CN114605187A - Rubber tree cutting nutrient solution - Google Patents
Rubber tree cutting nutrient solution Download PDFInfo
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- CN114605187A CN114605187A CN202210287297.9A CN202210287297A CN114605187A CN 114605187 A CN114605187 A CN 114605187A CN 202210287297 A CN202210287297 A CN 202210287297A CN 114605187 A CN114605187 A CN 114605187A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a rubber tree cutting nutrient solution which is prepared from the following raw materials in parts by weight: 30-40 parts of composite amino acid powder, 60-90 parts of deionized water, 10-20 parts of molybdenum boride mixture and 15-25 parts of mineral rare earth; the invention uses trace elements and rare earth chelated by amino acid, is rich in more than ten amino acids and more than ten chelated trace rare elements required by crops, and organic matters are particularly rich in high-activity chelated boron and molybdenum elements, can be directly absorbed and utilized by crops, has the advantages of small dosage, quick effect, simple production process, capability of improving photosynthesis, activating biological enzyme, enhancing nutrient absorption and transformation of crops, preventing and treating physiological diseases such as white leaves of yellow leaves, fallen leaves of small leaves, shrunken leaves of cluster leaves, more fallen flowers and fruits, fruit cracking of small fruits, curare fruits, bad coloration, plant dwarf and the like caused by potassium deficiency, boron deficiency, zinc deficiency and the like, effectively enhances the disease resistance, freezing resistance, drought resistance and saline alkali resistance of plants, and obviously improves the quality and yield of crops.
Description
Technical Field
The invention relates to boron-molybdenum-rare earth, in particular to a rubber tree cutting nutrient solution, belonging to the technical field of amino acid fertilizers.
Background
The rubber tree is a typical tropical rainforest tree species, is a tall tree with a perennial heat zone on the upper layer of the tropical rainforest, has the economic life of 30-40 years, and the secreted latex is an important industrial raw material.
Meanwhile, in order to meet the requirement of agricultural modernization development, the production of chemical fertilizers is developing towards high-efficiency compounding, fertilization mechanization, fertilizer transportation pipelining and water-fertilizer sprinkling irrigation instrumentation in addition to continuously increasing the yield. Liquid ammonia, ammonium polyphosphate, amino acid and the like become main chemical fertilizer varieties which are vigorously developed due to the advantages of high nutrient concentration or few side components and the like, and various amino acid nutrient solutions are developed at the same time so as to be applied to trees.
Disclosure of Invention
The invention aims to provide a rubber tree cutting nutrient solution to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: the rubber tree cutting nutrient solution is composed of the following raw materials in parts by weight:
30-40 parts of composite amino acid powder, 60-90 parts of deionized water, 10-20 parts of molybdenum boride mixture and 15-25 parts of mineral rare earth.
As a preferred technical scheme of the invention, the compound amino acid powder is formed by mixing one or more of aspartic acid, alanine, arginine, glycine, glutamic acid, lysine, serine, threonine, isoleucine and leucine.
As a preferred technical scheme of the invention, the preparation method of the rubber tree cutting nutrient solution comprises the following steps:
s1: adding compound amino acid powder into the stirring pot, simultaneously adding deionized water in parts by weight of the total preparation solution of the rubber tree cutting nutrient solution, and stirring at 80-90 ℃ for 5-10min until the compound amino acid powder is completely dissolved to obtain a compound amino acid solution;
s2: adding a molybdenum boride mixture with the molar mass fraction of 5-9% of the total preparation solution into a stirring pot, and continuing stirring until the molybdenum boride mixture is fully mixed with the compound amino acid solution;
s3: adding mineral rare earth which accounts for 7-9% of the total weight of the prepared solution into a stirring pot, wherein the content of rare earth elements in the mineral rare earth is more than or equal to 0.5%, continuously heating the mixed solution to 95-98 ℃, stirring until the mineral rare earth is completely dissolved, keeping the temperature of the solution more than or equal to 95 ℃, keeping the temperature for 2-3 hours, and naturally cooling to form the rubber tree cutting nutrient solution.
As a preferable technical scheme of the invention, the molybdenum boride mixture is one or a mixture of more of Mo2B, MoB2, Mo2B5 and MoB4, and the content of molybdenum element in the molybdenum boride mixture is more than or equal to 35%.
