CN115227611A

CN115227611A - Moisturizing and repairing mask and preparation method thereof

Info

Publication number: CN115227611A
Application number: CN202210799755.7A
Authority: CN
Inventors: 赵昌锋; 杨惠馨; 张健
Original assignee: Guangxi Gongle Biotechnology Co ltd
Current assignee: Guangxi Gongle Biotechnology Co ltd
Priority date: 2022-07-08
Filing date: 2022-07-08
Publication date: 2022-10-25

Abstract

The invention discloses a moisturizing and repairing mask, which at least comprises the following active ingredients: tremella extract, ganoderma atrum extract, pseudo-ginseng extract, collagen extract, mangnolia officinalis extract, licorice root extract, tea polyphenol, calendula extract and vitamin E. The moisturizing and repairing facial mask disclosed by the invention has the advantages that the reasonable compounding is carried out by adopting various active ingredients through the combined coordination and synergism of various active ingredients. When in use, the skin softening cream softens the cuticle of the skin, expands pores, and has effective components penetrating into the skin to achieve deep and long-acting water replenishing. The damaged skin is restored. Meanwhile, the licorice root extract is added, so that the effects of various medicines and the drug property can be adjusted, the drug effect of active ingredients can be fully exerted, the activity of the aminohydrolase can be inhibited, the oxygen eye base can be removed, and the skin can be whitened. Can accelerate basal metabolism of skin, has the functions of activating skin and resisting aging, and also has good moisturizing capability.

Description

Moisturizing and repairing mask and preparation method thereof

Technical Field

The invention relates to the technical field of cosmetics, and particularly relates to a moisturizing and repairing facial mask and a preparation method thereof.

Background

The skin is the natural outer coat of the human body, the stratum corneum, the outermost layer of the skin, plays an important role in the integrity of the skin barrier function. Skin barrier means that the skin has barrier, absorption, secretion, excretion, metabolism, immunity, thermoregulation and sensory functions. Among them, the skin barrier (skinbarrier) functions are the basis, i.e. against the invasion of antigenic substances, microorganisms, sunlight, etc. to the outside, preventing the loss of nutrients and water in the body, maintaining the normal physiological function of the skin, and preventing certain skin diseases. If the skin barrier is compromised and transepidermal water loss (TEWL) increases, the skin will become dry and desquamated. At the same time, the resistance to external antigens and microorganisms is weakened, and certain skin diseases can be induced and aggravated.

The skin covered on the surface of a human body is affected most by external factors such as environment and the like, so that the skin is very easy to lose moisture, and the skin loses elasticity after being lack of water, and the repair and regeneration speed is reduced, so that the skin problems such as shrivelled, aged and poor in elasticity occur, and therefore the skin moisturizing repair becomes a theme of modern cosmetics.

The information disclosed in this background section is only for enhancement of understanding of the general background of the invention and should not be taken as an acknowledgement or any form of suggestion that this information forms the prior art already known to a person skilled in the art.

Disclosure of Invention

The invention aims to provide a moisturizing and repairing mask, so that the defects that a skin care product is poor in moisturizing effect, cannot achieve repairing effect and the like are overcome.

The invention also aims to provide a preparation method of the moisturizing and repairing mask.

In order to achieve the purpose, the invention provides a moisturizing and repairing mask, and the active ingredients of the mask at least comprise the following raw materials: tremella extract, ganoderma atrum extract, pseudo-ginseng extract, collagen extract, mangnolia officinalis extract, licorice root extract, tea polyphenol, calendula extract and vitamin E.

Preferably, in the above technical scheme, the moisturizing repair mask comprises the following active ingredients in percentage by weight: 2-7% of tremella extract, 0.5-5% of ganoderma atrum extract, 1-5% of pseudo-ginseng extract, 0.1-3% of collagen extract, 0.5-2% of magnolia officinalis extract, 0.1-4% of licorice root extract, 0.1-4% of tea polyphenol, 1-7% of calendula extract, 0.5-3% of vitamin E and the balance of water.

Preferably, in the technical scheme, the moisturizing and repairing mask comprises the following active ingredients in percentage by weight: 3.6-5.4% of tremella extract, 2.3-3.8% of ganoderma atrum extract, 1.4-2.8% of pseudo-ginseng extract, 1.2-2.4% of collagen extract, 0.8-1.6% of mangnolia officinalis extract, 0.5-2.2% of licorice root extract, 2.1-3.3% of tea polyphenol, 3-5% of calendula extract, 1.5-2.5% of vitamin E and the balance of water.

