CN114892051B - Aluminum alloy automobile transmission shaft tube and manufacturing method thereof - Google Patents

Aluminum alloy automobile transmission shaft tube and manufacturing method thereof Download PDF

Info

Publication number
CN114892051B
CN114892051B CN202210586543.0A CN202210586543A CN114892051B CN 114892051 B CN114892051 B CN 114892051B CN 202210586543 A CN202210586543 A CN 202210586543A CN 114892051 B CN114892051 B CN 114892051B
Authority
CN
China
Prior art keywords
aluminum alloy
percent
transmission shaft
pipe
shaft tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202210586543.0A
Other languages
Chinese (zh)
Other versions
CN114892051A (en
Inventor
许丹娣
郑志荣
秦丽艳
夏建奎
李春生
潘洪波
李春
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dawei Materials Baotou Co ltd
Original Assignee
Dawei Materials Baotou Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dawei Materials Baotou Co ltd filed Critical Dawei Materials Baotou Co ltd
Priority to CN202210586543.0A priority Critical patent/CN114892051B/en
Publication of CN114892051A publication Critical patent/CN114892051A/en
Application granted granted Critical
Publication of CN114892051B publication Critical patent/CN114892051B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/02Alloys based on aluminium with silicon as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/02Making non-ferrous alloys by melting
    • C22C1/026Alloys based on aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/06Alloys based on aluminium with magnesium as the next major constituent
    • C22C21/08Alloys based on aluminium with magnesium as the next major constituent with silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/12Alloys based on aluminium with copper as the next major constituent
    • C22C21/18Alloys based on aluminium with copper as the next major constituent with zinc
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/043Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with silicon as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/047Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with magnesium as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/057Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with copper as the next major constituent

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Shafts, Cranks, Connecting Bars, And Related Bearings (AREA)

Abstract

The invention discloses an aluminum alloy automobile transmission shaft tube and a manufacturing method thereof, wherein the transmission shaft tube comprises the following components in percentage by mass: si:0.6 to 1.0 percent; cu:0.5 to 0.7 percent; fe is less than or equal to 0.3%; mn:0.2 to 0.5 percent; mg:0.7 to 1.0 percent; zn is less than or equal to 0.2 percent; cr:0.1 to 0.2 percent; ni is less than or equal to 0.1 percent; ti is less than or equal to 0.2%; the rare earth element Sc is also contained in the alloy: 0.1 to 0.2 percent; ce:0.15 to 0.25 percent; la:0.15 to 0.25 percent and the balance of Al; the manufacturing method comprises the following steps: batching, smelting, casting, ingot homogenization treatment, extrusion, annealing, cold rolling, solution quenching, artificial aging and straightening. The beneficial effects are that: the invention provides an aluminum alloy automobile transmission shaft tube, which meets the mechanical property requirement of an automobile on the aluminum alloy transmission shaft tube; the deformation amount in the cold rolling process is improved, the occurrence of cracks of the transmission shaft tube in the cold rolling process is avoided, the forming rate of the transmission shaft tube is improved, the processing procedure of the transmission shaft tube is simplified, and the efficiency is improved.