As a preferred technical scheme of the invention, the preparation method of the molybdenum boride mixture comprises the following steps:
the first step is as follows: weighing boron powder and boron powder in a certain molar ratio, adding the boron powder and the boron powder into a ball mill, carrying out ball milling for 5-6h, transferring the mixed powder into a tray after the ball milling is finished, placing the tray in a vacuum drying oven, and carrying out drying treatment at the temperature of 80-110 ℃;
the second step is as follows: transferring the mixed powder subjected to drying treatment in the first step into a graphite crucible with the inner wall coated with boron nitride powder, transferring the graphite crucible into a vacuum furnace, and sintering for 9-15h under the condition that the pressure is 10-20 GPa to obtain molybdenum boride particles for later use;
the third step: and (3) putting the molybdenum boride particles prepared in the second step into a grinder to be ground into powder, and screening the powder through a screen to obtain a molybdenum boride mixture, wherein the diameter of the aperture of the screen is less than or equal to 0.005 mm.
As a preferred technical scheme of the present invention, in the first step, before the boron powder and the boron powder are weighed in a certain molar ratio, the boron powder and the boron powder also need to be subjected to reduction treatment, and the specific reduction method is as follows:
respectively placing boron powder and boron powder in a crucible, placing the crucible in a reduction furnace, introducing rare gas into the reduction furnace, reducing under the protection of the rare gas, and adjusting the reduction temperature to 700-900 ℃.
Compared with the prior art, the invention has the beneficial effects that:
the rubber tree cutting nutrient solution disclosed by the invention is prepared from trace elements chelated by amino acid and rare earth, is rich in more than ten amino acids and more than ten chelated trace rare elements required by crops, and organic matters particularly rich in high-activity chelated boron and molybdenum elements, can be directly absorbed and utilized by crops, is low in dosage, quick in effect, simple in production process, capable of improving photosynthesis, activating biological enzyme, enhancing nutrient absorption and transformation of crops, preventing and treating physiological diseases such as yellow leaf white leaves, small leaf fallen leaves, cluster leaf contracted leaves, more flower fallen fruits, fruit contracted and cracked fruits, curare fruits, poor coloring, plant dwarf and the like caused by potassium deficiency, boron deficiency, zinc deficiency and the like, effectively enhancing the disease resistance, freezing resistance, drought resistance and saline alkali resistance of plants, and remarkably improving the quality and yield of crops.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
The first embodiment is as follows:
the rubber tree cutting nutrient solution is composed of the following raw materials in parts by weight:
30 parts of composite amino acid powder, 60 parts of deionized water, 10 parts of molybdenum boride mixture and 15 parts of mineral rare earth.
Wherein the compound amino acid powder is formed by mixing one or more of aspartic acid, alanine, arginine, glycine, glutamic acid, lysine, serine, threonine, isoleucine and leucine, wherein the content of the compound amino acid is more than or equal to 2%.
The preparation method of the rubber tree cutting nutrient solution comprises the following steps:
s1: adding the composite amino acid powder into the stirring pot, simultaneously adding deionized water in parts by weight of the total preparation solution of the rubber tree cutting nutrient solution, and stirring at the temperature of 80-90 ℃ for 5-10min until the composite amino acid powder is completely dissolved to obtain a composite amino acid solution;
s2: adding a molybdenum boride mixture with the molar mass fraction of 5-9% of the total preparation solution into a stirring pot, and continuing stirring until the molybdenum boride mixture is fully mixed with the compound amino acid solution;
specifically, the molybdenum boride mixture is one or a mixture of more of Mo2B, MoB2, Mo2B5 and MoB4, and the content of molybdenum element in the molybdenum boride mixture is more than or equal to 35%.
The preparation method of the molybdenum boride mixture comprises the following steps:
before weighing boron powder and boron powder with a certain molar ratio, respectively placing the boron powder and the boron powder in a crucible, placing the crucible in a reduction furnace, introducing rare gas into the reduction furnace, reducing under the protection of the rare gas, and adjusting the reduction temperature to 700-900 ℃.
Weighing reduced boron powder and reduced boron powder with a certain molar ratio, adding the weighed reduced boron powder and reduced boron powder into a ball mill, carrying out ball milling for 5-6h, transferring the mixed powder into a tray after the ball milling is finished, placing the tray into a vacuum drying oven, and carrying out drying treatment at the temperature of 80-110 ℃;
transferring the mixed powder subjected to drying treatment in the first step into a graphite crucible with the inner wall coated with boron nitride powder, transferring the graphite crucible into a vacuum furnace, and sintering for 9-15h under the condition that the pressure is 10-20 GPa to obtain molybdenum boride particles for later use;
and (3) putting the molybdenum boride particles prepared in the second step into a grinder to be ground into powder, and screening the powder through a screen to obtain a molybdenum boride mixture, wherein the diameter of the aperture of the screen is less than or equal to 0.005 mm.