Preferably, in the above technical scheme, the moisturizing and repairing mask further comprises the following raw materials: sericin, carbomer, hyaluronic acid, 1,3 butanediol, glycerol and preservative.

Preferably, in the above technical scheme, the moisturizing repair mask further comprises the following raw materials in percentage by weight: 0.5-3.5% of sericin, 1-5% of carbomer, 1-5% of hyaluronic acid, 1-5% of 1,3 butanediol, 2-6% of glycerol and 0.01-1% of preservative.

Preferably, in the above technical scheme, the preservative is A91 or/and p-hydroxyacetophenone.

Preferably, in the above technical solution, the collagen extract is obtained by processing cod skin protein.

A preparation method of the moisturizing and repairing mask comprises the following steps:

(1) Weighing Tremella extract, cortex Magnolia officinalis extract, glycyrrhrizae radix extract, tea polyphenols, herba Sidae Rhombifoliae extract, vitamin E, sericin, carbomer, hyaluronic acid, 1,3 butanediol, glycerol and water at a certain proportion, and mixing well for use;

(2) Respectively hydrolyzing sliced Notoginseng radix with cellulase, pectinase, and alpha-amylase to obtain Notoginseng radix extractive solution, and mixing the separated Notoginseng radix extractive solution into container;

(3) Taking raw material codiaceae fish skin protein, treating the codiaceae fish skin protein by a biological enzymolysis method, drying to obtain powder, filtering by gel, and adding into a container according to a proportion for later use after testing that the molecular weight is less than 1000;

(4) After inactivation, adding a ganoderma atrum strain, fermenting for a period of time, then centrifuging to obtain a fermentation supernatant, and adding a preservative;

(5) And (6) filling.

Preferably, in the technical scheme, raw materials of tremella, mangnolia officinalis, licorice root and calendula are weighed and crushed to obtain raw material powder; adding water or ethanol into the raw material powder, purifying under vacuum degree of-0.1 MPa and temperature of 45-55 deg.C, and repeatedly purifying for 2-4 times; in each purification, the mass ratio of the mixed raw materials to water or ethanol is 1.

Preferably, in the above technical scheme, the adding amount of the cellulase in the step (2) accounts for 0.1-1% of the adding weight of the pseudo-ginseng, the adding amount of the pectinase accounts for 0.01-0.1% of the adding weight of the pseudo-ginseng, and the adding amount of the alpha-amylase accounts for 0.01-0.1% of the adding weight of the pseudo-ginseng.

Preferably, in the above technical scheme, the fermentation in step (3) is performed by controlling the pH value of the fermentation to be 5-6 and fermenting at 35-45 ℃ for 25-45h.

Compared with the prior art, the invention has the following beneficial effects:

(1) The moisturizing and repairing facial mask disclosed by the invention is prepared by reasonably compounding various active ingredients through the combined coordination and synergism of various active ingredients. When in use, the skin softening cream softens the cuticle of the skin, expands pores, and has effective components penetrating into the skin to achieve deep and long-acting water replenishing. The damaged skin is restored. Meanwhile, the licorice root extract is added, so that the effects of various medicines and the drug property can be adjusted, the drug effect of active ingredients can be fully exerted, meanwhile, the activity of the aminase can be inhibited, the oxygen eye base can be removed, and the skin whitening effect can be achieved. Can accelerate the basal metabolism of skin, has the functions of activating skin and resisting aging, and also has good moisturizing capability.

(2) The moisturizing and repairing mask is reasonable in raw material formula, remarkable in moisturizing and repairing effect, and suitable for industrial production. The raw materials of the invention can be used for preparing various facial masks. Or making into essence, cosmetic water, whitening and moisturizing milk, cream, etc.

Detailed Description

The following detailed description of the present invention will be given with reference to specific examples, but it should be understood that the scope of the present invention is not limited to the specific embodiments.

Example 1

The moisturizing and repairing mask comprises the following active ingredients in percentage by weight: 4.8% of tremella extract, 3.1% of ganoderma atrum extract, 2.5% of pseudo-ginseng extract, 1.6% of collagen extract, 1.3% of mangnolia officinalis extract, 1.8% of licorice root extract, 2.2% of tea polyphenol, 5.4% of calendula extract, 1.2% of vitamin E, 2.7% of silk fibroin, 3.2% of carbomer, 3.6% of hyaluronic acid, 2.4% of 1,3 butanediol, 3.3% of glycerol, 0.05% of preservative and the balance of water.

