CN115074890A - 一种防污防辐射面料及其制备工艺 - Google Patents

一种防污防辐射面料及其制备工艺 Download PDF

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CN115074890A
CN115074890A CN202210606651.XA CN202210606651A CN115074890A CN 115074890 A CN115074890 A CN 115074890A CN 202210606651 A CN202210606651 A CN 202210606651A CN 115074890 A CN115074890 A CN 115074890A
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parts
fiber
resin cotton
antifouling
cotton
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施经连
何淑理
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Jinjiang Ice Energy Garment Weaving Co ltd
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Abstract

本发明提供一种防污防辐射面料及其制备方法，包括经线和纬线，所述经线其原料各组成成分及其重量份数比为：桑蚕丝40‑55份、改性树脂棉2‑5份、纳米天丝2‑3份、马海毛纤维1‑4份、派力司纤维3‑5份、牛奶蛋白纤维4‑5份；所述纬线其原料各组成成分及其重量份数比为：桑蚕丝40‑50份、棉纶纤维2‑6份、改性树脂棉2‑5份、不锈钢纤维5‑8份、壳聚糖纤维5‑6份、纳米氧化锌纤维3‑5份、PTT纤维2‑4份、亚麻纤维1‑4份，通过制备经线和纬线，再将经线和纬线进行织造，最后将织造完成的面料浸入整理液中得到防污防辐射性能皆佳的面料。

