CN104473792B - A kind of snow of high moisturizing melts skin cream and preparation method thereof - Google Patents
A kind of snow of high moisturizing melts skin cream and preparation method thereof Download PDFInfo
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- CN104473792B CN104473792B CN201410821729.5A CN201410821729A CN104473792B CN 104473792 B CN104473792 B CN 104473792B CN 201410821729 A CN201410821729 A CN 201410821729A CN 104473792 B CN104473792 B CN 104473792B
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Abstract
Melt skin cream the invention provides one kind snow, it is consisted of the following components in percentage by weight：Disodium ethylene diamine tetraacetate 0.02%~0.05%, NMF 0.50%~20.00%, emulsion stabilizer 1.00%~8.00%, skin sense conditioning agent 1.00%~10.00%, emollient 0~10.00%, thickener 0.10%~0.50%, ethanol 1.00%~3.00%, appropriate nertralizer, appropriate essence, preservative 0.01%~1.00%, appropriate pigment, pure water surplus.The snow of the present invention melts skin cream appearance transparent, and especially, moisture retention is good for skin sense.
Description
Technical field
The invention belongs to cosmetic field, and in particular to a kind of skin cream, and particularly a kind of snow of high moisturizing melts skin cream,
And the snow melts the preparation method of skin cream.
Background technology
Presently commercially available transparent Gel miles, in order to keep the outward appearance that its is transparent, it is impossible to add oil-soluble moisturizing ingredient, so that
Its moistening effect is caused to be less than cream formula.And commercially available cream, it is the stirring by emulsifying agent and strength, oily (water) is dripped equal
It is even to be dispersed in water (oil).Although the moistening effect of cream is better than Gel miles, its outward appearance is typically opaque, it is impossible to consumer
Bring the outward appearance for allowing people to please as transparent Gel miles and skin sense.
The content of the invention
It is an object of the invention to the technical problem to be solved for more than there is provided a kind of appearance transparent, skin sense especially,
The good snow of performance of keeping humidity melts skin cream.
It is a further object to provide the preparation method that above-mentioned snow melts skin cream.
To achieve the above objectives, skin cream is melted the invention provides a kind of snow of high moisturizing, it is by following percentage by weight
Component composition：
Disodium ethylene diamine tetraacetate 0.02%~0.05%, NMF 0.50%~20.00%, emulsion stabilizer 1.00%
~8.00%, skin sense conditioning agent 1.00%~10.00%, emollient 0~10.00%, thickener 0.10%~0.50%, ethanol
1.00%~3.00%, appropriate nertralizer, appropriate essence, preservative 0.01%~1.00%, appropriate pigment, pure water surplus.
As a preferred embodiment, the snow of the high moisturizing of the present invention melts group of the skin cream by following percentage by weight
It is grouped into：
Disodium ethylene diamine tetraacetate 0.02%~0.04%, NMF 0.50%~5.50%, emulsion stabilizer 1.00%
~4.00%, skin sense conditioning agent 1.00%~5.00%, emollient 0~5.00%, thickener 0.10%~0.30%, ethanol
1.00%~2.00%, preservative 0.01%~1.00%, appropriate nertralizer, appropriate essence, appropriate pigment, pure water surplus.
As a preferred embodiment, the snow of the high moisturizing of the present invention melts group of the skin cream by following percentage by weight
It is grouped into：
Disodium ethylene diamine tetraacetate 0.04%~0.05%, NMF 5.50%~20.00%, emulsion stabilizer 4.00%
~8.00%, skin sense conditioning agent 5.00%~10.00%, emollient 5.00~10.00%, thickener 0.30%~0.50%,
Ethanol 2.00%~3.00%, preservative 0.20%~1.00%, appropriate nertralizer, appropriate essence, appropriate pigment, more than pure water
Amount.
Preferably, NMF includes polyalcohols (for example:Glycerine, propane diols, butanediol, DPG, diglycerol, first
Base propane diols, polyethylene glycol), glucose esters (for example:PPG-10 methyls ether, PPG-20 methyls ether, methyl
Alcohol polyethers -10), the biochemical class of macromolecule (for example：Trehalose, glycine betaine, hyaluronic acid, collagen) etc. aqueous NMF, can
To be above-mentioned cited one or more.
Preferably, emulsion stabilizer includes compound lard or wax of the fusing point one or more of between 30 to 60 DEG C, example
As cetanol ethylhexoate/hydrogenated vegetable oil/stearic acid/Tower rape oil, beeswax, ceresine, one kind in microwax or
It is a variety of.
