CN114392378A - Plant component deodorant and preparation method thereof - Google Patents

Plant component deodorant and preparation method thereof Download PDF

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Publication number
CN114392378A
CN114392378A CN202210076919.3A CN202210076919A CN114392378A CN 114392378 A CN114392378 A CN 114392378A CN 202210076919 A CN202210076919 A CN 202210076919A CN 114392378 A CN114392378 A CN 114392378A
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extract
plant component
odor
surfactant
deodorant
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CN114392378B (en
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于素凤
孙成武
刘静雯
刘浩
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Anhui Yuezhi Huiyuan Biotechnology Co ltd
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Anhui Yuezhi Huiyuan Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Botany (AREA)
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  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

A plant component deodorant and a preparation method thereof relate to the technical field of deodorants. Is prepared from pomegranate rind extract 4-10%, eucalyptus leaf extract 1-4%, clove extract 3-5%, cinnamon bark extract 3-8%, camphor leaf extract 1-4%, catechin 0.1-0.5%, surfactant 0.1-0.2%, benzalkonium bromide 0.01-0.05% and water in balance. The natural plant deodorant disclosed by the invention is non-toxic, harmless, non-irritant, safe, environment-friendly, high in deodorization effect, safe and reliable. The method is suitable for reaction removal of odor generated by fermentation of polyglutamic acid, garbage and excrement pool, and converts odor substances into chemical substances without peculiar smell, thereby achieving the effect of deodorization. After the spraying, the odor immediately disappears, and a faint scent is left, so that the odor is eliminated, and the cleanness and no odor of the ambient air are ensured.

