out ultrasonic treatment with the field strength of 100-200W/cm & lt 2 & gt for 30-50 min, carrying out centrifugal filtration after ultrasonic treatment, removing upper-layer suspended matters to obtain degreased yolk liquid, adding protease, phospholipase and lipase, stirring and carrying out enzymolysis for 20-45 min at the temperature of 40-60 ℃ and the pH value of 6-7 to obtain enzymatic hydrolysate, and carrying out spray drying to obtain hydrolyzed yolk powder;
and S3, mixing the noni pulp powder, the erythritol, the cream powder, the banana powder, the seaweed powder and the hydrolyzed egg yolk powder according to the parts by weight, and performing particle homogenization on the mixture to prepare solid beverage powder with particles of 1-3mm in size.
4. The method for preparing a solid beverage for promoting bone growth and development according to claim 3, wherein: the electric field intensity of the S1 is 2.0-2.3 kV, and the pulse frequency is 2000-2200 Hz.
5. The method for preparing a solid beverage for promoting bone growth and development according to claim 3, wherein: the mass ratio of the egg yolk liquid, the protease, the phospholipase and the lipase in the S2 is (100).
6. The method for preparing a solid beverage for promoting bone growth and development according to claim 3, wherein: the protease in S2 is selected from one or more of neutral protease, carboxypeptidase A, carboxypeptidase B and papain.
7. The method for preparing a solid beverage for promoting bone growth and development according to claim 3, wherein: the phospholipase in S2 is selected from one or more of phospholipase A1, phospholipase A2, phospholipase B and phospholipase C.
8. The method for preparing a solid beverage for promoting bone growth and development according to claim 3, wherein: the lipase in S2 is selected from one or more of phosphatase, sterol enzyme and carboxylesterase.
9. The method for preparing a solid beverage for promoting bone growth and development according to claim 3, wherein: in the S2 spray drying, the air inlet temperature is set to be 140-200 ℃, the air outlet temperature is set to be 60-80 ℃, and the flow rate of the material liquid is set to be 80-100 mL/min.
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Application publication date: 20221129 |