Description

Aluminum alloy automobile transmission shaft tube and manufacturing method thereof
Technical field:
the invention relates to a manufacturing method of an automobile transmission shaft tube, in particular to an aluminum alloy automobile transmission shaft tube and a manufacturing method thereof.
The background technology is as follows:
the transmission shaft is an important part in a chassis system of a commercial vehicle, and is made of steel materials at present and is widely applied to 45 # steel. With the development of light weight of automobiles, aluminum alloy materials are gradually adopted to replace steel materials, the weight can be reduced to about 1/3 of the original weight, the oil consumption is reduced, and the method has great significance for realizing weight and emission reduction.
The patent with publication number CN112853176A discloses a high-strength aluminum alloy for an automobile transmission shaft and a preparation method thereof, wherein the performance of the material reaches that the tensile strength is more than or equal to 450Mpa, the yield strength is more than or equal to 420Mpa, the elongation is more than or equal to 11%, the strength of a welded joint after welding meets the requirement of more than 70% of a base metal, but the magnesium content in the components of the aluminum alloy disclosed in the patent is higher than 1.2-1.8%, cold rolling treatment cannot be carried out to prepare the transmission shaft tube, if the aluminum alloy is subjected to cold rolling treatment, cracks can appear, the prepared part is directly scrapped, the material waste is caused, the cost is increased, and the efficiency is low.
The patent with publication number CN113684401A discloses an aluminum alloy for a high-service transmission shaft and a preparation method thereof, wherein the performance of the aluminum alloy meets the requirements of tensile strength of 380-450 MPa, yield strength of 350-420 MPa, elongation of 10-12%, hardness of 125-145 HB, weld strength of 75% higher than that of a base metal, yield torque of more than 1.5 times of rated torque, and fatigue life of the transmission shaft reaches 28.5 ten thousand times. However, the aluminum alloy disclosed in this patent has a high magnesium content of 1.05-1.9% and cannot be cold rolled to produce a driveshaft tube, and if the aluminum alloy is cold rolled, cracks occur, so that the driveshaft tube is processed in a forging manner, but the forged driveshaft tube has poor precision, requires re-finishing treatment, is complicated in process, and has low efficiency.
The invention comprises the following steps:
in view of the above, the present invention is directed to an aluminum alloy automotive driveshaft tube and a manufacturing method thereof, which can meet the mechanical performance requirements of automobiles on the aluminum alloy driveshaft tube.
The technical scheme of the invention discloses an aluminum alloy automobile transmission shaft tube, which comprises the following components in percentage by mass: si:0.6 to 1.0 percent; cu:0.5 to 0.7 percent; fe is less than or equal to 0.3%; mn:0.2 to 0.5 percent; mg:0.7 to 1.0 percent; zn is less than or equal to 0.2 percent; cr:0.1 to 0.2 percent; ni is less than or equal to 0.1 percent; ti is less than or equal to 0.2%; the rare earth element Sc is also contained in the alloy: 0.1 to 0.2 percent; ce:0.15 to 0.25 percent; la:0.15 to 0.25 percent and the balance of Al.
The component design thought in the invention is specifically as follows:
the addition of Mg and Si in the aluminum alloy transmission shaft tube mainly gives full play to the aging effect of the main alloy element Mg and Si (the main reinforcement item is Mg 2 Si). On the basis, the proportion of Mg and Si elements is optimized. From the AI-Mg-Si equilibrium diagram (shown in FIG. 1), it is known that when Mg:1.17%, si: at 0.68% (when the mass ratio of Mg to Si elements is 1.73), a pseudo-binary eutectic cross section is formed, the left and right sides of the cross section each having a eutectic system, alpha (Al) Mg near one side of Si 2 The intensity in the Si three-phase region is the largest (after heat treatment). On one hand, the micro-excessive Si can promote the precipitation of atomic clusters, so that the size of the strengthening phase is finer; on the other hand, a small excess of Si forms beta phase or Fe with Fe (when Si is larger than Fe) element 2 Si 2 Al 9 The three-phase compound acts as a nucleation point during crystallization of the crystal grains and has the function of refining the crystal grains, so that a small amount of Fe is also added into the alloy and is controlled within 0.3 percent. A slight excess of Si is beneficial to the strength improvement of the product; however, when the Mg content in the alloy is too high, cracks can appear on the transmission shaft tube manufactured by the later cold rolling, so the alloy is designed to have Si content ranging from 0.6 to 1.0 percent and Mg content ranging from 0.7 to 1.0 percent.
Cu is added into the aluminum alloy transmission shaft tube. The plasticity during hot working can be improved, the heat treatment strengthening effect can be increased, the extrusion effect can be restrained, and the anisotropism of the alloy due to Mn addition can be reduced. If the addition amount is high, the heat crack tendency of the welded joint is increased, so the Cu content of the alloy design is 0.5-0.7%.