Description

Plant component deodorant and preparation method thereof
Technical Field
The invention relates to the technical field of deodorizers, and particularly relates to a plant component deodorizer and a preparation method thereof.
Background
Gamma-PGA (polyglutamic acid) is a polyglutamic acid compound synthesized by microorganisms, is formed by condensing glutamic acid monomers with gamma-carboxyl and amino, is a biopolymer material with excellent water solubility, has a plurality of unique physicochemical and biological properties, has the properties of water retention, film forming, biodegradability and the like, and is widely applied to the fields of food, agriculture, cosmetics, biomedicine and the like. The polyglutamic acid is used as a carrier of the medicine, the release rate of the medicine in a human body is controlled, so that the treatment effect is achieved, for example, the taxol or other medicines are coupled, so that the medicine is more stable and better in water solubility, and is used for slow release of the medicine, so that the medicine can act on tumor cells for a long time; the polyglutamic acid also has good compatibility with gelatin and is suitable for preparing adhesives, hemostatics and sealants for surgical medicament operations. Meanwhile, the polyglutamic acid can also be used as a flocculating agent, has a better flocculation effect on the treatment of sewage, and is mainly used for precipitating suspension in the sewage.
Polyglutamic acid can be fermented by various microorganisms including various bacteria by different methods, and the fermentation methods can be divided into liquid fermentation and solid fermentation. The disadvantage of liquid fermentation is that as the fermentation time increases, the viscosity of the medium increases and the concentration of oxygen decreases, slowing the fermentation process. Whereas solid fermentation avoids this problem. When the bacillus is used for fermenting the soybeans to obtain the polyglutamic acid, the obtained product has high yield and good quality, but the method has the defects that the pungent ammonia stink is easily generated, the environment around the fermentation is polluted, and the work of experimenters is not facilitated. The ammonia odor during fermentation of polyglutamic acid has great influence on the environment, and meanwhile, the acid substances mainly comprising 2-ethylbutyric acid and the pyrazine substances mainly comprising 2, 5-dimethylpyrazine are the main sources of the mildew and rot odor.
Therefore, in order to solve the ammonia fishy smell generated in the fermentation process of the polyglutamic acid, the natural plant component deodorant capable of removing the ammonia smell generated in the fermentation process of the polyglutamic acid is prepared, so that the environment is protected, and a good working environment is provided for experiments and production personnel.
Disclosure of Invention
The plant component deodorant can be used for removing odor generated in polyglutamic acid fermentation and odor generated in the treatment process of garbage and excrement pools, eliminating odor and promoting clean and no odor in ambient air.
The technical scheme adopted by the invention is as follows: a plant component deodorant is prepared from the following components in percentage by mass:
4-10% of pomegranate bark extract, 1-4% of eucalyptus leaf extract, 3-5% of clove extract, 3-8% of cassia bark extract, 1-4% of camphor leaf extract, 0.1-0.5% of catechin, 0.1-0.2% of surfactant, 0.01-0.05% of benzalkonium bromide and the balance of water.
Preferably, the plant component deodorant is prepared from the following components in percentage by mass:
7% of pomegranate bark extract, 2.5% of eucalyptus leaf extract, 4% of clove extract, 5% of cinnamon extract, 2.5% of camphor leaf extract, 0.2% of catechin, 0.15% of surfactant, 0.05% of benzalkonium bromide and 78.6% of water.
Further preferably, the component surfactant is selected from fatty acid monoglyceride and the component water is selected from deionized water.
A preparation method of plant component deodorant comprises the following steps:
(1) dissolving: adding pomegranate bark extract, eucalyptus leaf extract, clove extract, cassia bark extract, camphor leaf extract and catechin into water according to mass percentage, heating and stirring for dissolving;
(2) centrifuging: centrifuging the dissolved mixed solution, removing the precipitate, and taking the supernatant for later use;
(3) and (3) dissolving again: taking out the centrifuged supernatant, adding water in an amount which is 3-4 times the weight of the centrifuged supernatant for dilution, heating and stirring, adding a surfactant, continuously stirring, dissolving and uniformly mixing, and then continuously stirring until the mixed solution is cooled to room temperature;
(4) canning to obtain a finished product: adding benzalkonium bromide into the cooled mixed solution, and packaging in a container to obtain the plant component deodorant stock solution.
As a preferred technical scheme of the invention, the preparation method comprises the following steps:
heating to 35-45 ℃ in the step (1), stirring and dissolving for 10-30 min; the centrifugal rotating speed in the step (2) is 3000-; and (4) after dilution in the step (3), heating the solution to 55-60 ℃, adding a surfactant, and stirring the solution at a constant temperature for 20-40min to completely dissolve the surfactant.
Compared with the prior art, the invention has the beneficial effects that:
1. the deodorant is a pure natural plant component deodorant, is non-toxic, harmless, non-irritant, safe, environment-friendly, high in deodorization effect, safe and reliable.
2. The plant component deodorant product has a remarkable deodorizing effect, and the deodorizing effect is not affected by conditions such as temperature and environment.
3. The plant component deodorant product is convenient to use, is easy to dissolve in water, and can be sprayed by a spraying tool after being diluted. The method is suitable for reaction removal of odor generated by fermentation of polyglutamic acid, garbage and excrement pool, and converts odor substances into chemical substances without peculiar smell, thereby achieving the effect of deodorization. After the spraying, the odor immediately disappears, and a faint scent is left, so that the odor is eliminated, and the cleanness and no odor of the ambient air are ensured.
4. The deodorant stock solution prepared by the plant component deodorant formula has high and stable concentration, is convenient to store and use, has no corrosivity on equipment, and can be filled and stored in a plastic bottle.
Detailed Description
The starting materials used in the following examples are all commercially available products.
Example 1
A plant component deodorant is prepared from the following components:
5g of pomegranate bark extract, 3g of eucalyptus leaf extract, 2.5g of clove extract, 4g of cassia bark extract, 2g of camphor leaf extract, 0.2g of catechin, 0.1g of fatty acid monoglyceride, 0.05g of benzalkonium bromide and 83.15g of deionized water.
The preparation method comprises the following steps:
