CN115196883B - 一种钙钛矿介孔玻璃的制备方法及其应用 - Google Patents
一种钙钛矿介孔玻璃的制备方法及其应用 Download PDFInfo
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- CN115196883B CN115196883B CN202210874951.6A CN202210874951A CN115196883B CN 115196883 B CN115196883 B CN 115196883B CN 202210874951 A CN202210874951 A CN 202210874951A CN 115196883 B CN115196883 B CN 115196883B
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- perovskite
- mesoporous
- mesoporous glass
- perovskite precursor
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- 239000011521 glass Substances 0.000 title claims abstract description 96
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000002243 precursor Substances 0.000 claims abstract description 69
- 239000000463 material Substances 0.000 claims abstract description 35
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000007788 liquid Substances 0.000 claims abstract description 27
- 239000003960 organic solvent Substances 0.000 claims abstract description 16
- 238000001035 drying Methods 0.000 claims abstract description 14
- 150000004820 halides Chemical class 0.000 claims abstract description 11
- 238000002791 soaking Methods 0.000 claims abstract description 11
- 229910052792 caesium Inorganic materials 0.000 claims abstract description 8
- -1 cesium halide Chemical class 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims description 20
- 238000001291 vacuum drying Methods 0.000 claims description 10
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 4
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000000758 substrate Substances 0.000 abstract description 7
- 238000000137 annealing Methods 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract description 3
- 238000001179 sorption measurement Methods 0.000 abstract description 3
- 229910052719 titanium Inorganic materials 0.000 abstract description 3
- 239000010936 titanium Substances 0.000 abstract description 3
- 239000013078 crystal Substances 0.000 abstract description 2
- 230000015572 biosynthetic process Effects 0.000 description 5
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 4
- ZASWJUOMEGBQCQ-UHFFFAOYSA-L dibromolead Chemical compound Br[Pb]Br ZASWJUOMEGBQCQ-UHFFFAOYSA-L 0.000 description 4
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- XQPRBTXUXXVTKB-UHFFFAOYSA-M caesium iodide Chemical compound [I-].[Cs+] XQPRBTXUXXVTKB-UHFFFAOYSA-M 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 239000011358 absorbing material Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- LYQFWZFBNBDLEO-UHFFFAOYSA-M caesium bromide Chemical compound [Br-].[Cs+] LYQFWZFBNBDLEO-UHFFFAOYSA-M 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000000295 emission spectrum Methods 0.000 description 1
- 238000002189 fluorescence spectrum Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000031700 light absorption Effects 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000004020 luminiscence type Methods 0.000 description 1
- 238000003760 magnetic stirring Methods 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002159 nanocrystal Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/001—General methods for coating; Devices therefor
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/0095—Solution impregnating; Solution doping; Molecular stuffing, e.g. of porous glass
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K50/00—Organic light-emitting devices
- H10K50/10—OLEDs or polymer light-emitting diodes [PLED]