The preservative is A91, and the collagen extract is obtained by processing cod skin protein.

(1) Extracting raw materials: weighing raw materials of tremella, mangnolia officinalis, licorice root and calendula, and crushing to obtain raw material powder; the raw materials are purified respectively. Adding ethanol into the raw material powder, purifying under vacuum degree of-0.1 MPa and temperature of 50 deg.C, and repeatedly purifying for 3 times; for each purification, the mass ratio of the mixed raw material to ethanol was 1. Mixing the filtrates, and filtering with 200nm ceramic membrane to obtain clear solution. Concentrating the clear solution at 50 deg.C under-0.1 MPa to obtain extractive solution.

(2) Weighing Tremella extract, cortex Magnolia officinalis extract, glycyrrhrizae radix extract, tea polyphenols, herba Sidae Rhombifoliae extract, vitamin E, sericin, carbomer, hyaluronic acid, 1,3 butanediol, glycerol and water at a certain proportion, and mixing well for use.

(3) Weighing Notoginseng radix, pulverizing, performing enzymolysis, adding cellulase, stirring, performing first enzymolysis, adding pectase, stirring, performing second enzymolysis, adding alpha-amylase, performing third enzymolysis to obtain Notoginseng radix extract, and mixing the separated Notoginseng radix extract with container in proportion.

Wherein, the addition amount of the cellulase accounts for 0.5 percent of the addition amount of the pseudo-ginseng, the addition amount of the pectinase accounts for 0.03 percent of the addition amount of the pseudo-ginseng, and the addition amount of the alpha-amylase accounts for 0.06 percent of the addition amount of the pseudo-ginseng.

(4) Treating cod skin protein by biological enzymolysis, oven drying to obtain powder, gel filtering, and adding into container at a certain proportion when the molecular weight is less than 1000.

(5) Inactivating, adding Ganoderma atrum strain, fermenting at pH of 5.6 at 40 deg.C for 32 hr, detecting viscosity, centrifuging to obtain fermented supernatant, adding antiseptic, and adjusting with water to appropriate skin feeling parameters.

(6) And (5) filling after the inspection is qualified.

Example 2

The moisturizing and repairing mask comprises the following active ingredients in percentage by weight: 2% of tremella extract, 5% of ganoderma atrum extract, 1% of pseudo-ginseng extract, 0.1% of collagen extract, 0.5% of mangnolia officinalis extract, 4% of licorice root extract, 0.1% of tea polyphenol, 1% of calendula extract, 0.5% of vitamin E, 3.5% of sericin, 1% of carbomer, 5% of hyaluronic acid, 1% of 1,3 butanediol, 2% of glycerol, 0.01% of preservative and the balance of water.

The preservative is A91. The collagen extract is obtained by processing cod skin protein.

(1) Extracting raw materials: weighing raw materials of tremella, mangnolia officinalis, licorice root and calendula, and crushing to obtain raw material powder; the raw materials are purified respectively. Adding ethanol into the raw material powder, purifying under vacuum degree of-0.1 MPa and temperature of 45 deg.C, and repeatedly purifying for 4 times; for each purification, the mass ratio of the mixed raw material to ethanol was 1. Mixing the filtrates, and filtering with 200nm ceramic membrane to obtain clear solution. Concentrating the clear solution at 55 deg.C under-0.1 MPa to obtain extractive solution.

Wherein, the adding amount of the cellulase accounts for 1 percent of the adding weight of the pseudo-ginseng, the adding amount of the pectinase accounts for 0.01 percent of the adding weight of the pseudo-ginseng, and the adding amount of the alpha-amylase accounts for 0.01 percent of the adding weight of the pseudo-ginseng.

(5) Inactivating, adding Ganoderma atrum strain, fermenting at pH of 6, fermenting at 35 deg.C for 45 hr, detecting viscosity, centrifuging to obtain fermented supernatant, adding antiseptic, and adjusting with water to appropriate skin feeling parameters.

(6) And (5) filling after the inspection is qualified.

Example 3

The moisturizing and repairing mask comprises the following active ingredients in percentage by weight: 7% of tremella extract, 0.5% of ganoderma atrum extract, 5% of pseudo-ginseng extract, 3% of collagen extract, 2% of magnolia officinalis extract, 0.1% of licorice root extract, 4% of tea polyphenol, 7% of calendula extract, 3% of vitamin E, 0.5% of sericin, 5% of carbomer, 1% of hyaluronic acid, 5% of 1,3 butanediol, 6% of glycerol, 1% of preservative and the balance of water.