(1) dissolving: adding pericarpium Granati extract, folium Eucalypti Globueli extract, flos Caryophylli extract, cortex Cinnamomi Japonici extract, folium Cinnamomi Camphorae extract and catechin into deionized water, heating to 45 deg.C, stirring and dissolving for 10 min.
(2) Centrifuging: and (4) centrifuging the dissolved mixed solution, removing the precipitate, and taking the supernatant for later use. Wherein the centrifugal speed is 4000rpm, and the centrifugal time is 20 min.
(3) And (3) dissolving again: taking out supernatant after centrifugation, adding deionized water according to 3 times of the weight of the supernatant for dilution, heating to 55 ℃, stirring, adding fatty monoglyceride, stirring at constant temperature for 35min to completely dissolve the fatty monoglyceride, and continuously stirring until the mixed solution is cooled to room temperature.
(4) Canning to obtain a finished product: adding benzalkonium bromide into the cooled mixed solution, and packaging in a container to obtain the plant component deodorant stock solution.
(5) The using method comprises the following steps: diluting the stock solution with tap water at a ratio of 1: 100, and spraying onto the area to be treated with a suitable spraying tool to remove odor.
Example 2
A plant component deodorant is prepared from the following components:
6g of pomegranate bark extract, 3g of eucalyptus leaf extract, 3g of clove extract, 5g of cassia bark extract, 3g of camphor leaf extract, 0.2g of catechin, 0.1g of fatty acid monoglyceride, 0.05g of benzalkonium bromide and 79.65g of deionized water.
The preparation method comprises the following steps:
(1) dissolving: adding pericarpium Granati extract, folium Eucalypti Globueli extract, flos Caryophylli extract, cortex Cinnamomi Japonici extract, folium Cinnamomi Camphorae extract and catechin into deionized water, heating to 38 deg.C, stirring and dissolving for 20 min.
(2) Centrifuging: and (4) centrifuging the dissolved mixed solution, removing the precipitate, and taking the supernatant for later use. Wherein the centrifugation speed is 3800rpm, and the centrifugation time is 22 min.
(3) And (3) dissolving again: taking out supernatant after centrifugation, adding deionized water according to 4 times of the weight of the supernatant for dilution, heating to 60 ℃, stirring, adding fatty monoglyceride, stirring at constant temperature for 20min to completely dissolve the fatty monoglyceride, and continuously stirring until the mixed solution is cooled to room temperature.
(4) Canning to obtain a finished product: adding benzalkonium bromide into the cooled mixed solution, and packaging in a container to obtain the plant component deodorant stock solution.
(5) The using method comprises the following steps: diluting the stock solution with tap water at a ratio of 1: 100, and spraying onto the area to be treated with a suitable spraying tool to remove odor.
Example 3
A plant component deodorant is prepared from the following components:
10g of pomegranate bark extract, 4g of eucalyptus leaf extract, 5g of clove extract, 8g of cassia bark extract, 4g of camphor leaf extract, 0.2g of catechin, 0.2g of fatty acid monoglyceride, 0.05g of benzalkonium bromide and 68.55g of deionized water.
The preparation method comprises the following steps:
(1) dissolving: adding pericarpium Granati extract, folium Eucalypti Globueli extract, flos Caryophylli extract, cortex Cinnamomi Japonici extract, folium Cinnamomi Camphorae extract and catechin into deionized water, heating to 42 deg.C, stirring and dissolving for 15 min.
(2) Centrifuging: and (4) centrifuging the dissolved mixed solution, removing the precipitate, and taking the supernatant for later use. Wherein the centrifugation speed is 3300rpm, and the centrifugation time is 27 min.
(3) And (3) dissolving again: taking out supernatant after centrifugation, adding deionized water according to 3 times of the weight of the supernatant for dilution, heating to 58 ℃, stirring, adding fatty monoglyceride, stirring at constant temperature for 25min to completely dissolve the fatty monoglyceride, and continuously stirring until the mixed solution is cooled to room temperature.
(4) Canning to obtain a finished product: adding benzalkonium bromide into the cooled mixed solution, and packaging in a container to obtain the plant component deodorant stock solution.
(5) The using method comprises the following steps: diluting the stock solution with tap water at a ratio of 1: 100, and spraying onto the area to be treated with a suitable spraying tool to remove odor.
Example 4
A plant component deodorant is prepared from the following components:
7g of pomegranate bark extract, 2.5g of eucalyptus leaf extract, 4g of clove extract, 5g of cassia bark extract, 2.5g of camphor leaf extract, 0.2g of catechin, 0.15g of fatty acid monoglyceride, 0.05g of benzalkonium bromide and 78.6g of deionized water.
The preparation method comprises the following steps:
(1) dissolving: adding pericarpium Granati extract, folium Eucalypti Globueli extract, flos Caryophylli extract, cortex Cinnamomi Japonici extract, folium Cinnamomi Camphorae extract and catechin into deionized water, heating to 40 deg.C, stirring and dissolving for 10 min.
(2) Centrifuging: and (4) centrifuging the dissolved mixed solution, removing the precipitate, and taking the supernatant for later use. Wherein the centrifugal speed is 3500rpm, and the centrifugal time is 25 min.
(3) And (3) dissolving again: taking out supernatant after centrifugation, adding deionized water according to 4 times of the weight of the supernatant for dilution, heating to 55 ℃, stirring, adding fatty monoglyceride, stirring at constant temperature for 30min to completely dissolve the fatty monoglyceride, and continuously stirring until the mixed solution is cooled to room temperature.
(4) Canning to obtain a finished product: adding benzalkonium bromide into the cooled mixed solution, and packaging in a container to obtain the plant component deodorant stock solution.
(5) The using method comprises the following steps: diluting the stock solution with tap water at a ratio of 1: 100, and spraying onto the area to be treated with a suitable spraying tool to remove odor.
And (3) detecting the deodorization performance of the plant component deodorant:
the plant component deodorant prepared in examples 1 to 4 was sprayed on the fermented soybeans, and the ammonia gas concentration was measured before and after 2 minutes of spraying, and the results of the measurement are shown in table 1.
TABLE 1 deodorizing Effect of plant component deodorizers prepared in examples 1 to 4
Figure BDA0003483572100000051
As can be seen from the data in Table 1, the plant component deodorant can achieve 88.1% of deodorization after 2min (example 4), and has ideal deodorization effect and high deodorization efficiency. The active ingredients of the plant component deodorant prepared by the invention can rapidly react with the odor substances, so that the odor substances are converted into chemical substances without peculiar smell, and the deodorization effect is achieved.
The foregoing is merely exemplary and illustrative of the principles of the present invention and various modifications, additions and substitutions of the specific embodiments described herein may be made by those skilled in the art without departing from the principles of the present invention or exceeding the scope of the claims set forth herein.