Preferably, skin sense conditioning agent include it is following in one or more：The model of DOW CORNING companies production
DC9041, DC9045, DC9046, DC9546, FB-9586, EL-9240, the model KSG-15 of ShinEtsu companies production,
KSG-15AP, KSG-16, KSG-016F, KSG-18A, KSG-19, USG-103, the type of GRANT INDUSTRIES companies production
Number it is GI CD-9, GI CD-10, GI CD-96, Gransil DM-10, AZELIS ELA BASE, MOMENTIVE companies give birth to
The elastomer silicones such as model VELVESIL DM, VELVESIL 125, the SFE839 of production and structure contain polydimethylsiloxanes
Alkane/vinyldimethylsiloxane cross-linked polymer, Dimethicone Crosspolymer or dimethyl silicone polymer/phenyl
The elastomer of vinyl dimethione cross-linked polymer.
Preferably, emollient include it is following in one or more：Ring five dimethyl silicone polymer, polydimethylsiloxanes
It is alkane, phenyl trimethicone, isopropyl stearate, dicaprylyl ether, laurate ethylhexyl, ethylhexyl stearate, different
The different nonyl ester of n-nonanoic acid, diethyl hexylcarbonate, ethylhexyl palmitate, cetostearyl alcohol ethylhexoate, caprylic/capric glycerine three
The capric acid of ester, glycerine three (thylhexoic acid) ester, isopropyl isostearate, isooctadecanol isostearate, propylene/bis-
Ester, different tridecanol isononoate.
Preferably, thickener includes one in carbomer and acrylate/C10-30 alkyl acrylate cross-linked copolymers
Plant or a variety of.
Preferably, nertralizer include potassium hydroxide, sodium hydroxide, triethanolamine, aminomethyl propanol, aminomethyl propane diols and
One or more in tromethamine.
Preferably, preservative includes methylisothiazolinone, Phenoxyethanol, double hydroxy methylimidazole ureines, iodine propilolic alcohol
Butylamino acid esters, parabens, DMDMH etc..
Pigment used in the present invention can be commercially available water colo(u)r.
Essence used in the present invention is essence commonly used in the art.
Present invention also offers the preparation method that the snow melts skin cream, its step is as follows：
(1) disodium ethylene diamine tetraacetate, NMF, nertralizer are added in pure water, is heated to 80 DEG C, heat preservation for standby use；
(2) emulsion stabilizer, emollient and skin sense conditioning agent are heated to 80 DEG C；
(3) mixture of step (2) is added in the mixture of step (1), homogeneous is after 1 minute, insulated and stirred；
(4) carbomer is added, is cooled after stirring；
(5) 50 DEG C are cooled to, ethanol, essence, preservative and pigment is added and is stirred until homogeneous.
Compared with prior art, snow of the invention melts skin cream and had the following advantages that：
1st, unique outward appearance and skin sense：White " snowflake " is evenly distributed in coloured transparent gel, is applied to skin
There is outlet effect when upper and " snowflake " can melt, produce unique skin sense and produce one layer of moisture film on skin simultaneously；
2nd, oil-soluble moisturizing ingredient is added in transparent Gel miles, screening and special technique by oil-soluble ingredients,
Oil-soluble ingredients is not emulsified, and be distributed in stable and uniform and the state that is of moderate size in Gel miles, it is and existing transparent
Gel miles is compared, with efficient moistening effect.
The transparent gel shape of product of the present invention, the inside suspended white be similar to snowflake shape moisturizing particle.By applying
Smear, moisturizing elite gel can form out water state in skin surface, be absorbed by the skin rapidly.And similar and flakes moisturizing
Grain melts under skin temperature, by smearing, and one layer strong moisture film is formed on skin, and produces the silk of uniqueness and slides skin sense,
Reach the lasting moistening effect of strength.Outward appearance and the skin sense of Gel miles of pleasant had so both been remained, there is cream kind product again
Moistening effect.
Embodiment
Technical scheme is described in further detail with reference to specific embodiment, but protection scope of the present invention
It is not limited in following examples.
Each component is weighed according to following percentage by weight, following each component can be bought by commercial channel and be obtained.
The snow for making embodiment 1~3 melts skin cream, and its step is as follows：
1. by disodium ethylene diamine tetraacetate, NMF (glycerine, PPG-10 methyls ether or hyaluronic acid), nertralizer
(triethanolamine, potassium hydroxide or sodium hydroxide) is added in pure water, is heated to 80 DEG C, heat preservation for standby use；
2. by emulsion stabilizer (microwax, ceresine or cetanol ethylhexoate/hydrogenated vegetable oil/stearic acid/low erucic acid
Rape seed oil), emollient (ring five dimethyl silicone polymer or isopropyl stearate) and skin sense conditioning agent (KSG-15AP, FB-9586
Or GICD-9) it is heated to 80 DEG C；
3. in the mixture that the mixture of step 2 is added to step 1, homogeneous is after 1 minute, insulated and stirred；
4. adding carbomer, cool after being stirred until homogeneous；
5. being cooled to 50 DEG C, ethanol, essence, preservative (methylisothiazolinone, Phenoxyethanol or double methylol miaows are added
Oxazolidinyl urea) and pigment be stirred until homogeneous.
Obtaining the snow of the present embodiment 1~3, to melt skin cream be that the color for having white " snowflake " to be evenly distributed in lotion is saturating
Bright gel, being applied on skin has outlet effect and " snowflake " can melt, and produces unique skin sense, while producing one layer on skin
Moisture film.Through long-term shelf storage experiment (lower 3 years of normal temperature) and repeatedly it is heat-resisting (40 ± 1 DEG C, 24 hours recover room temperatures after it is not muddy
It is turbid), cold-resistant (- 15 ± 1 DEG C, recover after room temperatures for 24 hours, system is normal, no turbid phenomenon) destructive testing, product items sense
See index, physical and chemical index, sanitary index and meet corresponding national standard.
Using effect is tested：
1st, moistening effect is assessed
(1) present invention has carried out test evaluation to the moisture retention that the snow of embodiment 1/2/3 melts skin cream, and using commercially available
Bright Gel miles is used as control sample.
(2) subjects：2 males, 25 women, average age 25.5 ± 11.2 years old.Recipient site：In double forearms
Recipient site at side, mark two, is randomly assigned as sample area and check plot, sample area smearing tested material, check plot smearing control
All product.Application area：3cm × 3cm, smears dosage：2mg/cm2。
(3) method of testing：Subject sits quietly after 20min, with dry paper handkerchief scrape skin surface before test, measures recipient site
Tested material and control sample are smeared by prescribed dose after keratoderma water content, record data before being smeared with check plot, contrast is real
Apply after example and control sample are smeared 30 minutes, 1 hour, 4 hours and 8 hours recipient site keratoderma water content of skin and record
Related data.In process of the test, the exposure of subject's forearm is placed in test mode, keeps loosening.
(4) result of the test：Moisture measurement experiment is done to embodiment 1, embodiment 2, embodiment 3 and control sample respectively.According to
Data analysis is drawn a conclusion, and embodiment 1, embodiment 2, the contrast control sample moistening effect of embodiment 3 are obvious, and moistening effect is held
Long.
2nd, skin sense evaluation test
(1) present invention has carried out test evaluation to the skin sense that the snow of embodiment 1/2/3 melts skin cream, and uses commercial samples
A (cream) is contrasted.
(2) subjects：30 women commonly using moisturiser, average age 25 ± 3 years old.Recipient site：Double forearms
Recipient site at inner side, mark two, is randomly assigned as sample area and check plot, sample area smearing tested material, check plot smearing pair
Sample in the same old way.Application area：3cm × 3cm, smears dosage：2mg/cm2。
(3) method of testing：With dry paper handkerchief scrape skin surface before test, embodiment and commercial samples A, contrast are directly smeared
Smear and feel.Testing evaluation is as follows：The sense of 5=skins especially, enjoys a lot；The sense of 4=skins especially, is delithted with；The sense of 3=skins especially, is liked
Vigorously；2=skin senses are general；1=is not liked；0=is not liked very much.
(4) test result：The record data that scored after 30 subjects is averaged and (see the table below) to analyze and draws a conclusion,
The snow of embodiment 1, embodiment 2 and embodiment 3 melts skin cream and commercial samples A compares, and skin sense is especially, fine and smooth soft, tested
Person is delithted with snow defrosting skin sense.
Claims (4)
1. a kind of snow of high moisturizing melts skin cream, it is characterised in that consist of the following components in percentage by weight：
Disodium ethylene diamine tetraacetate 0.02%~0.05%, NMF 0.50%~20.00%, emulsion stabilizer 1.00%~8.00%,
Skin sense conditioning agent 1.00%~10.00%, emollient 0~10.00%, thickener 0.10%~0.50%, ethanol 1.00%~3.00%,
Appropriate nertralizer, appropriate essence, preservative 0.01%~1.00%, appropriate pigment, pure water surplus；
The emulsion stabilizer is cetanol ethylhexoate/hydrogenated vegetable oil/stearic acid/Tower rape oil, ceresine, crystallite
The mixture of wax；
The skin sense conditioning agent is following mixture：Model FB-9586, ShinEtsu of DOW CORNING companies production
The model GI CD-9 of model KSG-15AP, the GRANT INDUSTRIES companies production of company's production organosilicone elastic
Body；
The emollient is the mixture of ring five dimethyl silicone polymer and isopropyl stearate；
The thickener is carbomer；
The NMF is the mixture of glycerine, hyaluronic acid and PPG-10 methyl ethers.
2. snow according to claim 1 melts skin cream, it is characterised in that consist of the following components in percentage by weight：
Disodium ethylene diamine tetraacetate 0.02%~0.04%, NMF 0.50%~5.50%, emulsion stabilizer 1.00%~4.00%,
Skin sense conditioning agent 1.00%~5.00%, emollient 0~5.00%, thickener 0.10%~0.30%, ethanol 1.00%~2.00% is prevented
Rotten agent 0.01%~1.00%, appropriate nertralizer, appropriate essence, appropriate pigment, pure water surplus.
3. snow according to claim 1 melts skin cream, it is characterised in that consist of the following components in percentage by weight：
Disodium ethylene diamine tetraacetate 0.04%~0.05%, NMF 5.50%~20.00%, emulsion stabilizer 4.00%~8.00%,
Skin sense conditioning agent 5.00%~10.00%, emollient 5.00~10.00%, thickener 0.30%~0.50%, ethanol 2.00%~
3.00%, preservative 0.20%~1.00%, appropriate nertralizer, appropriate essence, appropriate pigment, pure water surplus.
4. any one of claims 1 to 3 is described to avenge the preparation method for melting skin cream, its step is as follows：
（1）Disodium ethylene diamine tetraacetate, NMF, nertralizer are added in pure water, 80 DEG C, heat preservation for standby use are heated to；
（2）Emulsion stabilizer, emollient and skin sense conditioning agent are heated to 80 DEG C；
（3）By step（2）Mixture add step（1）Mixture in, homogeneous is after 1 minute, insulated and stirred；
（4）Carbomer is added, is cooled after stirring；
（5）50 DEG C are cooled to, ethanol, essence, preservative and pigment is added and is stirred until homogeneous.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410821729.5A CN104473792B (en) | 2014-12-23 | 2014-12-23 | A kind of snow of high moisturizing melts skin cream and preparation method thereof |
| JP2015141262A JP6266567B2 (en) | 2014-12-23 | 2015-07-15 | Skin care cream and method for preparing the same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410821729.5A CN104473792B (en) | 2014-12-23 | 2014-12-23 | A kind of snow of high moisturizing melts skin cream and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104473792A CN104473792A (en) | 2015-04-01 |
| CN104473792B true CN104473792B (en) | 2017-11-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410821729.5A Expired - Fee Related CN104473792B (en) | 2014-12-23 | 2014-12-23 | A kind of snow of high moisturizing melts skin cream and preparation method thereof |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JP6266567B2 (en) |
| CN (1) | CN104473792B (en) |
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| ITUB20153461A1 (en) * | 2015-09-08 | 2017-03-08 | Novamont Spa | Lipophilic cosmetic compositions containing esters of pelargonic acid |
| CN106265330A (en) * | 2016-08-29 | 2017-01-04 | 杭州千岛湖蓝色天使实业有限公司 | The cream that a kind of wrinkle removing is anti-ageing |
| CN106491442A (en) * | 2016-12-06 | 2017-03-15 | 广州聚禅现代农业研究院有限公司 | A kind of ivory white foundation emulsion containing Amaranthus mangostanus L. polyphenol |
| CN106511134B (en) * | 2016-12-13 | 2019-09-17 | 泉州师范学院 | A kind of astaxanthin facial mask nutrient solution and preparation method thereof |
| CN106619301B (en) * | 2016-12-29 | 2019-11-15 | 广州市科能化妆品科研有限公司 | A kind of composition and preparation method thereof containing flakes particle |
| CN107411991B (en) * | 2017-08-21 | 2020-07-31 | 广州神采化妆品有限公司 | Instant-to-apply ice cream and preparation method thereof |
| CN109363993A (en) * | 2018-11-29 | 2019-02-22 | 四川省中医药科学院 | A kind of step emulsifying cooling and shaping method and its application |
| CN112294707B (en) * | 2019-07-31 | 2022-07-29 | 太和康美(北京)中医研究院有限公司 | Cream with moisturizing effect and preparation method thereof |
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| CN114903838A (en) * | 2021-06-07 | 2022-08-16 | 安婕妤化妆品科技股份有限公司 | Face brightening snow cream and preparation method thereof |
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| CN114569508A (en) * | 2022-03-14 | 2022-06-03 | 为美而生(广东)实业控股有限公司 | Moisturizing and skin-moistening facial cream containing collagen components and preparation method thereof |
| CN115475107A (en) * | 2022-09-09 | 2022-12-16 | 广州环亚化妆品科技股份有限公司 | Water-in-oil type skin cream and preparation method thereof |
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Also Published As
| Publication number | Publication date |
|---|---|
| JP2016117703A (en) | 2016-06-30 |
| CN104473792A (en) | 2015-04-01 |
| JP6266567B2 (en) | 2018-01-24 |
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