CN114988946A - High-temperature-resistant coating agent for non-heading Chinese cabbage seeds and preparation and use methods thereof - Google Patents

High-temperature-resistant coating agent for non-heading Chinese cabbage seeds and preparation and use methods thereof Download PDF

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CN114988946A
CN114988946A CN202210625129.6A CN202210625129A CN114988946A CN 114988946 A CN114988946 A CN 114988946A CN 202210625129 A CN202210625129 A CN 202210625129A CN 114988946 A CN114988946 A CN 114988946A
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parts
coating agent
chinese cabbage
seeds
temperature
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Inventor
袁凌云
张胜男
汪承刚
张利婷
黄兴学
朱世东
侯金锋
唐小燕
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Anhui Wanjiang Vegetable Industry Technology Research Institute Co ltd
Anhui Agricultural University AHAU
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Anhui Wanjiang Vegetable Industry Technology Research Institute Co ltd
Anhui Agricultural University AHAU
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F11/00Other organic fertilisers
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C1/00Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
    • A01C1/06Coating or dressing seed
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Soil Sciences (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Pretreatment Of Seeds And Plants (AREA)

Abstract

The invention provides a high-temperature-resistant coating agent for non-heading Chinese cabbage seeds, which comprises the following raw materials in parts by weight: nano TiO 2 2 1-5 parts of brassinosteroid, 0.15-0.25 part of phytotrophin, 0.1-0.5 part of plant-feeding peptide, 100.1-0.5 part of ubiquinone, 0.1-0.5 part of lycopene, 0.1-0.5 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 5-10 parts of emulsifier. The invention also provides a preparation method and a using method of the coating agent. The invention has the advantages that: the coating agent can obviously reduce environmental pollution, improve the high temperature resistance of the non-heading Chinese cabbage seeds, improve the germination rate and activity of the seeds and enhance the stress resistance of seedlings.

Description

High-temperature-resistant coating agent for non-heading Chinese cabbage seeds and preparation and use methods thereof
Technical Field
The invention relates to the technical field of coating agents, in particular to a high-temperature-resistant coating agent for non-heading Chinese cabbage seeds and a preparation method and a using method thereof.
Background
Non-heading Chinese cabbage (Brassica campestris ssp. Chinese Makino) belongs to Brassicaceae (Cruciferae) Brassica (Brassica) Brassica subspecies, commonly called pakchoi, cabbage and rape, has high content of nutrients such as vitamins and minerals, and is a main vegetable on a dining table in southern areas of China. Because the non-heading Chinese cabbages are cool in nature and do not resist high temperature, the non-heading Chinese cabbages are mainly planted in various parts of China in autumn and winter at present, but with the occurrence of global warming and southern climate problems, the sowing temperature is not suitable for the germination of seeds, so that the non-heading Chinese cabbages have low germination rate and slow reproductive growth, the plants are short and small in the harvesting period, the survival rate is low, the influence of low yield, poor quality and the like is caused, and the development of the non-heading Chinese cabbages industry is severely limited. Therefore, the improvement of the high temperature resistance of the non-heading Chinese cabbage seeds becomes a problem to be solved urgently at present.
The seed coating agent is a technology for uniformly adhering components such as chemical fertilizers, pesticides and nutrient elements necessary for plant growth on the surface of seeds by using an adhesive or a film-forming agent, can pellet the seeds, improve the mechanical sowing efficiency, provide a microscopic living environment for the seeds, and quickly absorb nutrients in the coating agent after the seeds are sowed so as to promote the seed development. The coating agent has the characteristics of improving the germination rate of seeds, promoting the growth of seedlings, reducing the occurrence of diseases, pests and weeds in fields, reducing the use of pesticides and chemical fertilizers and the like, can achieve the aims of high yield and quality of agricultural products and reducing environmental pollution, and is a scientific concept of novel agricultural development.