Claims (9)

1. The plant component deodorant is characterized by being prepared from the following components in percentage by mass:
4-10% of pomegranate bark extract, 1-4% of eucalyptus leaf extract, 3-5% of clove extract, 3-8% of cassia bark extract, 1-4% of camphor leaf extract, 0.1-0.5% of catechin, 0.1-0.2% of surfactant, 0.01-0.05% of benzalkonium bromide and the balance of water.
2. The plant component deodorant according to claim 1, which is prepared from the following components in mass percent:
7% of pomegranate bark extract, 2.5% of eucalyptus leaf extract, 4% of clove extract, 5% of cinnamon extract, 2.5% of camphor leaf extract, 0.2% of catechin, 0.15% of surfactant, 0.05% of benzalkonium bromide and 78.6% of water.
3. A plant component deodorant according to claim 1 or 2 wherein the component surfactant is selected from fatty acid monoglyceride.
4. A botanical component deodorant as claimed in claim 1 or claim 2 wherein the component water is selected from deionised water.
5. A method for preparing a plant component deodorant according to any one of claims 1 to 4, characterized by comprising the steps of:
(1) dissolving: adding pomegranate bark extract, eucalyptus leaf extract, clove extract, cassia bark extract, camphor leaf extract and catechin into water according to mass percentage, heating and stirring for dissolving;
(2) centrifuging: centrifuging the dissolved mixed solution, removing the precipitate, and taking the supernatant for later use;
(3) and (3) dissolving again: taking out the centrifuged supernatant, adding water in an amount which is 3-4 times the weight of the centrifuged supernatant for dilution, heating and stirring, adding a surfactant, continuously stirring, dissolving and uniformly mixing, and then continuously stirring until the mixed solution is cooled to room temperature;
(4) canning to obtain a finished product: adding benzalkonium bromide into the cooled mixed solution, and packaging in a container to obtain the plant component deodorant stock solution.
6. The method of claim 5, wherein the temperature is raised to 35-45 ℃ in the step (1) and the mixture is dissolved for 10-30min with stirring.
7. The method as claimed in claim 5, wherein the centrifugation speed in step (2) is 3000-4000rpm and the centrifugation time is 20-30 min.
8. The method of claim 5, wherein the surfactant is added after heating to 55-60 ℃ after dilution in step (3), followed by stirring at a constant temperature for 20-40min to completely dissolve the surfactant.
9. The use of the plant component deodorant according to claim 1 or 2, wherein the plant component deodorant is suitable for the reaction removal of odor generated by fermentation of polyglutamic acid, garbage and odor generated during the treatment of excrement and urine, and converts the odor substances into odor-free chemical substances, thereby achieving the effect of deodorization.
CN202210076919.3A 2022-01-22 2022-01-22 Plant component deodorant and preparation method thereof Active CN114392378B (en)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0430857A (en) * 1990-05-28 1992-02-03 Matsushita Electric Works Ltd Deodorant
JP2002224202A (en) * 2001-02-05 2002-08-13 Sekisui Chem Co Ltd Deodorant
KR20030070487A (en) * 2002-02-25 2003-08-30 김대승 The preparation of antimicrobial cleansing deodorant
CN104307019A (en) * 2014-10-30 2015-01-28 上海今拓环保设备工程有限公司 Plant extract deodorizer for removing harmful gases
CN106890349A (en) * 2017-03-24 2017-06-27 合肥慧谷农业科技有限公司 A kind of deodorant for farm and preparation method thereof
JPWO2021215325A1 (en) * 2020-04-23 2021-10-28
CN113730635A (en) * 2020-05-29 2021-12-03 诸暨市光洁环保净化剂有限公司 Household garbage deodorant and preparation method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0430857A (en) * 1990-05-28 1992-02-03 Matsushita Electric Works Ltd Deodorant
JP2002224202A (en) * 2001-02-05 2002-08-13 Sekisui Chem Co Ltd Deodorant
KR20030070487A (en) * 2002-02-25 2003-08-30 김대승 The preparation of antimicrobial cleansing deodorant
CN104307019A (en) * 2014-10-30 2015-01-28 上海今拓环保设备工程有限公司 Plant extract deodorizer for removing harmful gases
CN106890349A (en) * 2017-03-24 2017-06-27 合肥慧谷农业科技有限公司 A kind of deodorant for farm and preparation method thereof
JPWO2021215325A1 (en) * 2020-04-23 2021-10-28
CN113730635A (en) * 2020-05-29 2021-12-03 诸暨市光洁环保净化剂有限公司 Household garbage deodorant and preparation method thereof

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