- H10K50/11—OLEDs or polymer light-emitting diodes [PLED] characterised by the electroluminescent [EL] layers
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Electroluminescent Light Sources (AREA)
- Glass Compositions (AREA)
Abstract
Description
Claims (7)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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CN202111357070 | 2021-11-16 | ||
CN2021113570709 | 2021-11-16 |
Publications (2)
Publication Number | Publication Date |
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CN115196883A CN115196883A (zh) | 2022-10-18 |
CN115196883B true CN115196883B (zh) | 2024-04-05 |
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CN202210874951.6A Active CN115196883B (zh) | 2021-11-16 | 2022-07-25 | 一种钙钛矿介孔玻璃的制备方法及其应用 |
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Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102002357A (zh) * | 2009-09-02 | 2011-04-06 | 海洋王照明科技股份有限公司 | 发光玻璃元件及其制备方法 |
CN103396147A (zh) * | 2008-02-25 | 2013-11-20 | 诺利塔克股份有限公司 | 氧分离膜元件、接合方法和接合材料 |
CN105489764A (zh) * | 2015-12-21 | 2016-04-13 | 成都新柯力化工科技有限公司 | 一种钙钛矿-云母光伏材料及其制备方法 |
CN106058049A (zh) * | 2016-06-17 | 2016-10-26 | 南京理工大学 | 一种大晶粒钙钛矿薄膜忆阻器存储单元的制备方法 |
CN106634986A (zh) * | 2016-11-09 | 2017-05-10 | 南京理工大学 | 一种提高钙钛矿钙钛矿稳定性的金属有机框架复合方法 |
CN108258126A (zh) * | 2018-01-29 | 2018-07-06 | 芜湖乐知智能科技有限公司 | 一种基于无机钙钛矿的光电探测器及其制备方法 |
CN111662705A (zh) * | 2020-05-21 | 2020-09-15 | 南京邮电大学 | 一种提高钙钛矿稳定性的方法 |
CN112993067A (zh) * | 2019-12-13 | 2021-06-18 | 中国科学院大连化学物理研究所 | 一种无机钙钛矿太阳能电池及其制备方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9305715B2 (en) * | 2014-08-01 | 2016-04-05 | Hunt Energy Enterprises Llc | Method of formulating perovskite solar cell materials |
US11203817B2 (en) * | 2017-06-30 | 2021-12-21 | Uchicago Argonne, Llc | One-step in situ solution growth for lead halide perovskite |
-
2022
- 2022-07-25 CN CN202210874951.6A patent/CN115196883B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103396147A (zh) * | 2008-02-25 | 2013-11-20 | 诺利塔克股份有限公司 | 氧分离膜元件、接合方法和接合材料 |
CN102002357A (zh) * | 2009-09-02 | 2011-04-06 | 海洋王照明科技股份有限公司 | 发光玻璃元件及其制备方法 |
CN105489764A (zh) * | 2015-12-21 | 2016-04-13 | 成都新柯力化工科技有限公司 | 一种钙钛矿-云母光伏材料及其制备方法 |
CN106058049A (zh) * | 2016-06-17 | 2016-10-26 | 南京理工大学 | 一种大晶粒钙钛矿薄膜忆阻器存储单元的制备方法 |
CN106634986A (zh) * | 2016-11-09 | 2017-05-10 | 南京理工大学 | 一种提高钙钛矿钙钛矿稳定性的金属有机框架复合方法 |
CN108258126A (zh) * | 2018-01-29 | 2018-07-06 | 芜湖乐知智能科技有限公司 | 一种基于无机钙钛矿的光电探测器及其制备方法 |
CN112993067A (zh) * | 2019-12-13 | 2021-06-18 | 中国科学院大连化学物理研究所 | 一种无机钙钛矿太阳能电池及其制备方法 |
CN111662705A (zh) * | 2020-05-21 | 2020-09-15 | 南京邮电大学 | 一种提高钙钛矿稳定性的方法 |
Non-Patent Citations (3)
Title |
---|
"Advances in metal halide perovskite lasers: synthetic strategies, morphology control, and lasing emission";Zhiping Hu, et al.;《Advanced Photonics》;第1-23页 * |
Fengxian Zhou, et al."Ultra-Rapid Synthesis of Perovskite Micro/Nanocubes Induced by Nanoporous Surface for Micro/Nanolasers".《Advance optical materials》.2023,第1-7页. * |
钙钛矿太阳能电池的制备工艺与光伏性能研究;李成辉;郑海松;刘俊;肖志明;招瑜;魏爱香;;人工晶体学报;20170715(07);97-102 * |
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CN115196883A (zh) | 2022-10-18 |
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Inventor after: Hu Zhiping Inventor after: Liu Tanghao Inventor after: Liu Zhengzheng Inventor after: Chen Chunlin Inventor after: He Jin Inventor after: Du Juan Inventor before: Hu Zhiping Inventor before: Chen Chunlin Inventor before: Liu Zhengzheng Inventor before: He Jin Inventor before: Du Juan |
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