CN1152126C - Process for extracting essence oil from plant and its application - Google Patents
Process for extracting essence oil from plant and its application Download PDFInfo
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- CN1152126C CN1152126C CNB021138737A CN02113873A CN1152126C CN 1152126 C CN1152126 C CN 1152126C CN B021138737 A CNB021138737 A CN B021138737A CN 02113873 A CN02113873 A CN 02113873A CN 1152126 C CN1152126 C CN 1152126C
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Abstract
The present invention discloses a method for extracting plant essential oil and an application thereof. Leaves of scented wood trees are taken as raw materials, and then a washing and dirt removal step, a material preparation breaking step, a digestion extraction step, a distillation concentration step, etc. are carried out; thereby, the purely natural plant essential oil is extracted. The extracted purely natural plant essential oil can be eaten, has no toxic or side effect and has the pharmacologic therapeutic effect for benefiting livers, reducing fever, relieving inflammation, absorbing clots and tranquilizing mind. The plant essential oil can reinforce appetite and improve the immunizing power of the human body. The plant essential oil has wide application space in medical preparation industry, tobacco curing industry, brewing industry, food drink and perfume industry, cosmetic industry, etc. The method for extracting plant essential oil and the application thereof have very important social, environmental protection and economic benefits.
Description
Technical field:
The present invention relates to from the incense wood tree plant to extract the method for volatile oil and volatile oil at pharmacy, tobacco curing, brewage, the Application and Development technology in numerous industries such as food-drink and perfume, makeup, a kind of extracting method of essence oil from plant and application thereof specifically.
Background technology:
We know, essence is at tobacco curing, brewage, food-drink and pharmacy, all have in the various fields such as makeup very widely and use, to improving the mouthfeel of numerous life articles for daily use, the comfort level of sense of smell and improving the quality of products, abundant to a greater degree and satisfy people's living needs and all played active effect, the essence that uses roughly is divided into two classes at present: a class is with chemical process synthetic essence, this class is bigger with chemical process synthetic essence output, production cost is lower, another kind of is the pure natural essence that extracts from spice berry, because be subjected to the restriction of spice berry resource, the turnout of pure natural essence is few, price is also very expensive.For now, the essence that generally uses in numerous manufacturings field is chemical process synthetic essence mostly, though this employing chemical process synthetic essence also can meet the needs of production, but with regard to the comfortableness of the natural pure of its fragrance odor type and human body sense organ, still exist bigger gap than the pure natural essence that from spice berry, extracts, moreover, producing essence with chemical process pollutes bigger to physical environment, in throwing in use, inevitably can be to finished product, even also can cause certain pollution side effect to human body itself, in general industry hygienic standard the usage quantity of chemical process synthetic essence has also been made restrictive regulation, its application has certain limitation.For further satisfying the living needs of people's science health, create the ecotope space of environmental type, improve people's quality of life, develop spice berry resource, alternative with chemical process synthetic essence to a greater degree with the essence of pure natural, and the essence of developing pure natural to a greater extent at pharmacy, tobacco curing, brewage, the utilisation technology in numerous industries such as food, beverage, perfume and makeup, have very important social, environmental protection and economic benefit undoubtedly.
Summary of the invention:
The present invention is based on a kind of like this discovery and finishes, the contriver does to find when herbarium is gathered the wild incense wood tree of a kind lemon section in the open air, fragrance is dense pure, the odor type uniqueness, through introducing a fine variety the improvement cultivation and cultivating domestication for many years, now artificial propagation and successfully commerial growing survive, identify through the relevant expert: artificial culture 5 years, set all high 3～4 meters, 10～13 in single branches and leaves, aiphyllium lemon section yields positive results once every year, is pencil, ripe naked the taking on a red color of fruit, the phase of bearing fruit is more than 100 days, stem, branches and leaves, flowers and fruits are the strong citrus type aromatising flavour of volatilization throughout the year, through the plant quarantine analysis: stem, be rich in essence oil from plant in branches and leaves and the flowers and fruits cell.The objective of the invention is to propose to extract a kind of stem from above-mentioned incense wood tree, the branches and leaves method of essence oil from plant, another purpose is the Application and Development of above-mentioned essence oil from plant.
