CN113057904A - Moisture-retaining pressed powder containing fibroin and preparation method thereof - Google Patents
Moisture-retaining pressed powder containing fibroin and preparation method thereof Download PDFInfo
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- CN113057904A CN113057904A CN202110323312.6A CN202110323312A CN113057904A CN 113057904 A CN113057904 A CN 113057904A CN 202110323312 A CN202110323312 A CN 202110323312A CN 113057904 A CN113057904 A CN 113057904A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
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Abstract
The invention discloses a fibroin-containing moisturizing pressed powder and a preparation method thereof, and belongs to the technical field of cosmetics. The fibroin-containing moisturizing powder cake disclosed by the invention takes silkworm sericin as a skin conditioner, and is matched with ethylhexyl palmitate and caprylic/capric triglyceride with specific content as a humectant, so that the fibroin-containing moisturizing powder cake has good moisture absorption and retention performance, has no irritation to the skin of a user, can realize natural moisture regulation, can improve the nutrition of the skin of a human body after being used, prevents the skin from wrinkling, and enables the skin to be more tender; the product has soft and smooth texture, high stability and safety and good spreadability. The invention also discloses a preparation method of the fibroin-containing moisturizing powder cake, which is simple in operation steps and can realize industrial large-scale production.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a fibroin-containing moisturizing pressed powder and a preparation method thereof.
Background
With the improvement of living standard of people, people pay more attention to self image, and cosmetics become necessities of daily life. The pressed powder is used as a beauty cosmetic prepared by mixing and pressing powder and a matrix, is convenient to carry and use. However, the existing pressed powder products have the following defects: (1) the powder on the powder cake is not fine enough, and the touch of the skin of a user is not fine and smooth enough when the powder cake is applied; (2) the cake powder has insufficient skin-fitting performance, so that the makeup is not uniform when the cake powder is used; (3) the powder of the pressed powder is too dry and has poor moisture retention to skin.
Disclosure of Invention
Based on the defects of the prior art, the invention aims to provide the fibroin-containing moisturizing powder cake which is fine and smooth in powder, good in makeup uniformity, and has certain oil control performance and good and lasting moisture absorption and retention performance.
In order to achieve the purpose, the invention adopts the technical scheme that:
the fibroin-containing moisturizing powder cake comprises the following components in percentage by mass: 3-5% of a colorant, 10-15% of a skin conditioner, 6-15% of a softening agent, 4-8% of a humectant and the balance of a filler; the skin conditioner comprises sericin; the humectant comprises ethylhexyl palmitate and caprylic/capric triglyceride.
In the components of the moisturizing powder cake, the ethylhexyl palmitate mainly plays a moisturizing role and can effectively prevent the moisture in the skin of a human body from evaporating outwards, so that the skin is moisturized, and the product has strong affinity with the skin, good permeability and no greasy feeling when in use; caprylic/capric triglyceride is a common moisturizing factor base material, can be effectively used as a moisturizing agent in cosmetics, and can also be used as a stabilizer, an antifreezing agent and a homogenizing agent to a certain extent; the sericin protein has a structure similar to human skin keratin protein, has good affinity with the human skin keratin protein, can effectively enhance the activity and elasticity of skin cells, and has good moisture absorption and retention properties.
The fibroin-containing moisturizing powder cake disclosed by the invention takes silkworm sericin as a skin conditioner, and is matched with ethylhexyl palmitate and caprylic/capric triglyceride with specific content as a humectant, so that the fibroin-containing moisturizing powder cake has good moisture absorption and retention properties, has no irritation to the skin of a user, realizes natural moisture regulation, can improve the nutrition of the skin of a human body after being used, prevents the skin from wrinkling, and enables the skin to be more tender; the product has soft and smooth texture, high stability and safety and good spreadability.
Preferably, the skin conditioner further comprises boron nitride, chinlon-12, edible corn starch, magnesium stearate and pearl powder.
Among the components, boron nitride is a common cosmetic additive, and can make the skin have a transparent and glittering effect, so that the light is reflected out of the skin, thereby blurring wrinkles and flaws on the skin. In addition, the powder can adsorb redundant oil on the skin, so that the powder has good makeup uniformity; the chinlon-12 also has the function of adsorbing redundant oil of the skin, and meanwhile, the substance has fresh skin feel and good soft-focus effect; the edible corn starch can increase the luster and elasticity of the skin and effectively care the skin; the pearl powder contains a certain amount of keratin, has high affinity to skin when being used for pressed powder products, and can endow certain whitening effect to the skin.