Cr is added into the aluminum alloy transmission shaft tube pipe, so that Mg can be inhibited 2 The precipitation of Si phase in grain boundary delays natural aging process and improves strength after artificial aging. Cr can refine grains and make the recrystallized grains slender, thereby improving the corrosion resistance of the alloy. However, excessive Cr forms a insoluble phase with Fe and is easy to become a fatigue crack source, so Cr is designedThe content is 0.1-0.2%.
Mn is added into the aluminum alloy transmission shaft tube, so that the strength can be improved, and the corrosion resistance, the impact toughness and the bending property can be improved. However, excessive Mn forms AlMgSi phase with Si, which reduces the alloy strengthening effect and also leads to intra-crystal segregation. Therefore, the Mn content is designed to be in the range of 0.2 to 0.5%.
Ti and Zn are added into the aluminum alloy transmission shaft tube. Ti can further refine grains, promote the strengthening effect of alloy fine grains, and Zn element can promote Mg in the aging process 2 And Si is separated out, so that the ageing response speed of the alloy is improved.
Rare earth elements Sc, ce and La are added into the aluminum alloy transmission shaft tube. Rare earth elements are added into the aluminum alloy, so that the components are supercooled, grains are refined, secondary crystal spacing is reduced, the mixing of gases in the aluminum alloy is reduced, and the inclusion phase tends to spheroidize during casting of the aluminum alloy. The method can also reduce the surface tension of the melt, increase the fluidity, be beneficial to casting into ingots, have obvious influence on the technological performance, and can excite the deterioration effect of the magnesium-containing aluminum alloy. The addition amount of rare earth elements is Sc:0.1 to 0.2 percent; 0.15 to 0.25 percent of Ce; la:0.15 to 0.25 percent.
The technical scheme of the invention also discloses a manufacturing method of the aluminum alloy automobile transmission shaft tube, which comprises the following specific manufacturing processes: batching, smelting, casting, ingot homogenization treatment, extrusion, annealing, cold rolling, solution quenching, artificial aging and straightening.
Further, the casting procedure adopts a hot top casting mode to prepare an aluminum alloy cast ingot, the diameter of the aluminum alloy cast ingot prepared by the hot top casting mode is phi 275-277mm, the casting speed is 50-70mm/min, and the cooling water flow is controlled to be 100-130m 3 /h。
Further, the ingot homogenizing treatment process specifically comprises the following steps: heating the aluminum alloy cast ingot to 510-540 ℃, preserving heat for 8-16 h, and naturally cooling to obtain the aluminum alloy cast rod.
Further, the extrusion process specifically includes: preheating the aluminum alloy casting rod with the length of 0.35-0.40m to 440-520 ℃, and then extruding the aluminum alloy casting rod into a seamless pipe with the wall thickness of 5-11mm and the inner diameter of phi 102-156mm in an extruder (2500T double-acting extruder, manufacturer: wuxi Shi Yi Zhang mechanical manufacturing Co., ltd.); wherein the temperature of the extrusion die is 430-450 ℃, the temperature of the extrusion barrel is 400-450 ℃, the extrusion coefficient is 8-35, and the extrusion speed is 2.0-3.0 m/min; and during extrusion molding, the surface temperature of the seamless pipe is 430-510 ℃, and the seamless pipe is naturally cooled after extrusion.
Further, before preheating, the oxide skin on the surface of the aluminum alloy casting rod is removed.
Further, the annealing process specifically includes: heating the annealing furnace to 400-450 ℃, then loading the annealing furnace into the seamless pipe until the surface temperature of the seamless pipe is raised to 400-450 ℃, preserving heat for 2-5 h, and then discharging and air cooling to obtain a blank pipe.
Further, the cold rolling process specifically includes: and (3) adopting a two-roller tube mill (manufacturer: changzhou Xingtong mechanical manufacturing Co., ltd.; model: LG-150-G) to perform cold rolling on the blank tube at room temperature of 10-35 ℃, wherein the deformation of the cold rolling is 70-80%, and the feeding speed of the two-roller tube mill in the cold rolling process is 15-40 r/min, so as to obtain the aluminum alloy tube with the outer diameter phi of 110-160 mm, the wall thickness of 2.5-7.9 mm and the length of 3000-7000 mm.
Further, the solution hardening step specifically includes: heating the quenching furnace to 510-530 ℃, placing the aluminum alloy pipe in the quenching furnace, preserving heat for 60-180 min, and immersing the aluminum alloy pipe in water at 10-35 ℃ for not more than 20s.
Further, the artificial aging process specifically includes: heating the aging furnace to 150-160 ℃, then placing the aluminum alloy pipe subjected to solution quenching in the aging furnace, preserving heat for 10-16 h for aging, and then naturally cooling.
The invention has the advantages that:
1. the invention provides an aluminum alloy automobile transmission shaft tube, the mechanical property of which reaches the tensile strength of 400-430 Mpa, the yield strength of 380-405 Mpa, the elongation of 10-13% and the hardness of 115-130HB, thereby meeting the mechanical property requirement of the automobile on the aluminum alloy transmission shaft tube.
2. The content of Mg element is reduced in the aluminum alloy of the transmission shaft tube, and the rare earth elements Sc, ce and La are added, so that the structure crystal grains in the cast alloy are fine and uniform, the deformation in the cold rolling process is improved, the transmission shaft tube is prevented from cracking in the cold rolling process, and the forming rate of the transmission shaft tube is improved.