A kind of extracting method of essence oil from plant, it is a raw material with stem, the branches and leaves material of incense wood tree plant, is undertaken by following step successively:
(1) washing decontamination: with clear water stem, the branches and leaves material of incense wood tree plant are cleaned,
(2) fragmentation is got the raw materials ready: stem, the branches and leaves material of cleaned incense wood tree plant are cut into pieces, and control chip length :≤3mm,
It is characterized in that:
(3) boiling extraction: container is put in stem, the weighing of branches and leaves material of the incense wood tree plant that cuts into pieces, extraordinarily go into clear water by 2～3 of stem, branches and leaves material weight, constantly stir and soak extraction 20～40 minutes, the boiling 50～80 minutes of heating then, the control boiling temperature is 80～95 ℃, impels the protoplasma synersis in the cell walls of stem, branches and leaves, the cohesion distortion, the whole extractions of essence oil from plant in the cytolemma are dissolved in the water, and filter and remove residue promptly makes the extraction liquid of essence oil from plant
(4) distillation concentrates: the extraction liquid of essence oil from plant is put into still kettle, and controlled temperature is 95～100 ℃, the extraction liquid of essence oil from plant is distilled concentrated, can export purified essence oil from plant by the distillation conduit, and the packing bottling gets final product.
The present invention also has following technical characterictic:
The application of essence oil from plant in the medicine of preparation treatment or preventing cold.
The application of essence oil from plant in preparation treatment externally applied anti-inflammation pruritus medicine.
Essence oil from plant is done the application of spice additive in producing tobacco product.
The application of essence oil from plant in manufacturing perfume products.
The application of essence oil from plant in manufacturing air freshener.
Essence oil from plant is done the application of spice additive in manufacturing food.
Essence oil from plant is done the application of spice additive in manufacturing beverage.
Essence oil from plant is done the application of degradation agents in manufacturing plastics.
Embodiment:
Can help to understand technology contents of the present invention effectively by the following examples, but they are not limitation of the invention.
Embodiment one:
A kind of extracting method of essence oil from plant, it is a raw material with stem, the branches and leaves material of incense wood tree plant, is undertaken by following step successively:
(1) washing decontamination: with clear water stem, the branches and leaves material of incense wood tree plant are cleaned,
(2) fragmentation is got the raw materials ready: stem, the branches and leaves material of cleaned incense wood tree plant are cut into pieces, and control chip length :≤3mm,
(3) boiling extraction: container is put in stem, the weighing of branches and leaves material of the incense wood tree plant that cuts into pieces, extraordinarily go into clear water by 2.5 of stem, branches and leaves material weight, constantly stir and soak extraction 30 minutes, the boiling 70 minutes of heating then, the control boiling temperature is 95 ℃, impels the protoplasma synersis in the cell walls of stem, branches and leaves, the cohesion distortion, the whole extractions of essence oil from plant in the cytolemma are dissolved in the water, and filter and remove residue promptly makes the extraction liquid of essence oil from plant
(4) distillation concentrates: the extraction liquid of the essence oil from plant that makes behind the filter and remove residue is put into still kettle, and controlled temperature is 98 ℃, and the extraction liquid distillation is concentrated, and can export purified essence oil from plant by the distillation conduit, and the packing bottling gets final product.After measured: the stem of 100kg, branches and leaves material can extract the purified essence oil from plant of 1000ml.
The essence oil from plant that makes can be made the product of purity at different levels for using through vacuum concentration again.
Also spissated essence oil from plant further can be handled through spraying drying again, promptly be can be made into powdered plant essence powder product for using.