Description

一种防污防辐射面料及其制备工艺
技术领域
本发明涉及纺织品技术领域，具体涉及一种防污防辐射面料及其制备工艺。
背景技术
随着经济的高速发展，我们所处的社会环境也越来越多样化复杂化。在日常生活中，我们总是会不可避免的碰到一些污渍，厨房的油污、饮料的滴溅、食物的掉落等，这些都是我们身边无形的服装杀手。需要一种能隔绝这些污渍的面料，而现有的疏水防污面料大多是通过直接在面料上设置涂层制备，其疏水防油性能较好，但直接在面料上设置涂层会极大地降低了面料的透气性，且手感较差，此外，防辐射的功能也是现如今消费者对面料以抵抗电子产品辐射的要求之一。
发明内容
针对现有技术中存在的不足之处，本发明提供一种防污防辐射面料及其制备工艺，采用如下技术方案：
作为本发明的第一方面提供一种防污防辐射面料，包括经线和纬线，所述经线其原料各组成成分及其重量份数比为：桑蚕丝40-55份、改性树脂棉2-5份、纳米天丝2-3份、马海毛纤维1-4份、派力司纤维3-5份、牛奶蛋白纤维4-5份；所述纬线其原料各组成成分及其重量份数比为：桑蚕丝40-50份、棉纶纤维2-6份、改性树脂棉2-5份、不锈钢纤维5-8份、壳聚糖纤维5-6份、纳米氧化锌纤维3-5份、PTT纤维2-4份、亚麻纤维1-4份。
进一步地，所述的马海毛线密度为1.70dtex；所述的牛奶蛋白纤维线密度为1.75dtex；所述的PTT纤维线密度为1.32dtex；所述的亚麻纤维线密度为1.26dtex；所述的壳聚糖纤维线密度为1.67dtex。
进一步地，所述的改性树脂棉制备方法为：取将树脂棉30-40份经丙酮、乙醇和去离子水洗净后在50-60℃下烘干，去除树脂棉中的杂质；取顺丁烯二酸酐25-30份、聚乙二醇12-18 份、1，2，3，4-丁烷四羧酸8-10份置于反应釜中，然后加入烘干的树脂棉进行浸渍接枝1.8-2h，然后进行等离子体照射，设置照射时间为3-5min，将经过等离子体照射后的接枝树脂棉用 75-80℃的去离子水振荡洗涤50-60min，再用干净的去离子水重复振荡洗涤，彻底除去附在其表面的单体和低聚物，然后将经过洗涤后的接枝树脂棉放入烘箱中在45-50℃下烘干即得到改性树脂棉。
作为本发明的第二方面提供一种如上所述的一种防污防辐射面料的制备工艺，包括以下步骤：
步骤1)经线的制备：将桑蚕丝40-55份、改性树脂棉2-5份、纳米天丝2-3份、马海毛纤维1-4份、派力司纤维3-5份、牛奶蛋白纤维4-5份先网络复合，然后在加捻度为1500-1600捻/米条件下完成加捻；
步骤2)纬线的制备：棉纶纤维2-6份、改性树脂棉2-5份、不锈钢纤维5-8份、壳聚糖纤维5-6份、纳米氧化锌纤维3-5份、PTT纤维2-4份、亚麻纤维1-4份进行网络复合作为芯线，再将桑蚕丝40-50份分成两股对芯线进行包覆，设置包覆机工艺中加捻度为1700捻/ 米，并且采用左右线包覆；
步骤3)将制备得到的经线和纬线在喷气织机上进行织造，车速为700-730r/min，采用二左二右的线型结构排列；
步骤4)将制备得到的面料浸入整理液中，二浸二轧，然后在50-60℃下预烘4min，再在 100-110℃下烘干，水洗后晾干即得到防污防辐射面料。
进一步地，所述的整理液原料各组成成分为：蚕蛹壳聚糖4-8份、柠檬酸2-5份、烷基酰胺甜菜碱3-5份、牵牛花提取液2-5份、酢浆草提取液3-4份、防污剂1-5份。
进一步地，按质量份数计，包括5～10份二甲基二烯丙基氯化铵-不饱和酸酐共聚物，5～ 8份质量份的轻稀土化合物，以及15份质量份的生物提取物；
所述轻稀土化合物为氧化镧和氧化铈中的一种或者多种混合物；
所述生物提取物为姜辣素和辣椒素中的一种或者多种混合物。
进一步地，所述二甲基二烯丙基氯化铵-不饱和酸酐共聚物的制备方法如下：
按质量份数计，将5份的不饱和酸酐、5～10份的二甲基二烯丙基氯化铵和20份的四氢呋喃搅拌均匀形成混合物体系，再在混合体系中加入5份的引发剂溶液，蒸馏回收四氢呋喃溶剂，得到二甲基二烯丙基氯化铵-不饱和酸酐共聚物。