3. The transmission shaft tube prepared by the method disclosed by the invention through cold deformation, solution quenching, artificial aging and straightening has high precision, can be directly used for assembling an automobile transmission shaft, does not need to be finished again, simplifies the processing procedure of the transmission shaft tube, and improves the efficiency.
Description of the drawings:
FIG. 1 is an AI-Mg-Si equilibrium diagram.
Fig. 2 is a photograph of the shaft tube after cold rolling, wherein (a) is a photograph of the shaft tube after cold rolling of example 2, (b) is a photograph of the shaft tube after cold rolling of comparative example 1, and (c) is a photograph of the shaft tube after cold rolling of comparative example 2.
Fig. 3 is a metallographic photograph of an aluminum alloy cast bar after casting, wherein (a) is a metallographic photograph of an aluminum alloy cast bar after casting of example 2, and (b) is a metallographic photograph of an aluminum alloy cast bar after casting of comparative example 3.
Fig. 4 is a metallographic view of the driveshaft tube, where (a) is a metallographic view of the driveshaft tube of example 2 and (b) is a metallographic view of the driveshaft tube of comparative example 4.
The specific embodiment is as follows:
the present invention will be described in further detail by way of examples.
Example 1: the aluminum alloy automobile transmission shaft tube comprises the following components in percentage by mass: si:0.7%; cu:0.55%; fe:0.3%; mn:0.25%; mg:0.8%; zn:0.2%; cr:0.12%; ni:0.1%; ti:0.2%; the rare earth element Sc is also contained in the alloy: 0.14%; ce:0.2%; la:0.2%, the balance being Al.
The specific manufacturing process of the aluminum alloy automobile transmission shaft tube comprises the following steps: batching, smelting, casting, ingot homogenization treatment, extrusion, annealing, cold rolling, solution quenching, artificial aging and straightening.
The casting process adopts a hot top casting mode to prepare an aluminum alloy cast ingot, the diameter of the aluminum alloy cast ingot prepared by the hot top casting mode is phi 275-277mm, the casting speed is 50-70mm/min, and the cooling water flow is controlled to be 100-130m 3 /h。
The ingot homogenizing treatment process specifically comprises the following steps: heating the aluminum alloy cast ingot to 510-540 ℃, preserving heat for 8-16 h, and naturally cooling to obtain the aluminum alloy cast rod.
The extrusion process specifically comprises the following steps: removing the oxide skin on the surface of an aluminum alloy casting rod with the thickness of 0.35-0.40m, preheating the aluminum alloy casting rod to 440-520 ℃, and extruding the aluminum alloy casting rod into a seamless pipe with the wall thickness of 5-11mm and the inner diameter of phi 102-156mm in an extruder; wherein the temperature of the extrusion die is 430-450 ℃, the temperature of the extrusion barrel is 400-450 ℃, the extrusion coefficient is 8-35, and the extrusion speed is 2.0-3.0 m/min; when in extrusion molding, the surface temperature of the seamless pipe is 430-510 ℃, and the seamless pipe is naturally cooled after extrusion.
The annealing process specifically comprises the following steps: heating the annealing furnace to 400-450 ℃, then filling the annealing furnace into a seamless pipe, keeping the temperature for 2-5 hours after the surface temperature of the seamless pipe is heated to 400-450 ℃, and then discharging the annealing furnace for air cooling to obtain a blank pipe.
The cold rolling process specifically includes: and (3) carrying out cold rolling on the blank pipe by adopting a two-roller pipe mill at the room temperature of 10-35 ℃, wherein the deformation of the cold rolling is 70%, the feeding speed of the two-roller pipe mill in the cold rolling process is 15-40 r/min, and the aluminum alloy pipe with the outer diameter of phi 110-160 mm, the wall thickness of 2.5-7.9 mm and the length of 3000-7000mm is obtained.
The solution hardening process specifically includes: heating the quenching furnace to 510-530 ℃, placing the aluminum alloy pipe in the quenching furnace, preserving heat for 60-180 min, and immersing the aluminum alloy pipe in water at 10-35 ℃ for transfer time not exceeding 20s.
The artificial aging process specifically comprises the following steps: heating the aging furnace to 150-160 ℃, then placing the aluminum alloy pipe subjected to solution quenching in the aging furnace, preserving heat for 10-16 h for aging, and then naturally cooling.
Mechanical property detection is performed on the aluminum alloy automobile transmission shaft tubes disclosed in the embodiment of different specifications, and detailed results are shown in table 1:
table 1 mechanical properties of the aluminum alloy automotive driveshaft tube of example 1
Figure BDA0003666162000000081
As can be seen from Table 1, the tensile strength of the aluminum alloy automobile transmission shaft pipe manufactured in example 1 is greater than 400MPa, the yield strength is greater than 380MPa, the elongation is greater than 10% and the hardness is greater than 115HB, thereby meeting the mechanical property requirements of the aluminum alloy automobile transmission shaft pipe.
Example 2: the aluminum alloy automobile transmission shaft tube comprises the following components in percentage by mass: si:0.95%; cu:0.6%; fe:0.1%; mn:0.35%; mg:1.0%; zn:0.2%; cr:0.16%; ni:0.0031%; ti:0.034%; the rare earth element Sc is also contained in the alloy: 0.18%; ce:0.15%; la:0.15% and the balance of Al.