S3: adding mineral rare earth with the content of more than or equal to 0.5 percent of the rare earth element into a stirring pot according to the weight percent of 7-9 percent of the total prepared solution, continuously heating the mixed solution to 95-98 ℃, stirring until the mineral rare earth is completely dissolved, keeping the temperature of the solution more than or equal to 95 ℃ for 2-3 h, naturally cooling to form the rubber tree cutting nutrient solution,
when the rubber tree cutting nutrient solution is used specifically, the rubber tree cutting nutrient solution is diluted by 800 times (500 g/bottle is added with 300 kg of water) and can be sprayed from the seedling stage to the flowering and fruiting stage of crops, the rubber tree cutting nutrient solution can be sprayed for 1 time every 10-20 days and continuously sprayed for 2-3 times, and a proper amount of diluent of 3000 times of 2000 times and 3000 times can be used for root irrigation, and the trunk and main branches of trees such as fruit trees and the like can be coated with the diluent of 200 times of 100 times.
Example two:
the rubber tree cutting nutrient solution is composed of the following raw materials in parts by weight:
40 components of composite amino acid powder, 90 components of deionized water, 20 components of molybdenum boride mixture and 15 components of mineral rare earth.
Wherein the compound amino acid powder is formed by mixing one or more of aspartic acid, alanine, arginine, glycine, glutamic acid, lysine, serine, threonine, isoleucine and leucine.
The preparation method of the rubber tree cutting nutrient solution comprises the following steps:
s1: adding compound amino acid powder into the stirring pot, simultaneously adding deionized water in parts by weight of the total preparation solution of the rubber tree cutting nutrient solution, and stirring at 80-90 ℃ for 5-10min until the compound amino acid powder is completely dissolved to obtain a compound amino acid solution;
s2: adding a molybdenum boride mixture with the molar mass fraction of 5-9% of the total preparation solution into a stirring pot, and continuing stirring until the molybdenum boride mixture is fully mixed with the compound amino acid solution;
specifically, the molybdenum boride mixture is one or a mixture of more of Mo2B, MoB2, Mo2B5 and MoB4, and the content of molybdenum element in the molybdenum boride mixture is more than or equal to 35%.
The preparation method of the molybdenum boride mixture comprises the following steps:
before weighing boron powder and boron powder with a certain molar ratio, respectively placing the boron powder and the boron powder in a crucible, placing the crucible in a reduction furnace, introducing rare gas into the reduction furnace, reducing under the protection of the rare gas, and adjusting the reduction temperature to 700-900 ℃.
Weighing reduced boron powder and reduced boron powder with a certain molar ratio, adding the weighed reduced boron powder and reduced boron powder into a ball mill, carrying out ball milling for 5-6h, transferring the mixed powder into a tray after the ball milling is finished, placing the tray into a vacuum drying oven, and carrying out drying treatment at the temperature of 80-110 ℃;
transferring the mixed powder subjected to drying treatment in the first step into a graphite crucible with the inner wall coated with boron nitride powder, transferring the graphite crucible into a vacuum furnace, and sintering for 9-15h under the condition that the pressure is 10-20 GPa to obtain molybdenum boride particles for later use;
and (3) putting the molybdenum boride particles prepared in the second step into a grinder to be ground into powder, and screening the powder through a screen to obtain a molybdenum boride mixture, wherein the diameter of the aperture of the screen is less than or equal to 0.005 mm.
S3: adding mineral rare earth 7-9 wt% of the total solution into a stirring pot, wherein the content of rare earth elements in the mineral rare earth is more than or equal to 0.5%, continuously heating the mixed solution to 95-98 ℃, stirring until the mineral rare earth is completely dissolved, keeping the temperature of the solution more than or equal to 95 ℃, keeping for 2-3 h, naturally cooling to form a rubber tree cutting nutrient solution,
when the rubber tree cutting nutrient solution is used specifically, the rubber tree cutting nutrient solution is diluted by 800 times (500 g/bottle is added with 300 kg of water) and can be sprayed from the seedling stage to the flowering and fruiting stage of crops, the rubber tree cutting nutrient solution can be sprayed for 1 time every 10-20 days and continuously sprayed for 2-3 times, and a proper amount of diluent of 3000 times of 2000 times and 3000 times can be used for root irrigation, and the trunk and main branches of trees such as fruit trees and the like can be coated with the diluent of 200 times of 100 times.
