CN114948776A - Tea polyphenol allergy-relieving fresh toothpaste and preparation method thereof - Google Patents
Tea polyphenol allergy-relieving fresh toothpaste and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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Abstract
The invention provides tea polyphenol allergy-relieving refreshing toothpaste and a preparation method thereof, wherein the tea polyphenol allergy-relieving refreshing toothpaste comprises the following raw materials: silicon dioxide, sorbitol, sodium lauryl sulfate, carrageenan, cellulose gum, essence, hydrated silica particles, polyethylene glycol-8, saccharin sodium, xylitol, tea polyphenol, sodium phytate, lactobacillus paracasei, strontium chloride, trisodium phosphate, sodium benzoate, menthone glycerol ketal and the balance of water. The invention has the beneficial effects that: the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the invention is prepared by taking silicon dioxide as a main carrier, and matching with beneficial oral components, namely tea polyphenol, and multiple functional components, namely strontium chloride, sodium phytate, refreshing mint derivatives, namely menthone glycerol ketal, hydrated silica friction particles and the like, so that the toothpaste integrating multiple effects of bacteriostasis, allergy relieving, stain removing, whitening and breath clearing is prepared.
Description
Technical Field
The invention belongs to the technical field of daily cleaning products, and particularly relates to tea polyphenol allergy-relieving fresh toothpaste and a preparation method thereof.
Background
Toothpaste is one of tooth cleaning products, generally in a gel shape, and is usually applied to a toothbrush, and the mechanical friction of the toothbrush is used for cleaning the surfaces of teeth, cleaning the teeth and the periphery of the teeth and purifying and refreshing the oral cavity. Along with the improvement of living standard of people, the quality requirement of toothpaste is gradually improved. In terms of performance, toothpaste is generally required to be able to remove pellicle and plaque from the tooth surface without damaging enamel and dentin; has good function of cleaning the oral cavity and the periphery thereof; no toxicity and no stimulation to oral mucosa; has comfortable fragrance and taste, and has cool and fresh feeling after use.
The dentin structure is not dense, and under a microscope, many dense and numb dentinal tubules filled with interstitial fluid and communicated with the interstitial fluid of the dental pulp are visible. Under the protection of enamel, the dentin tubule liquid is basically in a static state. However, the dentin is exposed due to long-term abrasion, and the small mouth of the dentin is communicated with the outside. When the teeth are stimulated in a physiological range, such as brushing teeth, temperature of overheating and supercooling, sour and hot food and the like, the pain rapidly appears and disappears along with the coming and leaving of the stimulation. Tooth sensitivity is common among the elderly, as enamel loss is a result of the long-term aging. Some patients have more sensitive teeth and inaccurate positioning of allergic regions, and doctors are more inclined to adopt a conservative treatment mode when the sensitivity degree is lower, so that the desensitizing toothpaste becomes the best choice. About 29.7% of adults in China have dentin hypersensitivity to different degrees. Therefore, it is important to develop an effective treatment for dentin hypersensitivity, and there are many methods for treating dentin hypersensitivity in clinical practice, among which desensitizing toothpastes containing certain specific ingredients are the first choice for patients.
Disclosure of Invention
The invention aims to provide tea polyphenol allergy-relieving fresh toothpaste with allergy-relieving effect and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the tea polyphenol allergy-relieving fresh toothpaste comprises the following raw materials in percentage by weight: 15-25% of silicon dioxide, 30-70% of sorbitol, 1.5-2.5% of sodium lauryl sulfate, 0.1-0.5% of carrageenan, 0.1-1.0% of cellulose gum, 0.6-1.5% of essence, 0.1-2% of hydrated silica particles, 80.5-2.5% of polyethylene glycol, 0.1-1% of saccharin sodium, 0.1-3% of xylitol, 0.01-1% of tea polyphenol, 1-3% of sodium phytate, 0.01-1% of lactobacillus paracasei, 0.1-1% of strontium chloride, 0.1-1% of trisodium phosphate, 0.1-0.5% of sodium benzoate, 0.1-1% of menthone glycerol ketal and the balance of water.