The specific manufacturing process of the aluminum alloy automobile transmission shaft tube comprises the following steps: batching, smelting, casting, ingot homogenization treatment, extrusion, annealing, cold rolling, solution quenching, artificial aging and straightening.
The casting process adopts a hot top casting mode to prepare an aluminum alloy cast ingot, the diameter of the aluminum alloy cast ingot prepared by the hot top casting mode is phi 275-277mm, the casting speed is 50-70mm/min, and the cooling water flow is controlled to be 100-130m 3 /h。
The ingot homogenizing treatment process specifically comprises the following steps: heating the aluminum alloy cast ingot to 510-540 ℃, preserving heat for 8-16 h, and naturally cooling to obtain the aluminum alloy cast rod.
The extrusion process specifically comprises the following steps: removing the oxide skin on the surface of an aluminum alloy casting rod with the thickness of 0.35-0.40m, preheating the aluminum alloy casting rod to 440-520 ℃, and extruding the aluminum alloy casting rod into a seamless pipe with the wall thickness of 5-11mm and the inner diameter of phi 102-156mm in an extruder; wherein the temperature of the extrusion die is 430-450 ℃, the temperature of the extrusion barrel is 400-450 ℃, the extrusion coefficient is 8-35, and the extrusion speed is 2.0-3.0 m/min; when in extrusion molding, the surface temperature of the seamless pipe is 430-510 ℃, and the seamless pipe is naturally cooled after extrusion.
The annealing process specifically comprises the following steps: heating the annealing furnace to 400-450 ℃, then filling the annealing furnace into a seamless pipe, keeping the temperature for 2-5 hours after the surface temperature of the seamless pipe is heated to 400-450 ℃, and then discharging the annealing furnace for air cooling to obtain a blank pipe.
The cold rolling process specifically includes: and (2) carrying out cold rolling on the blank pipe by adopting a two-roller pipe mill at the room temperature of 10-35 ℃, wherein the deformation of the cold rolling is 75%, the feeding speed of the two-roller pipe mill in the cold rolling process is 15-40 r/min, and the aluminum alloy pipe with the outer diameter of phi 110-160 mm, the wall thickness of 2.5-7.9 mm and the length of 3000-7000mm is obtained, and the photo is taken for the aluminum alloy pipe, so that the photo is shown in figure 2 (a).
The solution hardening process specifically includes: heating the quenching furnace to 510-530 ℃, placing the aluminum alloy pipe in the quenching furnace, preserving heat for 60-180 min, and immersing the aluminum alloy pipe in water at 10-35 ℃ for transfer time not exceeding 20s.
The artificial aging process specifically comprises the following steps: heating the aging furnace to 150-160 ℃, then placing the aluminum alloy pipe subjected to solution quenching in the aging furnace, preserving heat for 10-16 h for aging, and then naturally cooling.
Mechanical property detection is performed on the aluminum alloy automobile transmission shaft tubes disclosed in the embodiment of different specifications, and detailed results are shown in table 2:
table 2 mechanical properties of the aluminum alloy automotive driveshaft tube of example 2
Figure BDA0003666162000000101
As can be seen from Table 2, the tensile strength of the aluminum alloy automobile transmission shaft pipe manufactured in example 2 is between 410 and 430Mpa, the yield strength is between 390 and 403Mpa, the elongation is more than 10%, the hardness is between 120 and 129HB, and the mechanical property requirements of the aluminum alloy automobile transmission shaft pipe are met.
Example 3: the aluminum alloy automobile transmission shaft tube comprises the following components in percentage by mass: si:0.6%; cu:0.7%; fe:0.2%; mn:0.5%; mg:0.7%; zn:0.1%; cr:0.2%; ni:0.01%; ti:0.1%; the rare earth element Sc is also contained in the alloy: 0.2%; ce:0.25%; la:0.25%, the balance being Al.
The specific manufacturing process of the aluminum alloy automobile transmission shaft tube comprises the following steps: batching, smelting, casting, ingot homogenization treatment, extrusion, annealing, cold rolling, solution quenching, artificial aging and straightening.
The casting process adopts a hot top casting mode to prepare an aluminum alloy cast ingot, the diameter of the aluminum alloy cast ingot prepared by the hot top casting mode is phi 275-277mm, the casting speed is 50-70mm/min, and the cooling water flow is controlled to be 100-130m 3 /h。
The ingot homogenizing treatment process specifically comprises the following steps: heating the aluminum alloy cast ingot to 510-540 ℃, preserving heat for 8-16 h, and naturally cooling to obtain the aluminum alloy cast rod.
The extrusion process specifically comprises the following steps: removing the oxide skin on the surface of an aluminum alloy casting rod with the thickness of 0.35-0.40m, preheating the aluminum alloy casting rod to 440-520 ℃, and extruding the aluminum alloy casting rod into a seamless pipe with the wall thickness of 5-11mm and the inner diameter of phi 102-156mm in an extruder; wherein the temperature of the extrusion die is 430-450 ℃, the temperature of the extrusion barrel is 400-450 ℃, the extrusion coefficient is 8-35, and the extrusion speed is 2.0-3.0 m/min; when in extrusion molding, the surface temperature of the seamless pipe is 430-510 ℃, and the seamless pipe is naturally cooled after extrusion.
The annealing process specifically comprises the following steps: heating the annealing furnace to 400-450 ℃, then filling the annealing furnace into a seamless pipe, keeping the temperature for 2-5 hours after the surface temperature of the seamless pipe is heated to 400-450 ℃, and then discharging the annealing furnace for air cooling to obtain a blank pipe.