According to research, the high-temperature-resistant seed coating agent has an obvious improvement effect on the problems of low germination rate, weak growth potential and the like of seeds subjected to high temperature, but the high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds does not appear in the current market.
Disclosure of Invention
The invention aims to solve the technical problem of providing a high-temperature-resistant coating agent for non-heading Chinese cabbage seeds and a preparation method and a using method thereof.
The invention adopts the following technical scheme to solve the technical problems:
a high-temperature-resistant coating agent for non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 1-5 parts of brassinosteroid, 0.15-0.25 part of phytotrophin, 0.1-0.5 part of plant-feeding peptide, 100.1-0.5 part of ubiquinone, 0.1-0.5 part of lycopene, 0.1-0.5 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 5-10 parts of emulsifier.
As one of the preferable modes of the invention, the feed comprises the following raw materials in parts by weight: nano TiO 2 2 3 parts, 0.25 part of brassinosteroid, 0.3 part of plant-feeding peptide, 100.5 parts of ubiquinone, 0.3 part of lycopene, 0.3 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
As one of the preferable modes of the invention, the compound fertilizer comprises basic elements and trace elements; the basic element is N, P, K, and the microelements are B, Cu, Fe, Mn, Zn and Mo.
In a preferable mode of the invention, the addition amount of N, P, K in the compound fertilizer is 10 parts by mass, and the total addition amount of trace elements is 0.02-0.03 part by mass.
As one of the preferred modes of the present invention, the emulsifier comprises poloxamer and sucrose ester; the mixing ratio of the poloxamer to the sucrose ester is 1: 1.
in a preferred embodiment of the present invention, the coating agent is capable of resisting a high temperature of 32 to 37 ℃ in the non-heading Chinese cabbage seed.
A preparation method of the high-temperature resistant coating agent for the non-heading Chinese cabbage seeds comprises the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the brassinosteroid, the plant feeding peptide, the ubiquinone 10, the lycopene, the rutin, the hymexazol and the imidacloprid in the suspension according to the parts by weight; finally, adding the residual starch and the emulsifier into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
A use method of the high-temperature resistant coating agent for the non-heading Chinese cabbage seeds comprises the steps of mixing and dressing the coating agent until the surface of the non-heading Chinese cabbage seeds is coated with a uniform protective layer of 0.5-0.8 mm; and then, fishing out the seeds, and placing the seeds in a dryer for drying at the temperature of 20-24 ℃ and the humidity of 10% -15% for 6-8 h.
In the present invention, the nano TiO is 2 Is a novel nano material, has good ultraviolet shielding effect and good photocatalytic property, antibacterial property and chemical property stability; adding nano TiO into coating agent 2 The high temperature resistance of the seeds can be improved, the germination of the non-heading Chinese cabbage seeds and the activity of the seeds are stably promoted, the stress resistance of plants is improved, harmful ingredients in soil can be degraded, and the environmental pollution is reduced.
The brassinosteroid is a plant hormone, and has the capabilities of stimulating the differentiation of adventitious roots of plants, improving the high temperature resistance of the plants and coordinating the nutrient supply in the plants.
The plant feeding peptide can supplement medium trace elements required by plants, improve the utilization rate of fertilizer, improve cell metabolism, promote plant growth and enhance the capability of the plants to adapt to adverse environments.
The ubiquinone 10, the lycopene and the rutin have oxidation resistance, can improve the high temperature resistance of seeds and promote the growth of plants.
The hymexazol is a systemic bactericide, can efficiently inhibit or kill pathogenic fungi mycelia with low toxicity, and can promote the survival rate of crops.
The imidacloprid is a systemic insecticide, has the characteristics of high efficiency and low toxicity, can prevent and control aphids, plant hoppers, thrips and other pests, does not influence the growth of crops, and has the pesticide effect lasting for about 25 days.