The silica has the function of an abrasive in toothpaste, and when teeth are brushed, the silica is suspended in foam to fill the oral cavity and widely contact tartar, so that the tartar is easily brushed off under the friction action of a toothbrush and is spit out along with mouthwash.
Sorbitol has good effects of keeping freshness, fragrance and color, can keep water, fragrance, color and freshness of toothpaste, and can be replaced by sorbitol in almost all fields using glycerol or propylene glycol.
The main raw material fatty alcohol of sodium lauryl sulfate is a pure natural plant (coconut kernel and palm kernel) extract, and is non-toxic and harmless. Sodium lauryl sulfate is easy to dissolve in water, has excellent emulsifying property and washing capacity, and is the safest, efficient and optimal product as a foaming agent in toothpaste. The abundant foam generated in the mouth can clean teeth and remove tartar when brushing teeth.
Carrageenan, also known as carrageenan or carrageenin, is a natural polysaccharide vegetable gum extracted from red algae. The carrageenan not only has excellent salt resistance and enzyme resistance, but also can improve the thixotropy and the dispersibility of the paste. Can obviously improve and improve the appearance of the toothpaste, and the paste is very fine, smooth and high-cleanness.
Cellulose gum acts as a thickener and stabilizer. In addition to altering the behavior of water, cellulose gums can be used to alter flowability, increase texture, and enhance mouthfeel.
The hydrated silica particles are made of silicon dioxide as a matrix and have a particle size which gives the toothpaste a colorful granular impression and has the function of cleaning tartar.
Tea polyphenols are the general name of polyphenols in tea, and are white amorphous powder, which are easily soluble in water, soluble in ethanol, methanol, acetone, ethyl acetate, and insoluble in chloroform. The tea polyphenol comprises the following main components: flavanones, anthocyanidins, flavonols, anthocyanins, phenolic acids, depside 6 compounds, and flavonoids in tea polyphenols can effectively inhibit harmful bacteria in oral cavity.
The sodium phytate is an organic matter, white powder or crystal, is an important pure natural green additive, and has the most remarkable characteristics of strong chelating action with metal ions, strong oxidation resistance and strong color protection.
The lactobacillus paracasei is a probiotic, mainly exists in intestinal tracts of human bodies, and has the effects of enhancing immunity, maintaining the balance of intestinal flora, promoting digestion and the like. Has certain bactericidal effect on gram-positive bacteria, staphylococcus aureus and escherichia coli.
Strontium chloride is one of the inorganic salts, the most common strontium salt, and aqueous solutions exhibit weak acidity, which can reduce tooth sensitivity by occluding dentinal tubules.
Menthone glycerol ketal is a chemical substance, a colorless transparent viscous liquid, used in formulations requiring cooling action, can enhance mint flavor in oral care products, can be used in gum confection, syrup, spicy flavoring agents, and can mask bitter taste in pharmaceutical formulations.
The tea polyphenol allergy-relieving refreshing toothpaste is a preferred embodiment and comprises the following raw materials in percentage by weight: 18-22% of silicon dioxide, 40-60% of sorbitol, 1.8-2.2% of sodium lauryl sulfate, 0.2-0.4% of carrageenan, 0.3-0.8% of cellulose gum, 0.8-1.2% of essence, 0.5-1.2% of hydrated silica particles, 81.5-2.2% of polyethylene glycol, 0.2-0.8% of saccharin sodium, 1-2% of xylitol, 0.05-0.5% of tea polyphenol, 1.2-2.2% of sodium phytate, 0.05-0.5% of lactobacillus paracasei, 0.3-0.8% of strontium chloride, 0.3-0.8% of trisodium phosphate, 0.2-0.4% of sodium benzoate, 0.2-0.8% of menthone glycerol ketal and the balance of water.
The tea polyphenol allergy-relieving refreshing toothpaste is a preferred embodiment and comprises the following raw materials in percentage by weight: 20% of silicon dioxide, 50% of sorbitol, 2% of sodium lauryl sulfate, 0.3% of carrageenan, 0.5% of cellulose gum, 1.0% of essence, 0.8% of hydrated silica particles, 81.8% of polyethylene glycol, 0.5% of sodium saccharin, 1.5% of xylitol, 0.2% of tea polyphenol, 2% of sodium phytate, 0.2% of lactobacillus paracasei, 0.5% of strontium chloride, 0.5% of trisodium phosphate, 0.3% of sodium benzoate, 0.5% of menthone glycerol ketal and the balance of water.