The plant essence oil production that makes as stated above is creamy white, and it is dense pure lasting to have strong pure natural citrus type aromatising flavour, fragrance.Because essence oil from plant of the present invention or flavor powder products at different levels are to extract with physics method from the incense wood tree plant of pure natural, do not add any additives and sanitas in leaching process, non-secondary pollution is the green product of pure natural.
Do the sterilizing air simulated experiment through Sichuan Province HSPH of Huaxi Medical Univ, put down in writing according to " survey report " (No. 980922): " at 20m
3The space in, controlled temperature is 28 ℃, relative humidity is 80.5%, sprays the essence oil from plant that the 10ml aforesaid method makes, and act on after 30 minutes can reaching 99.79% to the aerocolloidal killing rate of air golden yellow staphylococcus ".
Do the quantitative sterilization check through Chengdu, Sichuan Province health and epidemic prevention station again, put down in writing according to " survey report " (2000 No. 4006): " to golden yellow staphylococcus ATCC6538 10/1000 mass action 30 minutes; its average kill ratio is 99.94%; to intestinal bacteria 2/1000 mass action 20 minutes; its average kill ratio is 99.93%, ".According to surveying and determination: the plant essence oil production that makes as stated above, can take, without any side effects, the pharmacology curative effect that has sharp liver and clearing heat, anti-inflammatory stagnation resolvation and calm the nerves, take for a long time and can whet the appetite and improve body immunity, particularly to good treatment and prophylactic effect being arranged because of diseases such as weak regular, the intractable cat fever that causes, headache, pharyngolaryngitis.
Application Example one:
The medicine that the essence oil from plant of gained of the present invention is used for preparing the treatment flu, can improve result of treatment significantly, can improve curative ratio effectively,, the preventing cold disease also be had good effect because essence oil from plant has the effect that improves body immunity to cold disease.
Application Example two:
The plant essence oil production of gained of the present invention is used for preparation treatment externally applied anti-inflammation pruritus medicine, because essence oil from plant has extremely strong kill golden yellow staphylococcus and colibacillary effect, anti-inflammation and sterilization pruritus pharmacological effect can be improved significantly, the efficient and curative ratio of anti-inflammatory anti-itch medicine can be improved effectively.
Application Example three:
Essence oil from plant or flavor powder product with gained of the present invention, make spice additive and add the cigarette of producing in the pipe tobacco, repaying evaluation through relevant expert's product thinks: can obviously improve the mouthfeel of cigarette, improve the inlet purity and the suction comfort level of cigarette effectively, through certificate of analysis: coal-tar middle oil content of cigarette and nicotine content all have decline by a relatively large margin, obviously improved the grade of cigarette, shown that essence oil from plant (or flavor powder) product of gained of the present invention has the effect of objectionable impurities such as contained tar and Nicotine in the pipe tobacco that decomposes cigarette.
Application Example four:
The plant essence oil production of gained of the present invention is made the perfume products that raw material production is made, use evaluation to think through the relevant expert: can obviously improve the delicate fragrance purity of perfume and the level of comfort of human body sense of smell sense organ, and can prolong the time length of fragrance effectively.
Application Example five:
The plant essence oil production of gained of the present invention is made the air freshener product that raw material production is made, use evaluation to think through the relevant expert: can obviously improve effect with fresh air, and odor type uniqueness with fresh air, human body sense of smell sense organ is comfortable.
Application Example six:
The food-drink that the plant essence oil production of gained of the present invention is used to manufacture as spice additive, can obviously improve the color, smell and taste of food-drink, repaying evaluation through relevant expert's product thinks: the mouthfeel that can obviously improve food-drink, the results showed, can prolong the freshness date and the quality guaranteed period of food-drink effectively.
Application Example seven:
Essence oil from plant (or flavor powder) product of gained of the present invention allocated into as degradation agents produce the plastics that to degrade in the raw material; through examining and determine: can impel plastics to degrade step by step effectively until whole decomposition; thoroughly eliminate white pollution, have crucial meaning protecting environment effectively.