Compared with the prior art, the invention has the advantages that:
(1) the invention utilizes nano TiO 2 The high-temperature resistance of the seeds can be effectively improved under the synergistic action of the brassinosteroid, the plant feeding peptide, the ubiquinone 10, the lycopene and the rutin, the germination of the non-heading Chinese cabbage seeds and the vitality of the seeds are stably promoted, and the stress resistance of plants is improved;
(2) according to the invention, the high temperature resistance of the seeds is improved, and at the same time, as the plant hormone, the pesticide, the bactericide and the fertilizer are added, stable and appropriate environmental conditions can be provided for the germination of the seeds and the growth of seedlings, so that the purposes of strengthening the seedlings and the roots are achieved;
(3) the coating agent can also degrade harmful ingredients in soil and reduce environmental pollution.
Detailed Description
The following examples are given for the detailed implementation and specific operation of the present invention, but the scope of the present invention is not limited to the following examples.
Example 1
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 1 part, 0.2 part of brassinosteroid, 0.5 part of plant feeding peptide, 100.5 parts of ubiquinone, 0.3 part of lycopene, 0.3 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 5 parts of emulsifier.
Specifically, in this embodiment, the compound fertilizer includes basic elements and trace elements; the basic element is N, P, K, and the microelements are B, Cu, Fe, Mn, Zn and Mo. Furthermore, according to the mass parts, the addition amount of N, P, K is 10 parts respectively, and the total addition amount of trace elements is 0.02 part in the compound fertilizer.
Specifically, in this embodiment, the emulsifier includes poloxamer and sucrose ester; the mixing mass ratio of the poloxamer to the sucrose ester is 1: 1.
the preparation method comprises the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the brassinosteroid, the plant feeding peptide, the ubiquinone 10, the lycopene, the rutin, the hymexazol and the imidacloprid in the suspension according to the parts by weight; finally, adding the residual starch and the emulsifying agent into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
Example 2
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 3 parts of brassinosteroid, 0.25 part of phytotrophin, 0.3 part of phytotrophin, 100.5 parts of ubiquinone, 0.3 part of lycopene, 0.3 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
Specifically, in this embodiment, the compound fertilizer includes basic elements and trace elements; the basic element is N, P, K, and the microelements are B, Cu, Fe, Mn, Zn and Mo. Furthermore, in the compound fertilizer, the addition amount of N, P, K is 10 parts respectively, and the total addition amount of trace elements is 0.025 part.
Specifically, in this embodiment, the emulsifier includes poloxamer and sucrose ester; the mixing mass ratio of the poloxamer to the sucrose ester is 1: 1.
the preparation method comprises the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, the brassinosteroid, the plant feeding peptide and the plant feeding peptide are mixed according to the corresponding weight parts,Adding ubiquinone 10, lycopene, rutin, hymexazol and imidacloprid into the suspension; finally, adding the residual starch and the emulsifier into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
Example 3
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 5 parts of brassinosteroid, 0.15 part of phytol, 0.1 part of plant-feeding peptide, 100.1 parts of ubiquinone, 0.5 part of lycopene, 0.5 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 9 parts of emulsifier.
Specifically, in this embodiment, the compound fertilizer includes basic elements and trace elements; the basic element is N, P, K, and the microelements are B, Cu, Fe, Mn, Zn and Mo. Furthermore, according to the mass parts, the addition amount of N, P, K is 10 parts respectively, and the total addition amount of trace elements is 0.025 part in the compound fertilizer.
Specifically, in this embodiment, the emulsifier includes poloxamer and sucrose ester; the mixing mass ratio of the poloxamer to the sucrose ester is 1: 1.
the preparation method comprises the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the brassinosteroid, the plant feeding peptide, the ubiquinone 10, the lycopene, the rutin, the hymexazol and the imidacloprid in the suspension according to the parts by weight; finally, adding the residual starch and the emulsifier into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
Example 4
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 5 parts of brassinosteroid, 0.15 part of phytol, 0.1 part of plant feeding peptide, 100.25 parts of ubiquinone, 0.1 part of lycopene, 0.1 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 10 parts of emulsifier.