More preferably, the skin conditioner comprises 1-5% of boron nitride, 1-5% of chinlon-12, 4-10% of edible corn starch, 3-7% of magnesium stearate, 0.2-1% of sericin and 0.3-3% of pearl powder by mass of the moisturizing powder cake.
More preferably, the skin conditioner comprises 3% of boron nitride, 3% of chinlon-12, 8% of edible corn starch, 5% of magnesium stearate, 0.5% of sericin and 2% of pearl powder by mass of the moisturizing compact.
The skin conditioner mixed according to the proportion can effectively improve the luster and the water wettability of the skin of a user and repair wrinkles and flaws on the skin.
Preferably, the humectant comprises 2-4% of ethylhexyl palmitate and 2-4% of caprylic/capric triglyceride based on the mass of the moisturizing pressed powder.
The humectant in the proportion can make the product have stronger hygroscopicity and longer moisture retention.
More preferably, the humectant comprises 3% ethylhexyl palmitate and 3% caprylic/capric triglyceride by mass of the moisturizing compact.
Preferably, the filler comprises talc and mica powder.
More preferably, the filler comprises talcum powder and mica powder, wherein the talcum powder accounts for 15-50% of the mass of the moisturizing pressed powder, and the mica powder accounts for 5-30%.
More preferably, the filler comprises 35% of talc powder and 19% of mica powder by mass of the moisturizing compact.
Preferably, the colorants include CI77492, CI77491, titanium dioxide, and CI 77499.
More preferably, the colorant comprises CI77492 accounting for 0.5-1.5% of the mass of the moisturizing pressed powder, CI77491 accounting for 0.2-1%, titanium dioxide accounting for 1-5% of the mass of the moisturizing pressed powder and CI77499 accounting for 0.1-0.5%.
More preferably, the colorant comprises 1% of CI77492, 0.6% of CI77491, 2.5% of titanium dioxide and 0.3% of CI77499 by mass of the moisturizing compact.
The coloring agent is mixed according to a specific ratio to prepare a product which is more natural and uniform in color development and better in make-up effect.
Preferably, the emollient comprises silica and tridecyl trimellitate.
More preferably, the emollient comprises silica accounting for 5-12% of the mass of the moisturizing powder cake and tridecyl alcohol trimellitate accounting for 1-3%.
More preferably, the emollient comprises 10% silica and 2% tridecyl trimellitate by mass of the moisturizing compact.
In the components, silica is a common nontoxic lubricant for cosmetics, and the skin touch feeling and the overall texture of the product can be effectively improved by matching with the high-viscosity tridecyl alcohol trimellitate.
Preferably, the components of the moisturizing powder cake further comprise an emulsifier, a preservative and an antioxidant.
More preferably, the emulsifier comprises sorbitan sesquioleate; the preservative comprises phenoxyethanol and hexylethyl glycerol; the antioxidant comprises tocopherol acetate.
The tocopherol acetate is a common additive for personal care and sanitary products, and can improve the protection of the products on skin injury when being used for the products, thereby further enriching the functions of the products; the sorbitan sesquioleate, the phenoxyethanol and the hexylethyl glycerol are also common cosmetic addition auxiliaries, and the components are safe and non-toxic.
More preferably, the emulsifier comprises sorbitan sesquioleate accounting for 0.5-1.5% of the mass of the moisturizing powder cake; the preservative comprises phenoxyethanol accounting for 0.5-1% of the mass of the moisturizing powder cake and hexylethyl glycerol accounting for 0.1-0.3%; the antioxidant comprises tocopherol acetate which accounts for 0.05-0.2% of the mass of the moisturizing powder cake.
More preferably, the emulsifier comprises sorbitan sesquioleate at 1% by mass of the moisturizing compact; the preservative comprises phenoxyethanol accounting for 0.85 percent of the mass of the moisturizing powder cake and hexylethyl glycerol accounting for 0.15 percent of the mass of the moisturizing powder cake; the antioxidant comprises tocopherol acetate which accounts for 0.1% of the mass of the moisturizing powder cake.
The invention also aims to provide a preparation method of the fibroin-containing moisturizing powder cake, which comprises the following steps:
(1) stirring and mixing the filler and the colorant for 2-5 s to obtain a phase A;
(2) adding the phase B into the phase A obtained in the step (1), stirring and mixing for 2-3 s; the phase B comprises boron nitride, chinlon-12, silica, edible corn starch and magnesium stearate;
(3) mixing and stirring the phase C and the phase D uniformly, adding the mixture obtained in the step (2), and stirring and mixing for 4-5 s; the phase C comprises tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride and sorbitan sesquioleate, and the phase D is a preservative;
(4) adding the phase E into the mixture obtained in the step (3), stirring and mixing for 2-3 s, then adding the phase F, stirring and mixing for 1-3 s, and obtaining the fibroin-containing moisturizing powder cake; the phase E comprises sericin and tocopherol acetate; the phase F is pearl powder.