Claims (1)
1, a kind of extracting method of essence oil from plant is characterized in that stem, the branches and leaves material with the incense wood tree plant is raw material, carries out according to the following steps successively:
(1) washing decontamination: stem, the branches and leaves material of incense wood tree plant are cleaned with clear water;
(2) fragmentation is got the raw materials ready: stem, the branches and leaves material of cleaned incense wood tree plant are cut into pieces, and the control chip length is≤3 millimeters;
(3) boiling extraction: container is put in stem, the weighing of branches and leaves material of the incense wood tree plant that cuts into pieces, extraordinarily go into clear water by 2～3 of stem, branches and leaves material weight, stir and soak extraction 20～40 minutes, the boiling 50～80 minutes of heating, the control boiling temperature is 80～95 ℃, makes the extraction liquid of essence oil from plant;
(4) distillation concentrates: extraction liquid is put into still kettle, and controlled temperature is 95～100 ℃, and the extraction liquid distillation is concentrated, and exports purified essence oil from plant by the distillation conduit.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021138737A CN1152126C (en) | 2002-06-13 | 2002-06-13 | Process for extracting essence oil from plant and its application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021138737A CN1152126C (en) | 2002-06-13 | 2002-06-13 | Process for extracting essence oil from plant and its application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1386837A CN1386837A (en) | 2002-12-25 |
| CN1152126C true CN1152126C (en) | 2004-06-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB021138737A Expired - Fee Related CN1152126C (en) | 2002-06-13 | 2002-06-13 | Process for extracting essence oil from plant and its application |
Country Status (1)
| Country | Link |
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| CN (1) | CN1152126C (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1887389B (en) * | 2006-06-05 | 2010-05-26 | 阮慧聪 | Making process of playing cards with lasting fragrance |
| CN104651053A (en) * | 2013-11-22 | 2015-05-27 | 房世平 | Method for extracting essential oil by utilization of Xiangzi plant stems, branches and leaves |
| CN104651052A (en) * | 2013-11-22 | 2015-05-27 | 房世平 | Method for extracting essential oil by utilization of Xiangzi plant stems, branches and leaves |
| CN104651054A (en) * | 2013-11-22 | 2015-05-27 | 房世平 | Method for extracting essential oil by utilization of Xiangzi plant stems, branches and leaves |
| CN104403801A (en) * | 2014-12-19 | 2015-03-11 | 杨玉峰 | Method for extracting orange peel essential oil with surfactant aqueous solution |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5764608A (en) * | 1980-10-06 | 1982-04-19 | Shiseido Co Ltd | Preparation of low contact sensitinogenic jasmine oil |
| CN1012832B (en) * | 1985-11-13 | 1991-06-12 | 西泽润一 | Holder with semiconductor lighting device |
| CN1327038A (en) * | 2001-07-18 | 2001-12-19 | 孙传经 | Process for extracting rosemary antioxidant by super-critical reverse CO2 extraction |
-
2002
- 2002-06-13 CN CNB021138737A patent/CN1152126C/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5764608A (en) * | 1980-10-06 | 1982-04-19 | Shiseido Co Ltd | Preparation of low contact sensitinogenic jasmine oil |
| CN1012832B (en) * | 1985-11-13 | 1991-06-12 | 西泽润一 | Holder with semiconductor lighting device |
| CN1327038A (en) * | 2001-07-18 | 2001-12-19 | 孙传经 | Process for extracting rosemary antioxidant by super-critical reverse CO2 extraction |
Non-Patent Citations (1)
| Title |
|---|
| 《化工分离》 1995年10月 周荣琪《天然香料分离技术的研究》 * |
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| Publication number | Publication date |
|---|---|
| CN1386837A (en) | 2002-12-25 |
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Granted publication date: 20040602 |