Specifically, in this embodiment, the compound fertilizer includes basic elements and trace elements; the basic element is N, P, K, and the microelements are B, Cu, Fe, Mn, Zn and Mo. Furthermore, according to the mass parts, the addition amount of N, P, K is 10 parts respectively, and the total addition amount of trace elements is 0.03 part.
Specifically, in this embodiment, the emulsifier includes poloxamer and sucrose ester; the mixing mass ratio of the poloxamer to the sucrose ester is 1: 1.
the preparation method comprises the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the brassinosteroid, the plant feeding peptide, the ubiquinone 10, the lycopene, the rutin, the hymexazol and the imidacloprid in the suspension according to the parts by weight; finally, adding the residual starch and the emulsifier into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
Example 5
The application method of the coating agent in the embodiment 1-4 comprises the following steps:
mixing the coating agent and seed dressing until the surface of the non-heading Chinese cabbage seed is coated with a uniform 0.5mm protective layer; then, the seeds are fished out and placed in a dryer for drying at the temperature of 20 ℃ and the humidity of 10 percent for 6 hours.
Example 6
The application method of the coating agent of the embodiment 1-4 comprises the following steps:
mixing the coating agent and seed dressing until the surface of the non-heading Chinese cabbage seeds is coated with a uniform 0.6mm protective layer; then, the seeds are fished out and placed in a dryer to be dried for 7 hours at the temperature of 22 ℃ and the humidity of 12 percent.
Example 7
The application method of the coating agent in the embodiment 1-4 comprises the following steps:
mixing the coating agent and seed dressing until the surface of the non-heading Chinese cabbage seeds is coated with a uniform 0.8mm protective layer; then, the seeds are fished out and placed in a dryer for drying at the temperature of 24 ℃ and the humidity of 15 percent for 8 hours.
Experimental verification of the coating agents of the above examples 1-4:
the non-heading Chinese cabbage variety is Hefeng-2, seeds are provided by a vegetable genetic breeding team of the university of agriculture in Anhui, and seeds with full seeds and consistent sizes are selected as test materials.
Experimental treatment: the coating agent was produced according to the preparation and production methods of the corresponding examples (examples 1 to 4) (application method of coating agent refer to example 6), the coated seeds and the uncoated seeds were obtained, and were sown into 105-hole trays, 3 replicates were designed at the same time, the trays were cultured in a climatic chamber, 4 temperature gradients of 37 ℃, 33 ℃, 29 ℃ and 25 ℃ (room temperature) were set, and seed germination vigor was counted at 24h after sowing, seed germination rate was counted at 48h, and seedling height, root length, overground part fresh weight and root fresh weight were measured at 45 days.
Germination potential (%) (number of germination seeds/number of test seeds at 24 h) × 100%;
germination rate (%) - (number of germinated seeds/number of seeds tested on day 48) × 100%.
The experimental results are as follows: as shown in tables 1, 2-1 and 2-2.
TABLE 1 influence of different examples on the germination vigour and germination rate of non-heading Chinese cabbage seeds
Figure BDA0003676830440000081
(Note: in the table, the lower case letters indicate that there is a significant difference (p <0.05) between different temperatures in the same example, and the lower case letters indicate that there is no significant difference in the same example)
Table 1 shows that: the germination vigor and the germination rate of the uncoated seeds and the coated seeds are gradually reduced along with the increase of the temperature; when the seeds are stressed by high temperature, the germination potential and the germination rate of the uncoated seeds are greatly reduced, and the reduction range of the germination potential and the germination rate of the coated seeds is smaller; and the germination potential and the germination rate of the coating agent seeds are higher than those of the uncoated seeds under the same temperature treatment.
Therefore, the composite coating agent can obviously improve the germination of the non-heading Chinese cabbage seeds stressed by high temperature.