The second aspect of the invention provides a preparation method of tea polyphenol allergy-relieving fresh toothpaste, which comprises the following steps:
(1) mixing and stirring the raw materials uniformly to prepare a mixture;
(2) and (3) starting a vacuum pump of the paste preparation kettle, sucking the mixture obtained in the step (1) and preparing paste to obtain the tea polyphenol allergy-relieving fresh toothpaste.
As a preferred embodiment, in the step (1), the mixing and stirring temperature is 30-40 ℃, and the mixing and stirring time is 15-20 min.
As a preferred embodiment, in the step (2), the preparation method of the tea polyphenol allergy-relieving refreshing toothpaste comprises the following steps: and opening a scraper, a stirrer and a colloid mill in the paste preparation kettle to prepare the paste.
As a preferred embodiment, the preparation time of the tea polyphenol allergy-relieving refreshing toothpaste is 40-60 min.
The invention has the beneficial effects that: the tea polyphenol allergy-relieving fresh toothpaste containing the tea polyphenol can inhibit various oral harmful bacteria, strontium chloride can block dentinal tubules to relieve tooth sensitivity as a desensitizer, sodium phytate can remove exogenous tooth stains of teeth, menthone glycerol ketal can provide comfortable coolness, and hydrated silica particle friction particles can remove tartar.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely a few embodiments of the invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The tea polyphenol allergy-relieving refreshing toothpaste disclosed by the embodiment 1 comprises the following raw materials in percentage by weight: 15% of silicon dioxide, 50% of sorbitol, 1.5% of sodium lauryl sulfate, 0.1% of carrageenan, 1.0% of cellulose gum, 0.6% of essence, 0.1% of hydrated silica particles, 80.5% of polyethylene glycol, 0.1% of saccharin sodium, 0.1% of xylitol, 0.05% of tea polyphenol, 1% of sodium phytate, 0.05% of lactobacillus paracasei, 0.3% of strontium chloride, 0.1% of trisodium phosphate, 0.1% of sodium benzoate, 0.1% of menthone glycerol ketal and the balance of water.
The preparation method of the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the embodiment 1 comprises the following steps of:
(1) mixing the raw materials at 30 deg.C for 20min, and stirring to obtain mixture;
(2) and (3) starting a vacuum pump of the paste making kettle, sucking the mixture obtained in the step (1), and starting a scraper, a stirrer and a colloid mill in the paste making kettle to make paste for 60min to obtain the tea polyphenol allergy-relieving fresh toothpaste.
Example 2
The tea polyphenol allergy-relieving refreshing toothpaste disclosed in embodiment 2 comprises the following raw materials in percentage by weight: 18% of silicon dioxide, 55% of sorbitol, 1.8% of sodium lauryl sulfate, 0.2% of carrageenan, 0.9% of cellulose gum, 1.2% of essence, 0.5% of hydrated silica particles, 81.5% of polyethylene glycol-sodium saccharin, 1% of xylitol, 0.05% of tea polyphenol, 1.2% of sodium phytate, 0.05% of lactobacillus paracasei, 0.35% of strontium chloride, 0.3% of trisodium phosphate, 0.2% of sodium benzoate, 0.2% of menthone glycerol ketal and the balance of water.
The preparation method of the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the embodiment 2 comprises the following steps of:
(1) mixing the raw materials at 35 deg.C for 15min, and stirring to obtain mixture;
(2) and (3) starting a vacuum pump of the paste making kettle, sucking the mixture obtained in the step (1), and starting a scraper, a stirrer and a colloid mill in the paste making kettle to make paste for 45min to obtain the tea polyphenol allergy-relieving fresh toothpaste.
