CN115363239A - High-smoke tobacco particles for heating non-combustible tobacco products and preparation method thereof - Google Patents
High-smoke tobacco particles for heating non-combustible tobacco products and preparation method thereof Download PDFInfo
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- CN115363239A CN115363239A CN202210820369.1A CN202210820369A CN115363239A CN 115363239 A CN115363239 A CN 115363239A CN 202210820369 A CN202210820369 A CN 202210820369A CN 115363239 A CN115363239 A CN 115363239A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
Abstract
The invention belongs to the field of production of auxiliary materials of heating non-combustible tobacco products, and particularly relates to a high-smoke tobacco particle of a heating non-combustible tobacco product and a preparation method thereof, wherein the high-smoke tobacco particle comprises a porous core material A and a smoke material B, and the porous core material A comprises the following components in parts by mass: tobacco powder: 5-40 parts of cassava starch: 10-40 parts of plantain seed shell powder: 1-40 parts of water: 15-50 parts of tobacco extract: 10-50 parts. According to the invention, the plantain seed shell powder is added into the high-smoke-generating tobacco particles, the particles are rapidly expanded after absorbing water, the high-porosity porous core material is obtained through wet granulation, and the porous core material can keep the pore structure after vacuum freeze drying, so that the high-smoke-generating tobacco particles have strong adsorbability and fillability, the smoke quantity of the particles is large, the fragrance loss is small, the smoke generating effect is good, the smoke quantity is stable, and the smoking sense and comfort are good.
Description
Technical Field
The invention belongs to the field of production of auxiliary materials of heating non-combustible tobacco products, and particularly relates to high-smoke tobacco particles of heating non-combustible tobacco products and a preparation method thereof.
Background
A heating non-combustion tobacco product is a novel product combining a heating appliance and a cigarette cartridge, and is a low-temperature cigarette designed by taking 'heating non-combustion' as the idea, wherein the processed tobacco shreds and the cigarette cartridge are heated to a certain temperature by a special heating device, and the cigarette cartridge is heated to a degree enough to give off smoke for people to absorb.
The tobacco pellet for heating the incombustible tobacco product is mainly divided into two types, namely a sheet technology and a particle technology. The slice technology is characterized in that herbaceous plants or tobacco-like components are crushed and mixed with natural fibers, adhesives and the like are added and uniformly stirred, and a slice product is prepared after constant-pressure drying. The particle technology has the advantages that residues after the heating core is heated are some dry carbonized particles which can be easily removed, but the defects are that the particles are easy to regain moisture, the heating is not uniform, the smoke amount is small, scorched flavor is easy to generate, the smoke amount before and after the smoke generation is inconsistent, and the cigarette fragrance cannot be maintained. Therefore, the development of the heating non-combustion smoke bomb with good dispersibility, large smoke amount and good smoking effect has important significance for the development of heating non-combustion tobacco products.
Disclosure of Invention
The invention mainly aims to solve the defects of the existing technology for heating non-combustible tobacco product particles and provide the high-smoke-generating particles with strong tobacco aroma and large smoke amount. The invention also provides a preparation method and application of the high-fuming particle.
The purpose of the invention is realized by the following technical scheme.
High-smoke tobacco particles for heating a non-combustible smoking article, comprising a porous core material A and a smoking material B, the porous core material A comprising tobacco leaf powder, tapioca starch, psyllium husk powder, tobacco extract and water.
The high-smoke-formation tobacco particles have the advantages that the core raw material is the tobacco leaf powder, the tobacco fragrance is rich, and the smoking feeling of smokers can be met. On the basis, plantain seed shell powder is added into particles, the plantain seed shell powder rapidly expands after absorbing water, and a high-porosity porous core material is obtained through wet granulation, can keep the pore structure of the porous core material, has strong adsorbability and fillability, enables the particles to have large smoke amount, less fragrance loss and good smoking effect, and endows the particles with high smoking characteristic, and the smoke amount is stable.
The high-smoke-forming tobacco particles also adopt the high-sugar content tobacco extract as an adhesive, and synthetic compounds are not introduced, so that the taste of the particles can be improved, the fragrance of the particles is fine, and the pleasure feeling is enhanced.
Preferably, the porous core material A comprises the following components in parts by mass: tobacco powder: 5-40 parts of cassava starch: 10-40 parts of plantain seed shell powder: 1-40 parts of water: 15-50 parts of tobacco extract: 10-50 parts.