The cold rolling process specifically includes: and (3) carrying out cold rolling on the blank pipe by adopting a two-roller pipe mill at the room temperature of 10-35 ℃, wherein the deformation of the cold rolling is 80%, the feeding speed of the two-roller pipe mill in the cold rolling process is 15-40 r/min, and the aluminum alloy pipe with the outer diameter of phi 110-160 mm, the wall thickness of 2.5-7.9 mm and the length of 3000-7000mm is obtained.
The solution hardening process specifically includes: heating the quenching furnace to 510-530 ℃, placing the aluminum alloy pipe in the quenching furnace, preserving heat for 60-180 min, and immersing the aluminum alloy pipe in water at 10-35 ℃ for transfer time not exceeding 20s.
The artificial aging process specifically comprises the following steps: heating the aging furnace to 150-160 ℃, then placing the aluminum alloy pipe subjected to solution quenching in the aging furnace, preserving heat for 10-16 h for aging, and then naturally cooling.
Mechanical property detection is performed on the aluminum alloy automobile transmission shaft tubes disclosed in the embodiment of different specifications, and detailed results are shown in table 3:
TABLE 3 mechanical Properties of the aluminum alloy automotive driveshaft tube of example 3
Figure BDA0003666162000000121
As can be seen from Table 3, the tensile strength of the aluminum alloy automobile transmission shaft pipe manufactured in example 3 is greater than 400MPa, the yield strength is greater than 380MPa, the elongation is greater than 10% and the hardness is greater than 115HB, thereby meeting the mechanical property requirements of the aluminum alloy automobile transmission shaft pipe.
Comparative example 1: an aluminum alloy disclosed in embodiment one of the patent CN113684401a was prepared into an aluminum alloy automotive driveshaft tube according to the manufacturing process disclosed in example 2 of this invention, in which a photograph of the tube after cold rolling is shown in fig. 2 (b).
Comparative example 2: an aluminum alloy disclosed in embodiment five of the patent CN112853176a was prepared into an aluminum alloy automotive driveshaft tube according to the manufacturing process disclosed in example 2 of this invention, in which a photograph of the tube after cold rolling is shown in fig. 2 (c).
As can be seen from fig. 2 (a), the surface of the aluminum alloy pipe after cold rolling in example 2 of the present invention has no cracks; as can be seen from fig. 2 (b) and fig. 2 (c), the surfaces of the aluminum alloy pipes of the comparative example 1 and the comparative example 2 after cold rolling have cracks, and the aluminum alloy automobile transmission shaft pipe disclosed by the invention reduces the content of Mg element and increases rare earth elements Sc, ce and La, so that cracks of the transmission shaft pipe in the cold rolling process are avoided, and the forming rate of the transmission shaft pipe is improved.
Comparative example 3: the only difference from example 2 is that the rare earth elements Sc, ce, and La are not added to the composition of the driveshaft tube material of this comparative example.
The aluminum alloy cast bars cast in example 2 and the aluminum alloy cast in comparative example 3 were each subjected to a metallographic treatment, and metallographic photographs were taken, as shown in fig. 3, with fig. 3 (a) being a metallographic photograph of the aluminum alloy cast bars cast in example 2, and fig. 3 (b) being a metallographic photograph of the aluminum alloy cast bars cast in comparative example 3.
The grains of the aluminum alloy cast bars cast in example 2 in fig. 3 (a) were significantly reduced in size as compared to those of the aluminum alloy cast bars cast in comparative example 3 in fig. 3 (b).
Comparative example 4: the difference from example 2 is only that in this comparative example, the annealing step was not followed by cold rolling but by forging at 460 to 530℃and with a forging deformation of 75%.
The driveshaft tube of example 2 and the driveshaft tube of comparative example 4 were each metallographic treated and a metallographic photograph was taken, as shown in fig. 4, with fig. 4 (a) being a metallographic photograph of the driveshaft tube of example 2 and fig. 4 (b) being a metallographic photograph of the driveshaft tube of comparative example 4.
The driveshaft tube of example 2 in fig. 4 (a) is finer in grain size than the driveshaft tube of comparative example 4 in fig. 4 (b), because cold rolling lengthens and breaks up the grain size, solution hardening and re-nucleation after artificial aging, and thus the grain size is fine and dense; the forging belongs to hot forging drawing, the structure is fibrous, crystal grains are drawn, and after solution quenching and artificial aging, the crystal grains are hardly re-nucleated and large.
Mechanical property measurements were performed on the driveshaft tubes of example 2 and comparative example 4, and the detailed results are shown in table 4:
Figure BDA0003666162000000141
the aluminum alloy automotive driveshaft tube manufactured in example 2 of this invention has significantly higher tensile strength and yield strength than the aluminum alloy automotive driveshaft tube manufactured in comparative example 4.
The foregoing is a preferred embodiment of the present invention, and it will be apparent to those skilled in the art that modifications and variations can be made without departing from the principles of the present invention, and such modifications and variations are to be regarded as being within the scope of the invention.