Example three:
the rubber tree cutting nutrient solution is composed of the following raw materials in parts by weight:
40 parts of composite amino acid powder, 90 parts of deionized water, 10 parts of molybdenum boride mixture and 25 parts of mineral rare earth.
Wherein the compound amino acid powder is formed by mixing one or more of aspartic acid, alanine, arginine, glycine, glutamic acid, lysine, serine, threonine, isoleucine and leucine.
The preparation method of the rubber tree cutting nutrient solution comprises the following steps:
s1: adding compound amino acid powder into the stirring pot, simultaneously adding deionized water in parts by weight of the total preparation solution of the rubber tree cutting nutrient solution, and stirring at 80-90 ℃ for 5-10min until the compound amino acid powder is completely dissolved to obtain a compound amino acid solution;
s2: adding a molybdenum boride mixture with the molar mass fraction of 5-9% of the total preparation solution into a stirring pot, and continuing stirring until the molybdenum boride mixture is fully mixed with the compound amino acid solution;
specifically, the molybdenum boride mixture is one or a mixture of more of Mo2B, MoB2, Mo2B5 and MoB4, and the content of molybdenum element in the molybdenum boride mixture is more than or equal to 35%.
The preparation method of the molybdenum boride mixture comprises the following steps:
before weighing boron powder and boron powder with a certain molar ratio, respectively placing the boron powder and the boron powder in a crucible, placing the crucible in a reduction furnace, introducing rare gas into the reduction furnace, reducing under the protection of the rare gas, and adjusting the reduction temperature to 700-900 ℃.
Weighing reduction boron powder and reduction boron powder with a certain molar ratio, adding the reduction boron powder and the reduction boron powder into a ball mill, performing ball milling for 5-6h, transferring the mixed powder into a tray after the ball milling is finished, placing the tray into a vacuum drying oven, and performing drying treatment at the temperature of 80-110 ℃;
transferring the mixed powder subjected to drying treatment in the first step into a graphite crucible with the inner wall coated with boron nitride powder, transferring the graphite crucible into a vacuum furnace, and sintering for 9-15h under the condition that the pressure is 10-20 GPa to obtain molybdenum boride particles for later use;
and (3) putting the molybdenum boride particles prepared in the second step into a grinder to be ground into powder, and screening the powder through a screen to obtain a molybdenum boride mixture, wherein the diameter of the aperture of the screen is less than or equal to 0.005 mm.
S3: adding mineral rare earth with the content of more than or equal to 0.5 percent of the rare earth element into a stirring pot according to the weight percent of 7-9 percent of the total prepared solution, continuously heating the mixed solution to 95-98 ℃, stirring until the mineral rare earth is completely dissolved, keeping the temperature of the solution more than or equal to 95 ℃ for 2-3 h, naturally cooling to form the rubber tree cutting nutrient solution,
when the rubber tree cutting nutrient solution is used specifically, the rubber tree cutting nutrient solution is diluted by 800 times (500 g/bottle is added with 300 kg of water) and can be sprayed from the seedling stage to the flowering and fruiting stage of crops, the rubber tree cutting nutrient solution can be sprayed for 1 time every 10-20 days and continuously sprayed for 2-3 times, and a proper amount of diluent of 3000 times of 2000 times and 3000 times can be used for root irrigation, and the trunk and main branches of trees such as fruit trees and the like can be coated with the diluent of 200 times of 100 times.
In the description of the present invention, it is to be understood that the indicated orientations or positional relationships are only for convenience in describing the present invention and for simplicity in description, and are not intended to indicate or imply that the indicated devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and are therefore not to be construed as limiting the present invention.
In the present invention, unless otherwise explicitly specified or limited, for example, it may be fixedly attached, detachably attached, or integrated; can be mechanically or electrically connected; the terms may be directly connected or indirectly connected through an intermediate, and may be communication between two elements or interaction relationship between two elements, unless otherwise specifically limited, and the specific meaning of the terms in the present invention will be understood by those skilled in the art according to specific situations.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The rubber tree cutting nutrient solution is characterized by consisting of the following raw materials in parts by weight:
30-40 parts of compound amino acid powder, 60-90 parts of deionized water, 10-20 parts of molybdenum boride mixture and 15-25 parts of mineral rare earth, wherein the content of compound amino acid in the compound amino acid powder is more than or equal to 2%.
2. The rubber tree cutting nutrient solution as claimed in claim 1, wherein: the compound amino acid powder is formed by mixing one or more of aspartic acid, alanine, arginine, glycine, glutamic acid, lysine, serine, threonine, isoleucine and leucine.