Preferably, the tobacco extract is obtained by carrying out water extraction and alcohol precipitation on tobacco, and the tobacco extract with high sugar content is used as an adhesive, does not introduce a synthetic compound, can improve the taste of the particles, enables the particles to have fine fragrance, and enhances pleasant feeling.
Preferably, the smoking material B comprises the following components in parts by mass: propylene glycol: 10-60 parts of glycerol: 40-90 parts.
In the preferred scheme of the invention, by improving the smoking material, preferably compounding the propylene glycol and the glycerol, compared with the single component, the smoke generating amount is larger and the smoke amount is more stable.
Preferably, the tobacco powder comprises a tobacco powder: 20-40 meshes: 10-80 parts, 80-160 meshes: 20-90 parts.
Preferably, the porous core material a is obtained by mixing raw materials and performing vacuum freeze-drying granulation. According to the invention, the porous core material formed by adding the psyllium husk powder is combined with the porous core material subjected to vacuum freeze drying, so that the pore structure of the psyllium husk powder can be better maintained. And partial bound water in the particles can be removed through vacuum freeze drying, so that the adsorption of the subsequent smoke agent is facilitated.
Preferably, the mass ratio of the porous core material A to the smoking material B is as follows: porous core material a:25-90 parts of a smoking material B:10-80 parts.
Preferably, the mesh number of the porous core material A is 80-160 meshes, and the moisture content is 3-4 wt%.
Furthermore, the mesh number of the high-smoking tobacco particles is 20-40 meshes, and the moisture content is 6-9 wt%.
It is another object of the present invention to provide a method of making the above-described high-smoke tobacco particles for heating a non-combustible article, comprising the steps of:
(1) Preparation of tobacco powder
20-40 meshes of tobacco powder: 10-80 parts, 80-160 meshes: 20-90 parts of the components are uniformly mixed to obtain tobacco powder.
(2) Preparation of porous core material A
Mixing tobacco powder: 5-40 parts of cassava starch: 10-40 parts of plantain seed husk powder: 1-40 parts of water: 15-50 parts of tobacco extract: 10-50 parts of the mixture is granulated, and then the porous core material A is obtained after vacuum freeze drying, crushing and screening;
(3) Preparation of smoking material B
Mixing propylene glycol: 10-60 parts of glycerol: 10-90 parts of a smoke material B is obtained by mixing;
(4) Preparation of high-smoke tobacco particles
Adsorbing a smoking material B on a porous core material A, wherein the mass ratio of the porous core material A to the smoking material B is as follows: porous core material a:5-60 parts of a smoking material B:10-60 parts of the tobacco particles with high smoke formation are obtained after vacuum freeze drying.
The invention has the following beneficial effects:
(1) According to the invention, the plantain seed shell powder is added into the high-smoke-generating tobacco particles, the particles are rapidly expanded after absorbing water, the high-porosity porous core material is obtained through wet granulation, and the porous core material can keep the pore structure after vacuum freeze drying, so that the high-smoke-generating tobacco particles have strong adsorbability and fillability, the smoke quantity of the particles is large, the fragrance loss is small, the smoke generating effect is good, the smoke quantity is stable, and the smoking sense and comfort are good.
(2) The high-smoke-forming tobacco particles adopt the high-sugar content tobacco extract as an adhesive, and synthetic compounds are not introduced, so that the taste of the particles can be improved, the fragrance of the particles is fine, and the pleasure feeling is enhanced.
(3) The high-smoke-formation tobacco particles prepared by the invention are dried by using a vacuum freeze drying method, so that part of bound water in the particles can be removed, the moisture content after drying is 3-4 wt%, the subsequent adsorption of a smoke agent is facilitated, the loss of aroma substances, aroma components and an atomizing agent of the particles after vacuum freeze drying is less, and the high-smoke-formation tobacco particles have better sensory product smoking experience during smoking.
Detailed Description
The embodiments of the present invention have been described in detail with reference to the examples, but the present invention is not limited to the described embodiments. It will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.
Example 1
This example provides a high-smoke tobacco particle for heating a non-combustible smoking article having a particle size of 20-40 mesh and a moisture content of 6%. The composition comprises the following components in parts by mass:
porous core material a:60 parts of a smoking material B:40 parts of the components. The mesh number of the porous core material A is 80-160 meshes, and the water content is 4%.