Example 3
The tea polyphenol allergy-relieving refreshing toothpaste disclosed in embodiment 3 comprises the following raw materials in percentage by weight: 20% of silicon dioxide, 50% of sorbitol, 2% of sodium lauryl sulfate, 0.3% of carrageenan, 0.8% of cellulose gum, 1.0% of essence, 0.8% of hydrated silica particles, 81.8% of polyethylene glycol, 0.5% of sodium saccharin, 1.5% of xylitol, 0.2% of tea polyphenol, 2% of sodium phytate, 0.2% of lactobacillus paracasei, 0.5% of strontium chloride, 0.5% of trisodium phosphate, 0.3% of sodium benzoate, 0.5% of menthone glycerol ketal and the balance of water.
The preparation method of the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the embodiment 3 comprises the following steps of:
(1) mixing the raw materials at 35 deg.C for 20min, and stirring to obtain mixture;
(2) and (3) starting a vacuum pump of the paste making kettle, sucking the mixture obtained in the step (1), and starting a scraper, a stirrer and a colloid mill in the paste making kettle to make paste for 50min to obtain the tea polyphenol allergy-relieving fresh toothpaste.
Example 4
The tea polyphenol allergy-relieving refreshing toothpaste disclosed by the embodiment 4 comprises the following raw materials in percentage by weight: 22% of silicon dioxide, 52% of sorbitol, 1.5% of sodium lauryl sulfate, 0.1% of carrageenan, 1.0% of cellulose gum, 0.6% of essence, 0.1% of hydrated silica particles, 80.5% of polyethylene glycol, 0.1% of saccharin sodium, 0.1% of xylitol, 1% of tea polyphenol, 1% of sodium phytate, 0.01% of lactobacillus paracasei, 0.1% of strontium chloride, 1% of trisodium phosphate, 0.5% of sodium benzoate, 0.5% of menthone glycerol ketal and the balance of water.
The preparation method of the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the embodiment 4 comprises the following steps of:
(1) mixing the raw materials at 40 deg.C for 15min, and mixing to obtain mixture;
(2) and (3) starting a vacuum pump of the paste making kettle, sucking the mixture obtained in the step (1), and starting a scraper, a stirrer and a colloid mill in the paste making kettle to make paste for 50min to obtain the tea polyphenol allergy-relieving fresh toothpaste.
Comparative example 1
The tea polyphenol allergy-free refreshing toothpaste disclosed in comparative example 1 is different from the tea polyphenol allergy-free refreshing toothpaste disclosed in example 1 in that the tea polyphenol allergy-free refreshing toothpaste disclosed in comparative example 1 does not contain raw materials such as tea polyphenol, lactobacillus paracasei and strontium chloride, and the rest raw materials and the preparation method are the same as those in example 1.
The anti-sensitivity research of the tea polyphenol allergy-relieving refreshing toothpaste comprises the following steps:
1. the number of the testees is 100, the testees at least have two crowds with sensitive tooth sources, the age range is 25-50 years, the number of the electron pressure sensitive probes (Yeaple probes) is 10-20 g in screening inspection, and the cold air sensitivity index (Schiff) is more than 2;
2. the experimental method comprises the following steps: the subjects were randomly and evenly divided into two groups, a test group and a control group, wherein the test group uses the tea polyphenol allergy-free refreshing toothpaste described in the embodiment 1 of the invention to brush teeth in the morning and at the evening every day, the control group uses the tea polyphenol allergy-free refreshing toothpaste described in the comparative example 1 to brush teeth in the morning and at the evening every day, the subjects did not take any anti-tooth sensitivity medicines during the test period, and the test results after 1 week, 3 weeks and 4 weeks are respectively shown in table 1:
TABLE 1
As can be seen from table 1: the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the invention has a good anti-allergy effect, and the anti-allergy effect of the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the invention is superior to that of the tea polyphenol allergy-relieving refreshing toothpaste disclosed by the comparative example 1.
The above description is only a preferred embodiment of the present application and is not intended to limit the present application, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present application shall be included in the protection scope of the present application.