有益效果
与现有技术相比，本发明具有的有益效果为：
本发明制备得到的面料具有良好的防污防辐射性能，同时抗菌性强，吸湿透气性强，穿着舒适、自然，相比于现有的面料在表层涂覆防污涂层虽然起到防污功能但阻碍了面料的透气性，本发明的面料不仅具备良好的防污性能，且面料的透气性良好。
具体实施方式
现详细描述根据本发明的实施例1-2。
实施例1
作为本发明的第一方面提供一种防污防辐射面料，包括经线和纬线，所述经线其原料各组成成分及其重量份数比为：桑蚕丝40份、改性树脂棉2份、纳米天丝2份、马海毛纤维1 份、派力司纤维3份、牛奶蛋白纤维4份；所述纬线其原料各组成成分及其重量份数比为：桑蚕丝40份、棉纶纤维2份、改性树脂棉2份、不锈钢纤维5份、壳聚糖纤维5份、纳米氧化锌纤维3份、PTT纤维2份、亚麻纤维1份。
进一步地，所述的马海毛线密度为1.70dtex；所述的牛奶蛋白纤维线密度为1.75dtex；所述的PTT纤维线密度为1.32dtex；所述的亚麻纤维线密度为1.26dtex；所述的壳聚糖纤维线密度为1.67dtex。
进一步地，所述的改性树脂棉制备方法为：取将树脂棉30份经丙酮、乙醇和去离子水洗净后在50℃下烘干，去除树脂棉中的杂质；取顺丁烯二酸酐25份、聚乙二醇12份、1，2，3，4-丁烷四羧酸8份置于反应釜中，然后加入烘干的树脂棉进行浸渍接枝2h，然后进行等离子体照射，设置照射时间为5min，将经过等离子体照射后的接枝树脂棉用80℃的去离子水振荡洗涤60min，再用干净的去离子水重复振荡洗涤，彻底除去附在其表面的单体和低聚物，然后将经过洗涤后的接枝树脂棉放入烘箱中在50℃下烘干即得到改性树脂棉。
作为本发明的第二方面提供一种如上所述的一种防污防辐射面料的制备工艺，包括以下步骤：
步骤1)经线的制备：将桑蚕丝40份、改性树脂棉2份、纳米天丝2份、马海毛纤维1份、派力司纤维3份、牛奶蛋白纤维4份先网络复合，然后在加捻度为1500捻/米条件下完成加捻；
步骤2)纬线的制备：棉纶纤维2份、改性树脂棉2份、不锈钢纤维5份、壳聚糖纤维5份、纳米氧化锌纤维3份、PTT纤维2份、亚麻纤维1份进行网络复合作为芯线，再将桑蚕丝40份分成两股对芯线进行包覆，设置包覆机工艺中加捻度为1700捻/米，并且采用左右线包覆；
步骤3)将制备得到的经线和纬线在喷气织机上进行织造，车速为700r/min，采用二左二右的线型结构排列；
步骤4)将制备得到的面料浸入整理液中，二浸二轧，然后在60℃下预烘4min，再在110℃下烘干，水洗后晾干即得到防污防辐射面料。
进一步地，所述的整理液原料各组成成分为：蚕蛹壳聚糖4份、柠檬酸2份、烷基酰胺甜菜碱3份、牵牛花提取液2份、酢浆草提取液3份、防污剂1份。
进一步地，按质量份数计，包括5份二甲基二烯丙基氯化铵-不饱和酸酐共聚物，5份质量份的轻稀土化合物，以及15份质量份的生物提取物；
所述轻稀土化合物为氧化铈；所述生物提取物为辣椒素中。
进一步地，所述二甲基二烯丙基氯化铵-不饱和酸酐共聚物的制备方法如下：
按质量份数计，将5份的不饱和酸酐、5份的二甲基二烯丙基氯化铵和20份的四氢呋喃搅拌均匀形成混合物体系，再在混合体系中加入5份的引发剂溶液，蒸馏回收四氢呋喃溶剂，得到二甲基二烯丙基氯化铵-不饱和酸酐共聚物。
在本实施例中，将完成的面料进行测试，易去污性能测试方法参照FZ/T14021-2011《防水、防油、易去污、免烫印染布》，其在经洗涤次数达10次时，去污等级为3级，在经洗涤次数为20次时，去污等级仍能达到2级，且在抗电离辐射的测试中，防电磁辐射性能测试中屏蔽率为99.55％；柔软等级为2级；透气率为686.22mm/s。
实施例2