Claims (8)

1. The aluminum alloy automobile transmission shaft tube is characterized by comprising the following components in percentage by mass: si:0.6 to 1.0 percent; cu:0.5 to 0.7 percent; fe is less than or equal to 0.3%; mn:0.2 to 0.5 percent; mg:0.7 to 1.0 percent; zn is less than or equal to 0.2 percent; cr:0.1 to 0.2 percent; ni is less than or equal to 0.1 percent; ti is less than or equal to 0.2%; the rare earth element Sc is also contained in the alloy: 0.1 to 0.2 percent; ce:0.15 to 0.25 percent; la:0.15 to 0.25 percent and the balance of Al;
the specific manufacturing process of the aluminum alloy automobile transmission shaft tube comprises the following steps: batching, smelting, casting, ingot homogenization treatment, extrusion, annealing, cold rolling, solution quenching, artificial aging and straightening;
the cold rolling process specifically comprises the following steps: and (3) carrying out cold rolling on the blank pipe obtained through the annealing process by adopting a two-roller pipe mill at the room temperature of 10-35 ℃, wherein the deformation of the cold rolling is 70-80%, the feeding speed of the two-roller pipe mill in the cold rolling process is 15-40 r/min, and the aluminum alloy pipe with the outer diameter of phi 110-160 mm, the wall thickness of 2.5-7.9 mm and the length of 3000-7000mm is obtained.
2. The aluminum alloy automobile transmission shaft tube according to claim 1, wherein the casting process adopts a hot top casting mode to prepare an aluminum alloy cast ingot, the diameter of the aluminum alloy cast ingot prepared by the hot top casting mode is phi 275-277mm, the casting speed is 50-70mm/min, and the cooling water flow is controlled to be 100-130m3/h.
3. The aluminum alloy automotive driveshaft tube according to claim 2, wherein the ingot homogenizing process is specifically: heating the aluminum alloy cast ingot to 510-540 ℃, preserving heat for 8-16 h, and naturally cooling to obtain the aluminum alloy cast rod.
4. An aluminum alloy automotive driveshaft tube according to claim 3, wherein the extrusion process specifically comprises: preheating the aluminum alloy casting rod with the length of 0.35-0.40m to 440-520 ℃, and then extruding the aluminum alloy casting rod into a seamless pipe with the wall thickness of 5-11mm and the inner diameter phi of 102-156mm in an extruder; wherein the temperature of the extrusion die is 430-450 ℃, the temperature of the extrusion barrel is 400-450 ℃, the extrusion coefficient is 8-35, and the extrusion speed is 2.0-3.0 m/min; and during extrusion molding, the surface temperature of the seamless pipe is 430-510 ℃, and the seamless pipe is naturally cooled after extrusion.
5. The aluminum alloy automotive driveshaft tube according to claim 4, wherein prior to preheating, an oxide skin on a surface of said aluminum alloy cast rod is removed.
6. The aluminum alloy automotive driveshaft tube according to claim 4 or 5, wherein the annealing process specifically includes: heating the annealing furnace to 400-450 ℃, then loading the annealing furnace into the seamless pipe until the surface temperature of the seamless pipe is raised to 400-450 ℃, preserving heat for 2-5 h, and then discharging and air cooling to obtain a blank pipe.
7. The aluminum alloy automotive driveshaft tube according to claim 6, wherein the solution hardening process specifically includes: heating the quenching furnace to 510-530 ℃, placing the aluminum alloy pipe in the quenching furnace, preserving heat for 60-180 min, and immersing the aluminum alloy pipe in water at 10-35 ℃ for not more than 20s.
8. The aluminum alloy automotive driveshaft tube according to claim 7, wherein the artificial aging process specifically comprises: heating the aging furnace to 150-160 ℃, then placing the aluminum alloy pipe subjected to solution quenching in the aging furnace, preserving heat for 10-16 h for aging, and then naturally cooling.
CN202210586543.0A 2022-05-27 2022-05-27 Aluminum alloy automobile transmission shaft tube and manufacturing method thereof Active CN114892051B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210586543.0A CN114892051B (en) 2022-05-27 2022-05-27 Aluminum alloy automobile transmission shaft tube and manufacturing method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210586543.0A CN114892051B (en) 2022-05-27 2022-05-27 Aluminum alloy automobile transmission shaft tube and manufacturing method thereof