Claims (7)
1. The tea polyphenol allergy-relieving fresh toothpaste is characterized by comprising the following raw materials in percentage by weight: 15-25% of silicon dioxide, 30-70% of sorbitol, 1.5-2.5% of sodium lauryl sulfate, 0.1-0.5% of carrageenan, 0.1-1.0% of cellulose gum, 0.6-1.5% of essence, 0.1-2% of hydrated silica particles, 80.5-2.5% of polyethylene glycol, 0.1-1% of saccharin sodium, 0.1-3% of xylitol, 0.01-1% of tea polyphenol, 1-3% of sodium phytate, 0.01-1% of lactobacillus paracasei, 0.1-1% of strontium chloride, 0.1-1% of trisodium phosphate, 0.1-0.5% of sodium benzoate, 0.1-1% of menthone glycerol ketal and the balance of water.
2. The tea polyphenol allergy-relieving refreshing toothpaste as claimed in claim 1, which is characterized by comprising the following raw materials in percentage by weight: 18-22% of silicon dioxide, 40-60% of sorbitol, 1.8-2.2% of sodium lauryl sulfate, 0.2-0.4% of carrageenan, 0.3-0.8% of cellulose gum, 0.8-1.2% of essence, 0.5-1.2% of hydrated silica particles, 81.5-2.2% of polyethylene glycol, 0.2-0.8% of saccharin sodium, 1-2% of xylitol, 0.05-0.5% of tea polyphenol, 1.2-2.2% of sodium phytate, 0.05-0.5% of lactobacillus paracasei, 0.3-0.8% of strontium chloride, 0.3-0.8% of trisodium phosphate, 0.2-0.4% of sodium benzoate, 0.2-0.8% of menthone glycerol ketal and the balance of water.
3. The tea polyphenol allergy-relieving refreshing toothpaste as claimed in claim 1, which is characterized by comprising the following raw materials in percentage by weight: 20% of silicon dioxide, 50% of sorbitol, 2% of sodium lauryl sulfate, 0.3% of carrageenan, 0.5% of cellulose gum, 1.0% of essence, 0.8% of hydrated silica particles, 81.8% of polyethylene glycol, 0.5% of sodium saccharin, 1.5% of xylitol, 0.2% of tea polyphenol, 2% of sodium phytate, 0.2% of lactobacillus paracasei, 0.5% of strontium chloride, 0.5% of trisodium phosphate, 0.3% of sodium benzoate, 0.5% of menthone glycerol ketal and the balance of water.
4. A process for preparing a tea polyphenol allergy-relieving refreshing toothpaste as claimed in any one of claims 1 to 3, comprising the steps of:
(1) mixing and stirring the raw materials uniformly to prepare a mixture;
(2) and (3) starting a vacuum pump of the paste preparation kettle, sucking the mixture obtained in the step (1) and preparing paste to obtain the tea polyphenol allergy-relieving fresh toothpaste.
5. The tea polyphenol allergy-relieving refreshing toothpaste as claimed in claim 4, wherein in the step (1), the mixing and stirring temperature is 30-40 ℃, and the mixing and stirring time is 15-20 min.
6. The tea polyphenol allergy-relieving refreshing toothpaste as claimed in claim 4, wherein in the step (2), the toothpaste preparation is as follows: and opening a scraper, a stirrer and a colloid mill in the paste preparation kettle to prepare paste.
7. The tea polyphenol allergy-relieving refreshing toothpaste as claimed in claim 6, wherein the time for preparing the toothpaste is 40-60 min.
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| US5505933A (en) * | 1994-06-27 | 1996-04-09 | Colgate Palmolive Company | Desensitizing anti-tartar dentifrice |
| WO2016015283A1 (en) * | 2014-07-31 | 2016-02-04 | 深圳市仁泰生物科技有限公司 | Antrodia cinnamomea chinese herbal toothpaste and preparation method therefor |
| CN111437216A (en) * | 2020-04-22 | 2020-07-24 | 苏州清馨健康科技有限公司 | Anti-allergy toothpaste |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5505933A (en) * | 1994-06-27 | 1996-04-09 | Colgate Palmolive Company | Desensitizing anti-tartar dentifrice |
| WO2016015283A1 (en) * | 2014-07-31 | 2016-02-04 | 深圳市仁泰生物科技有限公司 | Antrodia cinnamomea chinese herbal toothpaste and preparation method therefor |
| CN111437216A (en) * | 2020-04-22 | 2020-07-24 | 苏州清馨健康科技有限公司 | Anti-allergy toothpaste |
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