The preservative is p-hydroxyacetophenone. The collagen extract is obtained by processing cod skin protein.

(1) Extracting raw materials

Weighing raw materials of tremella, mangnolia officinalis, licorice root and calendula, and crushing to obtain raw material powder; the raw materials are purified respectively. Adding ethanol into the raw material powder, purifying under vacuum degree of-0.1 MPa and temperature of 55 deg.C, and repeatedly purifying for 3 times; for each purification, the mass ratio of the mixed raw material to ethanol was 1. Mixing the filtrates, and filtering with 200nm ceramic membrane to obtain clear solution. Concentrating the clear solution at 50 deg.C under-0.1 MPa to obtain extractive solution.

Wherein, the addition amount of the cellulase accounts for 0.1 percent of the addition weight of the pseudo-ginseng, the addition amount of the pectinase accounts for 0.1 percent of the addition weight of the pseudo-ginseng, and the addition amount of the alpha-amylase accounts for 0.1 percent of the addition weight of the pseudo-ginseng.

(5) Inactivating, adding Ganoderma atrum strain, fermenting at pH of 5 at 45 deg.C for 25 hr, detecting viscosity, centrifuging to obtain fermented supernatant, adding antiseptic, and adjusting with water to appropriate skin feeling parameters.

(6) And (5) filling after the inspection is qualified.

Example 4

The preparation method of the embodiment is basically the same as that of the embodiment 1, except that the raw materials of the moisturizing and repairing mask are different.

The moisturizing and repairing mask comprises the following active ingredients in parts by weight: 3.6% of tremella extract, 3.8% of ganoderma atrum extract, 1.4% of pseudo-ginseng extract, 1.2% of collagen extract, 0.8% of mangnolia officinalis extract, 2.2% of licorice root extract, 3.3% of tea polyphenol, 3% of calendula extract, 1.5% of vitamin E, 2.7% of silk fibroin, 3.2% of carbomer, 3.6% of hyaluronic acid, 2.4% of 1,3 butanediol, 3.3% of glycerol, 0.05% of preservative and the balance of water.

Example 5

The preparation method of this example is basically the same as that of example 2, except that the raw materials of the moisturizing repair mask are different.

The moisturizing and repairing mask comprises the following active ingredients in parts by weight: 5.4% of tremella extract, 2.3% of ganoderma atrum extract, 2.8% of pseudo-ginseng extract, 2.4% of collagen extract, 1.6% of mangnolia officinalis extract, 0.5% of licorice root extract, 2.1% of tea polyphenol, 5% of calendula extract, 2.5% of vitamin E, 2.7% of silk fibroin, 3.2% of carbomer, 3.6% of hyaluronic acid, 2.4% of 1,3 butanediol, 3.3% of glycerol, 0.05% of preservative and the balance of water.

Comparative example 1

This example differs from example 1 in that: the moisturizing and repairing mask does not contain the following raw materials: 4.8 percent of tremella extract and 3.1 percent of ganoderma atrum extract.

Comparative example 2

This example differs from example 1 in that: the raw materials of the moisturizing and repairing mask do not contain: 2.5 percent of pseudo-ginseng extract and 1.6 percent of collagen extract.

Comparative example 3

The present example differs from example 1 in that: the moisturizing and repairing mask does not contain the following raw materials: 3.1% of ganoderma atrum extract, 2.5% of pseudo-ginseng extract, 1.6% of collagen extract and 1.3% of magnolia bark extract.

Comparative example 4

This example differs from example 1 in that: the moisturizing and repairing mask does not contain the following raw materials: 1.3 percent of magnolia extract, 1.8 percent of licorice root extract and 2.2 percent of tea polyphenol.

The following are experimental verification data for the technical effects of examples 1 to 5 and comparative examples 1 to 4.

The test population: 90 volunteers of 22-57 years old, selected in the state of dry skin and water shortage, wherein 22 men and 68 women. Randomized into 9 groups of 10 people each. The test volunteers all perform sensitization test without anaphylaxis.

Experimental method 1

Preparing the raw materials of the examples and the comparative examples into a patch mask, cleaning hands of volunteers at room temperature, flatly shearing the patch mask into a square shape of 4 multiplied by 4cm, and selecting a blank group and soaking deionized water in mask paper; the facial mask of examples, comparative examples and blank group consisting of 10 selected persons aged 24-40 years, 1 male and 9 female were applied on the backs of the hands of the volunteers. Removing each substance after 30min and 60min, respectively, and measuring the skin of the subject applied with the facial mask with a digital skin moisture tester 0, 60, 120, and 240min after removing the facial mask to obtain skin moisture content.