Wherein, according to the part by mass, porous core material A includes: 30 parts of tobacco powder, 20 parts of cassava starch, 10 parts of plantain seed shell powder, 20 parts of water and 20 parts of tobacco extract (water extraction and alcohol precipitation extract of tobacco).
Wherein the tobacco powder comprises 10 parts of 20-40 mesh tobacco powder and 90 parts of 80-160 mesh tobacco powder by mass.
Wherein the smoking material B comprises 20 parts of propylene glycol and 80 parts of glycerol by mass.
The preparation method comprises the following steps:
(1) Preparation of tobacco powder
And (3) uniformly mixing the tobacco powder with the two particle sizes to obtain the tobacco powder.
(2) Preparation of porous core Material A
And mixing the raw materials of the porous core material A, granulating by a wet method, and then carrying out vacuum freeze drying, crushing and screening to obtain the porous core material A.
(3) Preparation of smoking material B
And mixing the propylene glycol and the glycerol to obtain the smoking material B.
(4) Preparation of high-smoke tobacco particles
Preparing the porous core material A and the smoking material B according to a required mass ratio, adsorbing the smoking material B by the porous core material A, and carrying out vacuum freeze drying to obtain the high-smoking tobacco particles.
Example 2
This embodiment provides a method of making high-smoke tobacco particles for heating a non-burning smoking article, comprising the steps of:
(1) Tobacco powder formulation
Mixing tobacco powder: 20-40 meshes: 20 parts by mass, 80-160 meshes: and 80 parts by mass of the components are uniformly mixed to obtain tobacco powder.
(2) Preparation of porous core material A
Mixing tobacco powder: 25 parts by mass of cassava starch: 10 parts by mass of plantain seed husk powder: 20 parts by mass of water: 20 parts by mass of a tobacco extract (water extraction and alcohol precipitation extract of tobacco): 25 parts by mass of the porous core material A are uniformly mixed, granulated, subjected to vacuum freeze drying, crushing and screening to obtain the porous core material A with the mesh number of 80-160 meshes and the moisture content of 4%;
(3) Preparation of smoking Material B
Mixing propylene glycol: 40 parts by mass of glycerol: 60 parts by mass of a mixture is mixed to obtain a smoking material B;
(4) High-smoke tobacco particle preparation
Adsorbing a smoking material B by using a porous core material A, wherein the mass ratio of the porous core material A to the smoking material B is as follows: porous core material a:55 parts by mass, a smoking material B:45 parts by mass, and obtaining the high-fuming tobacco particles with 20-40 meshes and 7wt% of water after vacuum freeze drying.
Example 3
This embodiment provides a method of making high-smoke tobacco particles for heating a non-burning smoking article, comprising the steps of:
(1) Tobacco powder formulation
Mixing tobacco powder: 20-40 meshes: 15 parts by mass, 80-160 meshes: 85 parts by mass of the components are uniformly mixed to obtain the tobacco powder.
(2) Preparation of porous core material A
Mixing tobacco powder: 35 parts by mass of cassava starch: 15 parts by mass of plantain seed husk powder: 15 parts by mass, water: 20 parts by mass of a tobacco extract (water extraction and alcohol precipitation extract of tobacco): 20 parts of the components are uniformly mixed, granulated, and subjected to vacuum freeze drying, crushing and screening to obtain a porous core material A with the mesh number of 80-160 meshes and the moisture content of 4 wt%;
(3) Preparation of smoking Material B
Mixing propylene glycol: 10 parts by mass of glycerol: mixing 90 parts by mass to obtain a smoking material B;
(4) Preparation of high-smoke tobacco particles
Adsorbing a smoking material B on a porous core material A, wherein the mass ratio of the porous core material A to the smoking material B is as follows: porous core material a:65 parts by mass of a smoking material B:35 parts by mass, and obtaining the high-smoking tobacco particles with 20-40 meshes and 8wt% of water after vacuum freeze drying.
Example 4
This embodiment provides a method of making high-smoke tobacco particles for heating a non-combustible smoking article, comprising the steps of:
(1) Preparation of tobacco powder
Mixing the tobacco powder: 20-40 meshes: 25 parts by mass, 80-160 meshes: 75 parts by mass of the components are uniformly mixed to obtain tobacco powder;
(2) Preparation of porous core Material A
Mixing tobacco powder: 20 parts by mass of cassava starch: 15 parts by mass of plantain seed husk powder: 25 parts by mass, water: 20 parts by mass of a tobacco extract (water extraction and alcohol precipitation extract of tobacco): 20 parts by mass of the porous core material A are uniformly mixed, granulated, subjected to vacuum freeze drying, crushing and screening to obtain the porous core material A with the mesh number of 80-160 meshes and the moisture content of 4%;
(3) Preparation of smoking Material B
Mixing propylene glycol: 30 parts by mass of glycerol: 70 parts by mass of a mixture is mixed to obtain a smoking material B;
(4) Preparation of high-smoke tobacco particles
Adsorbing a smoking material B on a porous core material A, wherein the mass ratio of the porous core material A to the smoking material B is as follows: porous core material a:60 parts by mass, a smoking material B:40 parts by mass, and obtaining the high-fuming tobacco particles with 20-40 meshes and 8wt% of water after vacuum freeze drying.
Comparative example 1
A method of preparing tobacco particles for heating a non-combustible smoking article, comprising the steps of:
(1) Tobacco powder formulation
Mixing tobacco powder: 20-40 meshes: 25 parts by mass, 80-160 meshes: 75 parts by mass of the components are uniformly mixed to obtain tobacco powder;
(2) Core material A preparation
Mixing tobacco powder: 20 parts by mass of cassava starch: 35 parts by mass, water: 20 parts by mass of a tobacco extract (water extraction and alcohol precipitation extract of tobacco): 20 parts by mass and 5 parts by mass of sodium carboxymethylcellulose are uniformly mixed, and the porous core material A with 80-160 meshes and 4% of water content is obtained after wet granulation, vacuum freeze drying, crushing and screening;
(3) Preparation of smoking Material B
Mixing propylene glycol: 30 parts by mass of glycerol: 70 parts by mass of a mixture is mixed to obtain a smoking material B;
(4) Preparation of heat-not-combustible granules
Adsorbing a smoking material B on a core material A, wherein the mass ratio of the core material A to the smoking material B is as follows: a core material A:80 parts by mass, a smoking material B:20 parts by mass, and obtaining the heating non-combustible particles with 20-40 meshes and 8wt% of water after vacuum freeze drying.
The high-smoke tobacco particles obtained in examples 1 to 4, comparative example, were applied to a heat non-combustible article by adding the high-smoke tobacco particles to the heat non-combustible article with a non-combustible cartridge, and the high-smoke particles were added in an amount of 0.170 ± 0.02g per heat non-combustible article with a non-combustible cartridge.
The performance of the heated non-burning cartridge prepared in the above example was tested, and sensory smoking evaluation and objective evaluation of smoking set contamination level after smoking were performed; and detecting the number of the smoking openings of the cigarettes, the content of total particulate matters, propylene glycol and glycerol. The test results and sensory evaluation are as follows:
from the detection results in the table above, compared with comparative example 1, the high-smoke tobacco particles for heating and non-combustion provided by the invention have the advantages that the content of the atomizing agent after heating is stable, the smoke amount in the smoking process is large, the smoking effect is good, the aerosol amount is stable, the total particle phase is 44-48 mg/cigarette, the tobacco fragrance is strong, and the sensory evaluation of smoking is good. The tobacco pellet with high smoke generation of the invention is processed into a non-burning heating pellet, the tobacco pellet is heated uniformly and is not easy to coke, the tobacco pellet is easy to take out after use, the pellet has no residue, and the use is convenient.
Claims (10)
1. The high-smoke-generation tobacco particles for heating the non-combustible tobacco product are characterized by comprising a porous core material A and a smoke generation material B, wherein the porous core material A comprises the following components in parts by mass: tobacco powder: 5-40 parts of cassava starch: 10-40 parts of plantain seed shell powder: 1-40 parts of water: 15-50 parts of tobacco extract: 10-50 parts.
2. The high-smoke tobacco particle for heating a non-combustible smoking article according to claim 1, wherein the porous core material a comprises the following components in parts by mass: tobacco powder: 10-30 parts of cassava starch: 20-30 parts of plantain seed shell powder: 10-30 parts of water: 20-30 parts of tobacco extract: 10-50 parts.
3. High-smoke tobacco particles for heating a non-combustible smoking article according to claim 1, wherein the smoking material B comprises the following components in parts by mass: propylene glycol: 10-60 parts of glycerol: 40-90 parts.
4. The high-smoke tobacco particle for heating a non-combustible smoking article according to claim 1, wherein the porous core material a is obtained by mixing raw materials and granulating by vacuum freeze drying.
5. The high-smoke tobacco particle for heating a non-combustible smoking article according to claim 1, wherein the mass ratio of the porous core material a and the smoking material B is: porous core material a:25-90 parts of a smoking material B:10-80 parts.
6. The high-smoke tobacco particle for heating a non-combustible smoking article according to claim 1, wherein said tobacco powder comprises 20-40 mesh tobacco powder: 10-80 parts, 80-160 meshes of tobacco powder: 20-90 parts.
7. The high-smoke tobacco particle for heating a non-combustible smoking article of claim 1, wherein the porous core material a has a moisture content of 3-4 wt%.
8. The high-smoke tobacco particle for heating a non-combustible smoking article according to claim 7, wherein the mesh number of the porous core material A is 80-160 mesh.
9. A method of making high-smoke tobacco particles for heating a non-combustible article according to claim 1, comprising the steps of:
(1) Preparation of porous core material A
Mixing the raw materials of the porous core material A, granulating, and then carrying out vacuum freeze drying, crushing and screening to obtain the porous core material A;
(2) Preparation of smoking material B
Mixing propylene glycol: 10-60 parts of glycerol: 10-90 parts of a smoke material B is obtained by mixing;
(3) Preparation of high-smoke tobacco particles
Adsorbing a smoking material B on a porous core material A, wherein the mass ratio of the porous core material A to the smoking material B is as follows: porous core material a:5-60 parts of a smoking material B:10-60 parts of the tobacco particles with high smoke formation are obtained after vacuum freeze drying.
10. The method of making high-smoke tobacco particles for heating a non-combustible article according to claim 9, wherein the high-smoke tobacco particles are of mesh 20-40 mesh and have a moisture content of 6wt% to 9wt%.
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| CN202210820369.1A CN115363239A (en) | 2022-07-13 | 2022-07-13 | High-smoke tobacco particles for heating non-combustible tobacco products and preparation method thereof |
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| CN202210820369.1A CN115363239A (en) | 2022-07-13 | 2022-07-13 | High-smoke tobacco particles for heating non-combustible tobacco products and preparation method thereof |
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Citations (6)
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| WO2008148700A1 (en) * | 2007-06-05 | 2008-12-11 | British American Tobacco (Investments) Limited | Humidifying capsule for use with tobacco products |
| CN110169606A (en) * | 2019-05-31 | 2019-08-27 | 广州市澳键丰泽生物科技股份有限公司 | It is a kind of to heat smoker particles inside and its preparation method and application of not burning |
| CN110477438A (en) * | 2019-08-26 | 2019-11-22 | 广东神农烟科技术有限公司 | It is a kind of to heat incombustible smoking article and preparation method thereof |
| CN111887468A (en) * | 2020-08-04 | 2020-11-06 | 福建中烟工业有限责任公司 | Smoking particle for cigarette capable of being heated and burned and preparation method thereof |
| CN113115975A (en) * | 2019-12-31 | 2021-07-16 | 广东省金叶科技开发有限公司 | Pericarpium citri reticulatae-containing particle-type tobacco core material capable of being heated and not combusted and preparation method thereof |
| WO2022003125A1 (en) * | 2020-07-01 | 2022-01-06 | Jt International Sa | Aerosol-generating substrate comprising granulated flavoured particles |
-
2022
- 2022-07-13 CN CN202210820369.1A patent/CN115363239A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008148700A1 (en) * | 2007-06-05 | 2008-12-11 | British American Tobacco (Investments) Limited | Humidifying capsule for use with tobacco products |
| CN110169606A (en) * | 2019-05-31 | 2019-08-27 | 广州市澳键丰泽生物科技股份有限公司 | It is a kind of to heat smoker particles inside and its preparation method and application of not burning |
| CN110477438A (en) * | 2019-08-26 | 2019-11-22 | 广东神农烟科技术有限公司 | It is a kind of to heat incombustible smoking article and preparation method thereof |
| CN113115975A (en) * | 2019-12-31 | 2021-07-16 | 广东省金叶科技开发有限公司 | Pericarpium citri reticulatae-containing particle-type tobacco core material capable of being heated and not combusted and preparation method thereof |
| WO2022003125A1 (en) * | 2020-07-01 | 2022-01-06 | Jt International Sa | Aerosol-generating substrate comprising granulated flavoured particles |
| CN111887468A (en) * | 2020-08-04 | 2020-11-06 | 福建中烟工业有限责任公司 | Smoking particle for cigarette capable of being heated and burned and preparation method thereof |
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