Publications (2)

Publication Number Publication Date
CN114892051A CN114892051A (en) 2022-08-12
CN114892051B true CN114892051B (en) 2023-06-09

Family

ID=82726933

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202210586543.0A Active CN114892051B (en) 2022-05-27 2022-05-27 Aluminum alloy automobile transmission shaft tube and manufacturing method thereof

Country Status (1)

Country Link
CN (1) CN114892051B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117431441A (en) * 2023-10-25 2024-01-23 大为材料(包头)有限公司 High-purity high-performance aluminum alloy seamless pipe for nuclear industry and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102703773A (en) * 2012-06-11 2012-10-03 东莞市闻誉实业有限公司 Aluminum alloy plate and production process thereof
CN105063522A (en) * 2010-09-08 2015-11-18 美铝公司 6xxx aluminum alloys, and methods for producing the same
CN110735073A (en) * 2019-11-04 2020-01-31 苏州大学 high-quality 6-series aluminum alloy extruded casting blank and preparation method thereof
CN112458344A (en) * 2020-11-04 2021-03-09 佛山科学技术学院 High-strength corrosion-resistant aluminum alloy and preparation method and application thereof

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR0312098A (en) * 2002-06-24 2005-03-29 Corus Aluminium Walzprod Gmbh Method for the production of high strength balanced al-mg-si alloy and weldable alloy product
FR2902442B1 (en) * 2006-06-16 2010-09-03 Aleris Aluminum Koblenz Gmbh ALLOY OF AA6XXX SERIES WITH HIGH DAMAGE TO AEROSPACE INDUSTRY
JP5160930B2 (en) * 2008-03-25 2013-03-13 株式会社神戸製鋼所 Aluminum alloy extruded material excellent in bending crushability and corrosion resistance and method for producing the same
CN103045918A (en) * 2012-04-10 2013-04-17 湖南晟通科技集团有限公司 High-weld-strength Al-Mg-Si alloy and section bar preparation method thereof
CN102732760B (en) * 2012-07-19 2013-11-06 湖南大学 Aluminum alloy plate for automobile bodies
CN103014443B (en) * 2013-01-11 2015-08-05 中国科学院长春应用化学研究所 A kind of rare earth aluminium alloy and preparation method thereof
US11313019B2 (en) * 2015-12-23 2022-04-26 Norsk Hydro Asa Method for producing a heat treatable aluminum alloy with improved mechanical properties
CN105838943B (en) * 2016-05-31 2018-01-16 广西南南铝加工有限公司 A kind of pressing method of Al Mg Si aluminium alloys and its section bar
CN108118210B (en) * 2017-11-28 2019-12-20 中铝材料应用研究院有限公司 Aluminum alloy and processing method of extruded section thereof
CN111910109A (en) * 2020-07-01 2020-11-10 浙江金裕铝业股份有限公司 Aluminum alloy section for corrosion-resistant high-strength automobile and motorcycle accessory and preparation method thereof
CN112375943A (en) * 2020-10-29 2021-02-19 天津忠旺铝业有限公司 Preparation process of 6111 aluminum alloy automobile plate with high formability
CN113245486B (en) * 2021-06-21 2021-10-08 鼎镁新材料科技股份有限公司 Preparation method of die forging of Al-Mg-Si series aluminum alloy for inhibiting coarse grain structure

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105063522A (en) * 2010-09-08 2015-11-18 美铝公司 6xxx aluminum alloys, and methods for producing the same
CN102703773A (en) * 2012-06-11 2012-10-03 东莞市闻誉实业有限公司 Aluminum alloy plate and production process thereof
CN110735073A (en) * 2019-11-04 2020-01-31 苏州大学 high-quality 6-series aluminum alloy extruded casting blank and preparation method thereof
CN112458344A (en) * 2020-11-04 2021-03-09 佛山科学技术学院 High-strength corrosion-resistant aluminum alloy and preparation method and application thereof

Also Published As

Publication number Publication date
CN114892051A (en) 2022-08-12

Similar Documents

Publication Publication Date Title
CN108774696B (en) Production process of series 6 aluminum alloy ultrathin circular tube extruded section
US8152940B2 (en) Aluminum alloy forging member and process for producing the same
US8372220B2 (en) Aluminum alloy forgings and process for production thereof
CN113293273B (en) Processing method of 2xxx series aluminum alloy bar and wire for fastener
EP1306455B1 (en) High-strength alloy based on aluminium and a product made of said alloy
CN111004950B (en) 2000 aluminium alloy section bar and its manufacturing method
EP1848835A2 (en) Aluminum-zinc-magnesium-scandium alloys and methods of fabricating same
JP2003027170A (en) Aluminum-alloy material with excellent room- temperature aging controllability and low-temperature age hardenability
KR20120068910A (en) Process for producing brake piston
CN109720036B (en) High-corrosion-resistance aluminum alloy brazing sheet and heat treatment process thereof
JP2004084058A (en) Method for producing aluminum alloy forging for transport structural material and aluminum alloy forging
JP2004292937A (en) Aluminum alloy forging material for transport carrier structural material, and production method therefor
CN114892051B (en) Aluminum alloy automobile transmission shaft tube and manufacturing method thereof
CN114540649A (en) High-forming baking-resistant 5xxx series aluminum alloy plate and preparation method thereof
JPH0995750A (en) Aluminum alloy excellent in heat resistance
JP2004315938A (en) Forged material of aluminum alloy for structural material in transport aircraft, and manufacturing method therefor
WO2023246736A1 (en) Method for manufacturing al-zn-mg-cu series aluminum alloy plate, and aluminum alloy plate
JP2003138356A (en) Method for manufacturing high-strength aluminum-alloy brazing sheet for heat exchanger, having excellent brazability, formability and erosion resistance
JP2008062255A (en) SUPERPLASTIC MOLDING METHOD FOR Al-Mg-Si BASED ALUMINUM ALLOY SHEET HAVING REDUCED GENERATION OF CAVITY, AND Al-Mg-Si BASED ALUMINUM ALLOY MOLDED SHEET
JP4286431B2 (en) Manufacturing method of aluminum alloy piping material
JPH10183287A (en) Aluminum alloy for cold forging and its production
JP2003147498A (en) Method for producing semi-molten cast billet of aluminum alloy for transport apparatus
KR102012952B1 (en) Aluminium alloy and manufacturing method thereof
JPH05171328A (en) Thin hollow shape of aluminum alloy excellent in bendability and its production
JPH09249953A (en) Production of aluminum extruded material forged product

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant