CN114288206A - Three-dimensional matte cosmetic composition and preparation method and application thereof - Google Patents
Three-dimensional matte cosmetic composition and preparation method and application thereof Download PDFInfo
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- CN114288206A CN114288206A CN202111642137.3A CN202111642137A CN114288206A CN 114288206 A CN114288206 A CN 114288206A CN 202111642137 A CN202111642137 A CN 202111642137A CN 114288206 A CN114288206 A CN 114288206A
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- 239000000203 mixture Substances 0.000 title claims abstract description 141
- 239000002537 cosmetic Substances 0.000 title claims abstract description 100
- 238000002360 preparation method Methods 0.000 title claims abstract description 28
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000000945 filler Substances 0.000 claims abstract description 21
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 18
- 239000003086 colorant Substances 0.000 claims abstract description 12
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 12
- 239000010445 mica Substances 0.000 claims abstract description 12
- 229910052618 mica group Inorganic materials 0.000 claims abstract description 12
- 239000003906 humectant Substances 0.000 claims abstract description 11
- 229920003217 poly(methylsilsesquioxane) Polymers 0.000 claims abstract description 11
- 239000000853 adhesive Substances 0.000 claims abstract description 10
- 230000001070 adhesive effect Effects 0.000 claims abstract description 10
- FKIQSOGFDBALHA-UHFFFAOYSA-L aluminum trimagnesium potassium dioxido(oxo)silane oxygen(2-) difluoride Chemical compound [O--].[F-].[F-].[Mg++].[Mg++].[Mg++].[Al+3].[K+].[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O FKIQSOGFDBALHA-UHFFFAOYSA-L 0.000 claims abstract description 9
- 229920003229 poly(methyl methacrylate) Polymers 0.000 claims abstract description 9
- 239000004926 polymethyl methacrylate Substances 0.000 claims abstract description 9
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 9
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 6
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 44
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 33
- 238000002156 mixing Methods 0.000 claims description 32
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims description 24
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 22
- 229940032094 squalane Drugs 0.000 claims description 22
- OQILCOQZDHPEAZ-UHFFFAOYSA-N Palmitinsaeure-octylester Natural products CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 claims description 21
- GJQLBGWSDGMZKM-UHFFFAOYSA-N ethylhexyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(CC)CCCCC GJQLBGWSDGMZKM-UHFFFAOYSA-N 0.000 claims description 21
- 238000003756 stirring Methods 0.000 claims description 18
- 239000000679 carrageenan Substances 0.000 claims description 15
- 235000010418 carrageenan Nutrition 0.000 claims description 15
- 229920001525 carrageenan Polymers 0.000 claims description 15
- 229940113118 carrageenan Drugs 0.000 claims description 15
- 239000000230 xanthan gum Substances 0.000 claims description 15
- 229920001285 xanthan gum Polymers 0.000 claims description 15
- 235000010493 xanthan gum Nutrition 0.000 claims description 15
- 229940082509 xanthan gum Drugs 0.000 claims description 15
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 15
- 235000011187 glycerol Nutrition 0.000 claims description 13
- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 claims description 12
- BTFJIXJJCSYFAL-UHFFFAOYSA-N arachidyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 claims description 12
- 235000019359 magnesium stearate Nutrition 0.000 claims description 12
- 239000003755 preservative agent Substances 0.000 claims description 12
- 230000002335 preservative effect Effects 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 229950008882 polysorbate Drugs 0.000 claims description 11
- 229920000136 polysorbate Polymers 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 8
- OJRQBZGHEZSVFW-UHFFFAOYSA-N 2-octadecanoyloxyoctadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC(C(O)=O)CCCCCCCCCCCCCCCC OJRQBZGHEZSVFW-UHFFFAOYSA-N 0.000 claims description 8
- 230000003750 conditioning effect Effects 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 8
- GLVSCNRMVJFZGM-UHFFFAOYSA-N icosan-9-ol octadecanoyl octadecanoate Chemical compound CCCCCCCCCCCC(O)CCCCCCCC.CCCCCCCCCCCCCCCCCC(=O)OC(=O)CCCCCCCCCCCCCCCCC GLVSCNRMVJFZGM-UHFFFAOYSA-N 0.000 claims description 8
- -1 polyethylene Polymers 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 229940015975 1,2-hexanediol Drugs 0.000 claims description 5
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 5
- 238000011049 filling Methods 0.000 claims description 5
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 claims description 5
- 229960005323 phenoxyethanol Drugs 0.000 claims description 5
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 claims description 5
- ZVUNTIMPQCQCAQ-UHFFFAOYSA-N 2-dodecanoyloxyethyl dodecanoate Chemical compound CCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCC ZVUNTIMPQCQCAQ-UHFFFAOYSA-N 0.000 claims description 4
- 229920002148 Gellan gum Polymers 0.000 claims description 4
- 239000002202 Polyethylene glycol Substances 0.000 claims description 4
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 claims description 4
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 4
- 239000000216 gellan gum Substances 0.000 claims description 4
- 235000010492 gellan gum Nutrition 0.000 claims description 4
- 229920001223 polyethylene glycol Polymers 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- 229950004959 sorbitan oleate Drugs 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 3
- 239000011230 binding agent Substances 0.000 claims description 3
- YSRVJVDFHZYRPA-UHFFFAOYSA-N melem Chemical compound NC1=NC(N23)=NC(N)=NC2=NC(N)=NC3=N1 YSRVJVDFHZYRPA-UHFFFAOYSA-N 0.000 claims description 3
- 229940105132 myristate Drugs 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 3
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 3
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 3
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 claims description 2
- 239000001814 pectin Substances 0.000 claims description 2
- 229920001277 pectin Polymers 0.000 claims description 2
- 235000010987 pectin Nutrition 0.000 claims description 2
- 239000004909 Moisturizer Substances 0.000 claims 1
- 230000001333 moisturizer Effects 0.000 claims 1
- 239000003921 oil Substances 0.000 abstract description 27
- 239000000843 powder Substances 0.000 abstract description 23
- 230000000694 effects Effects 0.000 description 31
- 230000000052 comparative effect Effects 0.000 description 21
- 238000012360 testing method Methods 0.000 description 20
- 238000005303 weighing Methods 0.000 description 9
- 230000008859 change Effects 0.000 description 7
- 239000007858 starting material Substances 0.000 description 6
- 238000000227 grinding Methods 0.000 description 5
- 239000013068 control sample Substances 0.000 description 4
- XNTUJOTWIMFEQS-UHFFFAOYSA-N octadecanoyl octadecaneperoxoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCCCCCCCC XNTUJOTWIMFEQS-UHFFFAOYSA-N 0.000 description 4
- 239000000523 sample Substances 0.000 description 4
- 239000008367 deionised water Substances 0.000 description 3
- 229910021641 deionized water Inorganic materials 0.000 description 3
- 239000004205 dimethyl polysiloxane Substances 0.000 description 3
- 210000004709 eyebrow Anatomy 0.000 description 3
- 229960005150 glycerol Drugs 0.000 description 3
- 230000003020 moisturizing effect Effects 0.000 description 3
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 239000000454 talc Substances 0.000 description 3
- 235000012222 talc Nutrition 0.000 description 3
- 229910052623 talc Inorganic materials 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 235000012907 honey Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000003607 modifier Substances 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- GLZWNFNQMJAZGY-UHFFFAOYSA-N octaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCO GLZWNFNQMJAZGY-UHFFFAOYSA-N 0.000 description 2
- MSRJTTSHWYDFIU-UHFFFAOYSA-N octyltriethoxysilane Chemical compound CCCCCCCC[Si](OCC)(OCC)OCC MSRJTTSHWYDFIU-UHFFFAOYSA-N 0.000 description 2
- 229960003493 octyltriethoxysilane Drugs 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 1
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
- PNZHZQKSQPVREF-UHFFFAOYSA-N C(CCCCCCCCCCCCCCCCC)(=O)OOC(CCCCCCCCCCCCCCCCC)=O.C(CCCCCCC)C(CCCCCCCCCCC)O Chemical compound C(CCCCCCCCCCCCCCCCC)(=O)OOC(CCCCCCCCCCCCCCCCC)=O.C(CCCCCCC)C(CCCCCCCCCCC)O PNZHZQKSQPVREF-UHFFFAOYSA-N 0.000 description 1
- 239000004472 Lysine Substances 0.000 description 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000009499 grossing Methods 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000031700 light absorption Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention provides a three-dimensional matte cosmetic composition and a preparation method and application thereof. The three-dimensional matte cosmetic composition comprises the following components in parts by weight: 10-40 parts of filler, 20-60 parts of first regulator, 2-4 parts of adhesive, 2-25 parts of colorant, 0.1-1 part of emulsifier, 0.1-0.5 part of humectant, 0.2-1 part of tackifier and 5-13 parts of second regulator; the filler comprises any one or the combination of at least two of mica, synthetic fluorophlogopite or talcum powder; the first regulator comprises any one of silicon dioxide, polymethyl methacrylate or polymethylsilsesquioxane or a combination of at least two of the silicon dioxide, the polymethyl methacrylate and the polymethylsilsesquioxane. The preparation method of the three-dimensional matte cosmetic composition is simple, can be used for preparing cosmetics such as pressed powder, eye shadow and the like, and has excellent matte degree, silkiness and oil control property.
Description
Technical Field
The invention belongs to the technical field of cosmetic preparation, and particularly relates to a three-dimensional matte cosmetic composition and a preparation method and application thereof.
Background
With the gradual increase of the domestic consumer's appeal to facial makeup products, the consumer prefers a makeup product with smooth texture, soft texture and unique 3D pattern appearance, namely a matte cosmetic. Cosmetics with matte surfaces (e.g., matte pressed powders, matte blushes, matte honeys, etc.) soften and weaken the appearance of such imperfections while also providing oil absorbing, refreshing, and clear benefits to the consumer during use, as compared to cosmetics with glossy surfaces that tend to highlight fine lines and wrinkles. Therefore, research on matte cosmetics is a focus and focus of research by researchers.
CN109966175A discloses a waterproof matte eyebrow powder and a manufacturing method thereof, wherein the method comprises the following steps: triethoxyoctylsilane-treated talc, lysine-treated mica powder, polymethyl methacrylate, triethoxyoctylsilane-treated porous silica, magnesium stearate, polydimethylsiloxane-treated boron nitride, polydimethylsiloxane, trimethylsiloxysilicate, polydimethylsiloxane, toner, phenoxyethanol/pyridone ethanolamine salt, and octylglycol/ethylhexylglycerol. The matte eyebrow powder is not dry and greasy, and can meet the requirements of people with different skin colors. However, the eyebrow powder is important in solving the problem of non-water resistance and preventing the appearance of faint makeup or falling off when a consumer sweats.
CN113425626A discloses a grease-free and talcum powder-free pressed powder and a preparation method thereof, wherein the grease-free and talcum powder-free pressed powder comprises the following components: nylon, silica, mica, synthetic fluorophlogopite. The powder cake without grease and talcum powder can enable the product to have extremely dry, smooth and silky surface touch, the matte makeup effect can be obtained by thinly spreading the powder cake on the face, the makeup effect is superior to that of the traditional powder cake, the makeup effect is natural, thin and light, the oil control is lasting, and the powder cake has good anti-falling performance. However, the powder cake aims at solving the problem that the traditional powder cake needs to be added with talcum powder and grease, and the pattern effect of the powder cake is not disclosed.
Based on the research, the existing matte cosmetics can not achieve high pattern stereovision and precision, are limited by the process, and have certain limitations on skin feel and stereovision. Therefore, the three-dimensional matte cosmetic composition is found, is used for preparing cosmetics such as blush, pressed powder or eye shadow, has a matte effect and high pattern stereoness and precision, and has great practical significance for the technical field of daily chemical products.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a three-dimensional matte cosmetic composition and a preparation method and application thereof. The three-dimensional matte cosmetic composition can be used for preparing cosmetics such as blush, pressed powder or eye shadow, can realize a fine 3D pattern effect, solves the problems of oil control, clothes sticking and powder flying prevention of skin, improves the make-up holding performance of products, and meets the requirements of modern consumers on advanced color make-up products.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the present invention provides a three-dimensional matte cosmetic composition comprising, in parts by weight: 10-40 parts of filler, 20-60 parts of first regulator, 2-4 parts of adhesive, 2-25 parts of colorant, 0.1-1 part of emulsifier, 0.1-0.5 part of humectant, 0.2-1 part of tackifier and 5-13 parts of second regulator.
According to the invention, the filler, the first regulator, the adhesive, the colorant, the emulsifier, the humectant, the tackifier, the second regulator and other components are matched and matched with each other, so that the finally obtained product has excellent matte degree, soft texture, extremely smooth touch and excellent oil control performance. Meanwhile, the cosmetic composition prepared by the invention can realize three-dimensional performance and pattern precision under the support of a silica gel mold, and can meet the requirements of modern consumers on high-grade color cosmetics.
The filler comprises any one or combination of at least two of mica, synthetic fluorophlogopite or talcum powder, the combination of at least two can be the combination of mica and synthetic fluorophlogopite or the combination of synthetic fluorophlogopite and talcum powder, and the like, and the mode of any combination of the rest can be selected, so that the repeated description is omitted.
The first regulator comprises any one or combination of at least two of silicon dioxide, polymethyl methacrylate or polymethylsilsesquioxane, the combination of at least two of the silicon dioxide and the polymethyl methacrylate or the combination of the polymethyl methacrylate and the polymethylsilsesquioxane can be selected, and the mode of any combination of the rest can be selected, so that the details are not repeated.
The 10-40 parts can be 10 parts, 12 parts, 14 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts, 26 parts, 28 parts, 30 parts, 32 parts, 34 parts, 36 parts, 38 parts or 40 parts and the like.
The 20-60 parts can be 20 parts, 25 parts, 30 parts, 35 parts, 40 parts, 45 parts, 50 parts, 55 parts or 60 parts and the like.
The 2 to 4 parts may be 2 parts, 2.2 parts, 2.4 parts, 2.6 parts, 2.8 parts, 3.0 parts, 3.2 parts, 3.4 parts, 3.6 parts, 3.8 parts, 4.0 parts or the like.
The 2 to 25 parts can be 2 parts, 4 parts, 6 parts, 8 parts, 10 parts, 12 parts, 14 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts or 25 parts and the like.
The amount of the above-mentioned 0.1 to 1 part may be 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1.0 part, etc.
The amount of the above-mentioned 0.1 to 0.5 part may be 0.1 part, 0.15 part, 0.2 part, 0.25 part, 0.3 part, 0.35 part, 0.4 part, 0.45 part or 0.5 part, etc.
The amount of the above-mentioned 0.2 to 1 part may be 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1.0 part, etc.
The amount of the above-mentioned 5 to 13 parts may be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts or 13 parts, etc.
Other point values within the above range can be selected, and are not described in detail herein.
The filler can endow the product with excellent coloring degree, reduce powder texture, increase permeability and increase the compatibility with a formula system.
The first regulator not only can endow the product with extremely smooth and fine touch feeling, but also can achieve soft focus and excellent oil control effect through light absorption and diffuse reflection.
The adhesive can increase the binding force of the product, and prevent the product from generating a powder flying phenomenon in the process of using the product through a beauty tool and influencing the using effect of consumers.
The colorant is capable of imparting color to the product.
The emulsifier can improve the moistening and smoothing effects of the product and is beneficial to improving the stability of the whole formula system.
The humectant can make the product have certain moisture retention.
The tackifier can support a three-dimensional through gel three-dimensional structure of the whole product, and the interaction among all components in a formula system of the whole product is increased.
The second regulator can regulate the moistening degree and the adhesive force of the product.
Preferably, the filler is mica and/or synthetic fluorophlogopite.
Preferably, the first conditioning agent is silica and/or polymethylsilsesquioxane.
In the invention, the binder comprises any one or combination of at least two of magnesium stearate, zinc stearate, melem myristate or polyethylene, the combination of at least two comprises the combination of magnesium stearate and zinc stearate or the combination of zinc stearate and melem myristate, and the like, and any combination mode of the rest can be selected, which is not repeated and is preferably magnesium stearate.
Magnesium stearate is preferred as a binder in the present invention because it provides better skin feel and binding ability.
In the present invention, the colorant includes a toner.
In the present invention, the emulsifier includes one or a combination of at least two of polysorbate, polyethylene glycol dilaurate and sorbitan oleate, where the combination of at least two of polysorbate, polyethylene glycol dilaurate and sorbitan oleate may be selected, and any combination of the remaining combination may be selected, which is not described herein again, and is preferably polysorbate.
Polysorbate is preferred as an emulsifier in the present invention because it is suitable for oil-in-water systems and its Hydrophile-lipophile balance (HLB) is moderate.
In the invention, the humectant comprises any one or combination of at least two of glycerin, 1, 3-butanediol or sodium hyaluronate, the combination of at least two of glycerin and 1, 3-butanediol or 1, 3-butanediol and sodium hyaluronate can be selected, and any combination mode of the rest can be selected, which is not described in detail herein, and glycerin is preferred.
Glycerin is preferred as the humectant in the present invention because of its good moisturizing properties and high cost performance.
In the invention, the tackifier comprises any one or combination of at least two of carrageenan, gellan gum, xanthan gum or pectin, the combination of at least two of carrageenan and gellan gum or combination of gellan gum and xanthan gum can be selected, and any combination mode can be selected, which is not described in detail herein, and is preferably the combination of carrageenan and xanthan gum.
According to the invention, the combination of carrageenan and xanthan gum is preferably selected as the tackifier, so that the synergistic tackifying effect can be realized to the maximum extent, and the higher difficult pattern three-dimensional and precision effects can be realized.
In the present invention, the second regulator includes any one or a combination of at least two of octyl dodecanol stearoyl stearate, squalane and ethylhexyl palmitate, where the combination of at least two of octyl dodecanol stearoyl stearate and squalane or squalane and ethylhexyl palmitate may be used, and any combination of the rest may be selected, and is not described herein again, and is preferably a combination of octyl dodecanol stearoyl stearate, squalane and ethylhexyl palmitate.
The combination of octyl dodecanol stearoyl stearate, squalane and ethylhexyl palmitate is preferred as the second modifier in the present invention because it can satisfy the moisture and oil feel of the product and provide the product with a certain binding capacity.
Preferably, the three-dimensional matte cosmetic composition further comprises a preservative.
Preferably, the preservative is 0.5-1 part by weight.
The amount of the above-mentioned 0.5 to 1 part may be 0.5 part, 0.55 part, 0.6 part, 0.65 part, 0.7 part, 0.75 part, 0.8 part, 0.85 part, 0.9 part, 0.95 part or 1 part, etc.
Other point values within the above range can be selected, and are not described in detail herein.
Preferably, the preservative comprises any one or a combination of at least two of phenoxyethanol, 1,2 hexanediol or octaethylene glycol, the combination of at least two of phenoxyethanol and 1,2 hexanediol or 1,2 hexanediol and octaethylene glycol, and the like, and any combination mode of the rest can be selected, which is not repeated herein.
In the invention, the three-dimensional matte cosmetic composition comprises the following components in parts by weight: 10-40 parts of a filling agent, 20-60 parts of a first regulator, 2-4 parts of magnesium stearate, 2-25 parts of a toner, 1-5 parts of octyl dodecanol stearoyl stearate, 2-4 parts of squalane, 2-4 parts of ethylhexyl palmitate, 0.1-1 part of polysorbate, 0.1-0.5 part of glycerol, 0.1-0.5 part of carrageenan, 0.1-0.5 part of xanthan gum and 0.5-1 part of a preservative.
The 10-40 parts can be 10 parts, 12 parts, 14 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts, 26 parts, 28 parts, 30 parts, 32 parts, 34 parts, 36 parts, 38 parts or 40 parts and the like.
The 20-60 parts can be 20 parts, 25 parts, 30 parts, 35 parts, 40 parts, 45 parts, 50 parts, 55 parts or 60 parts and the like.
The 2 to 4 parts may be 2 parts, 2.2 parts, 2.4 parts, 2.6 parts, 2.8 parts, 3.0 parts, 3.2 parts, 3.4 parts, 3.6 parts, 3.8 parts, 4.0 parts or the like.
The 2 to 25 parts can be 2 parts, 4 parts, 6 parts, 8 parts, 10 parts, 12 parts, 14 parts, 16 parts, 18 parts, 20 parts, 22 parts, 24 parts or 25 parts and the like.
The 1 to 5 parts may be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts or the like.
The amount of the above-mentioned 0.1 to 1 part may be 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1.0 part, etc.
The amount of the above-mentioned 0.1 to 0.5 part may be 0.1 part, 0.15 part, 0.2 part, 0.25 part, 0.3 part, 0.35 part, 0.4 part, 0.45 part or 0.5 part, etc.
The amount of the above-mentioned 0.5 to 1 part may be 0.5 part, 0.55 part, 0.6 part, 0.65 part, 0.7 part, 0.75 part, 0.8 part, 0.85 part, 0.9 part, 0.95 part or 1 part, etc.
Other point values within the above range can be selected, and are not described in detail herein.
Preferably, the three-dimensional matte cosmetic composition comprises the following components in parts by weight: 30-40 parts of a filling agent, 30-50 parts of a first regulator, 2-4 parts of magnesium stearate, 4-20 parts of a toner, 3-5 parts of octyl dodecanol stearoyl stearate, 2-4 parts of squalane, 2-4 parts of ethylhexyl palmitate, 0.5-1 part of polysorbate, 0.1-0.5 part of glycerol, 0.1-0.5 part of carrageenan, 0.1-0.5 part of xanthan gum and 0.5-1 part of a preservative.
In a second aspect, the present invention provides a process for preparing a three-dimensional matte cosmetic composition according to the first aspect, comprising the steps of:
(1) mixing the humectant, the tackifier and water, and heating to obtain a mixture A; mixing an emulsifier, a second regulator and an optional preservative, and heating to obtain a mixture B; mixing the obtained mixture A and the mixture B to obtain a mixture C;
(2) mixing the filler, the first regulator, the adhesive and the colorant to obtain a mixture D;
(3) mixing the mixture C obtained in the step (1) with the mixture D obtained in the step (2), and heating to obtain a mixture E;
(4) and (4) defoaming the mixture E obtained in the step (3), filling the mixture into a forming die, cooling, forming and baking to obtain the three-dimensional matte cosmetic composition.
Preferably, the mixing modes of obtaining the mixture A, obtaining the mixture B and obtaining the mixture C are stirring.
Preferably, the stirring speed is 500-.
The 500-800r/min can be 500r/min, 520r/min, 540r/min, 560r/min, 580r/min, 600r/min, 620r/min, 640r/min, 680r/min, 700r/min, 720r/min, 740r/min, 760r/min, 780r/min or 800 r/min.
Preferably, the temperature at which mixture a is obtained and mixture B is obtained is each independently selected from 50 to 90 ℃.
The temperature of 50-90 deg.C can be 50 deg.C, 55 deg.C, 60 deg.C, 65 deg.C, 70 deg.C, 75 deg.C, 80 deg.C, 85 deg.C or 90 deg.C, etc.
Preferably, the mixing in step (2) refers to crushing in a crushing pot and mixing uniformly.
Preferably, the stirring speed of the crushing pot is 2000-2500r/min, the crushing times are 1-3 times, and the time of each time of crushing is 2-8 s.
The 2500r/min for 2000-materials can be 2000r/min, 2050r/min, 2100r/min, 2150r/min, 2200r/min, 2250r/min, 2300r/min, 2350r/min, 2400r/min, 2450r/min or 2500r/min, etc.
The 2 to 8s may be 2s, 3s, 4s, 5s, 6s, 7s, 8s, or the like.
Other point values within the above range can be selected, and are not described in detail herein.
The number of the 1-3 times can be 1 time, 2 times or 3 times, etc.
Preferably, the mixing manner in the step (3) is stirring, and the stirring speed is 500-800 r/min.
The 500-800r/min can be 500r/min, 520r/min, 540r/min, 560r/min, 580r/min, 600r/min, 620r/min, 640r/min, 680r/min, 700r/min, 720r/min, 740r/min, 760r/min, 780r/min or 800r/min, etc.
Preferably, the temperature of the heating in the step (3) is 40-70 ℃.
The temperature of 40-70 deg.C can be 40 deg.C, 42 deg.C, 44 deg.C, 46 deg.C, 48 deg.C, 50 deg.C, 52 deg.C, 54 deg.C, 56 deg.C, 58 deg.C, 60 deg.C, 62 deg.C, 64 deg.C, 68 deg.C or 70 deg.C.
Preferably, the cooling temperature is-60-8 ℃, and the cooling time is 30-80 min.
The temperature of-60 to 8 ℃ can be-60 ℃, 55 ℃, 50 ℃, 45 ℃, 40 ℃, 35 ℃, 30 ℃, 25 ℃, 20 ℃, 15 ℃, 10 ℃, 5 ℃, 0 ℃, 5 ℃ or 8 ℃.
The time period of 30-80min can be 30min, 35min, 40min, 45min, 50min, 55min, 60min, 65min, 70min, 75min or 80 min.
Preferably, the baking temperature is 50-70 ℃, and the baking time is 8-24 h.
The temperature of 50-70 deg.C can be 50 deg.C, 52 deg.C, 54 deg.C, 56 deg.C, 58 deg.C, 60 deg.C, 62 deg.C, 64 deg.C, 68 deg.C or 70 deg.C, etc.
The 8-24h can be 8h, 9h, 10h, 11h, 12h, 13h, 14h, 15h, 16h, 17h, 18h, 19h, 20h, 21h, 22h, 23h or 24h and the like.
Other point values within the above range can be selected, and are not described in detail herein.
In a third aspect, the present invention provides a use of the three-dimensional matte cosmetic composition according to the first aspect in the preparation of a cosmetic.
The cosmetic includes, but is not limited to, any one of pressed powder, eye shadow or honey powder.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, the filler, the first regulator, the adhesive, the colorant, the emulsifier, the humectant, the tackifier, the second regulator and other components are matched and matched with each other, so that the finally obtained product has excellent matte degree, soft texture, extremely smooth touch and excellent oil control performance. Meanwhile, the cosmetic composition prepared by the invention can realize three-dimensional performance and pattern precision under the support of a silica gel mold, and can meet the requirements of modern consumers on high-grade color cosmetics.
Detailed Description
The technical solution of the present invention is further explained by the following embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.
Example 1
The embodiment provides a three-dimensional matte cosmetic composition which comprises the following components in parts by weight:
the preparation method comprises the following steps:
(1) weighing glycerol, carrageenan, xanthan gum and deionized water according to the formula ratio, mixing, and stirring at 50 ℃ and 600r/min to obtain a mixture A; weighing squalane, octyldodecanol stearoyloxy stearate, ethylhexyl palmitate, polysorbate and caprylyl glycol according to the formula ratio, mixing, stirring at 75 ℃ and 600r/min to obtain a mixture B, and mixing the mixture A and the mixture B to obtain a mixture C;
(2) weighing mica, silicon dioxide, magnesium stearate and toner according to the formula ratio, adding into a grinding pot, grinding for 2 times at 2000r/min, wherein the grinding time is 5s each time, and uniformly mixing to obtain a mixture D;
(3) mixing the mixture C obtained in the step (1) with the mixture D obtained in the step (2) to obtain a mixture E under the stirring condition of 50 ℃ and 600 r/min;
(4) and filling the obtained mixture E into a mold, vibrating for defoaming, cooling at-10 ℃ for 40min, taking out, demolding, baking at 60 ℃ for 10h, and thus obtaining the three-dimensional matte cosmetic composition.
Example 2
The embodiment provides a three-dimensional matte cosmetic composition which comprises the following components in parts by weight:
the preparation method comprises the following steps:
(1) weighing glycerol, carrageenan, xanthan gum and deionized water according to the formula ratio, mixing, and stirring at 50 ℃ at 700r/min to obtain a mixture A; weighing squalane, octyldodecanol stearoyloxy stearate, ethylhexyl palmitate, sorbitan oleate and phenoxyethanol according to the formula ratio, mixing, stirring at 75 ℃ and 600r/min to obtain a mixture B, and mixing the mixture A and the mixture B to obtain a mixture C;
(2) weighing synthetic fluorophlogopite, silicon dioxide, polymethylsilsesquioxane, zinc stearate and toner according to the formula ratio, adding into a grinding pot, grinding for 2 times at 2500r/min for 5s each time, and mixing uniformly to obtain a mixture D;
(3) mixing the mixture C obtained in the step (1) with the mixture D obtained in the step (2) to obtain a mixture E under the stirring condition of 50 ℃ and 600 r/min;
(4) and filling the obtained mixture E into a mold, vibrating for defoaming, cooling at-20 ℃ for 30min, taking out, demolding, baking at 50 ℃ for 15h, and thus obtaining the three-dimensional matte cosmetic composition.
Example 3
The embodiment provides a three-dimensional matte cosmetic composition which comprises the following components in parts by weight:
the preparation method comprises the following steps:
(1) weighing glycerol, carrageenan, xanthan gum and deionized water according to the formula ratio, mixing, and stirring at 50 ℃ and 800r/min to obtain a mixture A; weighing squalane, octyldodecanol stearoyloxy stearate, ethylhexyl palmitate, polyethylene glycol dilaurate and 1,2 hexanediol according to the formula ratio, mixing, stirring at 70 ℃ and 800r/min to obtain a mixture B, and mixing the mixture A and the mixture B to obtain a mixture C;
(2) weighing mica, silicon dioxide, polymethylsilsesquioxane, polyethylene and toner according to the formula ratio, adding into a crushing pot, crushing for 2 times at 2200r/min, wherein the crushing time is 5s each time, and uniformly mixing to obtain a mixture D;
(3) mixing the mixture C obtained in the step (1) with the mixture D obtained in the step (2) to obtain a mixture E under the stirring condition of 50 ℃ and 600 r/min;
(4) and filling the obtained mixture E into a mold, vibrating for defoaming, cooling at the temperature of 3 ℃ for 60min, taking out, demolding, baking at the temperature of 70 ℃ for 8h, and thus obtaining the three-dimensional matte cosmetic composition.
Example 4
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the raw materials do not include carrageenan, the reduced mass of which is complemented by xanthan gum, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 5
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the raw materials do not include xanthan gum, the reduced mass of which is complemented by carrageenan, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 6
This example provides a three-dimensional, stereoglossy cosmetic composition, differing from example 1 only in that the starting material does not comprise octyldodecanol stearoyloxystearate, the reduced mass of which is complemented by squalane and ethylhexyl palmitate, the mass ratio of squalane to ethylhexyl palmitate remaining unchanged, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 7
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the starting material does not comprise squalane, the reduced mass of which is complemented by octyldodecanol stearoyloxystearate and ethylhexyl palmitate, the mass ratio of octyldodecanol stearoyloxystearate to ethylhexyl palmitate remaining unchanged, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 8
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the starting material does not comprise ethylhexyl palmitate, the reduced mass of which is complemented by octyldodecanol stearoyloxystearate and squalane, the mass ratio of octyldodecanol stearoyloxystearate to squalane remaining unchanged, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 9
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the starting materials do not include squalane and ethylhexyl palmitate, the reduced mass of which is complemented by octyldodecanol stearoyloxy stearate, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 10
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the starting materials do not comprise octyldodecanol stearoyloxystearate and ethylhexyl palmitate, the reduced mass of which is complemented by squalane, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 11
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the starting materials do not comprise octyl dodecanol stearoyloxy stearate and squalane, the reduced mass of which is complemented by ethylhexyl palmitate, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 12
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the silica was replaced with polymethylsilsesquioxane in equal amounts, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Example 13
This example provides a three-dimensional matte cosmetic composition differing from example 1 only in that the silica was replaced with polymethyl methacrylate in equal amounts, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Comparative example 1
This comparative example provides a cosmetic composition differing from example 1 only in that the mica is present in 5 parts by weight, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Comparative example 2
This comparative example provides a cosmetic composition differing from example 1 only in that the mica is present in 45 parts by weight, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Comparative example 3
This comparative example provides a cosmetic composition differing from example 1 only in that the silica is present in 5 parts by weight, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Comparative example 4
This comparative example provides a cosmetic composition differing from example 1 only in that the silica is present in 65 parts by weight, the remaining parameters remaining in accordance with example 1. The preparation process is referred to example 1.
Test example 1
This test example performed a stability test on the three-dimensional matte cosmetic compositions prepared in examples 1 to 13, the test method being as follows:
cold resistance test: standing the product at-18 deg.C for 30 days, taking out, comparing with control sample (standing at 25 deg.C for 30 days), and observing color, odor and appearance changes;
and (3) heat resistance test: placing the product in a constant-temperature oven at 50 ℃ for 30 days, taking out the product, comparing the product with a control sample (placed at 25 ℃ for 30 days), and observing the change of color, smell and appearance;
and (3) cold-hot cycle testing: placing the product in a circulating device at the temperature of between 18 ℃ below zero and 50 ℃ for 30 days, taking out the product, comparing the product with a control sample (placed at the temperature of 25 ℃ for 30 days), and observing the change of color, smell and appearance;
and (3) illumination test: the product was placed under D65 and TL83 light source and uncapped for 30 days, and was compared with a control sample (placed at 25 ℃ for 30 days) to see if there was a color change.
The test results are statistically shown in table 1 below (the color, appearance and odor changes in the table below are the combined results of cold, heat, cold and heat cycling and light tests):
TABLE 1
| Group of | Stability of |
| Example 1 | Normal color and appearance, no peculiar smell |
| Example 2 | Normal color and appearance, no peculiar smell |
| Example 3 | Normal color and appearance, no peculiar smell |
| Example 4 | Normal color, slightly loose appearance and no peculiar smell |
| Example 5 | Normal color, slightly loose appearance and no peculiar smell |
| Example 6 | Normal color and appearance, no peculiar smell |
| Example 7 | Normal color and appearance, no peculiar smell |
| Example 8 | Normal color and appearance, no peculiar smell |
| Example 9 | Normal color and appearance, no peculiar smell |
| Example 10 | Normal color and appearance, no peculiar smell |
| Example 11 | Normal color and appearance, no peculiar smell |
| Example 12 | Normal color, slightly loose appearance and no peculiar smell |
| Example 13 | Colour(s)Slightly light, loose appearance, no peculiar smell |
As can be seen from the data in the table above, the three-dimensional matte cosmetic composition provided by the invention has good stability and can be stored for a long time.
Test example 2
The cosmetic compositions prepared in examples 1 to 13 and comparative examples 1 to 4 were subjected to the test for cosmetic effects (including matte gloss, silkiness) by the following methods:
grouping: selecting 170 volunteer subjects with neutral skin, dividing into 17 groups, applying the cosmetic compositions prepared in examples 1-13 and comparative examples 1-4 on each group, and 10 subjects in each group;
and (3) testing: after the skin of the subject is smeared with the moisturizing foundation liquid, the skin of the prepared cosmetic composition is dipped for one circle by a cosmetic brush, the skin of the subject is lightly paved on the whole face of the subject, and the subject scores matte degree and silkiness according to the blocking and mottled conditions of the face of the subject (the score is an integer n). The scoring criteria are shown in table 2 below:
TABLE 2
The test results are shown statistically in table 3 below (scores are the average of scores of 10 subjects per group, respectively):
TABLE 3
As can be seen from the data in the above table, the three-dimensional matte cosmetic composition provided in example 1 has superior matte gloss and smoothness compared to comparative examples 1 to 4, indicating that the addition amount of the filler and the first conditioning agent has an effect on the efficacy of the three-dimensional matte cosmetic composition. The makeup results of the three-dimensional matte cosmetic composition provided in example 1 were better than those of examples 4 to 11, indicating that the tackifier and the second modifier may have an effect on the efficacy of the three-dimensional matte cosmetic composition. The three-dimensional matte cosmetic compositions provided in example 1 had better cosmetic results than examples 12-13, indicating that the choice of the first conditioning agent may have an effect on the efficacy of the three-dimensional matte cosmetic composition.
Test example 3
The cosmetic compositions prepared in examples 1 to 13 and comparative examples 1 to 4 were used as samples in this test example, and the oil control property was measured by the following method:
grouping: selecting 170 volunteer subjects with neutral skin, dividing into 17 groups, applying the cosmetic compositions prepared in examples 1-13 and comparative examples 1-4 on each group, and 10 subjects in each group;
and (3) testing: first, the skin oil content of the cheeks of the subjects was measured with an oil tester SebumeterSM815 (purchased from Courage + Khazaha, germany), and then each subject applied a moisturizing foundation solution to the face and dipped into the prepared cosmetic composition surface with a cosmetic brush for one turn, lightly spread on the whole face, and applied for 8 hours, and then the skin oil content was measured. The oil control was evaluated based on the rate of change in the oil content of the skin before and after the use of the sample. The calculation formula of the change rate of the skin oil content is as follows:
skin oil content change rate (skin oil content after use of sample-skin oil content before use of sample)/skin oil content before use of sample × 100%;
the statistics of the test results are shown in table 4 below (the results are the average of the rate of change of the skin oil content of 10 subjects per group):
TABLE 4
As can be seen from the data in the above table, the three-dimensional matte cosmetic composition provided in example 1 has an excellent oil control effect compared to comparative examples 1 to 4, indicating that the addition amount of the filler and the first conditioning agent has an effect on the oil control of the three-dimensional matte cosmetic composition. The oil control of the three-dimensional matte cosmetic composition provided in example 1 was better than that of examples 4 to 11, indicating that the tackifier and the second adjusting agent may have an effect on the oil control effect of the three-dimensional matte cosmetic composition. The oil control effect of the three-dimensional matte cosmetic composition provided in example 1 was better than that of examples 12 to 13, indicating that the choice of the first conditioning agent may have an effect on the oil control of the three-dimensional matte cosmetic composition.
Test example 4
The present test example was conducted to test the three-dimensional effect and the degree of pattern precision of the cosmetic compositions prepared in examples 1 to 13 and comparative examples 1 to 4, according to the following methods:
the cosmetic compositions prepared in examples 1 to 13 and comparative examples 1 to 4 were molded by using silica gels of different stereometries and different precisions, and samples were obtained after freezing, demolding and drying, compared with the ordinary products (control group). And observing the three-dimensional effect of the pattern and the precision degree of the pattern presented by the appearance of the sample, and recording.
The statistics of the test results are shown in the following table 5 (wherein the more ═ is, the better the pattern stereoscopic effect or the pattern precision is):
TABLE 5
| Group of | Pattern stereo effect | Degree of pattern precision |
| Example 1 | ★★★★☆ | ★★★★☆ |
| Example 2 | ★★★★☆ | ★★★★☆ |
| Example 3 | ★★★★★ | ★★★★★ |
| Example 4 | ★★★☆☆ | ★★☆☆☆ |
| Example 5 | ★★★☆☆ | ★★☆☆☆ |
| Example 6 | ★★★☆☆ | ★★★★☆ |
| Example 7 | ★★★★☆ | ★★★★☆ |
| Example 8 | ★★★★☆ | ★★★★☆ |
| Example 9 | ★★★★☆ | ★★★★☆ |
| Example 10 | ★★★☆☆ | ★★★☆☆ |
| Example 11 | ★★★☆☆ | ★★★☆☆ |
| Example 12 | ★★★★☆ | ★★★☆☆ |
| Example 13 | ★★★☆☆ | ★★★☆☆ |
| Comparative example 1 | ★★★★☆ | ★★★★☆ |
| Comparative example 2 | ★★☆☆☆ | ★★☆☆☆ |
| Comparative example 3 | ★★★☆☆ | ★★★☆☆ |
| Comparative example 4 | ★★★★☆ | ★★★★☆ |
| Control group | ★★☆☆☆ | ★★☆☆☆ |
As can be seen from the data in the table above, the three-dimensional matte cosmetic composition provided by the invention has good pattern three-dimensional effect and pattern precision compared with the control group. From the data of comparative examples 1 to 4: the addition amount of the filler and the first adjusting agent has an influence on the pattern cubic effect and the pattern precision of the three-dimensional matte cosmetic composition. From the data of examples 4-11, it can be seen that: the tackifier and the second regulator can influence the pattern stereoscopic effect and the pattern precision degree of the three-dimensional matte cosmetic composition, wherein the effect of the tackifier is larger. From the data of examples 12-13, it can be seen that: the choice of the first conditioning agent will have an effect on the pattern definition and pattern definition of the three-dimensional matte cosmetic composition.
In conclusion, the three-dimensional matte cosmetic composition provided by the invention has the characteristics of unique cosmetic feel, soft texture, silky touch and excellent oil control property by optimizing a formula system and adopting the matching use of the components such as the filler, the first regulator, the adhesive, the colorant, the emulsifier, the humectant, the tackifier, the second regulator and the like, can realize the appearance design of three-dimensional precise patterns of products by combining a specific process and a mold, and meets the cosmetic effect requirements and appearance requirements of modern consumers on high-end color cosmetics such as pressed powder, blush and eye shadow products.
The above-mentioned embodiments are intended to illustrate the objects, technical solutions and advantages of the present invention in further detail, and it should be understood that the above-mentioned embodiments are only exemplary embodiments of the present invention, and are not intended to limit the present invention, and any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. The three-dimensional matte cosmetic composition is characterized by comprising the following components in parts by weight: 10-40 parts of filler, 20-60 parts of first regulator, 2-4 parts of adhesive, 2-25 parts of colorant, 0.1-1 part of emulsifier, 0.1-0.5 part of humectant, 0.2-1 part of tackifier and 5-13 parts of second regulator;
the filler comprises any one or the combination of at least two of mica, synthetic fluorophlogopite or talcum powder;
the first regulator comprises any one of silicon dioxide, polymethyl methacrylate or polymethylsilsesquioxane or a combination of at least two of the silicon dioxide, the polymethyl methacrylate and the polymethylsilsesquioxane.
2. The three-dimensional matte cosmetic composition according to claim 1, wherein the filler is mica and/or synthetic fluorophlogopite;
preferably, the first conditioning agent is silica and/or polymethylsilsesquioxane.
3. The three-dimensional matte cosmetic composition according to claim 1 or 2, wherein the binder comprises any one or a combination of at least two of magnesium stearate, zinc stearate, melem myristate or polyethylene, preferably magnesium stearate;
preferably, the colorant comprises toner;
preferably, the emulsifier comprises any one or a combination of at least two of polysorbate, polyethylene glycol dilaurate or sorbitan oleate, preferably polysorbate.
4. The three-dimensional matte cosmetic composition according to any one of claims 1 to 3, wherein the moisturizer comprises any one or a combination of at least two of glycerin, 1,3 butanediol, or sodium hyaluronate, preferably glycerin;
preferably, the viscosity increasing agent comprises any one or a combination of at least two of carrageenan, gellan gum, xanthan gum or pectin, preferably a combination of carrageenan and xanthan gum;
preferably, the second conditioning agent comprises any one or a combination of at least two of octyldodecanol stearoyloxystearate, squalane or ethylhexyl palmitate, preferably a combination of octyldodecanol stearoyloxystearate, squalane and ethylhexyl palmitate.
5. The three-dimensional matte cosmetic composition according to any one of claims 1 to 4, wherein the three-dimensional matte cosmetic composition further comprises a preservative;
preferably, the preservative is 0.5-1 part by weight;
preferably, the preservative comprises any one or a combination of at least two of phenoxyethanol, 1,2 hexanediol, or caprylyl glycol.
6. The three-dimensional matte cosmetic composition according to claim 5, wherein the three-dimensional matte cosmetic composition comprises, in parts by weight: 10-40 parts of a filling agent, 20-60 parts of a first regulator, 2-4 parts of magnesium stearate, 2-25 parts of a toner, 1-5 parts of octyl dodecanol stearoyl stearate, 2-4 parts of squalane, 2-4 parts of ethylhexyl palmitate, 0.1-1 part of polysorbate, 0.1-0.5 part of glycerol, 0.1-0.5 part of carrageenan, 0.1-0.5 part of xanthan gum and 0.5-1 part of a preservative;
preferably, the three-dimensional matte cosmetic composition comprises the following components in parts by weight: 20-40 parts of a filling agent, 30-50 parts of a first regulator, 2-4 parts of magnesium stearate, 4-20 parts of a toner, 3-5 parts of octyl dodecanol stearoyl stearate, 2-4 parts of squalane, 2-4 parts of ethylhexyl palmitate, 0.5-1 part of polysorbate, 0.1-0.5 part of glycerol, 0.1-0.5 part of carrageenan, 0.1-0.5 part of xanthan gum and 0.5-1 part of a preservative.
7. Process for the preparation of a three-dimensional matte cosmetic composition according to any one of claims 1 to 6, characterized in that it comprises the following steps:
(1) mixing the humectant, the tackifier and water, and heating to obtain a mixture A; mixing an emulsifier, a second regulator and an optional preservative, and heating to obtain a mixture B; mixing the mixture A with the mixture B to obtain a mixture C;
(2) mixing the filler, the first regulator, the adhesive and the colorant to obtain a mixture D;
(3) mixing the mixture C obtained in the step (1) with the mixture D obtained in the step (2), and heating to obtain a mixture E;
(4) and (4) defoaming the mixture E obtained in the step (3), filling the mixture into a forming die, cooling, forming and baking to obtain the three-dimensional matte cosmetic composition.
8. The method for preparing a three-dimensional matte cosmetic composition according to claim 7, wherein the mixture A, the mixture B and the mixture C are obtained by stirring;
preferably, the stirring speed is 500-;
preferably, the temperature at which mixture A is obtained and mixture B is obtained is independently selected from 50-90 ℃;
preferably, the mixing in the step (2) refers to crushing in a crushing pot and mixing uniformly;
preferably, the stirring speed of the crushing pot is 2000-2500r/min, the crushing times are 1-3 times, and the time of each time of crushing is 2-8 s.
9. The method for preparing a three-dimensional matte cosmetic composition according to claim 7 or 8, wherein the mixing in step (3) is stirring at a speed of 500-800 r/min;
preferably, the temperature of the heating in the step (3) is 40-70 ℃;
preferably, the cooling temperature is-60-8 ℃, and the cooling time is 30-80 min;
preferably, the baking temperature is 50-70 ℃, and the baking time is 8-24 h.
10. Use of the three-dimensional matte cosmetic composition according to any one of claims 1 to 6 for the preparation of a cosmetic.
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