作为本发明的第一方面提供一种防污防辐射面料，包括经线和纬线，所述经线其原料各组成成分及其重量份数比为：桑蚕丝55份、改性树脂棉5份、纳米天丝3份、马海毛纤维4 份、派力司纤维5份、牛奶蛋白纤维5份；所述纬线其原料各组成成分及其重量份数比为：桑蚕丝50份、棉纶纤维6份、改性树脂棉5份、不锈钢纤维8份、壳聚糖纤维6份、纳米氧化锌纤维5份、PTT纤维4份、亚麻纤维4份。
进一步地，所述的马海毛线密度为1.70dtex；所述的牛奶蛋白纤维线密度为1.75dtex；所述的PTT纤维线密度为1.32dtex；所述的亚麻纤维线密度为1.26dtex；所述的壳聚糖纤维线密度为1.67dtex。
进一步地，所述的改性树脂棉制备方法为：取将树脂棉40份经丙酮、乙醇和去离子水洗净后在50-60℃下烘干，去除树脂棉中的杂质；取顺丁烯二酸酐30份、聚乙二醇18份、1，2，3，4-丁烷四羧酸10份置于反应釜中，然后加入烘干的树脂棉进行浸渍接枝2h，然后进行等离子体照射，设置照射时间为5min，将经过等离子体照射后的接枝树脂棉用80℃的去离子水振荡洗涤60min，再用干净的去离子水重复振荡洗涤，彻底除去附在其表面的单体和低聚物，然后将经过洗涤后的接枝树脂棉放入烘箱中在50℃下烘干即得到改性树脂棉。
作为本发明的第二方面提供一种如上所述的一种防污防辐射面料的制备工艺，包括以下步骤：
步骤1)经线的制备：将桑蚕丝55份、改性树脂棉5份、纳米天丝3份、马海毛纤维4份、派力司纤维5份、牛奶蛋白纤维5份先网络复合，然后在加捻度为1600捻/米条件下完成加捻；
步骤2)纬线的制备：棉纶纤维6份、改性树脂棉5份、不锈钢纤维8份、壳聚糖纤维6份、纳米氧化锌纤维5份、PTT纤维4份、亚麻纤维4份进行网络复合作为芯线，再将桑蚕丝50份分成两股对芯线进行包覆，设置包覆机工艺中加捻度为1700捻/米，并且采用左右线包覆；
步骤3)将制备得到的经线和纬线在喷气织机上进行织造，车速为730r/min，采用二左二右的线型结构排列；
步骤4)将制备得到的面料浸入整理液中，二浸二轧，然后在60℃下预烘4min，再在110℃下烘干，水洗后晾干即得到防污防辐射面料。
进一步地，所述的整理液原料各组成成分为：蚕蛹壳聚糖8份、柠檬酸5份、烷基酰胺甜菜碱5份、牵牛花提取液5份、酢浆草提取液4份、防污剂5份。
进一步地，按质量份数计，包括10份二甲基二烯丙基氯化铵-不饱和酸酐共聚物，8份质量份的轻稀土化合物，以及15份质量份的生物提取物；
所述轻稀土化合物为氧化铈；所述生物提取物为辣椒素。
进一步地，所述二甲基二烯丙基氯化铵-不饱和酸酐共聚物的制备方法如下：
按质量份数计，将5份的不饱和酸酐、10份的二甲基二烯丙基氯化铵和20份的四氢呋喃搅拌均匀形成混合物体系，再在混合体系中加入5份的引发剂溶液，蒸馏回收四氢呋喃溶剂，得到二甲基二烯丙基氯化铵-不饱和酸酐共聚物。
在本实施例中，将完成的面料进行测试，易去污性能测试方法参照FZ/T14021-2011《防水、防油、易去污、免烫印染布》，其在经洗涤次数达10次时，去污等级为3级，在经洗涤次数为20次时，去污等级仍能达到2级，且在抗电离辐射的测试中，防电磁辐射性能测试中屏蔽率为99.64％；柔软等级为2级；透气率为688.35mm/s。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点，对于本领域技术人员而言，显然本发明不限于上述示范性实施例的细节，而且在不背离本发明的精神或基本特征的情况下，能够以其他的具体形式实现本发明。因此，无论从哪一点来看，均应将实施例看作是示范性的，而且是非限制性的，本发明的范围由所附权利要求而不是上述说明限定，因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内。
此外，应当理解，虽然本说明书按照实施方式加以描述，但并非每个实施方式仅包含一个独立的技术方案，说明书的这种叙述方式仅仅是为清楚起见，本领域技术人员应当将说明书作为一个整体，各实施例中的技术方案也可以经适当组合，形成本领域技术人员可以理解的其他实施方式。

Claims (7)

1.一种防污防辐射面料，其特征在于：包括经线和纬线，所述经线其原料各组成成分及其重量份数比为：桑蚕丝40-55份、改性树脂棉2-5份、纳米天丝2-3份、马海毛纤维1-4份、派力司纤维3-5份、牛奶蛋白纤维4-5份；所述纬线其原料各组成成分及其重量份数比为：桑蚕丝40-50份、棉纶纤维2-6份、改性树脂棉2-5份、不锈钢纤维5-8份、壳聚糖纤维5-6份、纳米氧化锌纤维3-5份、PTT纤维2-4份、亚麻纤维1-4份。
2.根据权利要求1所述的一种防污防辐射面料的制备工艺，其特征在于：所述的马海毛线密度为1.70dtex；所述的牛奶蛋白纤维线密度为1.75dtex；所述的PTT纤维线密度为1.32dtex；所述的亚麻纤维线密度为1.26dtex；所述的壳聚糖纤维线密度为1.67dtex。
3.根据权利要求1所述的一种防污防辐射面料的制备工艺，其特征在于：所述的改性树脂棉制备方法为：取将树脂棉30-40份经丙酮、乙醇和去离子水洗净后在50-60℃下烘干，去除树脂棉中的杂质；取顺丁烯二酸酐25-30份、聚乙二醇12-18份、1，2，3，4-丁烷四羧酸8-10份置于反应釜中，然后加入烘干的树脂棉进行浸渍接枝1.8-2h，然后进行等离子体照射，设置照射时间为3-5min，将经过等离子体照射后的接枝树脂棉用75-80℃的去离子水振荡洗涤50-60min，再用干净的去离子水重复振荡洗涤，彻底除去附在其表面的单体和低聚物，然后将经过洗涤后的接枝树脂棉放入烘箱中在45-50℃下烘干即得到改性树脂棉。
4.一种制备如权利要求1-3任一所述的一种防污防辐射面料的方法，其特征在于：包括以下步骤：
步骤1)经线的制备：将桑蚕丝40-55份、改性树脂棉2-5份、纳米天丝2-3份、马海毛纤维1-4份、派力司纤维3-5份、牛奶蛋白纤维4-5份先网络复合，然后在加捻度为1500-1600捻/米条件下完成加捻；
步骤2)纬线的制备：棉纶纤维2-6份、改性树脂棉2-5份、不锈钢纤维5-8份、壳聚糖纤维5-6份、纳米氧化锌纤维3-5份、PTT纤维2-4份、亚麻纤维1-4份进行网络复合作为芯线，再将桑蚕丝40-50份分成两股对芯线进行包覆，设置包覆机工艺中加捻度为1700捻/米，并且采用左右线包覆；
步骤3)将制备得到的经线和纬线在喷气织机上进行织造，车速为700-730r/min，采用二左二右的线型结构排列；
步骤4)将制备得到的面料浸入整理液中，二浸二轧，然后在50-60℃下预烘4min，再在100-110℃下烘干，水洗后晾干即得到防污防辐射面料。
5.根据权利要求4所述的一种防污防辐射面料的制备工艺，其特征在于：所述的整理液原料各组成成分为：蚕蛹壳聚糖4-8份、柠檬酸2-5份、烷基酰胺甜菜碱3-5份、牵牛花提取液2-5份、酢浆草提取液3-4份、防污剂1-5份。
6.根据权利要求5所述的一种防污防辐射面料的制备工艺，其特征在于：按质量份数计，包括5～10份二甲基二烯丙基氯化铵-不饱和酸酐共聚物，5～8份质量份的轻稀土化合物，以及15份质量份的生物提取物；
所述轻稀土化合物为氧化镧和氧化铈中的一种或者多种混合物；
所述生物提取物为姜辣素和辣椒素中的一种或者多种混合物。
7.根据权利要求6所述的一种防污防辐射面料的制备工艺，其特征在于：所述二甲基二烯丙基氯化铵-不饱和酸酐共聚物的制备方法如下：
按质量份数计，将5份的不饱和酸酐、5～10份的二甲基二烯丙基氯化铵和20份的四氢呋喃搅拌均匀形成混合物体系，再在混合体系中加入5份的引发剂溶液，蒸馏回收四氢呋喃溶剂，得到二甲基二烯丙基氯化铵-不饱和酸酐共聚物。
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CN103361842A (zh) * 2013-08-07 2013-10-23 吴江市旭阳纺织有限公司 经纬编织防污面料
CN206956261U (zh) * 2017-07-11 2018-02-02 浙江创达纺织有限公司 一种防污抑菌经编面料
CN108914327A (zh) * 2018-07-18 2018-11-30 广西南宁桂尔创环保科技有限公司 一种抗菌防辐射真丝绸面料及其制备方法
CN111574662A (zh) * 2020-06-05 2020-08-25 深圳海龙舰船涂料科技有限公司 二甲基二烯丙基氯化铵-不饱和酸酐共聚物的制备方法、防污剂及其制备方法和防污涂料

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* Cited by examiner, † Cited by third party
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CN103361842A (zh) * 2013-08-07 2013-10-23 吴江市旭阳纺织有限公司 经纬编织防污面料
CN206956261U (zh) * 2017-07-11 2018-02-02 浙江创达纺织有限公司 一种防污抑菌经编面料
CN108914327A (zh) * 2018-07-18 2018-11-30 广西南宁桂尔创环保科技有限公司 一种抗菌防辐射真丝绸面料及其制备方法
CN111574662A (zh) * 2020-06-05 2020-08-25 深圳海龙舰船涂料科技有限公司 二甲基二烯丙基氯化铵-不饱和酸酐共聚物的制备方法、防污剂及其制备方法和防污涂料

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Application publication date: 20220920