TABLE 2-1 Effect of different examples on the seedling height and root length of non-heading Chinese cabbage
Figure BDA0003676830440000091
(Note: in the table, different lower case letters indicate that there is a significant difference (p <0.05) between different temperatures in the same example, and lower case letters indicate that there is no significant difference between different temperatures in the same example)
TABLE 2-2 influence of different examples on the fresh weight of overground parts and roots of non-heading Chinese cabbage
Figure BDA0003676830440000092
(Note: in the table, different lower case letters indicate that there is a significant difference (p <0.05) between different temperatures in the same example, and lower case letters indicate that there is no significant difference between different temperatures in the same example)
Tables 2-1 and 2-2 show: the height, the root length, the fresh weight of the overground part and the fresh weight of the roots of the uncoated seedlings are reduced along with the rise of the temperature, and when the temperature reaches 37 ℃, the growth vigor of the plants is obviously inhibited; compared with the uncoated seed, the seed of the coating agent can obviously improve the seedling height, the root length, the fresh weight of the overground part and the fresh weight of the root of the seedling under the high-temperature stress, and the damage of the high temperature to the seedling is effectively reduced.
Therefore, the compound coating agent can obviously improve the growth vigor of the non-heading Chinese cabbage plants stressed by high temperature, and the coating agent in the corresponding raw material formula in the embodiment 2 has the best use effect.
Comparative example:
comparative example 1
Comparative example of this exampleA high-temperature-resistant coating agent for non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 5 parts of hymexazol, 5 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, adding hymexazol and imidacloprid in corresponding parts by weight into the suspension; finally, adding the residual starch and the emulsifying agent into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
Comparative example 2
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: 0.25 part of brassinosteroid, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
firstly, slowly adding 10 parts of starch into water, then adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the brassinosteroid, the hymexazol and the imidacloprid in corresponding parts by weight into the mixed solution; and finally, adding the residual starch and the emulsifier, and fully and uniformly stirring to obtain the starch-emulsifier composite.
Comparative example 3
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: 0.5 part of plant feeding peptide, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
firstly, slowly adding 10 parts of starch into water, then adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the plant feeding peptide, the hymexazol and the imidacloprid in corresponding parts by weight into the mixed solution; and finally, adding the residual starch and the emulsifier, and fully and uniformly stirring to obtain the starch-emulsifier composite.
Comparative example 4
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: 0.5 part of ubiquinone, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
firstly, slowly adding 10 parts of starch into water, then adding 12 parts of compound fertilizer, and uniformly stirring; then, adding ubiquinone, hymexazol and imidacloprid in corresponding parts by weight into the mixed solution; and finally, adding the residual starch and the emulsifier, and fully and uniformly stirring to obtain the starch emulsifier.
Comparative example 5
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: 0.5 part of lycopene, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
firstly, slowly adding 10 parts of starch into water, then adding 12 parts of compound fertilizer, and uniformly stirring; then, adding lycopene, hymexazol and imidacloprid in corresponding parts by weight into the mixed solution; and finally, adding the residual starch and the emulsifier, and fully and uniformly stirring to obtain the starch-emulsifier composite.
Comparative example 6
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: 0.5 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
firstly, slowly adding 10 parts of starch into water, then adding 12 parts of compound fertilizer, and uniformly stirring; then, adding rutin, hymexazol and imidacloprid in corresponding parts by weight into the mixed solution; and finally, adding the residual starch and the emulsifier, and fully and uniformly stirring to obtain the starch-emulsifier composite.