3. The rubber tree cutting nutrient solution as claimed in claim 1, wherein: the preparation method of the rubber tree cutting nutrient solution comprises the following steps:
s1: adding compound amino acid powder into the stirring pot, simultaneously adding deionized water in parts by weight of the total preparation solution of the rubber tree cutting nutrient solution, and stirring at 80-90 ℃ for 5-10min until the compound amino acid powder is completely dissolved to obtain a compound amino acid solution;
s2: adding a molybdenum boride mixture with the molar mass fraction of 5-9% of the total preparation solution into a stirring pot, and continuing stirring until the molybdenum boride mixture is fully mixed with the compound amino acid solution;
s3: adding mineral rare earth which accounts for 7-9% of the total weight of the prepared solution into a stirring pot, wherein the content of rare earth elements in the mineral rare earth is more than or equal to 0.5%, continuously heating the mixed solution to 95-98 ℃, stirring until the mineral rare earth is completely dissolved, keeping the temperature of the solution more than or equal to 95 ℃, keeping the temperature for 2-3 hours, and naturally cooling to form the rubber tree cutting nutrient solution.
4. The rubber tree cutting nutrient solution as claimed in claim 1, wherein: the molybdenum boride mixture is one or a mixture of more of Mo2B, MoB2, Mo2B5 and MoB4, and the content of molybdenum element in the molybdenum boride mixture is more than or equal to 35%.
5. The rubber tree cutting nutrient solution as claimed in claim 1, wherein: the preparation method of the molybdenum boride mixture comprises the following steps:
the first step is as follows: weighing boron powder and boron powder in a certain molar ratio, adding the boron powder and the boron powder into a ball mill, carrying out ball milling for 5-6h, transferring the mixed powder into a tray after the ball milling is finished, placing the tray in a vacuum drying oven, and carrying out drying treatment at the temperature of 80-110 ℃;
the second step is as follows: transferring the mixed powder subjected to drying treatment in the first step into a graphite crucible with the inner wall coated with boron nitride powder, transferring the graphite crucible into a vacuum furnace, and sintering for 9-15h under the condition that the pressure is 10-20 GPa to obtain molybdenum boride particles for later use;
the third step: and (3) putting the molybdenum boride particles prepared in the second step into a grinder to be ground into powder, and screening the powder through a screen to obtain a molybdenum boride mixture, wherein the diameter of the aperture of the screen is less than or equal to 0.005 mm.
6. The rubber tree cutting nutrient solution as claimed in claim 5, wherein: in the first step, before boron powder and boron powder are weighed according to a certain molar ratio, reduction treatment needs to be carried out on the boron powder and the boron powder, and the specific reduction method comprises the following steps:
respectively placing boron powder and boron powder in a crucible, placing the crucible in a reduction furnace, introducing rare gas into the reduction furnace, reducing under the protection of the rare gas, and adjusting the reduction temperature to 700-900 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210287297.9A CN114605187A (en) | 2022-03-22 | 2022-03-22 | Rubber tree cutting nutrient solution |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210287297.9A CN114605187A (en) | 2022-03-22 | 2022-03-22 | Rubber tree cutting nutrient solution |
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| CN114605187A true CN114605187A (en) | 2022-06-10 |
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| CN202210287297.9A Pending CN114605187A (en) | 2022-03-22 | 2022-03-22 | Rubber tree cutting nutrient solution |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1152565A (en) * | 1995-12-20 | 1997-06-25 | 郑州大学 | Mixed amino-acid complex state multielement micro-fertilizer and making method |
| CN106276941A (en) * | 2016-08-26 | 2017-01-04 | 洛阳金鹭硬质合金工具有限公司 | A kind of preparation method of molybdenum boride powder |
-
2022
- 2022-03-22 CN CN202210287297.9A patent/CN114605187A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1152565A (en) * | 1995-12-20 | 1997-06-25 | 郑州大学 | Mixed amino-acid complex state multielement micro-fertilizer and making method |
| CN106276941A (en) * | 2016-08-26 | 2017-01-04 | 洛阳金鹭硬质合金工具有限公司 | A kind of preparation method of molybdenum boride powder |
Non-Patent Citations (3)
| Title |
|---|
| 樊耀亭等: ""含稀土的混合氨基酸配合态多元微肥的研制及应用"", 《稀土》 * |
| 王国烘等: ""鳌合稀土钼在橡胶树上应用的研究"", 《稀土》 * |
| 罗明泉等: "《常见有毒和危险化学品手册》", 31 July 1992, 中国轻工业出版社 * |
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Application publication date: 20220610 |