The preparation method of the fibroin-containing moisturizing powder cake provided by the invention is simple in operation steps, and can realize industrial large-scale production.
Preferably, the rotation speed of the stirring in the steps (1) to (4) is 24000 to 26000 r/min.
All components are uniformly stirred and dispersed at the rotating speed, and the prepared product has high stability.
The invention has the beneficial effects that: the invention provides a fibroin-containing moisturizing powder cake, which takes silkworm sericin as a skin conditioner and is matched with ethylhexyl palmitate and caprylic/capric triglyceride with specific content as a humectant, so that the fibroin-containing moisturizing powder cake has good moisture absorption and retention performance, has no irritation to the skin of a user, can realize natural moisture regulation, can improve the nutrition of the skin of a human body after being used, prevents the skin from wrinkling and enables the skin to be more tender; the product has soft and smooth texture, high stability and safety and good spreadability. The invention also provides a preparation method of the fibroin-containing moisturizing powder cake, which is simple in operation steps and can realize industrial large-scale production.
Detailed Description
For better illustrating the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to specific examples, which are intended to be understood in detail, but not intended to limit the present invention.
Examples 1 to 3
Examples of the fibroin-containing moisturizing powder cakes according to the present invention, the formula of the fibroin-containing moisturizing powder cakes in each example is shown in table 1.
The preparation method of the fibroin-containing moisturizing pressed powder in each embodiment comprises the following steps:
(1) stirring and mixing the filler and the colorant for 3s to obtain a phase A;
(2) adding the phase B into the phase A obtained in the step (1), stirring and mixing for 3 s; the phase B comprises boron nitride, chinlon-12, silica, edible corn starch and CI 77491;
(3) mixing and stirring the phase C and the phase D uniformly, adding the mixture obtained in the step (2), and stirring and mixing for 5 s; the phase C comprises tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride and sorbitan sesquioleate, and the phase D is a preservative;
(4) adding phase E into the mixture obtained in the step (3), stirring and mixing for 3s, then adding phase F, stirring and mixing for 2s, and obtaining the fibroin-containing moisturizing powder cake; the phase E comprises sericin and tocopherol acetate; the F phase is pearl powder;
the rotating speed of the stirring is 25000 r/min.
TABLE 1
Comparative examples 1 to 5
The products of comparative examples 1 to 5 are different from the product of example 1 only in formulation, the method for preparing the moisturizing pressed powder is the same as that of example 1, and the formulation of the moisturizing pressed powder in each comparative example is shown in table 2.
TABLE 2
Effect example 1
In order to verify the use effect of the moisturizing powder cake obtained in the invention, the use experience evaluation test is performed on the products obtained in the examples 1-3 and the comparative examples 1-5. The test method comprises the following steps:
80 volunteers of 20-45 years old are screened, wherein the volunteers are patients without serious system diseases, immunodeficiency or autoimmune diseases, patients without active allergic diseases, patients without serious allergic history to cosmetics, patients who have not used hormone medicines and immunosuppressants in the last month, and other subjects of clinical testers. The volunteers were divided into 10 groups of 10 persons each, with no significant difference between groups, the face was selected as the test site, tested once before the test (i.e. without moisturizing cake product), the test product was used in the morning, noon and evening, timed from the time of use, and the stratum corneum moisture content of the test area was determined after 28 h. The tested products are the moisturizing powder cakes of examples 1-3 and comparative examples 1-5 respectively. The stratum corneum moisture content and Skin gloss were measured using a Skin moisture test probe Cornometer CM825 and a Skin gloss test probe Skin-Glossimeter GL200 (Courage + Khazaka, Germany, 50829Koln, Germany), respectively. After the use, the powder texture (comfort) and makeup uniformity of the product were evaluated by scores.
And (4) analyzing result data:
(1) calculation of moisture Change amount
Subtracting the blank control value of the test part before use from the measured value of the test part after using the sample to obtain the mean value of the variation of the moisture content of the horny layer of the test part before and after using the product, and calculating the formula as follows:
T＝(Mx-Mo) 10; wherein: t is the skin moisture variation; mxMeasurement of skin moisture 28 days after use of the product; moSkin moisture blank measurements.
(2) Evaluation of product texture and cosmetic Effect
1-5 points are respectively used for evaluating texture (the powder is fine and smooth, the evaluation of comfortable touch is 5 points at the highest point, then gradually decreased from one point to another, the powder is dry, the evaluation of poor touch is 1 point at the lowest point) and makeup effect (the powder is uniformly made up, the evaluation of easy makeup is 5 points at the highest point, then gradually decreased from one point to another, the powder is unevenly made up, and the evaluation of difficult makeup is the lowest point), and the evaluation of all volunteers is counted and the average point is calculated.
The statistical results of the tests are shown in table 3.
TABLE 3
As can be seen from table 3, the moisture-retaining pressed powders containing fibroin obtained in examples 1 to 3 have excellent skin moisture-retaining effect, good powder texture and easy makeup, uniform makeup effect, and strong user experience compared with the products obtained in comparative examples 1 to 5 in which the components and the mixture ratio thereof are not in the preferable range.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. The fibroin-containing moisturizing powder cake is characterized by comprising the following components in percentage by mass: 3-5% of a colorant, 10-15% of a skin conditioner, 6-15% of a softening agent, 4-8% of a humectant and the balance of a filler; the skin conditioner comprises sericin; the humectant comprises ethylhexyl palmitate and caprylic/capric triglyceride.
2. The moisturizing puff cake of claim 1 wherein the skin conditioner further comprises boron nitride, chinlon-12, edible corn starch, magnesium stearate, and pearl powder; preferably, the skin conditioner comprises boron nitride accounting for 1-5% of the mass of the moisturizing powder cake, chinlon-12 accounting for 1-5%, edible corn starch accounting for 4-10%, magnesium stearate accounting for 3-7%, sericin accounting for 0.2-1% and pearl powder accounting for 0.3-3%.
3. The moisturizing compact of claim 1, wherein the humectant comprises 2-4% ethylhexyl palmitate and 2-4% caprylic/capric triglyceride by weight of the moisturizing compact.
4. The moisturizing compact of claim 1, wherein the filler comprises talc and mica powder; preferably, the filler comprises talcum powder and mica powder, wherein the talcum powder accounts for 15-50% of the mass of the moisturizing pressed powder, and the mica powder accounts for 5-30%.
5. The moisturizing compact of claim 1, wherein the colorant comprises CI77492, CI77491, titanium dioxide, and CI 77499; preferably, the colorant comprises CI77492 accounting for 0.5-1.5% of the mass of the moisturizing pressed powder, CI77491 accounting for 0.2-1%, titanium dioxide accounting for 1-5% of the mass of the moisturizing pressed powder and CI77499 accounting for 0.1-0.5%.
6. The moisturizing compact of claim 1, wherein the emollient comprises silica and tridecyl trimellitate; preferably, the emollient comprises silica accounting for 5-12% of the mass of the moisturizing powder cake and tridecyl alcohol trimellitate accounting for 1-3% of the mass of the moisturizing powder cake.
7. The moisturizing compact of claim 1, wherein the components of the moisturizing compact further comprise emulsifiers, preservatives, and antioxidants; preferably, the emulsifier comprises sorbitan sesquioleate; the preservative comprises phenoxyethanol and hexylethyl glycerol; the antioxidant comprises tocopherol acetate.
8. The moisturizing compact of claim 7, wherein the emulsifier comprises sorbitan sesquioleate in an amount of 0.5-1.5% by mass of the moisturizing compact; the preservative comprises phenoxyethanol accounting for 0.5-1% of the mass of the moisturizing powder cake and hexylethyl glycerol accounting for 0.1-0.3%; the antioxidant comprises tocopherol acetate which accounts for 0.05-0.2% of the mass of the moisturizing powder cake.
9. The method for preparing the fibroin-containing moisturizing cake as claimed in any one of claims 1 to 8, comprising the steps of:
(1) stirring and mixing the filler and the colorant for 2-5 s to obtain a phase A;
(2) adding the phase B into the phase A obtained in the step (1), stirring and mixing for 2-3 s; the phase B comprises boron nitride, chinlon-12, silica, edible corn starch and magnesium stearate;
(3) mixing and stirring the phase C and the phase D uniformly, adding the mixture obtained in the step (2), and stirring and mixing for 4-5 s; the phase C comprises tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride and sorbitan sesquioleate, and the phase D is a preservative;
(4) adding the phase E into the mixture obtained in the step (3), stirring and mixing for 2-3 s, then adding the phase F, stirring and mixing for 1-3 s, and obtaining the fibroin-containing moisturizing powder cake; the phase E comprises sericin and tocopherol acetate; the phase F is pearl powder.
10. The method for preparing the fibroin-containing moisturizing cake as claimed in claim 9, wherein the stirring speed in steps (1) - (4) is 24000-26000 r/min.
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