Comparative example 7
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 5 parts of brassinosteroid, 0.25 part of hymexazol, 5 parts of imidacloprid and 12 parts of compound fertilizer22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the brassinosteroid, the hymexazol and the imidacloprid in corresponding parts by weight into the suspension; finally, adding the residual starch and the emulsifier into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
Comparative example 8
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: 0.5 part of plant feeding peptide, 100.5 parts of ubiquinone, 0.5 part of lycopene, 0.5 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
firstly, slowly adding 10 parts of starch into water, then adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the plant-feeding peptide, the ubiquinone 10, the lycopene, the rutin, the hymexazol and the imidacloprid in the mixed solution according to the parts by weight; and finally, adding the residual starch and the emulsifier, and fully and uniformly stirring to obtain the starch-emulsifier composite.
Comparative example 9
The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds comprises the following raw materials in parts by weight: nano TiO 2 2 5 parts of brassinosteroid, 0.25 part of phytotrophin, 0.5 part of phytotrophin, 100.5 parts of ubiquinone, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
The preparation method comprises the following steps:
(1) nano TiO is mixed with 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, the brassinosteroid ketone with the corresponding weight portion is plantedAdding fostering peptide, ubiquinone 10, hymexazol and imidacloprid into the suspension; finally, adding the residual starch and the emulsifier into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
Experimental verification of the coating agent of comparative examples 1 to 9:
the non-heading Chinese cabbage variety is Hefeng-2, seeds are provided by a vegetable genetic breeding team of the university of agriculture in Anhui, and seeds with full seeds and consistent sizes are selected as test materials.
Experimental treatment: the coating agent was produced according to the preparation and production method corresponding to the comparative examples (comparative examples 1 to 9) (the use method of the seed coating agent is referred to example 6), the coated seeds and the uncoated seeds were obtained and sown into 105-hole plug trays respectively, 3 replicates were designed at the same time, the plug trays were cultured in a climatic chamber, 4 temperature gradients of 37 ℃, 33 ℃, 29 ℃ and 25 ℃ (room temperature) were set, and the seed germination vigor was counted at 24 hours after sowing, the seed germination rate was counted at 48 hours, and the seedling height, root length, overground part fresh weight and root fresh weight were measured at 45 days.
Germination potential (%) (number of germination seeds/number of test seeds at 24 h) × 100%;
germination rate (%) × (number of germinated seeds/number of test seeds on day 48) × 100%.
The experimental results are as follows: shown in Table 3, Table 4-1 and Table 4-2.
TABLE 3 influence of different comparative examples on germination vigour and germination rate of non-heading Chinese cabbage seeds
Figure BDA0003676830440000141
(Note: in the table, different lower case letters indicate that there is a significant difference (p <0.05) between different temperatures in the same comparative example, and that lower case letters indicate that there is no significant difference between different temperatures in the same comparative example)
Table 3 shows that: when the components of the composite coating agent are independently prepared into the coating agent, the effect of improving the germination potential and the germination rate of the seeds is far higher than that of the seeds without the coating agent; however, when the components form a matched group, the components generate synergistic effect, and the capability of the coating agent is higher than that of a coating agent prepared from single components. Therefore, the components can improve the germination vigor and the germination rate at high temperature, and the synergistic effect is better.
TABLE 4-1 influence of different comparative examples on seedling height and root length of non-heading Chinese cabbage
Figure BDA0003676830440000142
Figure BDA0003676830440000151
(Note: in the table, different lower case letters indicate that there is a significant difference (p <0.05) between different temperatures in the same comparative example, and that lower case letters indicate that there is no significant difference between different temperatures in the same comparative example)
TABLE 4-2 Effect of different comparative examples on the fresh weight of overground parts and fresh weight of roots of non-heading Chinese cabbage
Figure BDA0003676830440000152
Figure BDA0003676830440000161
(Note: in the table, different lower case letters indicate that there is a significant difference (p <0.05) between different temperatures in the same comparative example, and that lower case letters indicate that there is no significant difference between different temperatures in the same comparative example)
Tables 4-1 and 4-2 show: when each component of the compound coating agent is independently prepared into the coating agent, the compound coating agent also has the enhancement effect on the seedling height, the root length, the fresh weight of the overground part and the fresh weight of the roots; compared with the uncoated seed, the seed of the coating agent can obviously improve the seedling height, the root length, the fresh weight of overground parts and the fresh weight of roots of seedlings under high temperature stress, and the effect of improving the growth vigor of the non-heading Chinese cabbage plants under high temperature stress by synergistic use is more obvious.