The foregoing descriptions of specific exemplary embodiments of the present invention have been presented for purposes of illustration and description. It is not intended to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. The exemplary embodiments were chosen and described in order to explain certain principles of the invention and its practical application to enable one skilled in the art to make and use various exemplary embodiments of the invention and various alternatives and modifications as are suited to the particular use contemplated. It is intended that the scope of the invention be defined by the claims and their equivalents.

Claims

1. The moisturizing and repairing mask is characterized in that active ingredients of the mask at least comprise the following raw materials: tremella extract, ganoderma atrum extract, pseudo-ginseng extract, collagen extract, mangnolia officinalis extract, licorice root extract, tea polyphenol, calendula extract and vitamin E.

2. The moisturizing repair mask as claimed in claim 1, wherein the active ingredients of the mask comprise at least the following raw materials in percentage by weight: 2-7% of tremella extract, 0.5-5% of ganoderma atrum extract, 1-5% of pseudo-ginseng extract, 0.1-3% of collagen extract, 0.5-2% of magnolia officinalis extract, 0.1-4% of licorice root extract, 0.1-4% of tea polyphenol, 1-7% of calendula extract, 0.5-3% of vitamin E and the balance of water.

3. The moisturizing and repairing mask as claimed in claim 1, wherein the active ingredients of the mask comprise at least the following raw materials by weight percent: 3.6-5.4% of tremella extract, 2.3-3.8% of ganoderma atrum extract, 1.4-2.8% of pseudo-ginseng extract, 1.2-2.4% of collagen extract, 0.8-1.6% of mangnolia officinalis extract, 0.5-2.2% of licorice root extract, 2.1-3.3% of tea polyphenol, 3-5% of calendula extract, 1.5-2.5% of vitamin E and the balance of water.

4. The moisturizing repair mask of claim 1, further comprising the following raw materials: sericin, carbomer, hyaluronic acid, 1,3 butanediol, glycerol and a preservative.

5. The moisturizing repair mask as claimed in claim 4, further comprising the following raw materials in percentage by weight: 0.5-3.5% of sericin, 1-5% of carbomer, 1-5% of hyaluronic acid, 1-5% of 1,3 butanediol, 2-6% of glycerol and 0.01-1% of preservative.

6. The hydrating repair mask of claim 4 or 5 wherein the preservative is A91 or/and p-hydroxyacetophenone.

7. The hydrating mask for repairing according to claim 1, wherein the collagen extract is obtained by treating cod skin protein.

8. The preparation method of the moisturizing and repairing mask is characterized by comprising the following steps:

(1) Weighing Tremella extract, cortex Magnolia officinalis extract, glycyrrhrizae radix extract, tea polyphenols, herba Sidae Rhombifoliae extract, vitamin E, sericin, carbomer, hyaluronic acid, 1,3 butanediol, glycerol and water in a container at a certain proportion, and mixing well for use;

(3) Taking raw material codiaceae fish skin protein, treating the codiaceae fish skin protein by a biological enzymolysis method, drying to obtain powder, filtering by gel, and adding into a container according to a proportion when the molecular weight is less than 1000;

(4) After inactivation, adding ganoderma atrum strains for fermentation for a period of time, then obtaining fermentation supernatant through centrifugation, and adding a preservative;

(5) And (6) filling.

9. The preparation method of the moisturizing and repairing mask as claimed in claim 8, wherein raw materials of tremella, magnolia officinalis, licorice root and calendula are weighed and crushed to obtain raw material powder; adding water or ethanol into the raw material powder, purifying under vacuum degree of-0.1 MPa and temperature of 45-55 deg.C, and repeatedly purifying for 2-4 times; in each purification, the mass ratio of the mixed raw materials to water or ethanol is 1;

in the step (2), the addition amount of the cellulase accounts for 0.1-1% of the addition weight of the pseudo-ginseng, the addition amount of the pectinase accounts for 0.01-0.1% of the addition weight of the pseudo-ginseng, and the addition amount of the alpha-amylase accounts for 0.01-0.1% of the addition weight of the pseudo-ginseng.

10. The preparation method of the mask for moisturizing and repairing according to claim 8, wherein the fermentation in the step (3) is performed by controlling the pH value of the fermentation to be 5-6 and fermenting at 35-45 ℃ for 25-45 hours.