As can be seen from tables 1 to 4, the seed coating agent of the present invention can improve the high temperature resistance of the non-heading Chinese cabbage seeds, and has an excellent effect of strengthening seedlings, and example 2 is the best formulation.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention are intended to be included within the scope of the present invention.

Claims (8)

1. The high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds is characterized by comprising the following raw materials in parts by weight: nano TiO 2 2 1-5 parts of brassinosteroid, 0.15-0.25 part of phytotrophin, 0.1-0.5 part of plant-feeding peptide, 100.1-0.5 part of ubiquinone, 0.1-0.5 part of lycopene, 0.1-0.5 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 5-10 parts of emulsifier.
2. The non-heading Chinese cabbage seed high-temperature-resistant coating agent as claimed in claim 1, which comprises the following raw materials in parts by weight: nano TiO 2 2 3 parts of brassinosteroid, 0.25 part of phytotrophin, 0.3 part of phytotrophin, 100.5 parts of ubiquinone, 0.3 part of lycopene, 0.3 part of rutin, 5 parts of hymexazol, 7 parts of imidacloprid, 12 parts of compound fertilizer, 22 parts of starch and 8 parts of emulsifier.
3. The non-heading Chinese cabbage seed high-temperature-resistant coating agent according to claim 1, wherein the compound fertilizer comprises basic elements and trace elements; the basic element is N, P, K, and the microelements are B, Cu, Fe, Mn, Zn and Mo.
4. The non-heading Chinese cabbage seed high-temperature-resistant coating agent as claimed in claim 3, wherein in the compound fertilizer, the addition amount of N, P, K is 10 parts, and the total addition amount of trace elements is 0.02-0.03 part by mass.
5. The non-heading Chinese cabbage seed high-temperature-resistant coating agent according to claim 1, wherein the emulsifier comprises poloxamer and sucrose ester; the mixing ratio of the poloxamer to the sucrose ester is 1: 1.
6. the high-temperature-resistant coating agent for the non-heading Chinese cabbage seeds as claimed in claim 1, wherein the coating agent can make the non-heading Chinese cabbage seeds resistant to high temperature of 32-37 ℃.
7. A method for preparing the high-temperature resistant coating agent for the non-heading Chinese cabbage seeds as claimed in any one of claims 1 to 6, comprising the following steps:
(1) mixing nanometer TiO 2 Mixing with water, and performing ultrasonic treatment for 1h to form uniform nano TiO 2 A suspension;
(2) firstly, preparing the prepared nano TiO 2 Slowly adding 10 parts of starch into the suspension, adding 12 parts of compound fertilizer, and uniformly stirring; then, adding the brassinosteroid, the plant feeding peptide, the ubiquinone 10, the lycopene, the rutin, the hymexazol and the imidacloprid in the suspension according to the parts by weight; finally, adding the residual starch and the emulsifier into the nano TiO 2 And (4) fully and uniformly stirring the suspension to obtain the product.
8. A use method of the high-temperature resistant coating agent for the non-heading Chinese cabbage seeds as claimed in any one of claims 1 to 6, characterized in that the coating agent is mixed and stirred until the surface of the non-heading Chinese cabbage seeds is coated with a uniform 0.5-0.8 mm protective layer; and then, fishing out the seeds, and drying the seeds in a dryer at the temperature of 20-24 ℃ and the humidity of 10% -15% for 6-8 h.
CN202210625129.6A 2022-06-02 2022-06-02 High-temperature-resistant coating agent for non-heading Chinese cabbage seeds and preparation and use methods thereof Pending CN114988946A (en)

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